RU2004101640A - Способ изготовления изделий из стекла и стеклокерамические изделия, полученные таким способом - Google Patents
Способ изготовления изделий из стекла и стеклокерамические изделия, полученные таким способом Download PDFInfo
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- RU2004101640A RU2004101640A RU2004101640/03A RU2004101640A RU2004101640A RU 2004101640 A RU2004101640 A RU 2004101640A RU 2004101640/03 A RU2004101640/03 A RU 2004101640/03A RU 2004101640 A RU2004101640 A RU 2004101640A RU 2004101640 A RU2004101640 A RU 2004101640A
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- 238000004519 manufacturing process Methods 0.000 title claims abstract 6
- 239000011521 glass Substances 0.000 title claims 83
- 238000000034 method Methods 0.000 title claims 64
- 239000002241 glass-ceramic Substances 0.000 title claims 6
- 239000000919 ceramic Substances 0.000 claims abstract 6
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract 6
- 150000004706 metal oxides Chemical class 0.000 claims abstract 6
- 229910052782 aluminium Inorganic materials 0.000 claims 10
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims 9
- 229910004298 SiO 2 Inorganic materials 0.000 claims 9
- 238000010438 heat treatment Methods 0.000 claims 8
- 239000002245 particle Substances 0.000 claims 3
- 239000000758 substrate Substances 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 2
- 238000004581 coalescence Methods 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 235000012907 honey Nutrition 0.000 claims 1
- 229910052738 indium Inorganic materials 0.000 claims 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Inorganic materials [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 abstract 1
- 229910052681 coesite Inorganic materials 0.000 abstract 1
- 229910052906 cristobalite Inorganic materials 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 230000009477 glass transition Effects 0.000 abstract 1
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum oxide Inorganic materials [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 abstract 1
- KTUFCUMIWABKDW-UHFFFAOYSA-N oxo(oxolanthaniooxy)lanthanum Chemical compound O=[La]O[La]=O KTUFCUMIWABKDW-UHFFFAOYSA-N 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 235000012239 silicon dioxide Nutrition 0.000 abstract 1
- 229910052682 stishovite Inorganic materials 0.000 abstract 1
- 229910052905 tridymite Inorganic materials 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
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- C09K3/00—Materials not provided for elsewhere
- C09K3/14—Anti-slip materials; Abrasives
- C09K3/1409—Abrasive particles per se
- C09K3/1418—Abrasive particles per se obtained by division of a mass agglomerated by sintering
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- C03B19/00—Other methods of shaping glass
- C03B19/06—Other methods of shaping glass by sintering, e.g. by cold isostatic pressing of powders and subsequent sintering, by hot pressing of powders, by sintering slurries or dispersions not undergoing a liquid phase reaction
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- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/1005—Forming solid beads
- C03B19/102—Forming solid beads by blowing a gas onto a stream of molten glass or onto particulate materials, e.g. pulverising
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- C03B32/02—Thermal crystallisation, e.g. for crystallising glass bodies into glass-ceramic articles
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
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- C03C3/00—Glass compositions
- C03C3/12—Silica-free oxide glass compositions
- C03C3/125—Silica-free oxide glass compositions containing aluminium as glass former
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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Claims (62)
1. Способ изготовления изделия из стекла, включающий в себя: размещение подложки с наружной поверхностью; получение по меньшей мере первичного стекла, которое состоит как минимум из двух различных оксидов металлов, характеризуется Тg и Тх, причем разница между Тg и Тх первичного стекла составляет как минимум 5 К, а само стекло содержит менее 20 мас.% SiO2, менее 20 мас.% В2О3 и менее 40 мас.% P2O5; нагревание первичного стекла до температуры свыше Тg так, чтобы хотя бы часть стекла смачивала по меньшей мере часть наружной поверхности подложки; и охлаждение стекла с получением продукта, представляющего собой керамическое изделие со стеклом, прикрепленным как минимум к части наружной поверхности подложки.
2. Способ по п.1, отличающийся тем, что разница между Тg и Тх составляет по меньшей мере 25 К.
3. Способ по п.2, отличающийся тем, стекло характеризуется T1, a соотношение Тg и T1 составляет по меньшей мере 0,5.
4. Способ по п.3, отличающийся тем, что первичное стекло содержит суммарно менее 40 мас.% стекла, состоящего из SiO2, В2О3 и Р2O5, по отношению к общей массе стекла.
5. Способ по п.3, отличающийся тем, что стекло - это система REO-Al2O3.
6. Способ по п.5, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3 и REO по отношению к общей массе стекла.
7. Способ по п.1, отличающийся тем, что стекло - это система REO-Al2О3-ZrO2.
8. Способ по п.7, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3, REO и ZrO2 по отношению к общей массе стекла.
9. Способ по п.1, отличающийся тем, что изделие представляет собой стекло, а сам способ включает в себя также термообработку стекла с получением стеклокерамики.
10. Изделие, изготовленное в соответствии со способом, описанным в п.9.
11. Изделие, изготовленное по п.1, причем разница между Тg и Тх составляет по меньшей мере 35 К.
12. Изделие, изготовленное в соответствии со способом, описанным в п.1.
13. Способ по п.1, отличающийся тем, что первая совокупность частиц представляет собой стекло.
14. Способ по п.13, отличающийся тем, что разница между Тg и Тх составляет по меньшей мере 25 К.
15. Способ по п.14, отличающийся тем, что стекло характеризуется T1, a соотношение Тg и T1 составляет по меньшей мере 0,5.
16. Способ по п.15, отличающийся тем, что стекло содержит в сумме менее 40 мас.% SiO2, B2O3 и P2O5 по отношению к общей массе стекла.
17. Способ по п.15, отличающийся тем, что стекло -REO-Al2О3 стекло.
18. Способ по п.17, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3 и REO по отношению к общей массе стекла.
19. Способ по п.13, отличающийся тем, что стекло - это система REO-Al2O3-ZrO2.
20. Способ по п.19, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3, REO и ZrO2 по отношению к общей массе стекла.
21. Способ по п.13, отличающийся тем, что изделие представляет собой стекло, а сам способ включает в себя также термообработку стекла с получением стеклокерамики.
22. Изделие, изготовленное в соответствии со способом, описанным в п.21.
23. Способ по п.13, отличающийся тем, что разница между Тg и Тх составляет по меньшей мере 35 К.
24. Изделие, изготовленное в соответствии со способом, описанным в п.13.
25. Способ изготовления изделия из стекла, включающий в себя: получение по меньшей мере первичного и вторичного стекол, причем первичное стекло состоит как минимум из двух разных оксидов металлов, где первичное стекло характеризуется Tg1 и Tx1, причем разница между Tg1 и Tx1 составляет как минимум 5 К, а само первичное стекло содержит менее 20 мас.% SiO2, менее 20 мас.% В2О3 и менее 40 мас.% P2O5; нагревание первичного и вторичного стекол до температуры по меньшей мере выше Tg1, причем первичное стекло спекается со вторичным стеклом с образованием изделия.
26. Способ по п.25, отличающийся тем, что разница между Tg1 и Tx1 составляет по меньшей мере 25 К.
27. Способ по п.26, отличающийся тем, что стекло характеризуется T1, a соотношение Tg1 и Т11 составляет по меньшей мере 0,5.
28. Способ по п.27, отличающийся тем, что первичное стекло содержит суммарно менее 40 мас.% SiO2, В2O3 и P2O5 по отношению к общей массе стекла.
29. Способ по п.28, отличающийся тем, что стекло - это система REO-Al2O3.
30. Способ по п.29, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3 и REO по отношению к общей массе стекла.
31. Способ по п.25, отличающийся тем, что стекло - это система REO-Al2O3-ZrO2.
32. Способ по п.31, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3, REO и ZrO2 по отношению к общей массе стекла.
33. Способ по п.25, отличающийся тем, что изделие представляет собой стекло, а сам способ включает в себя также термообработку стекла с получением стеклокерамики.
34. Изделие, изготовленное в соответствии со способом, описанным в п.33.
35. Способ по п.25, отличающийся тем, что разница между Tg1 и Tx1 составляет по меньшей мере 35 К.
36. Изделие, изготовленное в соответствии со способом, описанным в п.25.
37. Способ по п.25, отличающийся тем, что вторичное стекло характеризуется Тg2 и Тх2, причем разница между Тg2 и Тx2 составляет как минимум 5 К, а само вторичное стекло содержит менее 20 мас.% SiO2, менее 20% мас. В2O3 и менее 40% мас. Р2О5.
38. Способ по п.37, отличающийся тем, что разница между парами Tg1 и Tx1, а также Тg2 и Тх2 составляет по меньшей мере 25 К.
39. Способ по п.38, отличающийся тем, что соотношение меду парами Tg1 и Tx1, а также Тg2 и Тx2 составляет по меньшей мере 0,5.
40. Способ по п.39, отличающийся тем, что каждое из стекол первичных и вторичных содержит в сумме менее 40 мас.% SiO2, В2О3 и P2O5; по отношению к общей массе стекла.
41. Способ по п.39, отличающийся тем, что стекло - это система REO-Al2O3.
42. Способ по п.41, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3 и REO по отношению к общей массе стекла.
43. Способ по п.37, отличающийся тем, что стекло - это система REO-Al2O3-ZrO2.
44. Способ по п.43, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3, REO и ZrO2 по отношению к общей массе стекла.
45. Способ по п.37, отличающийся тем, что изделие представляет собой стекло, а сам способ включает в себя также термообработку стекла с получением стеклокерамики.
46. Изделие, изготовленное в соответствии со способом, описанным в п.45.
47. Способ по п.37, отличающийся тем, что разница между Тg и Тх составляет по меньшей мере 35 К.
48. Изделие, изготовленное в соответствии со способом, описанным в п.37, причем стекла первого и второго рядов имеют одинаковый состав.
49. Изделие, изготовленное в соответствии со способом, описанным в п.37, причем стекла первого и второго рядов имеют разный состав.
50. Изделие, изготовленное в соответствии со способом, описанным в п.37.
51. Способ изготовления изделия из стекла, включающий в себя: получение по меньшей мере первой совокупности частиц стекла, в котором содержатся как минимум два разных оксида металлов, а стекло характеризуется Тg и Тх, причем разница между Тg и Тх составляет как минимум 5 К, и содержит менее 20 мас.% SiO2, менее 20 мас.% В2O3 и менее 40 мас.% Р2O5; нагревание стекла до температуры выше Тg и коалесценция по меньшей мере части первой совокупности частиц с образованием изделия.
52. Способ по п.51, отличающийся тем, что разница между Тg и Тx составляет по меньшей мере 25 К.
53. Способ по п.52, отличающийся тем, что стекло характеризуется T1, a соотношение Тg и T1 составляет по меньшей мере 0,5.
54. Способ по п.53, отличающийся тем, что стекло содержит суммарно менее 40 мас.% стекла, состоящего из SiO2, В2О3 и Р2О5, по отношению к общей массе стекла.
55. Способ по п.53, отличающийся тем, что стекло - это система REO-Al2О3.
56. Способ по п.55, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3 и REO по отношению к общей массе стекла.
57. Способ по п.53, отличающийся тем, что стекло - это система REO-Al2O3-ZrO2.
58. Способ по п.57, отличающийся тем, что стекло содержит в сумме как минимум 80 мас.% Al2О3, REO и ZrO2 по отношению к общей массе стекла.
59. Способ по п.53, отличающийся тем, что изделие представляет собой стекло, а сам способ включает в себя также термообработку стекла с получением стеклокерамики.
60. Изделие, изготовленное в соответствии со способом, описанным в п.59.
61. Способ по п.53, отличающийся тем, что разница между Тg и Тх составляет по меньшей мере 35 К.
62. Изделие, изготовленное в соответствии со способом, описанным в п.53.
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- 2002-08-02 KR KR10-2004-7001552A patent/KR20040024600A/ko not_active Application Discontinuation
- 2002-08-02 ES ES02761219T patent/ES2295396T3/es not_active Expired - Lifetime
- 2002-08-02 WO PCT/US2002/024523 patent/WO2003011776A1/en active IP Right Grant
- 2002-08-02 CA CA002455953A patent/CA2455953A1/en not_active Abandoned
- 2002-08-02 DE DE60223550T patent/DE60223550T2/de not_active Expired - Lifetime
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- 2002-08-02 CN CNA028151267A patent/CN1714052A/zh active Pending
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Also Published As
Publication number | Publication date |
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JP2004536762A (ja) | 2004-12-09 |
CN1714052A (zh) | 2005-12-28 |
DE60223550T2 (de) | 2008-10-23 |
JP5237026B2 (ja) | 2013-07-17 |
CN101538114B (zh) | 2011-07-13 |
US20070135290A1 (en) | 2007-06-14 |
WO2003011776A1 (en) | 2003-02-13 |
CN101538119B (zh) | 2013-07-24 |
CN101538119A (zh) | 2009-09-23 |
JP2009190967A (ja) | 2009-08-27 |
JP2009013062A (ja) | 2009-01-22 |
BR0211576A (pt) | 2004-06-29 |
US8003217B2 (en) | 2011-08-23 |
CN101417860B (zh) | 2012-01-18 |
ES2295396T3 (es) | 2008-04-16 |
CN101538121B (zh) | 2012-09-05 |
DE60223550D1 (de) | 2007-12-27 |
KR20040024600A (ko) | 2004-03-20 |
KR20080086542A (ko) | 2008-09-25 |
CN101538121A (zh) | 2009-09-23 |
CN101538114A (zh) | 2009-09-23 |
JP2009179558A (ja) | 2009-08-13 |
CN101538120B (zh) | 2011-08-03 |
JP5324314B2 (ja) | 2013-10-23 |
CA2455953A1 (en) | 2003-02-13 |
JP2009179559A (ja) | 2009-08-13 |
JP2009221099A (ja) | 2009-10-01 |
CN101538120A (zh) | 2009-09-23 |
EP1412295B1 (en) | 2007-11-14 |
EP1412295A1 (en) | 2004-04-28 |
ATE378293T1 (de) | 2007-11-15 |
CN101417860A (zh) | 2009-04-29 |
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