ATE413408T1 - Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator - Google Patents
Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysatorInfo
- Publication number
- ATE413408T1 ATE413408T1 AT02780946T AT02780946T ATE413408T1 AT E413408 T1 ATE413408 T1 AT E413408T1 AT 02780946 T AT02780946 T AT 02780946T AT 02780946 T AT02780946 T AT 02780946T AT E413408 T1 ATE413408 T1 AT E413408T1
- Authority
- AT
- Austria
- Prior art keywords
- sulfur containing
- production
- phase transfer
- transfer catalyst
- formula
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title abstract 4
- 229910052717 sulfur Inorganic materials 0.000 title abstract 4
- 239000011593 sulfur Substances 0.000 title abstract 4
- 239000003444 phase transfer catalyst Substances 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 title 1
- 239000008346 aqueous phase Substances 0.000 abstract 3
- 150000003961 organosilicon compounds Chemical class 0.000 abstract 3
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- -1 sulfide compound Chemical class 0.000 abstract 2
- 229910052783 alkali metal Chemical group 0.000 abstract 1
- 150000001340 alkali metals Chemical group 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 238000003408 phase transfer catalysis Methods 0.000 abstract 1
- 229910000077 silane Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/895,719 US6534668B2 (en) | 2001-06-29 | 2001-06-29 | Preparation of sulfur-containing organosilicon compounds using a buffered phase transfer catalysis process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE413408T1 true ATE413408T1 (de) | 2008-11-15 |
Family
ID=25404951
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT02780946T ATE413408T1 (de) | 2001-06-29 | 2002-05-13 | Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6534668B2 (de) |
| EP (1) | EP1480989B1 (de) |
| JP (1) | JP4268039B2 (de) |
| KR (1) | KR100835875B1 (de) |
| CN (1) | CN1283644C (de) |
| AT (1) | ATE413408T1 (de) |
| AU (1) | AU2002308708A1 (de) |
| DE (1) | DE60229787D1 (de) |
| TW (1) | TW593326B (de) |
| WO (1) | WO2003002573A2 (de) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4035690B2 (ja) * | 2001-04-06 | 2008-01-23 | 信越化学工業株式会社 | 有機珪素化合物の製造方法 |
| US6740767B1 (en) * | 2002-11-12 | 2004-05-25 | Dow Corning Corporation | Method of making sulfur containing organosilicon compounds |
| US7125497B1 (en) * | 2003-05-22 | 2006-10-24 | Sandia Corporation | Reactive formulations for a neutralization of toxic industrial chemicals |
| US8008520B2 (en) * | 2003-07-03 | 2011-08-30 | Momentive Performance Materials Inc. | Process for the preparation of thiocarboxylate silane |
| US7794782B2 (en) * | 2004-06-09 | 2010-09-14 | Dow Corning Corporation | Phosphonate and sulfido silane anti-corrosion additive for electrical cable restoration fluid |
| CN1305879C (zh) * | 2004-06-09 | 2007-03-21 | 上海人怡精细化工有限公司 | 一种相转移催化剂制造硅－69的工艺 |
| US6998452B1 (en) | 2005-01-14 | 2006-02-14 | The Goodyear Tire & Rubber Company | Controlled free radical agent for nanocomposite synthesis |
| DE102005037690A1 (de) * | 2005-08-10 | 2007-02-15 | Degussa Ag | Verfahren zur Herstellung von Organosiliciumverbindungen |
| JP2007091677A (ja) * | 2005-09-30 | 2007-04-12 | Shin Etsu Chem Co Ltd | スルフィド鎖含有有機珪素化合物の製造方法 |
| JP2007091678A (ja) * | 2005-09-30 | 2007-04-12 | Shin Etsu Chem Co Ltd | スルフィド鎖含有有機珪素化合物の製造方法 |
| WO2007061550A1 (en) * | 2005-11-16 | 2007-05-31 | Dow Corning Corporation | Organosilanes and their preparation and use in elastomer compositions |
| DE102006041356A1 (de) * | 2006-09-01 | 2008-03-20 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Organosilanen |
| DE102007062282A1 (de) * | 2007-12-21 | 2009-06-25 | Saltigo Gmbh | Verfahren zur Herstellung von Thiodiglycolsäuredialkylestern |
| CA2737039C (en) * | 2008-10-09 | 2015-08-04 | Ceramatec, Inc. | Apparatus and method for reducing an alkali metal electrochemically at a temperature below the metal's melting temperature |
| US9475998B2 (en) | 2008-10-09 | 2016-10-25 | Ceramatec, Inc. | Process for recovering alkali metals and sulfur from alkali metal sulfides and polysulfides |
| US8551339B2 (en) * | 2009-03-06 | 2013-10-08 | Heritage Environmental Services Llc | Use of silica for the removal of organosilanes |
| CN102286017B (zh) * | 2011-07-12 | 2014-06-18 | 泰山医学院 | 一种双-[丙基三乙氧基硅烷]-二硫化物的合成方法 |
| CN102993228A (zh) * | 2012-12-06 | 2013-03-27 | 青岛晟科材料有限公司 | 一种双-[丙基三甲氧基硅烷]-二硫化物硅烷偶联剂的合成方法 |
| CN103772427B (zh) * | 2014-01-28 | 2016-03-02 | 南京曙光硅烷化工有限公司 | 双[丙基三乙氧基硅烷]二硫化物的制备方法 |
| JP6378100B2 (ja) * | 2015-01-28 | 2018-08-22 | 住友ゴム工業株式会社 | タイヤ用ゴム組成物およびタイヤ |
| EP3838905A1 (de) | 2019-12-18 | 2021-06-23 | Evonik Operations GmbH | Verfahren zur herstellung von polysulfansilanen mittels phasentransferkatalyse |
| CN111269258B (zh) * | 2020-03-19 | 2022-08-19 | 厦门威亮光学涂层技术有限公司 | 一种含硫有机硅化合物及其制备方法和用途 |
| DE102020211042A1 (de) | 2020-09-02 | 2022-03-03 | Evonik Operations Gmbh | Verfahren zur Herstellung von Polysulfansilanen mittels Phasentransferkatalyse |
| CN114478616B (zh) * | 2022-01-12 | 2024-05-10 | 湖北江瀚新材料股份有限公司 | 一种3-(n-咪唑)丙基三乙氧基硅烷及其合成方法 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3590065A (en) | 1969-07-18 | 1971-06-29 | Dow Corning | Method of preparing mercaptoalkylalkoxy silanes |
| US4082790A (en) | 1974-12-11 | 1978-04-04 | Dow Corning Corporation | Method of preparing mercaptans |
| US4401826A (en) | 1982-09-10 | 1983-08-30 | General Electric Company | Method for production of mercapto functional silanes |
| DE3346910C1 (de) | 1983-12-24 | 1985-05-02 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von Mercaptoalkylsilanen |
| DE4025866A1 (de) | 1990-08-16 | 1992-02-20 | Huels Chemische Werke Ag | Verfahren zur herstellung von mercaptosilanen |
| US5399739A (en) | 1994-04-18 | 1995-03-21 | Wright Chemical Corporation | Method of making sulfur-containing organosilanes |
| US5405985A (en) | 1994-07-08 | 1995-04-11 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5468893A (en) | 1994-07-08 | 1995-11-21 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5466848A (en) | 1994-09-28 | 1995-11-14 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5489701A (en) | 1994-09-28 | 1996-02-06 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5596116A (en) | 1995-09-11 | 1997-01-21 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5840952A (en) | 1995-11-02 | 1998-11-24 | Shin-Etsu Chemical Co., Ltd. | Method of manufacturing 3-mercaptopropylalkoxy silane |
| US5583245A (en) | 1996-03-06 | 1996-12-10 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5663396A (en) | 1996-10-31 | 1997-09-02 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| DE19651849A1 (de) | 1996-12-13 | 1998-06-18 | Degussa | Verfahren zur Herstellung von Bis(silylorganyl)-polysulfanen |
| DE19732725A1 (de) | 1997-07-30 | 1999-02-04 | Degussa | Mischungen, bestehend aus Bis(silylorganyl)polysulfanen und Silylorganylthiocyanaten, ihre Herstellung und Verwendung |
| DE19734295C1 (de) | 1997-08-08 | 1999-02-25 | Degussa | Verfahren zur Herstellung von Organosiliciumdisulfanen hoher Reinheit |
| JP3498559B2 (ja) | 1997-12-01 | 2004-02-16 | 信越化学工業株式会社 | 短鎖ポリスルフィドシラン混合物の製造方法 |
| JP3501008B2 (ja) | 1998-04-10 | 2004-02-23 | ダイソー株式会社 | 含硫黄有機珪素化合物の製造方法およびその合成中間体の製造方法 |
| US6172251B1 (en) * | 1998-07-24 | 2001-01-09 | The Goodyear Tire & Rubber Company | Solid/liquid phase transfer system |
| US6384256B1 (en) * | 2001-06-29 | 2002-05-07 | Dow Corning Corporation | Process for the preparation of sulfur-containing organosilicon compounds |
-
2001
- 2001-06-29 US US09/895,719 patent/US6534668B2/en not_active Expired - Lifetime
-
2002
- 2002-05-13 WO PCT/US2002/015162 patent/WO2003002573A2/en active Application Filing
- 2002-05-13 AT AT02780946T patent/ATE413408T1/de not_active IP Right Cessation
- 2002-05-13 AU AU2002308708A patent/AU2002308708A1/en not_active Abandoned
- 2002-05-13 KR KR1020037017132A patent/KR100835875B1/ko active IP Right Grant
- 2002-05-13 EP EP02780946A patent/EP1480989B1/de not_active Expired - Lifetime
- 2002-05-13 JP JP2003508954A patent/JP4268039B2/ja not_active Expired - Lifetime
- 2002-05-13 CN CNB028131177A patent/CN1283644C/zh not_active Expired - Lifetime
- 2002-05-13 DE DE60229787T patent/DE60229787D1/de not_active Expired - Lifetime
- 2002-05-31 TW TW091111716A patent/TW593326B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CN1639173A (zh) | 2005-07-13 |
| EP1480989A2 (de) | 2004-12-01 |
| TW593326B (en) | 2004-06-21 |
| US6534668B2 (en) | 2003-03-18 |
| US20030013901A1 (en) | 2003-01-16 |
| CN1283644C (zh) | 2006-11-08 |
| KR100835875B1 (ko) | 2008-06-09 |
| JP2005505512A (ja) | 2005-02-24 |
| EP1480989B1 (de) | 2008-11-05 |
| JP4268039B2 (ja) | 2009-05-27 |
| AU2002308708A1 (en) | 2003-03-03 |
| KR20040015304A (ko) | 2004-02-18 |
| WO2003002573A2 (en) | 2003-01-09 |
| DE60229787D1 (de) | 2008-12-18 |
| WO2003002573A3 (en) | 2004-09-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |