2009 Karthik
2009 Karthik
2009 Karthik
a r t i c l e i n f o a b s t r a c t
Article history: Shear punch testing has been a very useful technique for evaluating mechanical properties of irradiated
Received 11 February 2009 alloys using a very small volume of material. The load–displacement data is influenced by the compliance
Accepted 23 June 2009 of the fixture components. This paper describes a modified experimental approach where the complianc-
es of the punch and die components are eliminated. The analysis of the load–displacement data using the
modified setup for various alloys like low carbon steel, SS316, modified 9Cr–1Mo, 2.25Cr–1Mo indicate
that the shear yield strength evaluated at 0.2% offset of normalized displacement relates to the tensile
YS as per the Von Mises yield relation (rys = 1.73sys). A universal correlation of type UTS = msmax where
m is a function of strain hardening exponent, is seen to be obeyed for all the materials in this study. The
use of analytical models developed for blanking process are explored for evaluating strain hardening
exponent from the load–displacement data. This study is directed towards rationalizing the tensile–shear
empirical correlations for a more reliable prediction of tensile properties from shear punch tests.
Ó 2009 Elsevier B.V. All rights reserved.
1. Introduction ment. Finite element simulation and analysis of the shear punch
test by Toloczko et al. [4] revealed that the compliance in the test
The shear punch test is a very useful mechanical test technique frame and fixturing had a profound effect on the shape of the LDC.
for evaluating the mechanical properties viz. yield strength, maxi- To minimize the effects of test frame compliance on the LDC, the
mum strength and strain hardening exponent using very small vol- test setup was modified suitably to accommodate a displacement
umes of material [1]. The driving force for development of this sensor across the test fixture [5] or coupled to the moving punch
technique has been the material development programmes for fu- [6,7].
sion and fission reactors. The small volumes of specimens could be The other aspect that has caught the attention of many investi-
easily fitted into the existing irradiation space and permitted easy gators is the accurate measurement of the yield load from the LDC.
handling due to low radioactivity for mechanical property evalua- The point of deviation from linearity of the initial portion of LDC
tion [2]. As a spin-off, it has a variety of other applications in situ- was first used as an approximate measure of the shear yield load
ations where conventional mechanical tests are not possible such [2]. However, for materials exhibiting a very smooth transition
as weld joints [3], coatings and failure analysis. from the linear to the non-linear deformation, this method of locat-
The shear punch (ShP) test technique involves slow blanking of ing the yield load resulted in considerable scatter. In one of our
a thin disc material clamped between a set of dies at a constant earlier studies, it was shown that online acoustic emission moni-
speed as shown schematically in Fig. 1. The deformation occurs toring during the test led to accurate prediction of the yield load
in the small annular region of the punch–die clearance. The [8]. Researchers subsequently adopted the method of measuring
load–displacement curve (LDC) obtained during the blanking oper- yield stress at an offset shear strain analogous to the offset proce-
ation (Fig. 2) is very similar to that obtained in a conventional uni- dure used in tensile testing.
axial tensile test and the properties obtained by analyzing the ShP To rationalize the methodology for shear yield strength deter-
test curve can be correlated to the corresponding conventional ten- mination, Guduru et al. [9] carried out finite element analysis
sile properties. (FEA) of the initial stages of punch displacement. Based on the
Many investigators have evolved the experimental test setup development of plastic deformation zone completely through the
and the method of analyzing the LDC over a period of time. In specimen thickness, they concluded that an offset of 0.15% of initial
the initial period of its development, investigators used the cross- linear portion of FEA generated stress–normalized displacement
head movement as an approximate measure of punch displace- curve represent the shear yield stress. However, this corresponded
to an offset of 1% in the actual experiments due to the compliance
effects of the test fixtures. The shear yield strength corresponding
* Corresponding author. Tel.: +91 44 27480122; fax: +91 44 27480356.
E-mail address: karthik@igcar.gov.in (V. Karthik). to 1% offset in their study satisfied the relation rys = 1.77sys which
0022-3115/$ - see front matter Ó 2009 Elsevier B.V. All rights reserved.
doi:10.1016/j.jnucmat.2009.06.027
426 V. Karthik et al. / Journal of Nuclear Materials 393 (2009) 425–432
0.5% and 1% are compared with the tensile YS for the various mate-
rials. The offset criterion which produces the best fit between ten-
sile YS and shear yield strength is established and compared with
published results. The nature of correlations obtained for maxi-
mum strength in ShP test and the corresponding UTS is also inves-
tigated. It is found that UTS can be related to shear maximum
strength through a function involving the strain hardening expo-
nent without any alloy specific constants. Finally an attempt is
made to evaluate the strain hardening exponent from load–dis-
placement data using analytical models developed for blanking
process.
2. Experimental procedure
Fig. 3 shows the schematic of the shear punch test fixture devel-
oped at the authors’ laboratory. The test fixture consists of a flat
Fig. 1. Schematic of the shear punch test technique. punch of 3 mm diameter made of a hardened tool steel (RC 62)
and a set of dies between which the specimen is clamped. The
diameter of the receiving hole in the lower die is 3.04 mm. The test
fixture is placed on the compression platens of a universal test ma-
chine for carrying out the test. The load during the punch operation
is measured using a standard load cell of 4 kN. A linear variable dif-
ferential transformer (LVDT) of range ±2.5 mm is fixed at the bot-
tom of the test fixture as shown in Fig. 4. The LVDT is coupled to
the center of the specimen bottom using a stiff tungsten carbide
rod to measure the specimen displacement. The test fixture, LVDT
and the connecting rod are placed in line for accurate measure-
ment of the specimen deformation. The experimental setup has
also provisions for positioning the LVDT at the top of the moving
punch as shown in Fig. 5. This was to enable the comparison of
the LDC’s obtained using the two methods of displacement mea-
surement. The load and displacement data are acquired through
a 16 bit resolution data acquisition system built in the test ma-
chine controller.
2.2. Materials
Fig. 4. The experimental setup of shear punch tests showing the LVDT attachment
coupled to the bottom of the specimen clamped in the test fixture. 3. Results and discussion
Table 1
Chemical composition of the various steels used in this study.
In wt.% C Si Mn Cr Mo Ni N Nb V Fe Condition
AISI type 1025 carbon steel 0.23 0.40 Bal Annealed
2.25Cr–1Mo steel 0.06 0.18 0.48 2.18 0.93 Bal Normalized and tempered
Mod 9Cr–1Mo steel 0.096 0.32 0.46 8.72 0.90 0.10 0.05 0.08 0.22 Bal Normalized and tempered
AISI 316 SS 0.06 1.0 2.0 17.0 2.4 12.0 – – – Bal Annealed
428 V. Karthik et al. / Journal of Nuclear Materials 393 (2009) 425–432
Fig. 8. Comparison of the load–displacement plots obtained for SS316 using the
modified experimental setup before and after applying the compliance correction. Fig. 9. ShP test curves of SS 316 samples with different thicknesses.
V. Karthik et al. / Journal of Nuclear Materials 393 (2009) 425–432 429
The offset definition of 0.2% is much less than the value of 1% re-
ported by Toloczko and Guduru. A larger percentage offset re-
quired in their experiments was due to the finite compliances of
the die and punch components. In the present investigation, these
compliances are eliminated through (i) the use of LVDT at bottom
of the specimen and (ii) corrections through elastic loading tests. Fig. 11. Linear fit between the tensile and shear yield strengths of various materials
This resulted in steeper loading curve enabling accurate evaluation for different offsets.
of shear YS at 0.2% offset. This offset is in close agreement with the
FEA offset of 0.15% obtained by Guduru et al. [9] with rigid punch,
die and holder components. The equation of linear fit obtained be- 3.3.2. Maximum strength correlation
tween tensile YS and 0.2% offset shear yield strength is The UTS and corresponding shear maximum strength (smax) of
rys = 1.73sys which is exactly the same as Von Mises yield relation various alloys is plotted in Fig. 12. The linear correlation through
for shear deformation. origin yields a slope of 1.29 with R2 = 0.96 and standard deviation
The nature of tensile–shear correlations obtained from shear of ±45 MPa. In the earlier work by Hamilton et al. [10], Hankin et al.
punch tests has been a subject of debate over a period of years. [11] on various alloy systems, correlation equations of type UT-
Early studies led to development of material specific correlations S = A1smax + B1 were established with slope (A1) ranging from 1.8
of type r = As + B for yield and maximum strength with a range to 2.9 and intercept B1 ranging from 38 to 425 for various alloy
of A and B values for various alloy class. With the insights provided classes. Similar linear correlations for tensile–shear maximum
by FEA and improvements in displacement measurement for com- strength obtained in our earlier works using different heat treated
pliance corrections, the yield correlation simplified into a universal and cold worked microstructural conditions of 2.25Cr–1Mo [5],
equation of type rys = Asys with a material independent value for A. Mod 9Cr–1Mo [12] and SS316 is reproduced in Fig. 13. The limited
This work establishes that the offset definition for shear yield strength range over which the data were obtained for each alloy
strength with the modified experimental setup is 0.2% and the class could not force a best linear fit through origin and hence re-
shear YS so computed matches with the Von Mises yield relation. sulted in an intercept parameter B1. Hamilton et al. suggested that
The experimentally obtained universal value of A = 1.73 for yield the differences in the fit parameters between various alloys could
correlation clearly shows that the deformation in shear punch test be partly due to the size of the data base for each alloy class and
is shear dominant in the early stages of deformation. This enables partly due to punch–specimen–die friction. Based on these obser-
direct estimation of tensile yield strength of irradiated alloys using vations, a single correlation equation with a slope (A1) of 2.2 for
shear punch tests using the 0.2% offset definition without requiring all alloy data sets [10] were arrived by Hamilton et al. only after
any other material specific constants. subtracting the intercept values B1 from the respective data sets.
Table 2
Tensile and shear punch test results of various materials studied.
Fig. 14. Plot showing the excellent agreement between the experimental shear
maximum strength and that predicted using Eq. (4).
Fig. 12. The linear fit between UTS and shear maximum strength.
Fig. 16. Schematic of the shear deformation (a) pure shear and (b) with bending of the blank material fibers [16].
A universal correlation of type UTS = msmax, where ‘m’ is a func- [3] V. Karthik, K.V. Kasiviswanathan, K. Laha, Baldev Raj, Weld. J. (Res. Suppl.),
AWS (2002) 265s.
tion of strain hardening exponent, is found to be valid for all alloys
[4] M.B. Toloczko, Y. Yokokura, K. Abe, M.L. Hamilton, F.A. Garner, R.J. Kurtz, in:
in this study. The value of coefficient ‘m’ is found to be always less M.A. Sokolov, J.D. Landes, G.E. Lucas (Eds.), Small Specimen Test Techniques,
than the yield correlation constant. vol. 4, ASTM STP 1418, 2002, p. 371.
Analytical models of shearing process are found to be useful but [5] V. Karthik, K. Laha, K.V. Kasiviswanathan, Baldev Raj, in: M.A. Sokolov, J.D.
Landes, G.E. Lucas (Eds.), Small Specimen Test Techniques, vol. 4, ASTM STP
with limited success for accurately predicting the strain hardening 1418, 2002, p. 380.
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[7] R.K. Guduru, K.A. Darling, R. Kishore, R.O. Scattergood, C.C. Koch, K.L. Murty,
punch tests towards developing methodologies for accurate evalu- Mater. Sci. Eng. A 395 (2005) 307.
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[12] V. Karthik, K. Laha, P. Parameswaran, K.V. Kasiviswanathan, Baldev Raj, J. Test.
(IGCAR) during the course of the work.
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