CN110115706A - Resveratrol after-sun recovery product and its production method - Google Patents
Resveratrol after-sun recovery product and its production method Download PDFInfo
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- CN110115706A CN110115706A CN201910540274.2A CN201910540274A CN110115706A CN 110115706 A CN110115706 A CN 110115706A CN 201910540274 A CN201910540274 A CN 201910540274A CN 110115706 A CN110115706 A CN 110115706A
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61Q17/005—Antimicrobial preparations
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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Abstract
Resveratrol after-sun recovery product and its production method belong to Cosmetic Manufacture technical field, are first uniformly mixed chamomile hydrosol, rose, xanthan gum, hyaluronic acid and trehalose, obtain water phase mixture；The newborn wooden fruit rouge, Sweet Almond Oil, vitamin E, lanolin and emulsifier are uniformly mixed again, oil is obtained and mixes body；Oil is mixed body body mixed with water to mix, by emulsifying, cooling matrix；Resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide are mixed with matrix again after mixing, it is agitated uniformly after add bacteriostatic agent, then it is agitated, obtain resveratrol after-sun recovery product.The product that the method for the present invention is made is more stable, has higher tolerances to powder and pH-value, conducive to keep resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide activity, the using effect of product can be improved.
Description
Technical field
The invention belongs to Cosmetic Manufacture technical fields, and in particular to the production technology of after-sun recovery face cream or lotion.
Background technique
Ultraviolet light (Ultraviolet, UV) in daylight is broadly divided into UVA(320-400nm according to biological action difference)
And UVB(280-320nm) and UVC(100-280nm).Since atmospheric ozone layer is to the absorption of UVC, life is at the earth's surface
The mankind's mainly irradiation by UVA and a small amount of UVB.Skin is related with wavelength to ultraviolet ray transmissivity, the longer penetration power of wavelength
It is stronger.UVB damages epidermis mainly by epidermal absorption, and UVA can then go directly upper part of dermis, act on dermal vascular and other groups
It knits.It can express a series of defense reaction after skin exposure ultraviolet light, if Epidermal basal layer cells split speed is accelerated, cutin
Layer thickens, and pigment is deepened, and certain photochemical transformations occur for keratin, to hinder the transmission of incident ray.Action of ultraviolet radiation in
Various photoactive substances or color base in skin can induce and generate a large amount of free radical, destroy the antioxidant system of skin itself, make
Activities of antioxidant enzymes reduces and causes the accumulation of lipid peroxidation product.Free radical promotes DNA to form pyrimidine dimer simultaneously, makes
DNA oxidative damage, and then DNA chain fracture and base oxidation, finally cause skin photoage phenomenon
Skin is exposed to the sun by daylight, can dry water shortage, general red, if not carrying out sun-proof prevention, it is easy to appear red for skin
Phenomena such as swollen, tanned, shouting pain, bubble, decortication.Once skin is tanned severely, 6~8 hours after solarization are the skin first aid phases, and 72 is small after solarization
Shi Ze is golden period after shining, and can give different skin care modes, such as whitening, moisturizing or reparation for being exposed to the sun, improve skin
Skin restores rapidly skin condition before shining because of aging phenomenon caused by having shone a large amount of ultraviolet lights.If can be given within the gold reparation phase
It gives skin correctly to maintain, the chance of blackening or exsiccation can be greatly reduced.
Resveratrol is a kind of non-flavonoids polyphenolic substance with stilbene class formation, is primarily present in grape, peanut, mulberry
In the plants such as Shen and polygonum cuspidate, there is the various biologicals activity such as anti-oxidant, anti-aging, antitumor, prevention cardiovascular disease.It leads
It will be by removing or free radical being inhibited to generate, anti-lipid peroxidation adjusts anti-oxidant related enzyme activity, improves oxidation product
The mechanisms plays antioxidation such as content.Resveratrol can also reduce KIR, TYR, SLC45A2 etc. by the expression of downward MCR1
The expression of gene inhibits the activity of TYR enzyme from multi-signal approach, blocks the generation and transhipment of melanin, bright color.Have
Studies have shown that resveratrol can activate antioxidase directly in conjunction with DNA, effectively removing free radical is newest to protect DNA
Research finds that resveratrol can activate TyrRS and be inducted into core, to play the protective effect to DNA damage.Meanwhile it is white
Veratryl alcohol also has the function of moisturizing moisturizing, anti-inflammation and sterilization.
Gotu Kola P.E is the extract obtained from umbelliferae centella, containing there are many important ingredient, than
Such as essential oil, sterol, flavonols, match carbohydrate, polyethylene and saponin.Enzyme in newly-generated tissue can be improved in Gotu Kola P.E
Type and non-enzyme type polyphenoils mutase, hydrogen peroxide, glutathione peroxidase, vitamin E and ascorbic acid usp/bp
Content further proves that it, in the strong skin effect such as anti-oxidant, anti-aging, can also dispel the cuticula of aging, promote skin new
Old metabolism, increases skin elasticity, and the element that supplements the nutrients, and help promotes skin corium collagen to be formed, there is the effect for enabling skin compact
Fruit.Gotu Kola P.E has clearing heat and detoxicating, inducing diuresis and reducing edema effect, and helps there are many impaired skin tissue repairs and contain
The Triterpenoid of a- botany bar gum alcohol type has calm, stable effect, and calm skin can be helped by being added in skin care item, be alleviated
Sensitivity phenomenon.
Niacinamide also known as VB3 are important a member in vitamin family, it can accelerate metabolism, promote to contain melanin
Horn cell fall off, promote epidermis protein synthesis, improve skin quality；Vitamin E is a kind of liposoluble vitamin,
It is one of most important antioxidant, vitamin E, which enters Skin Cell, directly to help skin to free radical resisting, ultraviolet light and dirt
The infringement for contaminating object prevents skin from following the string because of some chronic or recessive injury until aging；Aloe vera extract
In natural anthraquinone glycoside be natural whitening and sunscreen ingredient, can effectively prevent the activity of ultraviolet light stimulation tyrosinase, prevent black
The generation and calmness of pigment, thus there is good bright color, remove yellow gas, whitening effect.Meanwhile there are also good for aloe
The effect of moisturizing moisturizing.Hyaluronic acid is also known as sodium hyaluronate, referred to as ideal natural moisturizing factor.It can improve skin-nourishing
Metabolism, make skin it is tender, it is smooth, go wrinkle, increase elasticity, prevent aging, be good Transdermal absorption rush again while moisturizing
Into agent.
Trehalose is widely present in nature, is a kind of carbohydrate for having close relation with biological life, in scientific circles
It is known as the laudatory title of " sugar of life ", its holding cell viability with super strength and the active function of large biological molecule in high temperature, are done
Under the environment such as dry, intensive ultraviolet, one layer of special protective film can be formed in cell surface, not only be able to maintain the original nutrition of skin
And moisture, moreover it is possible to nourishes rough skin cell, while melanin deposition, effective anti-aging can be reduced to avoid skin sunburn.
After-sun recovery frost at present on the market adds chemical component, more or less there is certain irritation to skin.It shines
Skin afterwards can a large amount of dehydration, it is serious can black it is rubescent, it is sensitive fragile.Therefore people first have to releive, Lavender Extract, give
Skin cooling, then gives skin certain replenishing water and preserving moisture, and whitening can be such that percutaneous absorption doubles while moisturizing.
Summary of the invention
An object of the present disclosure is to propose a kind of resveratrol after-sun recovery product, to provide one kind skin after solarization for people
The effect of timely nutrition, reparation is given in the case where skin injury, water shortage.
The present invention includes resveratrol, Gotu Kola P.E, aloe vera extract, niacinamide, vitamin E, transparent
The wooden fruit rouge of matter acid, cream, Sweet Almond Oil, trehalose, xanthan gum, lanolin, chamomile hydrosol, rose, virgin olive oil cream
Agent and bacteriostatic agent.
This after-sun recovery product can be repair cream, be also possible to repair latex, wherein natural active matter --- white Chenopodiaceae
Reed alcohol plays the role of improving and rehabilitating for skin after shining, and can supplement moisture of skin rapidly, reduces melanin deposition.This hair
It is bright to also added the substances such as niacinamide, vitamin E, Gotu Kola P.E and aloe vera extract, several active material phases
It is mutually synergistic, moisturizing, whitening and maintenance are carried out for the skin after shining.Formula is especially added with trehalose, it can effectively be protected
Shield DNA is the Conservative restoration factor of Skin Cell DNA, while it is suitable to improve Skin Cell from damaging caused by radioactive ray
Answer the ability of environment, intelligent moisturizing.Fine and smooth, soft non-stimulated, the non-greasy in repair cream frost constitution ground absorbs fast.It is antibacterial in formula
Agent selects nano antibacterial agent, to no skin irritation, has good inhibiting effect to various bacteria in weak acid environment.
Further, after above-mentioned resveratrol, Gotu Kola P.E, aloe vera extract, niacinamide account for solarization respectively
Repair 1~10%, 0.1~2%, 0.1~2%, the 1~5% of product gross mass.The after-sun recovery frost obtained according to this ratio, it is various
Effective component interacts with each other, synergistic, for that while skin repair, can better play moisturizing, whitening after shining
Effect.
80 wt % of asiatic centella total salidroside content or more in the Gotu Kola P.E.Asiaticoside is Gotu Kola P.E
Main effective ingredient, when asiatic centella total salidroside content reaches 80wt% or more, it has the strong skin effects such as anti-oxidant, anti-aging, also
The cuticula of aging can be dispelled, skin metabolism is promoted, increases skin elasticity, and the element that supplements the nutrients, repairs and is damaged after shining
Skin tissue, help promote skin corium collagen to be formed, there is the effect for enabling skin compact.
The present invention is another object is that propose the production method of the above resveratrol after-sun recovery frost.
Production method of the present invention the following steps are included:
1) chamomile hydrosol, rose, xanthan gum, hyaluronic acid and trehalose are mixed under 75~85 DEG C of environment temperature
Uniformly, water phase mixture is obtained；
2) the newborn wooden fruit rouge, Sweet Almond Oil, vitamin E, lanolin and emulsifier are mixed under 70~80 DEG C of environment temperature equal
It is even, it obtains oil and mixes body；
3) oil is mixed body body mixed with water to mix, by emulsifying, is cooled to 30~50 DEG C, obtains matrix；
4) resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide are mixed with matrix again after mixing,
It is agitated uniformly after add bacteriostatic agent, then it is agitated, obtain resveratrol after-sun recovery product.
Above step 1), 2) in the temperature condition that mixes it is different, be the heated aqueous because aqueous phase system heat dissipation is very fast
Temperature is higher than oily heat phase temperature.
Cooling condition can be cooled down using water-bath in step 3), also can choose natural cooling.
In step 4), since resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide are all natural work
Property substance, their non-refractories, in order to avoid causing active decline because of high temperature, so mixed with the matrix that is cooled to 30~50 DEG C again
It closes.
The present invention is more stable using the product that heat is made as method, has higher tolerances to powder and pH-value,
In addition the method for the present invention be conducive to keep resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide activity, can
Improve the using effect of product.Due to bacteriostatic agent non-refractory, the technics comparing of addition is simple, directly in the system mixed
It is added and mixes.
In addition, resveratrol of the present invention, Gotu Kola P.E, aloe vera extract and niacinamide the matter that feeds intake
Amount accounts for 1~10%, 0.1~2%, 0.1~2%, the 1~5% of after-sun recovery product gross mass of feeding intake respectively.
The mass ratio that feeds intake of the chamomile hydrosol and rose is 1: 1.5~2；Chamomile hydrosol and rose
Gross mass of feeding intake accounts for the 60~80% of after-sun recovery product gross mass of feeding intake.Chamomile hydrosol contains a large amount of esters compositions, Shu Minxiao
Fruit is particularly significant, can alleviate the skin of sunburn, and red and swollen skin after calm solarization, prevents melanin deposition, moreover it is possible to reinforcing group rapidly
It knits, increases elasticity；The comparison of ingredients of rose is complicated, and containing alcohol, aldehyde, acid, ester, ether etc., these ingredients all play oneself solely
Special effect, plays the effect of overall balance, and whatsoever skin quality can use, can moisturizing whitening, skin after solarization of releiving.
It by both hydrosols based on rose, feeds intake in proportion, skin after the solarization that can not only releive can more make skin keep bullet
Property, brilliant white.The two gross mass account for after-sun recovery product gross mass of feeding intake ratio can according to oneself hobby be adjusted: when than
Example is 60% or so, and white body state, which is presented, in the mixture worked it out can be made into emulsion form for mixture for ratio enlargement to 80%
State.
Bacteriostatic agent of the present invention preferably uses guanidine bacteriostatic agent, this bacteriostatic agent belongs to nano antibacterial agent, nontoxic, tasteless, without corruption
Corrosion, stability is good, safely and effectively, good antimicrobial effect.Nano antibacterial agent is sustained positively charged silver ion with controlled speed,
The cell wall of bacterium, mould is firmly adsorbed and penetrated, microorganism electron-transport system, respiratory system, mass transfer system are destroyed
System is to kill rapidly thallus；It can also be reacted with the hydroxyl of bacterium in into cell body, solidify bacterio protein, cell loss
The value-added ability of cell division and it is dead.
Specific embodiment
One, preparation process:
Embodiment one: resveratrol after-sun recovery frost is prepared
It weighs: resveratrol 5g, Gotu Kola P.E 0.3g, aloe vera extract 0.5g, niacinamide 1g, vitamin E
0.2g, hyaluronic acid 0.5g, cream wood fruit rouge 6g, Sweet Almond Oil 1g, xanthan gum 0.5g, trehalose 5g, lanolin 0.1g, mix pure
Chamomile hydrosol and the rose mixing that dew 72.85g(is 1: 1.5~2 by mass ratio form), emulsifier 7g, guanidine is antibacterial
Agent 0.05g.
Preparation method:
1, mixing hydrosol, xanthan gum, hyaluronic acid and trehalose are mixed, is uniformly mixed under 85 DEG C of water bath conditions, obtains water
Mix body.
2, the newborn wooden fruit rouge, Sweet Almond Oil, vitamin E, lanolin and emulsifier are mixed, is mixed under 80 DEG C of water bath conditions
Uniformly, it obtains oil and mixes body.
3, oil is mixed body to be slowly added in water phase mixture, emulsifying.
After the completion of emulsification, 40 DEG C are naturally cooled to, forms matrix.
4, resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide are first uniformly mixed, then slowly
Be added in matrix, quickly stir evenly, then add guanidine bacteriostatic agent, then it is agitated uniformly after to get 100g resveratrol
After-sun recovery frost.
Embodiment two: resveratrol after-sun recovery frost is prepared.
It weighs: resveratrol 6g, Gotu Kola P.E 0.2g, aloe vera extract 0.6g, niacinamide 2g, vitamin
E 0.2g, hyaluronic acid 0.6g, cream wood fruit rouge 8g, Sweet Almond Oil 2g, trehalose 6g, xanthan gum 0.6g, lanolin 0.1g, mixing
Chamomile hydrosol and the rose mixing that hydrosol 65.65g(is 1: 1.5~2 by mass ratio form), emulsifier 8g, guanidine suppression
Microbial inoculum 0.05g.
Preparation method:
1, mixing hydrosol, xanthan gum, hyaluronic acid and trehalose are mixed, is uniformly mixed under 80 DEG C of water bath conditions, obtains water
Mix body.
2, the newborn wooden fruit rouge, Sweet Almond Oil, vitamin E, lanolin and emulsifier are mixed, is mixed under 75 DEG C of water bath conditions
Uniformly, it obtains oil and mixes body.
3, oil is mixed body to be slowly added in water phase mixture, emulsifying；After the completion of emulsification, 35 are naturally cooled to
DEG C, form matrix.
4, first resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide are uniformly mixed, then slowly
Be added in matrix, quickly after mixing evenly, add guanidine bacteriostatic agent, then it is agitated uniformly after to get the solarization of 100g resveratrol
Repair cream afterwards.
Embodiment three: resveratrol after-sun recovery lotion is prepared.
It weighs: resveratrol 5g, Gotu Kola P.E 2g, aloe vera extract 0.6g, niacinamide 1g, vitamin E
1g, hyaluronic acid 0.5g, cream wood fruit rouge 2g, Sweet Almond Oil 2g, trehalose 4g, xanthan gum 0.5g, lanolin 0.1g, mix hydrosol
Chamomile hydrosol and the rose mixing that 78.28g(is 1: 1.5~2 by mass ratio form), emulsifier 3g, guanidine bacteriostatic agent
0.02g。
Preparation method:
1, mixing hydrosol, xanthan gum, hyaluronic acid and trehalose are mixed, is uniformly mixed under 80 DEG C of water bath conditions, obtains water
Mix body.
2, the newborn wooden fruit rouge, Sweet Almond Oil, vitamin E, lanolin and emulsifier are mixed, is mixed under 75 DEG C of water bath conditions
Uniformly, it obtains oil and mixes body.
3, oil is mixed body to be slowly added in water phase mixture, emulsifying；After the completion of emulsification, 35 are naturally cooled to
DEG C, form matrix.
4, first resveratrol, Gotu Kola P.E, aloe vera extract, niacinamide are uniformly mixed, then slowly
It is added in matrix, quickly stirs evenly, guanidine bacteriostatic agent is then added；It is agitated uniformly after to get 100g resveratrol shine after
Repair latex.
Two, experiment detection:
1, the pH value detection of product:
The repair cream and repair latex that Example one, two, three obtains detect pH value with pH meter, the results show that three's pH value
Between 6~7, faintly acid.Human normal skin surface pH value is about 5~7, resveratrol after-sun recovery frost of the invention and
The pH value of repair latex is close with skin, does not stimulate mildly.
2, irritation, anaphylaxis detection:
Detection method: first soaking one piece of gauze with distilled water or physiological saline, is screwed onto half-dried, and is folded into 4 layers about 1 square centimeter
Skin care item, are coated in the one side of gauze by size, are then applied and are stretched on side or back normal skin in forearm, then cover 1.5 squares lis
The air-locked glassine paper of rice or plastic film, with immobilization with adhesive tape.By observation in 24~48 hours, if itching or bright at test
Bitterly, show the being irritating to the skin property of skin care item, be then positive reaction, trier should be removed in time, rinsed with clear water.If
It is reacted at test without any discomfort, is then negative reaction, indicate the skin care item to no skin irritation, relatively safety.
Several volunteers are found, the repair cream and repair latex that embodiment one, two, three is obtained are according to above-mentioned method
Detection irritation and anaphylaxis, testing result are shown, by observation in 24~48 hours, are not gone out at all volunteer's detections
Existing any discomfort reaction indicates that the product, can be safe to use to no skin irritation and anaphylaxis, relatively safety.
3, repairing test:
60 female volunteers (age is between 25 ~ 55 years old) are randomly selected, they are divided into three groups, every group of 20 people make respectively
With the after-sun recovery frost of embodiment 1,2,3, application method is: after going out back daily, cleaning is carried out, by after-sun recovery frost
It is uniformly coated on the face and skin solarization position, it is complete to be gently massaged into absorption.Time is two weeks, observes after-sun recovery after two weeks
Effect.
After-sun recovery effect is divided into three grades:
The first estate: skin becomes that water is tender pale, more preferable than the skin quality before solarization.
Second grade: skin becomes calm, water profit of releiving by rubescent, nigrescence, redness, restores the skin quality before solarization.
The tertiary gradient: skin becomes pitch-dark, dry, does not play the role of after-sun recovery.
After-sun recovery effect, see the table below:
| The first estate | Second grade | The tertiary gradient | |
| Embodiment 1 | 16 | 3 | 1 |
| Embodiment 2 | 14 | 5 | 1 |
| Embodiment 3 | 18 | 2 | 0 |
It can be seen from the above result that after-sun recovery frost of the invention, after-sun recovery effect reach 90% or more, skin after solarization can be risen
To the effect of releive calm, moisturizing moisturizing, whitening.
Claims (7)
1. resveratrol after-sun recovery product, it is characterised in that extracted including resveratrol, Gotu Kola P.E, aloe barbadensis Miller
The wooden fruit rouge of object, niacinamide, vitamin E, hyaluronic acid, cream, Sweet Almond Oil, trehalose, xanthan gum, lanolin, chamomile hydrosol,
Rose, virgin olive oil emulsifier and bacteriostatic agent.
2. resveratrol after-sun recovery product according to claim 1, it is characterised in that the resveratrol, centella are extracted
Object, aloe vera extract, niacinamide account for 1~10%, 0.1~2%, 0.1~2%, the 1 of after-sun recovery product gross mass respectively
~5%.
3. resveratrol after-sun recovery product according to claim 2, it is characterised in that accumulated snow in the Gotu Kola P.E
Careless 80 wt % of total glycoside content or more.
4. the production method of resveratrol after-sun recovery product as described in claim 1, it is characterised in that the following steps are included:
1) chamomile hydrosol, rose, xanthan gum, hyaluronic acid and trehalose are mixed under 75~85 DEG C of environment temperature
Uniformly, water phase mixture is obtained；
2) the newborn wooden fruit rouge, Sweet Almond Oil, vitamin E, lanolin and emulsifier are mixed under 70~80 DEG C of environment temperature equal
It is even, it obtains oil and mixes body；
3) oil is mixed body body mixed with water to mix, by emulsifying, is cooled to 30~50 DEG C, obtains matrix；
4) resveratrol, Gotu Kola P.E, aloe vera extract and niacinamide are mixed with matrix again after mixing,
It is agitated uniformly after add bacteriostatic agent, then it is agitated, obtain resveratrol after-sun recovery product.
5. the production method of resveratrol after-sun recovery product according to claim 4, it is characterised in that the resveratrol,
The quality that feeds intake of Gotu Kola P.E, aloe vera extract and niacinamide accounts for after-sun recovery product gross mass of feeding intake respectively
1~10%, 0.1~2%, 0.1~2%, 1~5%.
6. the production method of resveratrol after-sun recovery product according to claim 4 or 5, it is characterised in that the chamomile
The mass ratio that feeds intake of hydrosol and rose is 1: 1.5~2；Chamomile hydrosol and the gross mass of feeding intake of rose are repaired after accounting for solarization
The 60~80% of duplicate gross mass of feeding intake.
7. the production method of resveratrol after-sun recovery product according to claim 4 or 5, it is characterised in that the bacteriostatic agent
For guanidine bacteriostatic agent.
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| WO2021127677A1 (en) * | 2019-12-16 | 2021-06-24 | Colgate-Palmolive Company | Personal care compositions and methods for the same |
| US12097280B2 (en) | 2019-12-16 | 2024-09-24 | Colgate-Palmolive Company | Personal care compositions and methods for the same |
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| WO2021127677A1 (en) * | 2019-12-16 | 2021-06-24 | Colgate-Palmolive Company | Personal care compositions and methods for the same |
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