CN117017869B - Whitening and freckle-removing cream and preparation method thereof - Google Patents
Whitening and freckle-removing cream and preparation method thereof Download PDFInfo
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- CN117017869B CN117017869B CN202311194796.4A CN202311194796A CN117017869B CN 117017869 B CN117017869 B CN 117017869B CN 202311194796 A CN202311194796 A CN 202311194796A CN 117017869 B CN117017869 B CN 117017869B
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- 230000002087 whitening effect Effects 0.000 title claims abstract description 50
- 208000003351 Melanosis Diseases 0.000 title claims abstract description 49
- 239000006071 cream Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title abstract description 14
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 42
- -1 ethylhexyl isopalmitate Chemical compound 0.000 claims abstract description 26
- 229940082500 cetostearyl alcohol Drugs 0.000 claims abstract description 25
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 25
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims abstract description 25
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 claims abstract description 25
- RTBWWWVNZWFNBV-SFHVURJKSA-N (2s)-3-phenyl-2-(undec-10-enoylamino)propanoic acid Chemical compound C=CCCCCCCCCC(=O)N[C@H](C(=O)O)CC1=CC=CC=C1 RTBWWWVNZWFNBV-SFHVURJKSA-N 0.000 claims abstract description 17
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 17
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 17
- DFPAKSUCGFBDDF-ZQBYOMGUSA-N [14c]-nicotinamide Chemical compound N[14C](=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-ZQBYOMGUSA-N 0.000 claims abstract description 17
- BJRNKVDFDLYUGJ-ZIQFBCGOSA-N alpha-Arbutin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-ZIQFBCGOSA-N 0.000 claims abstract description 17
- 229940033280 alpha-arbutin Drugs 0.000 claims abstract description 17
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N benzoic acid ethyl ester Natural products CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 claims abstract description 17
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims abstract description 17
- 235000011187 glycerol Nutrition 0.000 claims abstract description 17
- 239000003755 preservative agent Substances 0.000 claims abstract description 17
- 230000002335 preservative effect Effects 0.000 claims abstract description 17
- 241001673954 Magnolia sieboldii Species 0.000 claims abstract description 16
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960001631 carbomer Drugs 0.000 claims abstract description 9
- 229920002545 silicone oil Polymers 0.000 claims abstract description 9
- 230000001804 emulsifying effect Effects 0.000 claims description 32
- 238000003756 stirring Methods 0.000 claims description 24
- 238000001914 filtration Methods 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 8
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 8
- 239000000498 cooling water Substances 0.000 claims description 8
- 229940008099 dimethicone Drugs 0.000 claims description 8
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 8
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 8
- 238000007599 discharging Methods 0.000 claims description 8
- 229930182478 glucoside Natural products 0.000 claims description 8
- 150000008131 glucosides Chemical class 0.000 claims description 8
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 8
- 229940057910 shea butter Drugs 0.000 claims description 8
- 235000014121 butter Nutrition 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 235000003115 Diospyros discolor Nutrition 0.000 abstract description 8
- 240000000902 Diospyros discolor Species 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 6
- 230000000052 comparative effect Effects 0.000 description 25
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Substances C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 5
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 5
- CSHZYWUPJWVTMQ-UHFFFAOYSA-N 4-n-Butylresorcinol Chemical compound CCCCC1=CC=C(O)C=C1O CSHZYWUPJWVTMQ-UHFFFAOYSA-N 0.000 description 2
- 206010014970 Ephelides Diseases 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 241000218378 Magnolia Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A61K8/34—Alcohols
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
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- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
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- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a whitening and freckle-removing cream and a preparation method thereof, wherein the whitening and freckle-removing cream comprises the following components in parts by mass: 4-6 parts of ethylhexyl isopalmitate, 0.5-1 part of butter fruit, 1-5 parts of polydimethyl silicone oil, 1-5 parts of C12-15 alcohol benzoate, 2-4 parts of cetostearyl alcohol, 2.5-8 parts of emulsifying agent, 4-6 parts of glycerin, 4-6 parts of dipropylene glycol, 0.1-0.3 part of carbomer, 0.1-0.3 part of triethanolamine, 1-3 parts of nicotinamide, 0.1-0.5 part of undecylenoyl phenylalanine, 0.5-1 part of alpha-arbutin, 0.1-0.5 part of magnolia sieboldii extract, 0.1-1 part of 4-butyl isophthalol, 0.4-0.6 part of preservative and 0.05-0.15 part of essence; wherein the emulsifier comprises three of A165 emulsifier, montanov68 and DELTA MB; the whitening and freckle-removing cream and the preparation method thereof have the advantages of good absorbability, good whitening and freckle-removing effects, fine appearance and good skin feel.
Description
Technical Field
The invention relates to the technical field of skin care products, in particular to whitening and freckle removing cream and a preparation method thereof.
Background
Whitening is a durable and popular topic. Bright and uniform skin color has become a focus of attention, and more people desire to have healthy and fair skin. And the increase of environmental pollution and the load of ultraviolet rays, more and more color sinking and color spots become trouble. Therefore, various skin care products for whitening and removing freckles appear on the market, such as: whitening and freckle removing cream and the like. The 4-butyl resorcinol is a common component in whitening and freckle-removing products, but the 4-butyl resorcinol has the problems of difficult emulsification, poor skin feel and poor use experience, so that skin care products such as whitening and freckle-removing cream are easy to cause, are not easy to be absorbed by skin, cannot fully exert the whitening and freckle-removing effects, and have poor effects; and the appearance and skin feel of the product are poor.
Disclosure of Invention
The invention aims to provide whitening and freckle-removing cream and a preparation method thereof, and the whitening and freckle-removing cream has the advantages of good absorbability, good whitening and freckle-removing effects, fine appearance and good skin feel.
To achieve the purpose, the invention adopts the following technical scheme:
the whitening and freckle-removing cream comprises the following components in parts by mass: 4-6 parts of ethylhexyl isopalmitate, 0.5-1 part of butter fruit, 1-5 parts of polydimethyl silicone oil, 1-5 parts of C12-15 alcohol benzoate, 2-4 parts of cetostearyl alcohol, 2.5-8 parts of emulsifying agent, 4-6 parts of glycerin, 4-6 parts of dipropylene glycol, 0.1-0.3 part of carbomer, 0.1-0.3 part of triethanolamine, 1-3 parts of nicotinamide, 0.1-0.5 part of undecylenoyl phenylalanine, 0.5-1 part of alpha-arbutin, 0.1-0.5 part of magnolia sieboldii extract, 0.1-1 part of 4-butyl isophthalol, 0.4-0.6 part of preservative and 0.05-0.15 part of essence;
wherein the emulsifier comprises three of A165 emulsifier, montanov68 and DELTA MB.
As a preferable scheme of the whitening and freckle-removing cream, 0.5-2 parts of the A165 emulsifying agent, 1-3 parts of Montanov68 and 1-3 parts of DELTA MB are adopted.
As a preferable scheme of the whitening and freckle removing cream, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The invention also provides a preparation method of the whitening and freckle-removing cream, which comprises the following steps:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
The invention has the beneficial effects that: according to the whitening and freckle-removing cream and the preparation method thereof, the DELTA MB, the A165 emulsifier and the Montanov68 form the emulsifier, and the three components are mutually matched and emulsified, so that each component of the whitening and freckle-removing cream has high compatibility, and each component is mutually matched; the problems of poor appearance, stickiness and poor skin feel of the product are effectively solved, so that the product is finer in appearance, good in skin feel and easy to absorb, can fully play the roles of whitening and removing freckles, and is excellent in effect.
Detailed Description
Embodiments of the present disclosure are described in detail below.
Other advantages and effects of the present disclosure will become readily apparent to those skilled in the art from the following disclosure, which describes embodiments of the present disclosure by way of specific examples. It will be apparent that the described embodiments are merely some, but not all embodiments of the present disclosure. The disclosure may be embodied or practiced in other different specific embodiments, and details within the subject specification may be modified or changed from various points of view and applications without departing from the spirit of the disclosure. It should be noted that the following embodiments and features in the embodiments may be combined with each other without conflict. All other embodiments, which can be made by one of ordinary skill in the art without inventive effort, based on the embodiments in this disclosure are intended to be within the scope of this disclosure.
Example 1
The embodiment discloses a whitening and freckle-removing cream, which comprises the following components in parts by mass: 4 parts of ethylhexyl isopalmitate, 0.5 part of butter fruit, 1 part of polydimethyl silicone oil, 1 part of C12-15 alcohol benzoate, 2 parts of cetostearyl alcohol, 0.5 part of A165 emulsifier, 68 parts of Montanov, 1 part of DELTA MB, 4 parts of glycerin, 4 parts of dipropylene glycol, 0.1 part of carbomer, 0.1 part of triethanolamine, 1 part of nicotinamide, 0.1 part of undecylenoyl phenylalanine, 0.5 part of alpha-arbutin, 0.1 part of magnolia extract, 0.1 part of 4-butyl m-benzene glycol, 0.4 part of preservative and 0.05 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The preparation method of the whitening and freckle-removing cream comprises the following steps of:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
Example 2
The embodiment discloses a whitening and freckle-removing cream, which comprises the following components in parts by mass: 6 parts of ethylhexyl isopalmitate, 1 part of butter fruit, 5 parts of polydimethyl silicone oil, 5 parts of C12-15 alcohol benzoate, 4 parts of cetostearyl alcohol, 2 parts of A165 emulsifier, 68 parts of Montanov, 3 parts of DELTA MB, 6 parts of glycerin, 6 parts of dipropylene glycol, 0.3 part of carbomer, 0.3 part of triethanolamine, 3 parts of nicotinamide, 0.5 part of undecylenoyl phenylalanine, 1 part of alpha-arbutin, 0.5 part of magnolia sieboldii extract, 1 part of 4-butyl m-benzene glycol, 0.6 part of preservative and 0.15 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The preparation method of the whitening and freckle-removing cream comprises the following steps of:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
Example 3
The embodiment discloses a whitening and freckle-removing cream, which comprises the following components in parts by mass: 5 parts of ethylhexyl isopalmitate, 0.75 part of butter fruit, 3 parts of polydimethyl silicone oil, 3 parts of C12-15 alcohol benzoate, 3 parts of cetostearyl alcohol, 1 part of A165 emulsifier, 68 parts of Montanov, 2 parts of DELTA MB, 5 parts of glycerin, 5 parts of dipropylene glycol, 0.2 part of carbomer, 0.2 part of triethanolamine, 2 parts of nicotinamide, 0.3 part of undecylenoyl phenylalanine, 0.75 part of alpha-arbutin, 0.3 part of magnolia sieboldii extract, 0.5 part of 4-butyl isophthalol, 0.5 part of preservative and 0.1 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The preparation method of the whitening and freckle-removing cream comprises the following steps of:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
Comparative example 1
The whitening and freckle-removing cream of the comparative example 1 comprises the following components in parts by mass: 5 parts of ethylhexyl isopalmitate, 0.75 part of butter fruit, 3 parts of polydimethyl silicone oil, 3 parts of C12-15 alcohol benzoate, 3 parts of cetostearyl alcohol, 1 part of A165 emulsifier, 68 parts of Montanov, 5 parts of glycerin, 5 parts of dipropylene glycol, 0.2 part of carbomer, 0.2 part of triethanolamine, 2 parts of nicotinamide, 0.3 part of undecylenoyl phenylalanine, 0.75 part of alpha-arbutin, 0.3 part of magnolia sieboldii extract, 0.5 part of 4-butyl m-benzene glycol, 0.5 part of preservative and 0.1 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The preparation method of the whitening and freckle-removing cream comprises the following steps of:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
Comparative example 2
The whitening and freckle-removing cream of the comparative example 2 comprises the following components in parts by mass: 5 parts of ethylhexyl isopalmitate, 0.75 part of butter fruit, 3 parts of polydimethyl silicone oil, 3 parts of C12-15 alcohol benzoate, 3 parts of cetostearyl alcohol, 3 parts of A165 emulsifier, 68 parts of Montanov, 5 parts of glycerin, 5 parts of dipropylene glycol, 0.2 part of carbomer, 0.2 part of triethanolamine, 2 parts of nicotinamide, 0.3 part of undecylenoyl phenylalanine, 0.75 part of alpha-arbutin, 0.3 part of magnolia sieboldii extract, 0.5 part of 4-butyl m-benzene glycol, 0.5 part of preservative and 0.1 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The preparation method of the whitening and freckle-removing cream comprises the following steps of:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
Comparative example 3
The whitening and freckle-removing cream of the comparative example 3 comprises the following components in parts by mass: 5 parts of ethylhexyl isopalmitate, 0.75 part of butter fruit, 3 parts of polydimethyl silicone oil, 3 parts of C12-15 alcohol benzoate, 3 parts of cetostearyl alcohol, 1 part of A165 emulsifier, 68 parts of Montanov, 5 parts of glycerin, 5 parts of dipropylene glycol, 0.2 part of carbomer, 0.2 part of triethanolamine, 2 parts of nicotinamide, 0.3 part of undecylenoyl phenylalanine, 0.75 part of alpha-arbutin, 0.3 part of magnolia sieboldii extract, 0.5 part of 4-butyl m-benzene glycol, 0.5 part of preservative and 0.1 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
The preparation method of the whitening and freckle-removing cream comprises the following steps of:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
Comparative example 4
Comparative example 4 is one of the common whitening and freckle-removing creams product A on the market.
Comparative example 5
Comparative example 5 is one of the common whitening and freckle-removing creams product B on the market.
The difference between comparative example 1 and example 3 is: comparative example 1 mass parts of DELTA MB removed;
the difference between comparative example 2 and example 3 is: comparative example 2 DELTA MB was replaced with a165 emulsifier in parts by mass;
the difference between comparative example 3 and example 3 is: comparative example 3 the mass fraction of DELTA MB was replaced with Montanov 68.
Skin feel test
40 female consumers are selected as an evaluation member, and the appearance and skin feel of the product are evaluated, wherein the evaluation score is divided into: four grades, good, medium, bad, the object is: the whitening and freckle removing cream prepared in example 3, the whitening and freckle removing creams prepared in comparative examples 1 to 3, the product A of comparative example 4 and the product B of comparative example 5 are shown in Table 1:
TABLE 1
| Scoring of | Excellent (excellent) | Good grade (good) | In (a) | Difference of difference |
| Example 3 | 38 | 2 | 0 | 0 |
| Comparative example 1 | 0 | 0 | 19 | 21 |
| Comparative example 2 | 0 | 0 | 22 | 18 |
| Comparative example 3 | 0 | 2 | 18 | 20 |
| Comparative example 4 | 0 | 3 | 16 | 21 |
| Comparative example 5 | 0 | 10 | 16 | 14 |
As can be seen from Table 1, the whitening and freckle-removing cream prepared by the invention has better appearance and skin feel than other products of comparative examples, and is accepted and favored by female consumers.
The above description is for the purpose of illustrating the embodiments of the present invention and is not to be construed as limiting the invention, but is intended to cover all modifications, equivalents, improvements and alternatives falling within the spirit and principles of the invention.
Claims (2)
1. The whitening and freckle-removing cream is characterized by comprising the following components in parts by mass: 4-6 parts of ethylhexyl isopalmitate, 0.5-1 part of butter, 1-5 parts of polydimethyl silicone oil, 1-5 parts of C12-15 alcohol benzoate, 2-4 parts of cetostearyl alcohol, 0.5-2 parts of A165 emulsifier, 1-3 parts of Montanov68, 1-3 parts of DELTA MB, 4-6 parts of glycerin, 4-6 parts of dipropylene glycol, 0.1-0.3 part of carbomer, 0.1-0.3 part of triethanolamine, 1-3 parts of nicotinamide, 0.1-0.5 part of undecylenoyl phenylalanine, 0.5-1 part of alpha-arbutin, 0.1-0.5 part of magnolia sieboldii extract, 0.1-1 part of 4-butyl isophthalol, 0.4-0.6 part of preservative and 0.05-0.15 part of essence;
wherein, the Montanov68 comprises the following components in percentage by weight: 80% of cetostearyl alcohol and 20% of cetostearyl glucoside.
2. A method for preparing the whitening and freckle-removing cream as claimed in claim 1, which is characterized by comprising the following steps:
s1: heating the water phase to 80-85deg.C for dissolving, maintaining the temperature for 20min, and filtering, wherein the water phase is: glycerol, dipropylene glycol, carbomers, and triethanolamine;
s2: heating the oil phase at 80 ℃ for 180-300s, and filtering, wherein the oil phase is: ethylhexyl isopalmitate, shea butter, dimethicone, C12-15 alcohol benzoate, cetostearyl alcohol, A165 emulsifier, montanov68 and DELTA MB;
s3: adding the solutions obtained in the step S1 and the step S2 into a homogenizing emulsifying machine, preserving heat and stirring for 10min;
s4: continuously stirring by a homogenizing emulsifying machine, and simultaneously adding cooling water for cooling;
s5: when the temperature is reduced to 60-70 ℃, the homogenizing emulsifying machine is vacuumized and defoamed for 3 times;
s6: when the temperature drops below 60 ℃, phase C will be entered, wherein phase C is: nicotinamide, undecylenoyl phenylalanine, alpha-arbutin, magnolia sieboldii extract and 4-butylisophthalol;
s7: when the temperature is reduced to below 45 ℃, adding preservative and essence;
s8: stirring for 5-10min by using a homogenizing emulsifying machine;
s9: discharging when the temperature is reduced to 38-45 ℃;
s10: standing for 24 hours to obtain the whitening and freckle removing cream.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108210384A (en) * | 2018-01-04 | 2018-06-29 | 广州雅纯化妆品制造有限公司 | A kind of whitening spot-removing skin care item and preparation method thereof |
| WO2018144093A2 (en) * | 2016-11-03 | 2018-08-09 | Pinsky Mark A | Formulations for improved skin care |
| CN109106640A (en) * | 2018-09-12 | 2019-01-01 | 南昌欧泉琳化妆品有限公司 | A kind of whitening and spot eliminating cream and preparation method thereof |
| CN111956557A (en) * | 2020-09-16 | 2020-11-20 | 铭颜生物科技(广州)有限公司 | Composition and cosmetic with whitening and spot-fading effects and preparation method thereof |
| CN112932990A (en) * | 2021-04-15 | 2021-06-11 | 广州樊文花化妆品有限公司 | Anti-aging composition and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7277083B2 (en) * | 2018-06-12 | 2023-05-18 | ロレアル | Effervescent composition |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018144093A2 (en) * | 2016-11-03 | 2018-08-09 | Pinsky Mark A | Formulations for improved skin care |
| CN108210384A (en) * | 2018-01-04 | 2018-06-29 | 广州雅纯化妆品制造有限公司 | A kind of whitening spot-removing skin care item and preparation method thereof |
| CN109106640A (en) * | 2018-09-12 | 2019-01-01 | 南昌欧泉琳化妆品有限公司 | A kind of whitening and spot eliminating cream and preparation method thereof |
| CN111956557A (en) * | 2020-09-16 | 2020-11-20 | 铭颜生物科技(广州)有限公司 | Composition and cosmetic with whitening and spot-fading effects and preparation method thereof |
| CN112932990A (en) * | 2021-04-15 | 2021-06-11 | 广州樊文花化妆品有限公司 | Anti-aging composition and preparation method and application thereof |
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