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CN117017869B - 一种美白祛斑霜及制备方法 - Google Patents

一种美白祛斑霜及制备方法 Download PDF

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CN117017869B
CN117017869B CN202311194796.4A CN202311194796A CN117017869B CN 117017869 B CN117017869 B CN 117017869B CN 202311194796 A CN202311194796 A CN 202311194796A CN 117017869 B CN117017869 B CN 117017869B
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贺安然
贺键
黄桂香
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Abstract

本发明公开了一种美白祛斑霜及制备方法,按质量份计,美白祛斑霜的组分包括:异棕榈酸乙基己酯4‑6份、牛油果树果脂0.5‑1份、聚二甲基硅油1‑5份、C12‑15醇苯甲酸酯1‑5份、鲸蜡硬脂醇2‑4份、乳化剂2.5‑8份、甘油4‑6份、双丙甘醇4‑6份、卡波姆0.1‑0.3份、三乙醇胺0.1‑0.3份、烟酰胺1‑3份、十一碳烯酰基苯丙氨酸0.1‑0.5份、α‑熊果苷0.5‑1份、天女木兰提取物0.1‑0.5份、4‑丁基间苯二醇0.1‑1份、防腐剂0.4‑0.6份和香精0.05‑0.15份;其中乳化剂由A165乳化剂、Montanov 68和DELTA MB三种组成;该美白祛斑霜及制备方法具有吸收性好、美白祛斑效果好、外观细腻、肤感好的优点。

Description

一种美白祛斑霜及制备方法
技术领域
本发明涉及护肤品技术领域,具体涉及一种美白祛斑霜及制备方法。
背景技术
美白是一个经久不衰、永远流行的话题。明亮均匀的肤色已成为人们关注的焦点,越来越多的人群渴望拥有健康白皙的肌肤。而环境污染的增加和紫外线的负重,越来越多的色沉、色斑成为了大家的困扰。因此市场上出现各类美白祛斑的护肤产品,如:美白祛斑霜等。其中4-丁基间苯二酚是美白祛斑产品中常见的一种成分,但4-丁基间苯二酚存在难以乳化,以及肤感不好,使用体验感差的问题,从而容易导致美白祛斑霜等护肤品,不易被皮肤吸收,美白祛斑效果无法充分发挥,效果差;且产品的外观和肤感较差。
发明内容
本发明的目的在于提供一种美白祛斑霜及制备方法,其具有吸收性好、美白祛斑效果好、外观细腻、肤感好的优点。
为达此目的,本发明采用以下技术方案:
提供一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯4-6份、牛油果树果脂0.5-1份、聚二甲基硅油1-5份、C12-15醇苯甲酸酯1-5份、鲸蜡硬脂醇2-4份、乳化剂2.5-8份、甘油4-6份、双丙甘醇4-6份、卡波姆0.1-0.3份、三乙醇胺0.1-0.3份、烟酰胺1-3份、十一碳烯酰基苯丙氨酸0.1-0.5份、α-熊果苷0.5-1份、天女木兰提取物0.1-0.5份、4-丁基间苯二醇0.1-1份、防腐剂0.4-0.6份和香精0.05-0.15份;
其中乳化剂由A165乳化剂、Montanov 68和DELTA MB三种组成。
作为美白祛斑霜的一种优选方案,所述A165乳化剂为0.5-2份、Montanov68为1-3份、DELTA MB为1-3份。
作为美白祛斑霜的一种优选方案,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
本发明还提供一种美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
本发明的有益效果:本发明提出的美白祛斑霜及制备方法,通过DELTA MB与A165乳化剂、Montanov 68组成乳化剂,三者相互配合乳化使得美白祛斑霜各成分之间具有高度兼容性,且各成分相互配合;有效解决了产品外观差、黏腻、肤感不佳的问题,使得产品外观更加细腻,肤感好、易于吸收,能充分发挥美白祛斑的作用且效果优异。
具体实施方式
下面对本公开实施例进行详细描述。
以下通过特定的具体实例说明本公开的实施方式,本领域技术人员可由本说明书所揭露的内容轻易地了解本公开的其他优点与功效。显然,所描述的实施例仅仅是本公开一部分实施例,而不是全部的实施例。本公开还可以通过另外不同的具体实施方式加以实施或应用,本说明书中的各项细节也可以基于不同观点与应用,在没有背离本公开的精神下进行各种修饰或改变。需说明的是,在不冲突的情况下,以下实施例及实施例中的特征可以相互组合。基于本公开中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本公开保护的范围。
实施例1
本实施例公开了一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯4份、牛油果树果脂0.5份、聚二甲基硅油1份、C12-15醇苯甲酸酯1份、鲸蜡硬脂醇2份、A165乳化剂0.5份、Montanov 68 1份、DELTA MB 1份、甘油4份、双丙甘醇4份、卡波姆0.1份、三乙醇胺0.1份、烟酰胺1份、十一碳烯酰基苯丙氨酸0.1份、α-熊果苷0.5份、天女木兰提取物0.1份、4-丁基间苯二醇0.1份、防腐剂0.4份和香精0.05份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
上述美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
实施例2
本实施例公开了一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯6份、牛油果树果脂1份、聚二甲基硅油5份、C12-15醇苯甲酸酯5份、鲸蜡硬脂醇4份、A165乳化剂2份、Montanov 68 3份、DELTA MB 3份、甘油6份、双丙甘醇6份、卡波姆0.3份、三乙醇胺0.3份、烟酰胺3份、十一碳烯酰基苯丙氨酸0.5份、α-熊果苷1份、天女木兰提取物0.5份、4-丁基间苯二醇1份、防腐剂0.6份和香精0.15份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
上述美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
实施例3
本实施例公开了一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯5份、牛油果树果脂0.75份、聚二甲基硅油3份、C12-15醇苯甲酸酯3份、鲸蜡硬脂醇3份、A165乳化剂1份、Montanov 68 2份、DELTA MB 2份、甘油5份、双丙甘醇5份、卡波姆0.2份、三乙醇胺0.2份、烟酰胺2份、十一碳烯酰基苯丙氨酸0.3份、α-熊果苷0.75份、天女木兰提取物0.3份、4-丁基间苯二醇0.5份、防腐剂0.5份和香精0.1份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
上述美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
对比例1
对比例1的一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯5份、牛油果树果脂0.75份、聚二甲基硅油3份、C12-15醇苯甲酸酯3份、鲸蜡硬脂醇3份、A165乳化剂1份、Montanov 68 2份、甘油5份、双丙甘醇5份、卡波姆0.2份、三乙醇胺0.2份、烟酰胺2份、十一碳烯酰基苯丙氨酸0.3份、α-熊果苷0.75份、天女木兰提取物0.3份、4-丁基间苯二醇0.5份、防腐剂0.5份和香精0.1份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
上述美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
对比例2
对比例2的一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯5份、牛油果树果脂0.75份、聚二甲基硅油3份、C12-15醇苯甲酸酯3份、鲸蜡硬脂醇3份、A165乳化剂3份、Montanov 68 2份、甘油5份、双丙甘醇5份、卡波姆0.2份、三乙醇胺0.2份、烟酰胺2份、十一碳烯酰基苯丙氨酸0.3份、α-熊果苷0.75份、天女木兰提取物0.3份、4-丁基间苯二醇0.5份、防腐剂0.5份和香精0.1份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
上述美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
对比例3
对比例3的一种美白祛斑霜,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯5份、牛油果树果脂0.75份、聚二甲基硅油3份、C12-15醇苯甲酸酯3份、鲸蜡硬脂醇3份、A165乳化剂1份、Montanov 68 4份、甘油5份、双丙甘醇5份、卡波姆0.2份、三乙醇胺0.2份、烟酰胺2份、十一碳烯酰基苯丙氨酸0.3份、α-熊果苷0.75份、天女木兰提取物0.3份、4-丁基间苯二醇0.5份、防腐剂0.5份和香精0.1份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
上述美白祛斑霜的制备方法,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
对比例4
对比例4为市场上其中一款普通美白祛斑霜产品A。
对比例5
对比例5为市场上其中一款普通美白祛斑霜产品B。
对比例1与实施例3的区别为:对比例1去除DELTA MB的质量份;
对比例2与实施例3的区别为:对比例2将DELTA MB的质量份用A165乳化剂代替;
对比例3与实施例3的区别为:对比例3将DELTA MB的质量份用Montanov68代替。
肤感测试
选40位女性消费者作为测评员,对产品的外观及肤感进行使用测评,测评评分分为:优良、中、差四个等级,对象为:实施例3制备得到的美白祛斑霜、对比例1-3制备得到的美白祛斑霜、对比例4的产品A和对比例5的产品B,测试结果如表1所示:
表1
评分
实施例3 38 2 0 0
对比例1 0 0 19 21
对比例2 0 0 22 18
对比例3 0 2 18 20
对比例4 0 3 16 21
对比例5 0 10 16 14
由表1可知,本发明制备的美白祛斑霜相比其他对比例的产品外观及肤感更佳,更受女性消费者的认可和喜爱。
以上仅为说明本发明的实施方式,并不用于限制本发明,对于本领域的技术人员来说,凡在本发明的精神和原则之内,不经过创造性劳动所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。

Claims (2)

1.一种美白祛斑霜,其特征在于,按质量份计,所述美白祛斑霜的组分包括:异棕榈酸乙基己酯4-6份、牛油果树果脂0.5-1份、聚二甲基硅油1-5份、C12-15醇苯甲酸酯1-5份、鲸蜡硬脂醇2-4份、A165乳化剂0.5-2份、Montanov68 1-3份、DELTA MB 1-3份、甘油4-6份、双丙甘醇4-6份、卡波姆0.1-0.3份、三乙醇胺0.1-0.3份、烟酰胺1-3份、十一碳烯酰基苯丙氨酸0.1-0.5份、α-熊果苷0.5-1份、天女木兰提取物0.1-0.5份、4-丁基间苯二醇0.1-1份、防腐剂0.4-0.6份和香精0.05-0.15份;
其中,所述Montanov 68以重量百分含量计包含以下组分:鲸蜡硬脂醇80%和鲸蜡硬脂基葡糖苷20%。
2.一种权利要求1所述美白祛斑霜的制备方法,其特征在于,包括以下步骤:
S1:将水相加热到80-85℃溶解,并保温消毒20min,再过滤,其中水相为:甘油、双丙甘醇、卡波姆和三乙醇胺;
S2:将油相在80℃的温度下加热180-300s,再过滤,其中油相为:异棕榈酸乙基己酯、牛油果树果脂、聚二甲基硅油、C12-15醇苯甲酸酯、鲸蜡硬脂醇、A165乳化剂、Montanov 68和DELTA MB;
S3:将步骤S1和步骤S2得到的溶液加入到均质乳化机中,保温并搅拌10min;
S4:均质乳化机持续搅拌,同时加入冷却水进行冷却;
S5:当温度下降到60-70℃时,均质乳化机抽真空消泡3次;
S6:当温度下降到60℃以下时,将入C相,其中C相为:烟酰胺、十一碳烯酰基苯丙氨酸、α-熊果苷、天女木兰提取物和4-丁基间苯二醇;
S7:当温度下降到45℃以下时,加入防腐剂和香精;
S8:均质乳化机继续搅拌5-10min;
S9:当温度下降到38-45℃时,出料;
S10:静置24小时,获得美白祛斑霜。
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WO2018144093A2 (en) * 2016-11-03 2018-08-09 Pinsky Mark A Formulations for improved skin care
CN109106640A (zh) * 2018-09-12 2019-01-01 南昌欧泉琳化妆品有限公司 一种美白祛斑霜及其制备方法
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WO2018144093A2 (en) * 2016-11-03 2018-08-09 Pinsky Mark A Formulations for improved skin care
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CN109106640A (zh) * 2018-09-12 2019-01-01 南昌欧泉琳化妆品有限公司 一种美白祛斑霜及其制备方法
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