CN107669548A - A kind of crease-resistant Wash-free mask and preparation method thereof - Google Patents
A kind of crease-resistant Wash-free mask and preparation method thereof Download PDFInfo
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- CN107669548A CN107669548A CN201711031662.5A CN201711031662A CN107669548A CN 107669548 A CN107669548 A CN 107669548A CN 201711031662 A CN201711031662 A CN 201711031662A CN 107669548 A CN107669548 A CN 107669548A
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- Prior art keywords
- crease
- free mask
- wash
- resistant wash
- resistant
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
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- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of crease-resistant Wash-free mask and preparation method thereof, more particularly to cosmetic mask field, the crease-resistant Wash-free mask, which is removed, includes NMF, thickener, outside preservative and emulsifying agent, it also added micromolecular collagen, blood orange elite, urea and vitamin E, not only increase the content of functional component of facial mask, the micromolecular collagen and blood orange elite of addition are more beneficial for the absorption of skin, the effect of improving facial mask, preparation method of the invention by the way that aqueous phase to be added to oil phase in batches, the facial mask of preparation has film forming uniform, the advantages of facial mask stability is good.
Description
Technical field
The invention belongs to cosmetic technical field, is related to facial mask technical field, and in particular to a kind of crease-resistant Wash-free mask and
Its preparation method.
Background technology
Facial mask rises skin temperature by obstructing contact, suppression sebum secretion and evaporation of perspiration of the skin with air, flesh
It after skin temperature rises, will stimulate circulation, the active ingredient in facial mask is penetrated into epidermis or deeper, wider array of
Side.Blood circulation accelerates that skin can be made ruddy, glossy, and skin absorbs more juicy, nutrition elite and various active ingredients
Afterwards, skin water shortage and low and deep, reduction microgroove generation, delay skin aging can be effectively improved, and plays nti-freckle to a certain extent
The effect of with except acne；Using facial mask can also cutin-softening, expansion pore, promote sweat gland secretion and remove epidermal cell metabolin,
Reach cleaning and the effect of skin care.
The development speed of facial mask it is closely bound up with its effect soon.Facial mask can solve 5 big problem of skin simultaneously：Moisturizing,
Whitening, oil-control, antiallergic sense and anti-aging, and everyday skincare can not quickly change comprehensively often just for subproblem therein
Kind skin condition.Facial mask in the market can be classified as moisture saver mask, cleawhite pack according to effect, spot-relieving face mask, compact
Facial mask, anti-wrinkle face mask, shining skin facial mask, cleaning pack, compact pore facial mask and local facial mask；It can divide according to the formulation classification of facial mask
For tear-pull facial mask, paste mask, creams facial mask, gel facial mask and mounted facial mask.The effect of facial mask and added activity into
Dividing has much relations, and the facial mask of same effect may have a variety of categories, as China Patent Publication No. CN102319196A passes through
Addition moisturizing grease, NMF and skin conditioning agent etc. are prepared for the disposable sleep mask with replenishing water and preserving moisture.Chinese patent is public
The number of opening CN104666236A has moisturizing, water lock work(using the preparations such as glycerine, glycine betaine, glycosyl trehalose, dried tremella extract
The facial mask of energy, it is less for the active constituent content of cost-effective facial mask in the market, and the composition used is mostly skin
The molecule absorbed is not easy, but consumer pursues the attention rate being far above to price to the performance of product at present, absorbs model in skin
In enclosing, active constituent content is increased, facial mask performance just preferably improves.
The content of the invention
According to above the deficiencies in the prior art, the technical problems to be solved by the invention are to propose that one kind is easy to absorb, and are had
Imitate the high crease-resistant Wash-free mask of composition.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention is：
A kind of crease-resistant Wash-free mask, include the micromolecular collagen for accounting for the Wash-free mask gross weight 5-10%, 5-8%
Blood orange elite, 1-5% urea, 0.5-1% vitamin Es.
Preferably, the molecular weight of the micromolecular collagen is 480-530 dalton, is more beneficial for the absorption of skin.
Preferably, the purity of the blood orange elite is 99%, improves the content of active ingredient, and elite is more beneficial for skin
Absorb.
Preferably, it is 20-25% thickeners, 20-35% NMFs, 5- that the crease-resistant Wash-free mask, which also includes weight ratio,
8% emulsifying agent, 0.1-1% preservatives and water.
Preferably, the thickener is that mass ratio is 2:1 Bletilla glucomannan and sodium alginate mixture；The NMF is sweet
At least two in oil, vaseline, honey, propane diols and hyaluronic acid；The emulsifying agent is tristerin, poly dimethyl
At least two in siloxanes, Tween-60.
A kind of preparation method of crease-resistant Wash-free mask, is comprised the following steps that：
1) each component is weighed by formula rate, thickener and each raw material of vitamin E is mixed and heated to 80-85 DEG C, stirring
It is mixed to be formed uniformly oil phase, 30-35min is incubated, obtains oil phase；
2) NMF and micromolecular collagen are added in aqueous solution of urea, is heated to 80-85 DEG C, be stirred
It is even, emulsifying agent is then added, continues to stir, 30-35min is incubated, obtains aqueous phase；
3) under agitation, according to the mutually interspersed dropwise addition order of aqueous phase and blood orange elite, aqueous phase and blood orange elite are divided 3 times
Oil phase is slowly added to, drips stirring 10-20min every time, after dripping, high speed homogenization 5min, then keeps 60-65 DEG C of low speed
Emulsification defoaming 30min, naturally cools to 50 DEG C, adds preservative, low speed homogeneous 5min, and vacuum outgas, which is steeped to stopping at 40 DEG C, stirs
Mix, insulation ageing 24h, obtains crease-resistant Wash-free mask at 40 DEG C.
Preferably, the rotating speed of the stirring is 600-800r/min.
Preferably, the rotating speed of the high speed is 1800-2100r/min；The rotating speed of the low speed is 100-200r/min.
Compared with prior art, present invention has the advantages that:
1. the present invention is more beneficial for the absorption of skin using the blood orange elite and micromolecular collagen of purity 99%, have
Strengthen the effect of facial mask effect.
2. present invention addition urea has regulation facial mask pH and prevents dry and cracked, keratolysis is denatured, promotes cuticula
Aquation so that skin emolliency, increase the absorption of functional molecular.
3. the present invention is by the way that aqueous phase to be added to the preparation method of oil phase in batches, the facial mask of preparation has that film forming is uniform,
The advantages of facial mask stability is good.
Embodiment
Below by the description to embodiment, it is described in further detail, to help those skilled in the art to this hair
Bright inventive concept, technical scheme have more complete, accurate and deep understanding.
Embodiment 1
A kind of crease-resistant Wash-free mask in the present embodiment, comprising following weight than composition：
A kind of preparation method of crease-resistant Wash-free mask, is comprised the following steps that：
1) weigh each component by formula rate, by weight accounting 20% by mass ratio be 2:1 Bletilla glucomannan and alginic acid
The thickener and 0.8% vitamin E of sodium mixing are mixed and heated to 85 DEG C, and stirring is mixed to be formed uniformly oil phase, is incubated 30min, obtains oily
Phase；
2) by 30% by glycerine and hyaluronic acid in mass ratio 1:The NMF and 10% molecular weight of 1 mixing are 500
You are added in the aqueous solution of urea a micromolecular collagen, and aqueous solution of urea is to be dissolved in excess water to make by 4% urea
It is standby to form, be heated to 85 DEG C, be uniformly mixed in rotating speed 600r/min, then add 8% by tristerin and
Tween-60 presses quality 0.5:The emulsifying agent of 1 mixing, continues to stir in rotating speed 700r/min, is incubated 30min, obtains aqueous phase；
3) under rotating speed 800r/min stirrings, the above-mentioned aqueous phase of 1/3 amount is first added dropwise, rate of addition is in 60 drops/min, then
Blood orange elite is added dropwise, rate of addition is 40 drops/min, so mutually interspersed dropwise addition, divides 3 times slowly by aqueous phase and blood orange elite
Oil phase is added, the dropwise addition of second lot is carried out after each aqueous phase and blood orange elite drip after stirring 15min again, treats whole dropwise additions
After complete, the high speed homogenization 5min under rotating speed 2000r/min, 65 DEG C are then kept, the low speed emulsification defoaming under rotating speed 150r/min
30min, naturally cools to 50 DEG C, adds 4-HBA methyl esters preservative, the low speed homogeneous 5min under rotating speed 100r/min,
Vacuum outgas is steeped to stirring is stopped at 40 DEG C, and insulation ageing 24h, obtains crease-resistant Wash-free mask at 40 DEG C.
Embodiment 2
The preparation method of the crease-resistant Wash-free mask of the present embodiment with embodiment 1, unlike crease-resistant Wash-free mask, comprising as follows
Weight than composition：
Embodiment 3
The present embodiment is with embodiment 1, the difference is that NMF is glycerine, vaseline, honey and hyaluronic acid, mass ratio is
1:0.5:1:1；Emulsifying agent is tristerin, dimethyl silicone polymer and Tween-60, mass ratio 1:1:0.5.
The embodiment 1-3 facial masks prepared are tested by QB/T1857-2013 moisturizing cream quality standards, physical and chemical index
Smear and quantitative measurement, test data are as follows：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Outward appearance | White body uniform and smooth | White body is uniform | White body uniform and smooth |
| Centrifugal test | It is qualified | It is qualified | It is qualified |
| Long-time stability (3 months) | It is qualified | Slightly it is hardened | It is qualified |
| pH | 6.8 | 8.1 | 6.5 |
The present invention is exemplarily described above in conjunction with specific embodiment, it is clear that present invention specific implementation is not by upper
The limitation of mode is stated, if the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress is employed, or
It is not improved by the present invention design and technical scheme directly apply to other occasions, protection scope of the present invention it
It is interior.Protection scope of the present invention should be determined by the scope of protection defined in the claims.
Claims (8)
1. a kind of crease-resistant Wash-free mask, it is characterised in that include the small molecule collagen for accounting for the Wash-free mask gross weight 5-10%
Albumen, 5-8% blood orange elite, 1-5% urea, 0.5-1% vitamin Es.
2. crease-resistant Wash-free mask according to claim 1, it is characterised in that the molecular weight of the micromolecular collagen is
480-530 dalton.
3. crease-resistant Wash-free mask according to claim 1, it is characterised in that the purity of the blood orange elite is 99%.
4. crease-resistant Wash-free mask according to claim 1, it is characterised in that the crease-resistant Wash-free mask also includes weight ratio
For 20-25% thickeners, 20-35% NMFs, 5-8% emulsifying agents, 0.1-1% preservatives and water.
5. crease-resistant Wash-free mask according to claim 4, it is characterised in that the thickener is that mass ratio is 2:1 it is white
Splendid achnatherum glue and sodium alginate mixture；The NMF is at least two in glycerine, vaseline, honey, propane diols and hyaluronic acid
Kind；The emulsifying agent is at least two in tristerin, dimethyl silicone polymer, Tween-60.
6. the preparation method of the crease-resistant Wash-free mask described in a kind of any one of right 1-5, it is characterised in that comprise the following steps that：
1) each component is weighed by formula rate, thickener and each raw material of vitamin E is mixed and heated to 80-85 DEG C, stir the even shape that is mixed
Into oil phase, 30-35min is incubated, obtains oil phase；
2) NMF and micromolecular collagen are added in aqueous solution of urea, is heated to 80-85 DEG C, is uniformly mixed, so
After add emulsifying agent, continue to stir, be incubated 30-35min, obtain aqueous phase；
3) under agitation, according to the mutually interspersed dropwise addition order of aqueous phase and blood orange elite, 3 times are divided slowly by aqueous phase and blood orange elite
Oil phase is added, drips stirring 10-20min every time, after dripping, high speed homogenization 5min, then keeps 60-65 DEG C of low speed emulsification
30min is defoamed, naturally cools to 50 DEG C, adds preservative, low speed homogeneous 5min, vacuum outgas is steeped to stopping stirring at 40 DEG C,
Insulation ageing 24h, obtains crease-resistant Wash-free mask at 40 DEG C.
7. the preparation method of crease-resistant Wash-free mask according to claim 6, it is characterised in that the rotating speed of the stirring is
600-800r/min。
8. the preparation method of crease-resistant Wash-free mask according to claim 6, it is characterised in that the rotating speed of the high speed is
1800-2100r/min；The rotating speed of the low speed is 100-200r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711031662.5A CN107669548A (en) | 2017-10-28 | 2017-10-28 | A kind of crease-resistant Wash-free mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711031662.5A CN107669548A (en) | 2017-10-28 | 2017-10-28 | A kind of crease-resistant Wash-free mask and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107669548A true CN107669548A (en) | 2018-02-09 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711031662.5A Pending CN107669548A (en) | 2017-10-28 | 2017-10-28 | A kind of crease-resistant Wash-free mask and preparation method thereof |
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| CN (1) | CN107669548A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113304092A (en) * | 2021-06-22 | 2021-08-27 | 杭州琳雏科技有限公司 | Wash-free moisturizing mask and preparation method and application thereof |
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| CN113304092A (en) * | 2021-06-22 | 2021-08-27 | 杭州琳雏科技有限公司 | Wash-free moisturizing mask and preparation method and application thereof |
| CN113304092B (en) * | 2021-06-22 | 2022-02-18 | 维那斯(杭州)科技有限公司 | Wash-free moisturizing mask and preparation method and application thereof |
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Application publication date: 20180209 |