CN105669127B - 一种利用工业废渣的建筑保温板及其制备方法 - Google Patents
一种利用工业废渣的建筑保温板及其制备方法 Download PDFInfo
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/40—Porous or lightweight materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/52—Sound-insulating materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
本发明利用工业废渣的建筑保温板，是由以下重量份数的组分制成：普通硅酸盐水泥55～65份、埃洛石8～10份、电解锰渣15～18份、坡缕石8～10份、湿法炼锌废渣18～20份、松焦油6～8份、多晶氧化铝纤维棉8～10份、聚丙烯短纤维6～8份、二丁酸二辛酯磺酸钠1～2份、癸基葡萄糖苷3～4份、水55～60份、季戊四醇硬脂酸酯1～2份、硫酸铵1～2份、氧化镁5～6份、聚羧酸减水剂5～6份。本发明利用工业废渣的建筑保温板，节能利废，具有抗压强度高、质量轻，保温隔热，隔音，耐高温、防火性能好等特点。尤其是具有突出的抗压强度；可应用于建筑外墙防火隔离带和外墙保温等方面。
Description
技术领域
本发明属于建筑材料技术领域，具体为一种利用工业废渣的建筑保温板及其制备方法。
背景技术
混凝土保温板是将发泡剂加入到由水泥基胶凝材料、集料、掺合料、外加剂和水等制成的料浆中，经混合搅拌、浇注成型、自然或蒸汽养护而成的轻质多孔混凝土板材。混凝土保温板具有重量轻、保温隔热性能好、吸声隔音、防火等优良特性，适用于外墙保温及其防火隔离带，满足了外墙外保温市场的对防火安全的急迫需要。经过多年的研发，该技术目前已逐渐成熟，随着建筑防火力度的加大，这一产品将会逐步得到推广应用，成为未来建筑保温的主导产品之一。酚醛保温板由酚醛泡沫制成，酚醛泡沫是一种新型不燃、防火低烟保温材料，它是由酚醛树脂加入发泡剂、固化剂及其它助剂制成的闭孔硬质泡沫塑料。挤塑聚苯板(xps板)全称挤塑聚苯乙烯泡沫板，该材料是以聚苯乙烯树脂辅以聚合物在加热混合的同时，注入催化剂，而后挤塑押出连续性闭孔发泡的硬质泡沫塑料板。岩棉板是以玄武岩及其它天然矿石等为主要原料，经高温熔融成纤，加入适量粘结剂，固化加工而制成的；膨胀聚苯板(eps板)全称聚苯乙烯泡沫板，该材料是由含有挥发性液体发泡剂的可发性聚苯乙烯珠粒，经加热预发后在模具中加热成型的具有微细闭孔结构的白色固体。
发明内容
本发明目的在于克服现有技术中的不足，提供一种性能优异的的利用工业废渣的建筑保温板及其制备方法。
本发明利用工业废渣的建筑保温板，是由以下重量份数的组分制成：普通硅酸盐水泥55～65份、埃洛石8～10份、电解锰渣15～18份、坡缕石8～10份、湿法炼锌废渣18～20份、松焦油6～8份、多晶氧化铝纤维棉8～10份、聚丙烯短纤维6～8份、二丁酸二辛酯磺酸钠1～2份、癸基葡萄糖苷3～4份、水55～60份、季戊四醇硬脂酸酯1～2份、硫酸铵1～2份、氧化镁5～6份、聚羧酸减水剂5～6份。
作为优化，该利用工业废渣的建筑保温板，由以下重量份数的原料制成：普通硅酸盐水泥60份、埃洛石9份、电解锰渣16份、坡缕石9份、湿法炼锌废渣19份、松焦油7份、多晶氧化铝纤维棉9份、聚丙烯短纤维7份、二丁酸二辛酯磺酸钠1.5份、癸基葡萄糖苷3.5份、水58份、季戊四醇硬脂酸酯1.5份、硫酸铵1.5份、氧化镁5.5份、聚羧酸减水剂5.5份。
一种制备本发明利用工业废渣的建筑保温板的方法，包括以下步骤，按重量份数：
(1)将埃洛石9份、电解锰渣16份、坡缕石9份、湿法炼锌废渣19份，粉碎制成粒径10μm以下的混合粉末A；
(2)将松焦油7份、多晶氧化铝纤维棉9份、聚丙烯短纤维7份、混合粉末A，混合均匀，得到混合物B；
(3)将普通硅酸盐水泥60份、水58份、混合物B，以800～1000转/分钟转速搅拌40分钟，然后加入季戊四醇硬脂酸酯1.5份、硫酸铵1.5份、氧化镁5.5份、聚羧酸减水剂5.5份，以600～800转/分钟转速搅拌40分钟,得到混合物C；
(4)将二丁酸二辛酯磺酸钠1.5份、癸基葡萄糖苷3.5份,加入到混合物C中，在90～100℃条件下，以400～600转/分搅拌30分钟；然后送到压形机压制成形，送入蒸压釜蒸养5～7小时，冷却即得。
本发明利用工业废渣的建筑保温板，节能利废，具有抗压强度高、质量轻，保温隔热，隔音，耐高温、防火性能好等特点。尤其是具有突出的抗压强度；可应用于建筑外墙防火隔离带和外墙保温等方面。
对该建筑保温板性能指标做了以下检验，具体见表1。
表1相关性能指标检验结果
| 指标 | 实施例1 | 实施例2 | 实施例3 |
| 体积密度 | 433kg/m3 | 435kg/m3 | 439kg/m3 |
| 抗压强度≥ | 6.5MPa | 6.3MPa | 6.4MPa |
| 抗折强度≥ | 2.3MPa | 2.2MPa | 2.2MPa |
| 导热系数(常温)≤ | 0.065W/m.K | 0.065W/m.K | 0.066W/m.K |
| 隔音量≥ | 59db | 58db | 59db |
| 燃烧性能 | A级不燃 | A级不燃 | A级不燃 |
具体实施方式
下面给出的实施例拟对本发明作进一步说明，但不能理解为是对本发明保护范围的限制，本领域技术人员根据本发明内容对本发明的一些非本质的改进和调整，仍属于本发明的保护范围。
实施例1：
(1)将埃洛石9千克、电解锰渣16千克、坡缕石9千克、湿法炼锌废渣19千克，粉碎制成粒径10μm以下的混合粉末A；
(2)将松焦油7千克、苏州德鑫陶瓷新材料有限公司生产的纤维直径:2～4μm多晶氧化铝纤维棉9千克、北京鹏洋新型建筑有限公司生产的3～12mm聚丙烯短纤维7千克、混合粉末A，混合均匀，得到混合物B；
(3)将425普通硅酸盐水泥60千克、水58千克、混合物B，以800～1000转/分钟转速搅拌40分钟，然后加入季戊四醇硬脂酸酯1.5千克、硫酸铵1.5千克、氧化镁5.5千克、上海微析科技有限公司生产的wp12312聚羧酸减水剂5.5千克，以600～800转/分钟转速搅拌40分钟,得到混合物C；
(4)将二丁酸二辛酯磺酸钠1.5千克、癸基葡萄糖苷3.5千克,加入到混合物C中，在90～100℃条件下，以400～600转/分搅拌30分钟；然后送到压形机压制成形，送入蒸压釜蒸养5～7小时，冷却即得。
实施例2：
(1)将埃洛石10千克、电解锰渣18千克、坡缕石10千克、湿法炼锌废渣20千克，粉碎制成粒径10μm以下的混合粉末A；
(2)将松焦油8千克、苏州德鑫陶瓷新材料有限公司生产的纤维直径:2～4μm多晶氧化铝纤维棉10千克、北京鹏洋新型建筑有限公司生产的3～12mm聚丙烯短纤维8千克、混合粉末A，混合均匀，得到混合物B；
(3)将425普通硅酸盐水泥65千克、水60千克、混合物B，以800～1000转/分钟转速搅拌40分钟，然后加入季戊四醇硬脂酸酯2千克、硫酸铵2千克、氧化镁6千克、上海微析科技有限公司生产的wp12312聚羧酸减水剂6千克，以600～800转/分钟转速搅拌40分钟,得到混合物C；
(4)将二丁酸二辛酯磺酸钠2千克、癸基葡萄糖苷4千克,加入到混合物C中，在90～100℃条件下，以400～600转/分搅拌30分钟；然后送到压形机压制成形，送入蒸压釜蒸养5～7小时，冷却即得。
实施例3：
(1)将埃洛石8千克、电解锰渣15千克、坡缕石8千克、湿法炼锌废渣18千克，粉碎制成粒径10μm以下的混合粉末A；
(2)将松焦油6千克、苏州德鑫陶瓷新材料有限公司生产的纤维直径:2～4μm多晶氧化铝纤维棉8千克、北京鹏洋新型建筑有限公司生产的3～12mm聚丙烯短纤维6千克、混合粉末A，混合均匀，得到混合物B；
(3)将425普通硅酸盐水泥55千克、水55千克、混合物B，以800～1000转/分钟转速搅拌40分钟，然后加入季戊四醇硬脂酸酯1千克、硫酸铵1千克、氧化镁5千克、上海微析科技有限公司生产的wp12312聚羧酸减水剂5千克，以600～800转/分钟转速搅拌40分钟,得到混合物C；
(4)将二丁酸二辛酯磺酸钠1千克、癸基葡萄糖苷3千克,加入到混合物C中，在90～100℃条件下，以400～600转/分搅拌30分钟；然后送到压形机压制成形，送入蒸压釜蒸养5～7小时，冷却即得。
Claims (3)
1.一种利用工业废渣的建筑保温板，其特征在于，是由以下重量份数的组分制成：普通硅酸盐水泥55～65份、埃洛石8～10份、电解锰渣15～18份、坡缕石8～10份、湿法炼锌废渣18～20份、松焦油6～8份、多晶氧化铝纤维棉8～10份、聚丙烯短纤维6～8份、二丁酸二辛酯磺酸钠1～2份、癸基葡萄糖苷3～4份、水55～60份、季戊四醇硬脂酸酯1～2份、硫酸铵1～2份、氧化镁5～6份、聚羧酸减水剂5～6份。
2.根据权利要求1所述利用工业废渣的建筑保温板，其特征在于，是由以下重量份数的原料制成：普通硅酸盐水泥60份、埃洛石9份、电解锰渣16份、坡缕石9份、湿法炼锌废渣19份、松焦油7份、多晶氧化铝纤维棉9份、聚丙烯短纤维7份、二丁酸二辛酯磺酸钠1.5份、癸基葡萄糖苷3.5份、水58份、季戊四醇硬脂酸酯1.5份、硫酸铵1.5份、氧化镁5.5份、聚羧酸减水剂5.5份。
3.一种制备权利要求2所述利用工业废渣的建筑保温板的方法，其特征在于，包括以下步骤，按重量份数：
(1)将埃洛石9份、电解锰渣16份、坡缕石9份、湿法炼锌废渣19份，粉碎制成粒径10μm以下的混合粉末A；
(2)将松焦油7份、多晶氧化铝纤维棉9份、聚丙烯短纤维7份、混合粉末A，混合均匀，得到混合物B；
(3)将普通硅酸盐水泥60份、水58份、混合物B，以800～1000转/分钟转速搅拌40分钟，然后加入季戊四醇硬脂酸酯1.5份、硫酸铵1.5份、氧化镁5.5份、聚羧酸减水剂5.5份，以600～800转/分钟转速搅拌40分钟,得到混合物C；
(4)将二丁酸二辛酯磺酸钠1.5份、癸基葡萄糖苷3.5份,加入到混合物C中，在90～100℃条件下，以400～600转/分搅拌30分钟；然后送到压形机压制成形，送入蒸压釜蒸养5～7小时，冷却即得。
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