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US3831644A - Filling nozzle and installation for filling drums with liquid yellow phosphorus - Google Patents

Filling nozzle and installation for filling drums with liquid yellow phosphorus Download PDF

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Publication number
US3831644A
US3831644A US00280807A US28080772A US3831644A US 3831644 A US3831644 A US 3831644A US 00280807 A US00280807 A US 00280807A US 28080772 A US28080772 A US 28080772A US 3831644 A US3831644 A US 3831644A
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US
United States
Prior art keywords
trolley
nozzle
secured
filling
filling nozzle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US00280807A
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English (en)
Inventor
L Berg
G Lenemann
J Kinneging
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Knapsack AG
Original Assignee
Knapsack AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Knapsack AG filed Critical Knapsack AG
Application granted granted Critical
Publication of US3831644A publication Critical patent/US3831644A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/003—Phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/008—Feed or outlet control devices
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
    • B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
    • B67C3/30—Filling of barrels or casks
    • B67C3/34—Devices for engaging filling-heads with filling-apertures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67D—DISPENSING, DELIVERING OR TRANSFERRING LIQUIDS, NOT OTHERWISE PROVIDED FOR
    • B67D7/00—Apparatus or devices for transferring liquids from bulk storage containers or reservoirs into vehicles or into portable containers, e.g. for retail sale purposes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67D—DISPENSING, DELIVERING OR TRANSFERRING LIQUIDS, NOT OTHERWISE PROVIDED FOR
    • B67D7/00—Apparatus or devices for transferring liquids from bulk storage containers or reservoirs into vehicles or into portable containers, e.g. for retail sale purposes
    • B67D7/005—Spouts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/01—Treating phosphate ores or other raw phosphate materials to obtain phosphorus or phosphorus compounds
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16L—PIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L39/00—Joints or fittings for double-walled or multi-channel pipes or pipe assemblies
    • F16L39/04—Joints or fittings for double-walled or multi-channel pipes or pipe assemblies allowing adjustment or movement

Definitions

  • ABSTRACT Liquid yellow phosphorus is filled into drums by means of a filling noule or filling lance.
  • the filling nozzle comprises a control tube provided with a plurality of perforations and connected at its top end to a cylindrical member which carries an eye for the connection of a control unit via a connecting piece of piping.
  • a nozzle supporting tube which concentrically surrounds the control pipe is provided at its upper portion with a warm water inlet, and carries in its bottom portion a control cylinder with a control piston with a hole running through it.
  • the control cylinder is secured via a conical bottom to a nozzle pipe and the nozzle pipe has at its top end a gland with a supporting flange.
  • the nozzle pipe concentrically surrounds the nozzle supporting tube so as to form an annular chamber receiving yellow phosphorus.
  • a heating jacket is arranged around the nozzle pipe so as to form a heating chamber. The heating jacket is fitted it in its upper portion firstly with a double pipe running therethrough and delivering Warm water to the heating chamber, and delivering yellow phosphorus to the annular chamber, and secondly with a water outlet.
  • a supporting flange is fixed to the heating jacket and a spring-loaded water outlet valve is arranged at the bottom end of the control piston.
  • the installation filling drums with liquid yellow phosphorus with the use of the filling nozzle or lance comprises as its essential parts a rotating frame which control desk is arranged on the outside of the rotating frame.
  • the present invention relates to a filling nozzle or filling lance for liquid yellow phosphorous and to a plant for filling drums with liquid yellowphosphorus using this filling nozzle.
  • Liquid yellow phosphorus is commonly filled into drums from an overhead container by means of syphons and a flexible pipe, which commonly is made of lead or rubber, if desired. Before the containers are filled warm water is placed in them by hand. Following siphoning the liquid yellow phosphorus with warm water, the filling operation can be started; however, every time he changes the drum the operator must briefly interrupt the stream of phosphorus by holding the flexible pipe together with his fingers. Even though when filling liquid yellow phosphorus one always wears rubber gloves, there is always the risk of skin burns, especially if the rubber glove is defective when holding the flexible pipe together.
  • FIG. I shows the filling nozzle in longitudinal section.
  • the filling nozzle substantially comprises a nozzle pipe I, a heating jacket 2, a double tube (3, 4), a nozzle carrier tube 8 and a control tube 23.
  • the double tube (3, 4) passes through the heating jacket 2 on the one side of its top end; on the opposite side there is arranged a warm water outlet 5.
  • the heating jacket 2 and the nozzle pipe I are welded with the nozzle supporting pipe 8 via a lid 10, an intermediate ring 9 being arranged between the nozzle tube 1 and the nozzle supporting pipe 8.
  • the nozzle supporting tube 8 carries a control cylinder 11, which is welded via a conical bottom 12 to the nozzle tube 1.
  • a gland 13 with a supporting flange 14 for the entire filling nozzle.
  • a warm water inlet 15 Near to the top end of the nozzle supporting tube 8 there is arranged a warm water inlet 15.
  • the control tube 23 is screwed into a cylindrical member 24, which has a connecting piece of tubing 25 with an eye 26 screwed thereinto for the connection of a control unit.
  • the seal firstly between the control cylinder 11 and the control piston 17 and secondly between the gland l3 and the cylindrical member 24 is in each case effected by means of a two-piece packing 18 or 34 with a central spacer ring 20 or 35.
  • the paclcings 18 and 34 are pressed in position by gland nut 19 or by the clamping flange 27.
  • the screw union 30 is fixed in tube 3.
  • the pressure hose 29 is encased in a flexible hose 31 which ends between flanges 32, so as to ensure the connection with tube 4.
  • Placed between nozzle pipe I and heating jacket 2 is a U- shaped heating chamber 6, and between nozzle tube 1 and nozzle supporting tube 8 there is a phosphorus receiving annular chamber 16, and inside the nozzle supporting tube 8 there is a warm-water chamber 22.
  • FIG. 2 represents a plan view of the entire installation
  • FIG. 3 represents a front elevational view of the installation
  • FIG. 4 represents a complete side elevational view of the installation
  • FIG. 5 represents an enlarged section of the righthand half of FIG. 4.
  • a trolley 38 which can be moved horizontally and which can be displaced by a lifting cylinder 37.
  • a trolley 39 Secured to trolley 38 is a trolley 39 which can be moved vertically and which can be displaced by a lifting cylinder '40.
  • the vertically movable trolley 39 has a filling nozzle 41 together with its supporting flange 14 fastened thereto.
  • a lifting cylinder 56 is provided for actuating control piston 17 of filling nozzle 41, the control piston 17 being brought into the closed position after removal of the load from the lifting cylinder 56 by springs 53 which press on a pressure plate 54 connected with a coupling rod 55.
  • Supporting flange 28 of filling nozzle 41 is provided with a drum cover 44 which is connected to a supporting cross 47 via guide pins 46 provided with spiral springs 45.
  • On the supporting cross 47 there are probes (not shown in the drawing) for determining the level of phosphorus and water in drum 51.
  • the filling nozzle 41 is fitted with a flexible double pipe 29, 31, supplying yellow phosphorus and hot water. Warm water is fed in through warm-water inlet 15 and pipe 48. The water issuing through water outlet 5 runs via a control valve 49 and an inspection glass 50 into drum Sl which is to be filled with phosphorus.
  • Water feed pipes 52 are provided for the introduction of warm water into empty drums 51.
  • a switch and control desk 42 which is screened against the filling nozzle 41 by a transparent protective wall 43.
  • Empty drums 51 are placed in a double row in a semicircle underneath rotating frame 36. After warm water has been poured into an empty drum 51 through water feed pipe 52, rotary frame 36 is moved in such a way that the filling nozzle 41 is located above this drum. Following this, the filling nozzle 41 is lowered by actuating lifting cylinder 40. To this end, filling nozzle 41 is first brought into the correct position by displacing horizontal trolley 38 by means of lifting cylinder 39. After the supporting cross 47 with the probes for the phosphorus and water level has been placed on the rim of the drum and has been lowered further, guide pins 46 operate limit switches arranged on drum cover 44, after which filling nozzle 41 remains in this position.
  • the filling nozzle of the present invention comprises more particularly a control pipe 23 provided with a plurality of perforations 33, and connected at its top end to a cylindrical member 24 which, via a connecting piece of tubing 25, carries an eye 26 for connecting up a control unit; a nozzle supporting pipe 8, which concentrically surrounds the control pipe 23 and is provided in its upper part with a warm-water inlet 15, the nozzle supporting pipe 8 carrying at its bottom end a control cylinder 11 with a control piston 17 having a hole drilled through it which is fixed via a conical bottom 12 to a nozzle pipe 1, and at its lower end has a gland 13 with a supporting flange 14; the nozzle pipe 1 concentrically surrounding the nozzle supporting tube 8 so as to form an annular chamber receiving yellow phosphorus; a heating jacket 2 which is arranged around nozzle tube 1 so as to form a heating chamber *6, the heating jacket 2 having passed through it in its upper end portion firstly a double tube (3, 4) delivering warm water to heating chamber 6 and yellow phosphorus
  • FIG. 1 For preferred embodiments of the filling nozzle according to the invention, which can be used singly or in combination, provide: 5 a. for two longitudinal ribs 7 to be secured diametrically opposite one another to the outside of nozzle pipe b. for an intermediate ring 9 to be arranged near the top end of nozzle pipe 1 between pipe 1 and nozzle supporting pipe 8;
  • the installation according to the invention comprises more particularly a rotating frame 36 movable in a semi-circle; a trolley 38 secured thereto and capable of being moved horizontally by meansof lifting cylinder 37; a further trolley 39 which is fast with trolley 38 and can be moved vertically by means of lifting cylinder 40, filling nozzle 41 being arranged on trolley 39; a lifting cylinder 56 which is connected to control cylinder 17 of filling nozzle 41; and a switch and control desk 42 provided on the outside of rotating frame 36.
  • a transparent semicircular protective wall 43 to be arranged between filling nozzle 41 and switch and control desk 42;
  • the supporting cross 47 to be fitted with probes for measuring the phosphorus and water level; i. for the switching and control desk 42 to receive impulses from the probes on supporting cross 47 and from lifting cylinders 40 and to transmit adjustment instructions to lifting cylinder 56, the lifting cylinder 56 only opening the control piston 17 of the filling nozzle 41 when the filling nozzle 41 is dipping into water.
  • the annular chamber 16 of the filling nozzle of the present invention in which the phosphorus flows is surrounded on both sides with warm-water-heated chambers in view of the melting point of phosphorus (45C) (heating chamber 6, warm-water chamber 22). This ensures undisturbed actuation of control piston 17. In warm-water chamber 22 the water is always under a certain pressure which avoids penetration of phosphorus thereinto.
  • An important component of the control cylinder 11 is the two-part gland l8 interrupted by a spacer ring 20. In the zone of the spacer ring 20 it is possible for the phosphorus to leave filling nozzle 41 through annular chamber 16.
  • the installation of the present invention can be substantially automated by using the filling nozzle, which enables the flow of phosphorus to be arrested and restarted without manual interference, by means of an ordinary synchronised switching system.
  • An installation for filling drums with liquid yellow phosphorus comprising a rotating frame movable along a semi-circle; a first trolley being movable in a horizontal direction, being parallel with, and being disposed near the peripheral end of the rotating frame; a first lifting cylinder mounted upon the first trolley, the first lifting cylinder comprising a piston rod, which is secured to the rotating frame in a manner permitting the first trolley to be moved in horizontal direction; a second trolley being movable by means of a plurality of second lifting cylinders on a bracket disposed perpendicularly to the first trolley, the second lifting cylinders being secured to the second trolley and having piston rods which are secured to the first trolley; a filling nozzle comprising a plurality of coaxial tubes, a double-walled tubular inlet delivering yellow phosphorus and warm water, respectively, a water inlet and a water outlet, 21 first supporting flange which is secured to the outer of the coaxial tubes and a second supporting flanges which is secured to the head

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Basic Packing Technique (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Furnace Charging Or Discharging (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Devices For Medical Bathing And Washing (AREA)
  • Nozzles (AREA)
US00280807A 1971-08-18 1972-08-15 Filling nozzle and installation for filling drums with liquid yellow phosphorus Expired - Lifetime US3831644A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2141315A DE2141315C3 (de) 1971-08-18 1971-08-18 Vorrichtung zum BefUllen von Fässern mit flüssigem gelbem Phosphor

Publications (1)

Publication Number Publication Date
US3831644A true US3831644A (en) 1974-08-27

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ID=5817048

Family Applications (1)

Application Number Title Priority Date Filing Date
US00280807A Expired - Lifetime US3831644A (en) 1971-08-18 1972-08-15 Filling nozzle and installation for filling drums with liquid yellow phosphorus

Country Status (5)

Country Link
US (1) US3831644A (de)
CA (2) CA983445A (de)
DE (1) DE2141315C3 (de)
GB (1) GB1374314A (de)
NL (2) NL155516B (de)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4439403A (en) * 1980-03-08 1984-03-27 Herbert Brunner Apparatus for conditioning bioinjurious waste
US4447400A (en) * 1981-04-04 1984-05-08 Hoechst Aktiengesellschaft Metering device
US4674547A (en) * 1984-10-02 1987-06-23 Andriano Simonazzi Container filling apparatus with adjustable pressure sealing means
US4744959A (en) * 1982-05-18 1988-05-17 Ciba-Geigy Ag Apparatus for producing a suspension of cyanuric chloride in water, or for reacting cyanuric chloride with ammonia or with amines
US5106595A (en) * 1988-11-25 1992-04-21 El.Po S.R.L. Device for sterilizing the mouths of containers, in particular of bag type containers for foodstuffs
US5213140A (en) * 1990-11-23 1993-05-25 Atochem Method and apparatus for filling drums with immiscible liquids such as white phosphorus and water
US5566727A (en) * 1990-07-20 1996-10-22 Siemens Aktiengesellschaft Process and filling adapter for the in-drum drying of liquid radioactive waste
WO2007149146A2 (en) * 2006-06-19 2007-12-27 Saudi Arabian Oil Company Sulfur loading apparatus
US20090020181A1 (en) * 2007-07-16 2009-01-22 Martin Richard W Remote fill head with automatic drip tray
US20100193072A1 (en) * 2009-01-30 2010-08-05 Krones Ag Filling device
WO2022040190A1 (en) * 2020-08-17 2022-02-24 Avantech, Llc Apparatus and method for grout waste disposal

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3702109C1 (de) * 1987-01-24 1988-08-25 Hubert Skibowski Vorrichtung zum Abfuellen von fliesfaehigen Produkten in einzelne Gefaesse

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3190494A (en) * 1963-09-18 1965-06-22 Mansfield Sanitary Inc Method and apparatus for filling molds with slip
US3212128A (en) * 1963-03-20 1965-10-19 Air Prod & Chem Mold filling apparatus
US3537489A (en) * 1967-06-26 1970-11-03 Kelsey Hayes Co Foundry apparatus

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3212128A (en) * 1963-03-20 1965-10-19 Air Prod & Chem Mold filling apparatus
US3190494A (en) * 1963-09-18 1965-06-22 Mansfield Sanitary Inc Method and apparatus for filling molds with slip
US3537489A (en) * 1967-06-26 1970-11-03 Kelsey Hayes Co Foundry apparatus

Cited By (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4439403A (en) * 1980-03-08 1984-03-27 Herbert Brunner Apparatus for conditioning bioinjurious waste
US4447400A (en) * 1981-04-04 1984-05-08 Hoechst Aktiengesellschaft Metering device
US4744959A (en) * 1982-05-18 1988-05-17 Ciba-Geigy Ag Apparatus for producing a suspension of cyanuric chloride in water, or for reacting cyanuric chloride with ammonia or with amines
US4674547A (en) * 1984-10-02 1987-06-23 Andriano Simonazzi Container filling apparatus with adjustable pressure sealing means
US5106595A (en) * 1988-11-25 1992-04-21 El.Po S.R.L. Device for sterilizing the mouths of containers, in particular of bag type containers for foodstuffs
US5566727A (en) * 1990-07-20 1996-10-22 Siemens Aktiengesellschaft Process and filling adapter for the in-drum drying of liquid radioactive waste
US5213140A (en) * 1990-11-23 1993-05-25 Atochem Method and apparatus for filling drums with immiscible liquids such as white phosphorus and water
US5477898A (en) * 1990-11-23 1995-12-26 Societe Atochem Method and apparatus for filling drums with immiscible liquids such as white phosphorus and water
WO2007149146A3 (en) * 2006-06-19 2008-02-21 Saudi Arabian Oil Co Sulfur loading apparatus
EP2682361A1 (de) * 2006-06-19 2014-01-08 Aramco Services Company Schwefelfüllungsvorrichtung
WO2007149146A2 (en) * 2006-06-19 2007-12-27 Saudi Arabian Oil Company Sulfur loading apparatus
US20080011370A1 (en) * 2006-06-19 2008-01-17 Al-Awadh Mohammed S Sulfur loading apparatus
US20110088807A1 (en) * 2006-06-19 2011-04-21 Saudi Arabian Oil Company Sulfur Loading Apparatus
US7958913B2 (en) * 2006-06-19 2011-06-14 Saudi Arabian Oil Company Sulfur loading apparatus
US8118067B2 (en) 2006-06-19 2012-02-21 Saudi Arabian Oil Company Sulfur loading apparatus
US20120111442A1 (en) * 2006-06-19 2012-05-10 Saudi Arabian Oil Company Sulfur Loading Apparatus
US8424573B2 (en) * 2006-06-19 2013-04-23 Saudi Arabian Oil Company Sulfur loading apparatus
US20090020181A1 (en) * 2007-07-16 2009-01-22 Martin Richard W Remote fill head with automatic drip tray
US8720498B2 (en) 2007-07-16 2014-05-13 Energysolutions, Llc Remote fill head with automatic drip tray
US20100193072A1 (en) * 2009-01-30 2010-08-05 Krones Ag Filling device
CN101792102B (zh) * 2009-01-30 2013-06-26 克罗内斯股份公司 灌装装置
US8443850B2 (en) 2009-01-30 2013-05-21 Krones Ag Filling device
WO2022040190A1 (en) * 2020-08-17 2022-02-24 Avantech, Llc Apparatus and method for grout waste disposal

Also Published As

Publication number Publication date
DE2141315A1 (de) 1973-03-29
NL172048B (nl) 1983-02-01
DE2141315C3 (de) 1975-05-15
NL7801462A (en) 1978-08-31
NL7210298A (de) 1973-02-20
CA983445A (en) 1976-02-10
CA987640A (en) 1976-04-20
DE2141315B2 (de) 1974-09-05
NL155516B (nl) 1978-01-16
GB1374314A (en) 1974-11-20
NL172048C (nl) 1983-07-01

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