TW227553B - Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone - Google Patents
Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketoneInfo
- Publication number
- TW227553B TW227553B TW81106131A TW81106131A TW227553B TW 227553 B TW227553 B TW 227553B TW 81106131 A TW81106131 A TW 81106131A TW 81106131 A TW81106131 A TW 81106131A TW 227553 B TW227553 B TW 227553B
- Authority
- TW
- Taiwan
- Prior art keywords
- anthryl
- quinone
- dihydroxy
- tetrahydroxy
- dihydrogen
- Prior art date
Links
Landscapes
- Gas Separation By Absorption (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Method of making 2,3- dihydrogen -1,4,5,8- tetrahydroxy -9,10 anthryl diketone comprises: mixing 5-45% of fumed acid, 1,8- dihydroxy anthryl quinone and 1-3 equivalent of boric acid according to the equivalent of 1,8- dihydroxy anthryl quinone, adding nitric acid drop by drop to nitrify 1,8- dihydroxy anthryl quinone to produce 1,8- dihydroxy -4,5- dinitro anthryl quinone, washing the mixture with solvent and extracting the product with a solvent containing dimethyl amide at -10-50 deg.C; adding 60-90% of sulfuric acid and iron powder to reduce 1,8- dihydroxy -4,5- dinitro anthryl quinone into 1,8- dihydroxy -4,5- diamino anthryl quinone at 60-120 deg.C; adding alkaline solution with 5-25% oforganic solvent and 0.1-0.25 mole of sodium hydrosulfite to reduce 1,8- dihydroxy -4,5- diamino anthryl quinone into 2,3- dihydrogen -1,4,5,8- tetrahydroxy -9,10- anthryl diketone.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
TW81106131A TW227553B (en) | 1992-08-03 | 1992-08-03 | Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
TW81106131A TW227553B (en) | 1992-08-03 | 1992-08-03 | Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone |
Publications (1)
Publication Number | Publication Date |
---|---|
TW227553B true TW227553B (en) | 1994-08-01 |
Family
ID=51348426
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TW81106131A TW227553B (en) | 1992-08-03 | 1992-08-03 | Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone |
Country Status (1)
Country | Link |
---|---|
TW (1) | TW227553B (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101118901B (en) * | 2007-06-29 | 2010-06-09 | 日月光半导体制造股份有限公司 | Stack type chip packaging structure and manufacture process |
US8110928B2 (en) | 2007-10-05 | 2012-02-07 | Advanced Semiconductor Engineering, Inc. | Stacked-type chip package structure and method of fabricating the same |
-
1992
- 1992-08-03 TW TW81106131A patent/TW227553B/en not_active IP Right Cessation
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101118901B (en) * | 2007-06-29 | 2010-06-09 | 日月光半导体制造股份有限公司 | Stack type chip packaging structure and manufacture process |
US8110928B2 (en) | 2007-10-05 | 2012-02-07 | Advanced Semiconductor Engineering, Inc. | Stacked-type chip package structure and method of fabricating the same |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM4A | Annulment or lapse of patent due to non-payment of fees |