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TR200000299T2 - Serbest hidroksilaminden oluşan sulu bir çözeltinin imalatı için usul. - Google Patents

Serbest hidroksilaminden oluşan sulu bir çözeltinin imalatı için usul.

Info

Publication number
TR200000299T2
TR200000299T2 TR2000/00299T TR200000299T TR200000299T2 TR 200000299 T2 TR200000299 T2 TR 200000299T2 TR 2000/00299 T TR2000/00299 T TR 2000/00299T TR 200000299 T TR200000299 T TR 200000299T TR 200000299 T2 TR200000299 T2 TR 200000299T2
Authority
TR
Turkey
Prior art keywords
hydroxylamine
aqueous solution
solution consisting
low
manufacture
Prior art date
Application number
TR2000/00299T
Other languages
English (en)
Inventor
Watzenberger Otto
Mauer Peter
Str�Fer Eckhard
Schelling Heiner
Schneider Hans-Michael
Original Assignee
Basf Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Aktiengesellschaft filed Critical Basf Aktiengesellschaft
Publication of TR200000299T2 publication Critical patent/TR200000299T2/tr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1409—Preparation
    • C01B21/1445—Preparation of hydoxylamine from its salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

Bu bulus serbest hidroksilaminden olusan sulu bir çözeltinin üretilmesine yönelik bir yöntem ile ilgilidir; burada hidroksilamonyum tuzu bir seritleme sütunu içindeki ters akimda amonyak ile islenmektedir. Bunun sonucunda hidroksilamonyum serbest birakilir ve ayni anda elde edilen çözelti damitma yoluyla sulu bir hidroksilamin çözeltisi ile bir tuz kismina ayrilir. Bulusun anlayisinda olan usul basit olup yumusak bir islemdir ve büyük ölçeklerde gerçeklestirilebilir. Termik yüklenme az, hidroksilamin yogunlugu düsük ve usulde kalma süresi az oldugu için ayrisma tehlikesi en aza indirilmistir.
TR2000/00299T 1997-08-04 1998-08-04 Serbest hidroksilaminden oluşan sulu bir çözeltinin imalatı için usul. TR200000299T2 (tr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19733681A DE19733681A1 (de) 1997-08-04 1997-08-04 Verfahren zur Herstellung einer wäßrigen Lösung von freiem Hydroxylamin

Publications (1)

Publication Number Publication Date
TR200000299T2 true TR200000299T2 (tr) 2001-01-22

Family

ID=7837953

Family Applications (1)

Application Number Title Priority Date Filing Date
TR2000/00299T TR200000299T2 (tr) 1997-08-04 1998-08-04 Serbest hidroksilaminden oluşan sulu bir çözeltinin imalatı için usul.

Country Status (19)

Country Link
US (1) US6299734B1 (tr)
EP (1) EP1012114B1 (tr)
JP (1) JP3421013B2 (tr)
KR (1) KR100522063B1 (tr)
CN (1) CN1131843C (tr)
AT (1) ATE220386T1 (tr)
AU (1) AU748827B2 (tr)
BR (1) BR9811119A (tr)
CA (1) CA2299475C (tr)
DE (2) DE19733681A1 (tr)
ES (1) ES2180194T3 (tr)
IL (1) IL134094A (tr)
MY (1) MY123175A (tr)
NO (1) NO327773B1 (tr)
RU (1) RU2189350C2 (tr)
TR (1) TR200000299T2 (tr)
TW (1) TW440540B (tr)
UA (1) UA54540C2 (tr)
WO (1) WO1999007637A1 (tr)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19936594A1 (de) * 1999-08-04 2001-02-08 Basf Ag Verfahren zur Herstellung von hochreinen stabilisierten Hydroxylaminlösungen
DE10004818A1 (de) * 2000-02-04 2001-08-09 Basf Ag Verfahren zum Recycling hydroxylaminhaltiger Stripperlösungen
JP3394980B2 (ja) * 2000-03-13 2003-04-07 東レ・ファインケミカル株式会社 フリーヒドロキシルアミン水溶液の製造方法
JP3394981B2 (ja) * 2000-03-13 2003-04-07 東レ・ファインケミカル株式会社 フリーヒドロキシルアミン水溶液の製造方法
JP4582602B2 (ja) * 2000-03-24 2010-11-17 ビーエーエスエフ ソシエタス・ヨーロピア ヒドロキシルアミン水溶液およびその製造方法
JP3503115B2 (ja) * 2000-06-27 2004-03-02 東レ・ファインケミカル株式会社 フリーヒドロキシルアミン水溶液の製造方法
DE10134389A1 (de) * 2001-07-04 2003-01-16 Basf Ag Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung
DE10131788A1 (de) * 2001-07-04 2003-01-16 Basf Ag Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung
DE10131787A1 (de) * 2001-07-04 2003-01-16 Basf Ag Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung
DE10314492B4 (de) * 2003-03-27 2008-10-16 Domo Caproleuna Gmbh Verfahren zur Herstellung einer wässrigen Lösung von Hydroxylamin
FR2856400A1 (fr) * 2003-06-18 2004-12-24 Jean Pierre Schirmann Procede de fabrication de l'oxime de la methyl ethyl cetone et de l'hydroxylamine base
JP4578885B2 (ja) * 2003-08-13 2010-11-10 昭和電工株式会社 ヒドロキシルアミンの製造方法
TW200508176A (en) 2003-08-13 2005-03-01 Showa Denko Kk Process for producing hydroxylamine
EP1663862A2 (en) 2003-08-13 2006-06-07 Showa Denko K.K. Process for producing hydroxylamine
FR2860223B1 (fr) * 2003-09-26 2005-12-16 Jean Pierre Schirmann Procede de fabrication de solutions aqueuses d'hydroxylamine base
US7396519B2 (en) * 2004-01-26 2008-07-08 San Fu Chemical Company, Ltd. Preparation of a high purity and high concentration hydroxylamine free base
JP2005239702A (ja) * 2004-01-28 2005-09-08 Showa Denko Kk ヒドロキシルアミンの製造方法
JP2006056742A (ja) * 2004-08-19 2006-03-02 Hosoya Fireworks Co Ltd 硝酸ヒドロキシルアミン水溶液の製造方法
CN103539742B (zh) * 2013-10-15 2015-08-05 河北工业大学 一种离子液体型羟胺盐的制备方法
RU2561372C1 (ru) * 2014-04-24 2015-08-27 Федеральное государственное унитарное предприятие "Российский научный центр "Прикладная химия" Способ получения концентрированных растворов нитрата гидроксиламина
WO2017204935A1 (en) 2016-05-26 2017-11-30 Exxonmobil Chemical Patents Inc. Production of cyclic imides suitable for oxidation catalysis
US11014883B2 (en) 2016-05-26 2021-05-25 Exxonmobil Chemical Patents Inc. Production of cyclic imides suitable for oxidation catalysis
WO2018075176A1 (en) 2016-10-18 2018-04-26 Exxonmobil Chemical Patents Inc. Cyclic imide slurry compositions
RU2656663C1 (ru) * 2017-08-01 2018-06-06 Федеральное государственное унитарное предприятие "Российский научный центр "Прикладная химия" Способ обезвреживания нитрата гидроксиламина в сточных водах
CN107539966B (zh) * 2017-09-29 2019-02-01 江苏艾科维科技有限公司 硫酸羟胺的制备方法
KR20220045372A (ko) * 2020-10-05 2022-04-12 주식회사 엘지화학 스트리핑 장치 및 스트리핑 방법

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE621960A (tr) 1961-08-31
US4147623A (en) 1977-10-28 1979-04-03 Allied Chemical Corporation Hydroxylamine purification via ion exclusion
US4202765A (en) 1977-10-28 1980-05-13 Allied Chemical Corporation Hydroxylamine purification via cation exchange
DE3382155D1 (de) 1982-11-01 1991-03-14 Allied Signal Inc Herstellung von alkoholischen hydroxylaminloesungen aus hydroxylammoniumsulfat, von oximen, hydroxamsaeuren und von anderen hydroxylammoniumsalzen mittels alkoholischer hydroxylaminloesungen.
US4956168A (en) 1983-01-28 1990-09-11 The United States Of America As Represented By The Secretary Of The Navy Synthesis of hydroxylamine salts
DE3347259A1 (de) 1983-12-28 1985-07-11 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von waessrigen hydroxylaminloesungen
US4654579A (en) 1984-08-17 1987-03-31 Ken Hayashibara Frequency divider
DE3528463A1 (de) 1985-08-08 1987-02-19 Basf Ag Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin
DE3601803A1 (de) 1986-01-22 1987-07-23 Basf Ag Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin
DE3608495A1 (de) 1986-03-14 1987-09-17 Basf Ag Verfahren zur herstellung von waessrigen loesungen von hydroxylamin
US5266290A (en) 1992-07-10 1993-11-30 Thiokol Corporation Process for making high purity hydroxylammonium nitrate
US5510097A (en) * 1994-05-19 1996-04-23 Olin Corporation Hydroxylammonium nitrate free of ammonium nitrate
US5837107A (en) * 1995-12-20 1998-11-17 Basf Aktiengesellschaft Process for production of aqueous solutions of free hydroxylamine
HRP960601B1 (en) 1995-12-20 2001-12-31 Basf Ag Process for separating medium boiling substances from a mixture of low, medium and high boiling substances

Also Published As

Publication number Publication date
ATE220386T1 (de) 2002-07-15
AU748827B2 (en) 2002-06-13
CA2299475A1 (en) 1999-02-18
AU9158698A (en) 1999-03-01
CN1271331A (zh) 2000-10-25
DE19733681A1 (de) 1999-02-11
NO20000551L (no) 2000-04-04
JP3421013B2 (ja) 2003-06-30
IL134094A (en) 2003-11-23
WO1999007637A1 (de) 1999-02-18
BR9811119A (pt) 2000-07-18
UA54540C2 (uk) 2003-03-17
ES2180194T3 (es) 2003-02-01
KR20010022591A (ko) 2001-03-26
CN1131843C (zh) 2003-12-24
CA2299475C (en) 2008-12-02
RU2189350C2 (ru) 2002-09-20
NO20000551D0 (no) 2000-02-03
NO327773B1 (no) 2009-09-21
IL134094A0 (en) 2001-04-30
KR100522063B1 (ko) 2005-10-18
EP1012114A1 (de) 2000-06-28
MY123175A (en) 2006-05-31
EP1012114B1 (de) 2002-07-10
DE59804740D1 (de) 2002-08-14
US6299734B1 (en) 2001-10-09
TW440540B (en) 2001-06-16
JP2001513479A (ja) 2001-09-04

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