CN113712084B - 一种食品专用油脂基料油及其制备方法 - Google Patents
一种食品专用油脂基料油及其制备方法 Download PDFInfo
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- 235000013305 food Nutrition 0.000 title claims abstract description 20
- 239000002199 base oil Substances 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000003921 oil Substances 0.000 title claims description 41
- 238000005809 transesterification reaction Methods 0.000 claims abstract description 98
- 239000004519 grease Substances 0.000 claims abstract description 64
- 239000013078 crystal Substances 0.000 claims abstract description 51
- 239000007787 solid Substances 0.000 claims abstract description 34
- 235000021323 fish oil Nutrition 0.000 claims abstract description 28
- 241001092040 Crataegus Species 0.000 claims abstract description 25
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims abstract description 25
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims abstract description 25
- 235000009685 Crataegus X maligna Nutrition 0.000 claims abstract description 25
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims abstract description 25
- 235000009486 Crataegus bullatus Nutrition 0.000 claims abstract description 25
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims abstract description 25
- 235000009682 Crataegus limnophila Nutrition 0.000 claims abstract description 25
- 235000004423 Crataegus monogyna Nutrition 0.000 claims abstract description 25
- 235000002313 Crataegus paludosa Nutrition 0.000 claims abstract description 25
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 24
- 230000002255 enzymatic effect Effects 0.000 claims abstract description 17
- 150000002148 esters Chemical class 0.000 claims abstract description 12
- 235000019198 oils Nutrition 0.000 claims description 40
- 125000002252 acyl group Chemical group 0.000 claims description 29
- 239000000463 material Substances 0.000 claims description 12
- 238000005194 fractionation Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- 108090000790 Enzymes Proteins 0.000 claims description 10
- 102000004190 Enzymes Human genes 0.000 claims description 10
- 108090001060 Lipase Proteins 0.000 claims description 9
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- 239000004367 Lipase Substances 0.000 claims description 9
- 235000019421 lipase Nutrition 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 9
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims description 9
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 8
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 5
- 229910052740 iodine Inorganic materials 0.000 claims description 5
- 239000011630 iodine Substances 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
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- 230000035484 reaction time Effects 0.000 claims description 4
- 241000251468 Actinopterygii Species 0.000 claims description 3
- 108010048733 Lipozyme Proteins 0.000 claims description 3
- FCCDDURTIIUXBY-UHFFFAOYSA-N lipoamide Chemical compound NC(=O)CCCCC1CCSS1 FCCDDURTIIUXBY-UHFFFAOYSA-N 0.000 claims description 3
- 210000001835 viscera Anatomy 0.000 claims description 3
- 238000004090 dissolution Methods 0.000 claims description 2
- 238000006911 enzymatic reaction Methods 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 229940116364 hard fat Drugs 0.000 claims description 2
- 238000003860 storage Methods 0.000 abstract description 25
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- 238000002425 crystallisation Methods 0.000 abstract description 23
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- 230000008025 crystallization Effects 0.000 abstract description 22
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- 238000012986 modification Methods 0.000 abstract description 3
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- 230000003197 catalytic effect Effects 0.000 abstract 1
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- 230000037230 mobility Effects 0.000 description 21
- 239000000047 product Substances 0.000 description 19
- 238000004364 calculation method Methods 0.000 description 17
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- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 12
- 238000013508 migration Methods 0.000 description 7
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- 239000000203 mixture Substances 0.000 description 6
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 235000019197 fats Nutrition 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
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- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- 125000005456 glyceride group Chemical group 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 235000019737 Animal fat Nutrition 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000010828 elution Methods 0.000 description 2
- 125000004185 ester group Chemical group 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 241001391944 Commicarpus scandens Species 0.000 description 1
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 206010017472 Fumbling Diseases 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
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- 239000003054 catalyst Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
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- 238000005516 engineering process Methods 0.000 description 1
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- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 102000054765 polymorphisms of proteins Human genes 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000013557 residual solvent Substances 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- NRHMKIHPTBHXPF-TUJRSCDTSA-M sodium cholate Chemical compound [Na+].C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC([O-])=O)C)[C@@]2(C)[C@@H](O)C1 NRHMKIHPTBHXPF-TUJRSCDTSA-M 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
- 235000021404 traditional food Nutrition 0.000 description 1
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C12P7/6436—Fatty acid esters
- C12P7/6445—Glycerides
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Zoology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Fats And Perfumes (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
Description
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CN202110836433.0A CN113712084B (zh) | 2021-07-23 | 2021-07-23 | 一种食品专用油脂基料油及其制备方法 |
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CN202110836433.0A CN113712084B (zh) | 2021-07-23 | 2021-07-23 | 一种食品专用油脂基料油及其制备方法 |
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CN113712084A CN113712084A (zh) | 2021-11-30 |
CN113712084B true CN113712084B (zh) | 2024-05-24 |
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Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH09194876A (ja) * | 1996-01-25 | 1997-07-29 | Ueda Seiyu Kk | 可塑性油脂の製造方法 |
CN101255380A (zh) * | 2007-03-03 | 2008-09-03 | 苑洪德 | 甘油三酯型鱼油及其制作方法 |
CN101979622A (zh) * | 2010-09-13 | 2011-02-23 | 北京凯泰新世纪生物技术有限公司 | 一种脂肪酶催化合成鱼油乙酯的方法 |
WO2011068275A1 (ko) * | 2009-12-04 | 2011-06-09 | 씨제이제일제당(주) | 효소적 에스테르 교환반응을 통한 초콜릿 및 제과용 유지 제조 방법 |
CN102113574A (zh) * | 2009-12-30 | 2011-07-06 | 嘉里特种油脂(上海)有限公司 | 一种婴幼儿食品用油脂组合物的制备方法 |
CN103430893A (zh) * | 2013-09-06 | 2013-12-11 | 海南定大养殖有限公司 | 楂鱼人工育苗方法 |
CN105821088A (zh) * | 2016-05-26 | 2016-08-03 | 暨南大学 | 一种利用酶催化制备富含epa和dha甘油酯的方法 |
WO2016176987A1 (zh) * | 2015-05-06 | 2016-11-10 | 江南大学 | 一种富含1,3-二油酸-2-棕榈酸甘油三酯结构脂的制备方法 |
CN109699760A (zh) * | 2019-03-13 | 2019-05-03 | 广州市至润油脂食品工业有限公司 | 包含巴沙鱼油的脂肪组合物和制备方法以及在人造奶油中的应用 |
-
2021
- 2021-07-23 CN CN202110836433.0A patent/CN113712084B/zh active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH09194876A (ja) * | 1996-01-25 | 1997-07-29 | Ueda Seiyu Kk | 可塑性油脂の製造方法 |
CN101255380A (zh) * | 2007-03-03 | 2008-09-03 | 苑洪德 | 甘油三酯型鱼油及其制作方法 |
WO2011068275A1 (ko) * | 2009-12-04 | 2011-06-09 | 씨제이제일제당(주) | 효소적 에스테르 교환반응을 통한 초콜릿 및 제과용 유지 제조 방법 |
CN102113574A (zh) * | 2009-12-30 | 2011-07-06 | 嘉里特种油脂(上海)有限公司 | 一种婴幼儿食品用油脂组合物的制备方法 |
CN101979622A (zh) * | 2010-09-13 | 2011-02-23 | 北京凯泰新世纪生物技术有限公司 | 一种脂肪酶催化合成鱼油乙酯的方法 |
CN103430893A (zh) * | 2013-09-06 | 2013-12-11 | 海南定大养殖有限公司 | 楂鱼人工育苗方法 |
WO2016176987A1 (zh) * | 2015-05-06 | 2016-11-10 | 江南大学 | 一种富含1,3-二油酸-2-棕榈酸甘油三酯结构脂的制备方法 |
CN105821088A (zh) * | 2016-05-26 | 2016-08-03 | 暨南大学 | 一种利用酶催化制备富含epa和dha甘油酯的方法 |
CN109699760A (zh) * | 2019-03-13 | 2019-05-03 | 广州市至润油脂食品工业有限公司 | 包含巴沙鱼油的脂肪组合物和制备方法以及在人造奶油中的应用 |
Non-Patent Citations (3)
Title |
---|
Sử dụng enzyme lipase Candida rugosa làm xúc tác cho phản ứng tổng hợp biodiesel từ dầu cá tra (Pangasius hypophtalmus);Nguyễn Thị Tuyết Như等;SCIENCE & TECHNOLOGY DEVELOPMENT;20150331;第18卷(第1期);第29-39页 * |
脂肪酶催化饱和单甘酯与棕榈油酯交换制备含甘油二酯油及其结晶特性研究;刘尊;仇超颖;宋佳;杨雪;张宁;汪勇;;中国油脂;20170620(第06期);全文 * |
酶催化酯交换制备零反式脂肪酸食品专用油脂基料的性质研究;何;赵金利;张参;李清浩;汪勇;;中国油脂;20160920(第09期);全文 * |
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