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CN110125828A - A kind of preparation method of diamond tool - Google Patents

A kind of preparation method of diamond tool Download PDF

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Publication number
CN110125828A
CN110125828A CN201910448627.6A CN201910448627A CN110125828A CN 110125828 A CN110125828 A CN 110125828A CN 201910448627 A CN201910448627 A CN 201910448627A CN 110125828 A CN110125828 A CN 110125828A
Authority
CN
China
Prior art keywords
diamond tool
diamond
preparation
film
matrix
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910448627.6A
Other languages
Chinese (zh)
Inventor
王琳
孟普
熊德伟
李云东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bengbu College
Original Assignee
Bengbu College
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bengbu College filed Critical Bengbu College
Priority to CN201910448627.6A priority Critical patent/CN110125828A/en
Publication of CN110125828A publication Critical patent/CN110125828A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D18/00Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
    • B24D18/0018Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for by electrolytic deposition
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D18/00Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
    • B24D18/0054Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for by impressing abrasive powder in a matrix

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Polishing Bodies And Polishing Tools (AREA)

Abstract

The present invention discloses a kind of preparation method of diamond tool, comprising the following steps: S1, prepares diamond tool matrix;S2, film is covered in the working face of diamond tool matrix, film surface is equipped with one group of through-hole, and through-hole is in array distribution;S3, using film as template layer, diamond particles are plated on to the working face of diamond tool matrix by electroplating technology, diamond particles are arranged in the through-hole in array;S4, removal film, and solder is added in the working face of diamond tool matrix;S5, diamond tool matrix is brazed, obtains diamond tool;By film as template, make diamond particles ordered arrangement in solder, both the bond strength that can have possessed high-melting-point brazed diamond tool is high, resistance to grinding, the features such as solder is good to diamond wetability, brazing temperature can be reduced again, diamond thermal damage is reduced, performance and the service life of diamond tool are improved.

Description

A kind of preparation method of diamond tool
Technical field
The present invention relates to diamond tool technical field, the preparation method of specifically a kind of diamond tool.
Background technique
Brazed diamond tool bond strength is high, and height of protrusion is big, and resistance to grinding, high temperature resistance are good, but due to soldering temperature Degree is high, diamond heat damage and strength reduction, during heavy load grinding, diamond often occurs it is broken, be broken or even whole It falls off.Solder used at present mainly has Ni base, Ag base and Cu base.
In order to improve brazing filler metal fusing point, researcher is using Ag-Cu or Cu-Sn low-melting alloy as solder, and solder is to gold Hard rock wellability is good, and diamond thermal damage is small, and low-melting alloy solder hardness is not high, and resistance to grinding, high temperature resistance are poor, though It is to manufacture the ideal solder of diamond tool, but application range is restricted.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation method of diamond tool, this method can both possess high-melting-point pricker The bond strength for welding diamond tool is high, resistance to grinding, the features such as solder is good to diamond wetability, and can reduce soldering temperature Degree reduces diamond thermal damage, improves performance and the service life of diamond tool.
The technical solution adopted by the present invention to solve the technical problems is:
A kind of preparation method of diamond tool, comprising the following steps:
S1, diamond tool matrix is prepared;
S2, film is covered in the working face of diamond tool matrix, film surface is equipped with one group of through-hole, and through-hole is in array distribution;
S3, using film as template layer, diamond particles are plated on to the working face of diamond tool matrix by electroplating technology, gold Hard rock particle is arranged in the through-hole in array;
S4, removal film, and solder is added in the working face of diamond tool matrix;
S5, diamond tool matrix is brazed, obtains diamond tool.
Further, diamond tool matrix described in step S1 is prepared in the way of machining using 45# steel.
Further, 0.15~0.22mm of film thickness described in step S2, through-hole diameter 0.35mm, the spacing of adjacent through-holes For 1.1mm.
Further, diamond particle size described in step S3 is 250~350 μm, and diamond particle surfaces are coated with Ti gold Belong to layer.
Further, after diamond particles have been electroplated in step S3, the shape between diamond particles and diamond tool matrix At electroplated layer, electroplated layer is Ni-Co bianry alloy.
Further, solder described in step S4 is Cu-Sn alloy.
Further, temperature when step S5 is brazed is 800~900 DEG C, keeps the temperature 15~20min.
Further, step S5 soldering uses vacuum brazing process or brazing in controlled atmosphere method.
Further, the step of carrying out insulation processing the method also includes the non-working surface to diamond tool matrix.
The invention has the advantages that making diamond particles ordered arrangement in solder as template by film, both may be used Bond strength to possess high-melting-point brazed diamond tool is high, resistance to grinding, the features such as solder is good to diamond wetability, again Brazing temperature can be reduced, diamond thermal damage is reduced, improves performance and the service life of diamond tool;Using plating Ti diamond It may be implemented during the brazing process, Ti forms the chemical bonding of TiC with the C in diamond first, and solder is good to diamond wetability, The interface bond strength of diamond is improved, diamond order arrangement to avoid being segregated and gathering, can improve the work effect of tool Rate can reduce brazing temperature using low-temperature brazing filler metal, reduce diamond thermal damage, improve the service life of diamond tool.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples:
Fig. 1 is the schematic diagram of step S2 of the present invention;
Fig. 2 is the schematic diagram of step S3 of the present invention;
Fig. 3 is the schematic diagram of step S4 of the present invention.
Specific embodiment
The present invention provides a kind of preparation method of diamond tool, comprising the following steps:
S1, diamond tool matrix is prepared;45# steel can be used to be prepared in the way of machining, diamond tool matrix Shape according to the diamond tool shape of actually required preparation, the present invention unlimited fixture external shape first uses grinding wheel after preparation It polishes diamond tool matrix surface, removes rusty stain and grease stain, recycle acetone in ultrasonic cleaner to diamond Tool base cleans 10min, drying;
S2, as shown in Figure 1, the working face in diamond tool matrix 1 is covered with film 2,2 surface of film is equipped with one group of through-hole 3, leads to Hole 3 is in array distribution;Preferably, film 2 0.15~0.22mm of thickness, through-hole diameter 0.35mm, the spacing of adjacent through-holes For 1.1mm;
S3, as shown in connection with fig. 2, is template layer with film 2, diamond particles 4 is plated on diamond tool by electroplating technology The working face of matrix 1, diamond particles 4 are arranged in the through-hole 3 in array;
For diamond particles 4 having a size of 250~350 μm, 4 surface of diamond particles is coated with Ti metal layer;Diamond particles 4 are being electroplated The method that alkali process is combined with acid processing can be used to purify diamond particles table in preceding progress surface cleaning and hydrophilicity-imparting treatment Face, the sodium hydroxide solution of alkali process 2:1, diamond is placed in sodium hydroxide solution and boils half an hour on electric furnace, It cools down out, is washed to neutrality with distillation, is then impregnated with dust technology, then thoroughly cleaned up through hot water wash, cold water-washing step;
Before plating, diamond tool matrix 1 also carries out surface degreasing processing of rust removing again, makes diamond tool matrix metal inside Fresh lattice expose, convenient for the metal ion deposition in electroplate liquid in the state of activation metal crystal surface on, mainly Steps are as follows: strong acid etch → cold water embathes → again cold water wash → electrochemical activation → cold water embathes → again cold water wash → Mild acid etching activation → cold water is washed, and rear electrification enters electroplating bath and carries out rush of current, carries out pre-galvanized, dash current density is 2.0A/dm2, current density is adjusted to 1.5A/dm after 1min2, keep 10min;Then formal electroplated diamond particle;It has been electroplated After diamond particles, electroplated layer 5 is formed between diamond particles and diamond tool matrix, electroplated layer 5 is the conjunction of Ni-Co binary Gold;
S4, as shown in connection with fig. 3 removes film 2, and adds solder 6 in the working face of diamond tool matrix 1, and solder 6 uses Cu-Sn alloy;
S5, diamond tool matrix is brazed, soldering uses vacuum brazing process or brazing in controlled atmosphere method, temperature when soldering Degree is 800~900 DEG C, keeps the temperature 15~20min, obtains diamond tool.
This method further includes the steps that the non-working surface progress insulation processing to diamond tool matrix, insulation processing can adopt With plating insulation processing.
The above described is only a preferred embodiment of the present invention, being not intended to limit the present invention in any form;Appoint What those skilled in the art, without departing from the scope of the technical proposal of the invention, all using the side of the disclosure above Method and technology contents make many possible changes and modifications to technical solution of the present invention, or are revised as the equivalent reality of equivalent variations Apply example.Therefore, anything that does not depart from the technical scheme of the invention according to the technical essence of the invention do above embodiments Any simple modification, equivalent replacement, equivalence changes and modification, all of which are still within the scope of protection of the technical scheme of the invention.

Claims (9)

1. a kind of preparation method of diamond tool, which comprises the following steps:
S1, diamond tool matrix is prepared;
S2, film is covered in the working face of diamond tool matrix, film surface is equipped with one group of through-hole, and through-hole is in array distribution;
S3, using film as template layer, diamond particles are plated on to the working face of diamond tool matrix by electroplating technology, gold Hard rock particle is arranged in the through-hole in array;
S4, removal film, and solder is added in the working face of diamond tool matrix;
S5, diamond tool matrix is brazed, obtains diamond tool.
2. a kind of preparation method of diamond tool according to claim 1, which is characterized in that diamond described in step S1 Tool base is prepared in the way of machining using 45# steel.
3. a kind of preparation method of diamond tool according to claim 1, which is characterized in that film described in step S2 is thick 0.15~0.22mm, through-hole diameter 0.35mm are spent, the spacing of adjacent through-holes is 1.1mm.
4. a kind of preparation method of diamond tool according to claim 1, which is characterized in that diamond described in step S3 Particle size is 250~350 μm, and diamond particle surfaces are coated with Ti metal layer.
5. a kind of preparation method of diamond tool according to claim 1, which is characterized in that Buddha's warrior attendant has been electroplated in step S3 After stone particle, electroplated layer is formed between diamond particles and diamond tool matrix, electroplated layer is Ni-Co bianry alloy.
6. a kind of preparation method of diamond tool according to claim 1, which is characterized in that solder described in step S4 is Cu-Sn alloy.
7. a kind of preparation method of diamond tool according to claim 1, which is characterized in that temperature when step S5 is brazed Degree is 800~900 DEG C, keeps the temperature 15~20min.
8. a kind of preparation method of diamond tool according to claim 1, which is characterized in that step S5 soldering is using true Empty method for brazing or brazing in controlled atmosphere method.
9. a kind of preparation method of diamond tool according to claim 1, which is characterized in that the method also includes right The non-working surface of diamond tool matrix carries out the step of insulation processing.
CN201910448627.6A 2019-05-28 2019-05-28 A kind of preparation method of diamond tool Pending CN110125828A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910448627.6A CN110125828A (en) 2019-05-28 2019-05-28 A kind of preparation method of diamond tool

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910448627.6A CN110125828A (en) 2019-05-28 2019-05-28 A kind of preparation method of diamond tool

Publications (1)

Publication Number Publication Date
CN110125828A true CN110125828A (en) 2019-08-16

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CN (1) CN110125828A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110936303A (en) * 2019-12-26 2020-03-31 华侨大学 Electroplating-brazing composite preparation method of fine-grained superhard abrasive tool
CN111152143A (en) * 2020-01-16 2020-05-15 深圳西斯特科技有限公司 Directional arrangement method for superhard abrasives
CN113043178A (en) * 2021-03-17 2021-06-29 江苏韦尔博新材料科技有限公司 Brazing diamond grinding and polishing sheet and preparation process thereof
CN115026730A (en) * 2022-07-11 2022-09-09 河北锟洲科技有限公司 Roller diamond arrangement implantation method based on 3D printing
CN115106936A (en) * 2022-06-24 2022-09-27 中国地质大学(武汉) Diamond dressing disc and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106735778A (en) * 2016-12-14 2017-05-31 青岛科技大学 A kind of new method for making Study on Brazed Superabrasive Tools by arc cold-welding legal system
US20180311772A1 (en) * 2014-07-02 2018-11-01 United Technologies Corporation Abrasive Preforms and Manufacture and Use Methods
CN109352542A (en) * 2018-11-15 2019-02-19 娄底市安地亚斯电子陶瓷有限公司 Diamond abrasive tool and preparation method thereof
CN109702660A (en) * 2019-01-09 2019-05-03 南京航空航天大学 One kind being used for the precision machined super hard abrasive compliant tool of micro hole and its manufacturing method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20180311772A1 (en) * 2014-07-02 2018-11-01 United Technologies Corporation Abrasive Preforms and Manufacture and Use Methods
CN106735778A (en) * 2016-12-14 2017-05-31 青岛科技大学 A kind of new method for making Study on Brazed Superabrasive Tools by arc cold-welding legal system
CN109352542A (en) * 2018-11-15 2019-02-19 娄底市安地亚斯电子陶瓷有限公司 Diamond abrasive tool and preparation method thereof
CN109702660A (en) * 2019-01-09 2019-05-03 南京航空航天大学 One kind being used for the precision machined super hard abrasive compliant tool of micro hole and its manufacturing method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110936303A (en) * 2019-12-26 2020-03-31 华侨大学 Electroplating-brazing composite preparation method of fine-grained superhard abrasive tool
CN111152143A (en) * 2020-01-16 2020-05-15 深圳西斯特科技有限公司 Directional arrangement method for superhard abrasives
CN113043178A (en) * 2021-03-17 2021-06-29 江苏韦尔博新材料科技有限公司 Brazing diamond grinding and polishing sheet and preparation process thereof
CN115106936A (en) * 2022-06-24 2022-09-27 中国地质大学(武汉) Diamond dressing disc and preparation method thereof
CN115106936B (en) * 2022-06-24 2023-03-28 中国地质大学(武汉) Diamond dressing disc and preparation method thereof
CN115026730A (en) * 2022-07-11 2022-09-09 河北锟洲科技有限公司 Roller diamond arrangement implantation method based on 3D printing
CN115026730B (en) * 2022-07-11 2024-03-01 河北锟洲科技有限公司 Roller diamond arrangement implantation method based on 3D printing

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Application publication date: 20190816

RJ01 Rejection of invention patent application after publication