CN115553487A - Heating cigarette sheet and manufacturing method thereof - Google Patents
Heating cigarette sheet and manufacturing method thereof Download PDFInfo
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- CN115553487A CN115553487A CN202211253675.8A CN202211253675A CN115553487A CN 115553487 A CN115553487 A CN 115553487A CN 202211253675 A CN202211253675 A CN 202211253675A CN 115553487 A CN115553487 A CN 115553487A
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- parts
- pulp
- fruit pulp
- tobacco
- sheet
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 23
- 238000010438 heat treatment Methods 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- 241000208125 Nicotiana Species 0.000 claims abstract description 76
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 76
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 74
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000000843 powder Substances 0.000 claims abstract description 43
- 235000019737 Animal fat Nutrition 0.000 claims abstract description 34
- 239000000779 smoke Substances 0.000 claims abstract description 33
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 31
- 229920001131 Pulp (paper) Polymers 0.000 claims abstract description 27
- 239000000853 adhesive Substances 0.000 claims abstract description 24
- 230000001070 adhesive effect Effects 0.000 claims abstract description 24
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 13
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- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 9
- 229930182490 saponin Natural products 0.000 claims abstract description 9
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- 229920001864 tannin Polymers 0.000 claims abstract description 9
- 235000018553 tannin Nutrition 0.000 claims abstract description 9
- 239000001648 tannin Substances 0.000 claims abstract description 9
- 244000269722 Thea sinensis Species 0.000 claims abstract 10
- 239000000203 mixture Substances 0.000 claims description 40
- 238000002156 mixing Methods 0.000 claims description 37
- 238000003756 stirring Methods 0.000 claims description 18
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- 229910000831 Steel Inorganic materials 0.000 claims description 14
- 239000010959 steel Substances 0.000 claims description 14
- 238000001035 drying Methods 0.000 claims description 13
- 244000299461 Theobroma cacao Species 0.000 claims description 10
- 235000009470 Theobroma cacao Nutrition 0.000 claims description 10
- 238000005507 spraying Methods 0.000 claims description 10
- 238000010345 tape casting Methods 0.000 claims description 8
- 244000060011 Cocos nucifera Species 0.000 claims description 7
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- 238000000034 method Methods 0.000 claims description 7
- 238000012216 screening Methods 0.000 claims description 5
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- 238000000465 moulding Methods 0.000 claims description 2
- 230000000391 smoking effect Effects 0.000 claims 8
- 238000010521 absorption reaction Methods 0.000 abstract description 14
- 239000002994 raw material Substances 0.000 abstract description 12
- 229920002678 cellulose Polymers 0.000 abstract description 4
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- 235000019505 tobacco product Nutrition 0.000 abstract description 4
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 241001122767 Theaceae Species 0.000 description 50
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 48
- 239000002904 solvent Substances 0.000 description 25
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 9
- 238000004537 pulping Methods 0.000 description 9
- 239000000835 fiber Substances 0.000 description 8
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- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 244000070406 Malus silvestris Species 0.000 description 3
- BWPGKXYWPBQBPV-MWQJAWBESA-N Theasaponin Chemical compound O([C@H]1[C@H](O)[C@H](O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@@H](O)CO1)O[C@H]1[C@@H]([C@@H](O)[C@H](O)CO1)O)O[C@H]1CC[C@]2(C)[C@H]3CC=C4[C@@]([C@@]3(CC[C@H]2[C@@]1(CO)C)C)(C)C[C@@H](O)[C@@]1(CO)[C@@H](OC(C)=O)[C@@H](C(C[C@H]14)(C)C)OC(=O)C(\C)=C/C)C(O)=O)[C@@H]1O[C@H](CO)[C@H](O)[C@H](O)[C@H]1O BWPGKXYWPBQBPV-MWQJAWBESA-N 0.000 description 3
- BWPGKXYWPBQBPV-ZOADXXHESA-N Theasaponin Natural products O=C(O[C@@H]1[C@@H](OC(=O)C)[C@]2(CO)[C@@H](O)C[C@@]3(C)[C@@]4(C)[C@@H]([C@]5(C)[C@H]([C@@](CO)(C)[C@@H](O[C@@H]6[C@@H](O[C@@H]7[C@H](O[C@@H]8[C@@H](O)[C@H](O)[C@H](O)CO8)[C@H](O)[C@@H](O)CO7)[C@@H](O[C@H]7[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O7)[C@H](O)[C@@H](C(=O)O)O6)CC5)CC4)CC=C3[C@@H]2CC1(C)C)/C(=C/C)/C BWPGKXYWPBQBPV-ZOADXXHESA-N 0.000 description 3
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- 125000001165 hydrophobic group Chemical group 0.000 description 3
- 239000003760 tallow Substances 0.000 description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 description 3
- 239000008158 vegetable oil Substances 0.000 description 3
- 229920002907 Guar gum Polymers 0.000 description 2
- 235000021314 Palmitic acid Nutrition 0.000 description 2
- 241000219000 Populus Species 0.000 description 2
- 244000126002 Ziziphus vulgaris Species 0.000 description 2
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 235000021016 apples Nutrition 0.000 description 2
- 235000015278 beef Nutrition 0.000 description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 239000000665 guar gum Substances 0.000 description 2
- 229960002154 guar gum Drugs 0.000 description 2
- 235000010417 guar gum Nutrition 0.000 description 2
- 239000003906 humectant Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 239000000693 micelle Substances 0.000 description 2
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 2
- 235000019476 oil-water mixture Nutrition 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 229920001277 pectin Polymers 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 108010005094 Advanced Glycation End Products Proteins 0.000 description 1
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 1
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- 239000001116 FEMA 4028 Substances 0.000 description 1
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- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 241000703939 Gracilariopsis longissima Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 241001349804 Juncus alpinoarticulatus Species 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
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- 239000002253 acid Chemical group 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 125000003172 aldehyde group Chemical group 0.000 description 1
- 150000001299 aldehydes Chemical group 0.000 description 1
- 229940058573 b-d glucose Drugs 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 1
- 229960004853 betadex Drugs 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical group 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- -1 saccharide compounds Chemical class 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 239000002569 water oil cream Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating cigarette sheet and a manufacturing method thereof. The heating cigarette slice comprises water, an adhesive, a smoke agent, tobacco powder, wood pulp, tea fruit pulp and animal oil, wherein the tea fruit pulp comprises tannin and tea saponin, and the animal oil comprises glyceride. According to the application, the tea fruit pulp and the animal fat are added in the raw material of the slice, and the moisture absorption problem of the slice is effectively improved and the tensile strength of the slice is improved through the synergistic effect among cellulose, tannin, tea saponin and glyceride.
Description
Technical Field
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating cigarette sheet and a manufacturing method thereof.
Background
A heating non-combustion tobacco product is a novel product combining a heating appliance and a cigarette cartridge, and is a low-temperature cigarette designed by taking 'heating non-combustion' as the idea, wherein the processed tobacco shreds and the cigarette cartridge are heated to a certain temperature by a special heating device, and the cigarette cartridge is heated to a degree enough to emit smoke for people to absorb.
The tobacco product cartridge which can not burn by heating is mainly divided into two types, namely a particle technology and a sheet technology. The particle technology has the advantages that residues after the heating core is heated are some dry carbonized particles which can be easily removed, but the particle technology has the defects of uneven heating, small smoke amount, easy generation of burnt flavor, inconsistent front and back smoke amount and incapability of keeping the fragrance of cigarettes. The slice technology is that the herbaceous plant or the tobacco-like component is crushed and mixed with the natural fiber, the adhesive and the like are added and stirred evenly, and the slice product is prepared after constant pressure drying. But the disadvantage is that the thin slice is easy to absorb moisture, which affects the adaptability of the machine.
In order to solve the problem of moisture absorption of the sheet, it is common in the prior art to form a moisture-proof layer on the surface of the sheet, such as a moisture-proof humectant for preventing moisture absorption of tobacco sheets disclosed in patent document CN113907409A, which is characterized by comprising polyhydric alcohol, beta-cyclodextrin and polyglucosamine (1-4) -2-amino-B-D glucose, and preventing moisture absorption of the sheet by spraying the moisture-proof humectant. For another example, patent document CN114009826A discloses a material for heating cigarette core and a preparation method thereof, which comprises the following steps: the method comprises the following steps of smoke agent pretreatment, spice preparation, sizing material pretreatment, base material slurry preparation, powder material treatment, base material forming, powder spraying, sheet rolling, film laminating, drying and forming. The porous solid adsorbent is added into the smoke agent, the smoke agent is mixed with a glue system to embed the smoke agent in the base material slurry, and the moisture absorption problem of the prepared cigarette core material can be effectively solved by matching with the film coating process treatment.
In the scheme, on one hand, the moisture-proof layer is easy to fall off, so that the long-term storage effect of the sheet is influenced; on the other hand, the sheet itself has a problem of low tensile strength, and the material used for the moisture barrier does not have a positive influence on the tensile strength of the sheet.
Disclosure of Invention
The present invention is to solve the above problems, and provides a heated cigarette sheet and a method for producing the same.
According to the technical scheme for solving the problems, firstly, the heating cigarette sheet is provided, and comprises water, an adhesive, a smoke agent, tobacco powder, wood pulp, tea fruit pulp and animal oil, wherein the tea fruit pulp comprises tannin and tea saponin, and the animal oil comprises glyceride.
Wherein, water, adhesive, smoke agent, tobacco powder and wood pulp are common components of the slice.
The fuming agent is used for atomizing and generating smoke when being heated, and can be selected from common fuming agents such as propylene glycol and glycerol. Preferably, the smoke agent comprises 10-60 parts of propylene glycol and 40-90 parts of glycerol by mass.
The wood pulp is mainly used for providing supporting fibers for the slices and ensuring the basic strength of the slices, and is generally prepared by chemically pulping and physically pulping plant raw materials, wherein the plant raw materials can be woody plants such as coniferous wood, broadleaf wood and the like, can also be herbaceous plants such as Chinese alpine rush, cabo and the like, and can be directly purchased on the market.
The tobacco powder is used for providing the traditional cigarette fragrance for the slices and also providing certain supporting fiber, and is prepared by directly fermenting tobacco leaves and then freezing and crushing the fermented tobacco leaves.
The adhesive is used for combining the solid components, preferably is a nontoxic adhesive without pungent smell, and preferably comprises one or more of guar gum, chitosan, sodium carboxymethylcellulose and pectin.
Water is generally used for diluting the components, so that the components can be conveniently made into sheets in a subsequent papermaking process.
In order to solve the problems of moisture absorption and low tensile strength of the flakes, tea pulp and animal fat are creatively added to the raw materials of the flakes.
The tea fruit pulp is mainly obtained by extracting tea fruits under the condition of a solvent, wherein the tea fruits comprise outer shells and tea seeds in the outer shells, the shells contain high-content tannin, and the tea seeds contain high-content tea saponin and vegetable oil. The solvent for extracting the tea fruit is not limited, and a mixed solvent of propylene glycol and water is preferably used in the present invention. The amount ratio of propylene glycol to water is not limited, and as a preferred aspect of the present invention, the solvent comprises, by mass, 10 to 60 parts of propylene glycol and 20 to 90 parts of water. The ratio of the amount of the tea fruit to the solvent is not limited, and in order to improve the extraction rate, it is preferable in the present invention that 10 to 80 parts by mass of the tea fruit and 10 to 80 parts by mass of the solvent are mixed at the time of extraction.
The animal fat and oil mainly contains triglyceride of palmitic acid and stearic acid. Preferably, the animal fat comprises one or more of lard, beef tallow and mutton tallow.
When the tea fruit pulp and the animal fat are mixed for use, firstly, the tea fruit pulp and the animal fat can respectively act: in the tea fruit pulp: the wood pulp cellulose is subjected to condensation reaction with active hydrogen on tannin molecules through aldehyde groups (in the process of preparing wood pulp, the used bleaching agent oxidizes cellulose hydroxyl into groups such as aldehyde, ketone, acid and the like), and tannin is anchored on the fibers through covalent bonds to replace a hydrogen bond connection structure between the cellulose, so that the hydrophobicity of the sheet is improved, the moisture absorption is avoided, and the bonding strength between the fibers is improved to a certain extent, namely the tensile strength of the sheet is improved; the vegetable oil can form a hydrophobic film on the surface of the sheet through the hydrophobic groups of the vegetable oil, so that the hydrophobic property is improved to realize moisture resistance, and the internal stress of the sheet can be improved to increase the tensile strength of the sheet. In the animal fat and oil: the hydrophobic property is improved through the hydrophobic group, and the internal stress is improved.
Second, the tea fruit pulp and animal fat can act synergistically: due to the existence of water and animal fat, before the sheet is formed, slurry obtained by mixing all the raw materials is an oil-water mixture, and the theasaponin has good interfacial activity, can help the oil-water mixture to be emulsified, improves the uniformity of the slurry and improves the moisture-proof uniformity of the sheet. Meanwhile, the theasaponin can also be self-assembled to form micelles, the micelles can be self-assembled at an oil-water interface to form an ordered fibrous aggregate, and theasaponin molecules are adsorbed perpendicular to the interface, so that the tea saponin has extremely high elastic modulus and viscosity, shows a viscoelastic behavior, and improves the tensile strength of the sheet through viscoelasticity. The glyceride is also an amphiphilic molecule, glyceride in the oil phase tends to be adsorbed to the surface of oil drops, glyceride crystals can pierce fiber interface membranes of tea saponin to enter the water phase under a certain concentration, the glyceride part participates in interface formation, the glyceride and the tea saponin synergistically reduce the interface tension, formed emulsion drops are smaller, the stacking is tighter, the strength of the constructed three-dimensional network structure is higher, and therefore the mechanical property is improved.
In the process, the dosage of the tea fruit pulp and the animal fat has certain influence on the finally expressed hydrophobicity and tensile strength, and the dosage of the animal fat is too high, so that the dosage of glyceride is too high, the viscoelasticity of a fiber interface film is influenced, and the tensile strength of the sheet is influenced; the dosage of the animal fat is too low, so that the dosage of the glyceride is too low, on one hand, the hydrophobicity is insufficient, and on the other hand, the glyceride is not enough to pierce a fiber interface membrane, so that the synergistic effect of the glyceride and the tea saponin is influenced. Preferably, the animal fat is 3-5wt% of the tea fruit pulp.
The content of other raw materials also has certain influence, and as the optimization of the invention, the heating cigarette sheet comprises 10 to 60 parts of tobacco powder, 5 to 60 parts of tea fruit pulp, 10 to 40 parts of water, 0.2 to 5 parts of adhesive, 10 to 60 parts of smoke agent, 1 to 4 parts of wood pulp and 0.5 to 4 parts of animal fat according to the parts by mass.
In order to further improve the moisture absorption problem and tensile strength of the flakes, in the present application, as a preferred aspect of the present invention, the tobacco powder is prepared by baking a mixture of fruit pulp and fermented tobacco leaves at 140 to 160 ℃ and then pulverizing the mixture.
The traditional tobacco powder only comprises fermented tobacco leaves, and fruit pulp is added in the application for co-drying. The fruit pulp is mainly extracted from fruit raw materials under the condition of solvent, and contains saccharide compounds such as fructose and the like. The method can reduce harmful ingredients in tobacco leaves and simultaneously ferment to obtain amino acid by fermenting the tobacco leaves. The amino acid and the carbohydrate can generate Maillard reaction at a certain temperature, so that the fragrance of the slices is further improved, and the miscellaneous gas and the irritation are reduced; the obtained product including furfural can be covalently condensed with tannin in tea fruit pulp, so as to improve hydrophobicity and tensile strength of the sheet, and the compatibility of tobacco powder and wood pulp is better under the intermediary action of tannin.
In view of the amount of the Maillard reaction product, the tobacco powder preferably comprises 10 to 99 parts by mass of the fermented tobacco leaves and 1 to 30 parts by mass of the fruit pulp.
The fruit pulp can be solvent extract of any fruit raw material, such as apple pulp, jujube pulp, coconut pulp and the like, and coconut pulp is preferably used in the invention. As the oil content of coconut meat is 35%, the oil is rich in capric acid, palmitic acid, lauric acid, oleic acid, fatty acid and free fatty acid, and the hydrophobic group in coconut oil can be utilized to further improve the moisture absorption problem of the slices. The choice of the solvent for extracting the fruit pulp is not limited, and as the optimization of the invention, the solvent comprises 10 to 50 parts of propylene glycol and 30 to 80 parts of water by mass. The amount ratio of the fruit to the solvent is not limited, and as a preferable aspect of the present invention, 10 to 60 parts by weight of the fruit and 20 to 90 parts by weight of the solvent are mixed at the time of extraction.
The fermented tobacco leaves can be products of fresh tobacco leaves fermented in any way, and are preferably mixed fermentation products of the tobacco leaves and cocoa pulp. The tobacco leaves and cocoa pulp are fermented together to adjust the color of the tobacco leaves uniformly and increase the milk fragrance and bean fragrance of the tobacco leaves. Preferably, 10 to 80 parts by mass of cocoa pulp and 30 to 90 parts by mass of tobacco leaf are mixed and fermented.
It is a further object of the present application to provide a method of making a heated cigarette sheet comprising the steps of:
s1, uniformly mixing tobacco powder, tea fruit pulp, water, an adhesive, a smoke agent, wood pulp and animal fat according to the mass parts, and stirring at 50-60 ℃ to obtain thick pulp;
s2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, forming and drying to obtain a sheet.
In the application, the thick slurry is prepared by stirring at a specific temperature range of 50-60 ℃ to promote the stable forming of the oil-water emulsion, so that the subsequent hydrophobicity and tensile strength are ensured.
The sheet itself needs to have a certain moisture content to avoid the sheet from being too dry and fragile, and as a preferable aspect of the present invention, the sheet is obtained by drying the sheet after molding until the moisture content is 7 to 12%.
As a preferred aspect of the present invention, the tobacco powder is prepared by the steps of: mixing fresh cocoa pulp and tobacco leaf, and fermenting at 40-50 deg.C; taking out the fermentation product, and baking at 90-110 deg.C until the water content is 10-20% to obtain fermented tobacco leaf; mixing the fermented tobacco leaves and fruit pulp, baking at 140-160 deg.C until the water content is 4-7%, pulverizing, and sieving to obtain tobacco powder.
The invention has the beneficial effects that:
1. according to the application, the moisture absorption problem of the sheet is effectively improved and the tensile strength of the sheet is improved by adding tea fruit pulp and animal fat in the raw material of the sheet.
2. In this application, through the modified traditional tobacco powder of pulp, can also cooperate the use of tea pulp in order to further improve the sheet moisture absorption problem and improve tensile strength when improving the suction taste of sheet, can also improve the compatibility of tobacco powder and wood pulp in addition.
Detailed Description
The following are specific embodiments of the present invention and further describe the technical solutions of the present invention, but the present invention is not limited to these examples.
Example 1
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated by mass portion.
Preparing fruit pulp: uniformly mixing 20 parts of propylene glycol and 80 parts of water to obtain a solvent; and mixing 20 parts of coconut meat and 80 parts of solvent, crushing, pulping and filtering to obtain the fruit pulp.
Preparing tea fruit pulp: uniformly mixing 20 parts of propylene glycol and 80 parts of water to obtain a solvent; and mixing 20 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 30 parts of fresh cocoa pulp and 70 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at constant temperature of 45 ℃ for 7 days; taking out the mixture A, baking the mixture A in an oven at 100 ℃, and baking the mixture A until the water content is 16%; then, mixing 90 parts of the mixture A and 5 parts of the fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 145 ℃, and continuously baking until the moisture content is 7%; and crushing and screening the mixture B to obtain tobacco powder.
Preparing a smoke agent: 30 parts of propylene glycol and 70 parts of glycerol are uniformly mixed to obtain the smoke agent.
The animal oil is beef tallow. The adhesive is pectin. The wood pulp is selected from poplar pulp.
S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of smoke agent, 2 parts of wood pulp and 1 part of animal fat, and stirring at the constant temperature of 55 ℃ for 4 hours to obtain thick pulp.
S2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, and drying a formed sheet until the water content is 9%; and peeling the dried thin sheet from the steel belt, wrapping and sealing the thin sheet and packaging.
Example 2
This embodiment is substantially the same as embodiment 1, except that: the dosage of animal fat is increased.
In the step S1, 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of smoke agent, 2 parts of wood pulp and 2 parts of animal fat are uniformly mixed, and then stirred for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
Example 3
This embodiment is substantially the same as embodiment 1, except that: greatly increase the dosage of animal fat.
In the step S1, 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of smoke agent, 2 parts of wood pulp and 4 parts of animal fat are uniformly mixed, and then stirred for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
Example 4
This embodiment is substantially the same as embodiment 1, except that: no fruit pulp is used.
Preparing tobacco powder: uniformly mixing 30 parts of fresh cocoa pulp and 70 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at constant temperature of 45 ℃ for 7 days; taking out the mixture A, baking the mixture A in an oven at 100 ℃, and baking the mixture A until the water content is 16%; then, 90 parts of the mixture A is put into an oven at 145 ℃ to be continuously baked until the moisture content is 7 percent, and finally, the mixture A is crushed and sieved to obtain the tobacco powder.
Example 5
This embodiment is substantially the same as embodiment 1, except that: the tobacco leaves are not fermented.
Preparing tobacco powder: baking 100 parts of tobacco leaves in an oven at 100 ℃ until the moisture content is 16%; then, mixing 90 parts of tobacco leaves and 5 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 145 ℃, and continuously baking until the moisture content is 7%; and crushing and screening the mixture B to obtain tobacco powder.
Example 6
This embodiment is substantially the same as embodiment 1, except that: the pulp is replaced by apple pulp from coconut pulp.
Preparing fruit pulp: uniformly mixing 20 parts of propylene glycol and 80 parts of water to obtain a solvent; and mixing 20 parts of apples and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Example 7
This embodiment is substantially the same as embodiment 1, except that: the stirring temperature is too high.
Step S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of smoke agent, 2 parts of wood pulp and 1 part of animal fat, and stirring at the constant temperature of 40 ℃ for 4 hours to obtain thick pulp.
Example 8
This embodiment is substantially the same as embodiment 1, except that: the stirring temperature is too low.
Step S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of smoke agent, 2 parts of wood pulp and 1 part of animal fat, and stirring at the constant temperature of 80 ℃ for 4 hours to obtain thick pulp.
Example 9
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated by mass parts.
Preparing fruit pulp: uniformly mixing 10 parts of propylene glycol and 90 parts of water to obtain a solvent; and mixing 10 parts of apples and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 10 parts of propylene glycol and 90 parts of water to obtain a solvent; mixing 10 parts of tea fruit and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 20 parts of fresh cocoa pulp and 80 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at constant temperature of 40 ℃ for 7 days; taking out the mixture A, putting the mixture A into an oven, and baking the mixture A until the water content is 10%; then, mixing 99 parts of the mixture A and 1 part of the fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven to be continuously baked at 160 ℃ until the moisture content is 4%; and crushing and screening the mixture B to obtain tobacco powder.
Preparing a smoke agent: 10 parts of propylene glycol and 90 parts of glycerol are uniformly mixed to obtain the smoke agent.
The animal oil is lard. Guar gum is selected as the adhesive. The wood pulp is poplar wood pulp.
S1, uniformly mixing 60 parts of tobacco powder, 10 parts of tea fruit pulp, 40 parts of water, 5 parts of an adhesive, 60 parts of a smoke agent, 4 parts of wood pulp and 0.5 part of animal fat, and stirring at a constant temperature of 50 ℃ for 4 hours to obtain thick pulp.
S2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, and drying a formed sheet until the water content is 7%; and peeling the dried thin sheet from the steel belt, wrapping and sealing the thin sheet and packaging.
Example 10
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated by mass parts.
Preparing fruit pulp: uniformly mixing 60 parts of propylene glycol and 40 parts of water to obtain a solvent; mixing 80 parts of Chinese date and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 60 parts of propylene glycol and 40 parts of water to obtain a solvent; mixing 80 parts of tea fruit and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 70 parts of fresh cocoa pulp and 30 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A for 7 days at constant temperature of 50 ℃; taking out the mixture A, putting the mixture A into an oven, and baking the mixture A at 90 ℃ until the water content is 20%; then, mixing 10 parts of the mixture A and 30 parts of the fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven, and continuously baking at 140 ℃ until the moisture content is 5%; and crushing and screening the mixture B to obtain tobacco powder.
Preparing a smoke agent: 60 parts of propylene glycol and 40 parts of glycerol are uniformly mixed to obtain the smoke agent.
The animal oil is lard. The adhesive is sodium carboxymethylcellulose. The wood pulp is selected from Gracilaria verrucosa pulp.
S1, uniformly mixing 10 parts of tobacco powder, 60 parts of tea fruit pulp, 10 parts of water, 0.2 part of adhesive, 10 parts of smoke agent, 1 part of wood pulp and 1.8 parts of animal fat, and stirring at a constant temperature of 60 ℃ for 4 hours to obtain thick pulp.
S2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, and drying a formed sheet until the water content is 12%; and peeling the dried thin sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 1
This comparative example is essentially the same as example 1, except that: instead of using tea pulp, equal quality water was used instead of tea pulp.
S1, uniformly mixing 25 parts of tobacco powder, 60 parts of water, 1 part of adhesive, 11 parts of smoke agent, 2 parts of wood pulp and 1 part of animal fat, and stirring at the constant temperature of 55 ℃ for 4 hours to obtain thick slurry.
S2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, and drying a formed sheet until the water content is 9%; and peeling the dried thin sheet from the steel belt, wrapping and sealing the thin sheet and packaging.
Comparative example 2
This comparative example is essentially the same as example 1, except that: animal fat is replaced by equal mass of water without using animal fat.
S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 11 parts of water, 1 part of adhesive, 11 parts of smoke agent and 2 parts of wood pulp, and stirring at the constant temperature of 55 ℃ for 4 hours to obtain thick pulp.
S2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, and drying a formed sheet until the water content is 9%; and peeling the dried thin sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 3
This comparative example is essentially the same as example 1, except that: tea fruit pulp and animal oil and fat are not used, and equal-quality water is used for replacing the tea fruit pulp and the animal oil and fat.
S1, uniformly mixing 25 parts of tobacco powder, 61 parts of water, 1 part of adhesive, 11 parts of smoke agent and 2 parts of wood pulp, and stirring at the constant temperature of 55 ℃ for 4 hours to obtain thick slurry.
S2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, and drying a formed sheet until the water content is 9%; and peeling the dried thin sheet from the steel belt, wrapping, sealing and packaging.
[ PROPERTIES DETECTION ]
The tensile strength test was carried out on the sheets obtained in examples and comparative examples according to the test method of clause 6 in YC/T16-2014 reconstituted tobacco, and the test results are shown in Table 1 below.
The sheets obtained in the examples and comparative examples were placed in the same environment, and moisture was measured at different standing times, and the results of the measurements are shown in table 1 below.
Table 1.
As shown in Table 1, by comparing the examples with the comparative examples, it can be seen that the combination of tea fruit pulp and animal fat and oil is effective in improving the tensile strength of the sheet and reducing the moisture absorption of the sheet. Meanwhile, by comparing example 2 with examples 1 and 3, it can be seen that although the moisture absorption of the sheet improves with the increase in the amount of animal fat, the tensile strength of the sheet is affected by the excessively high amount of animal fat. By comparing example 1 with examples 4 and 5, it can be seen that co-baking the pulp with fermented tobacco leaves also improves tensile strength and reduces moisture absorption to some extent. By comparing example 1 with example 6, it can be seen that coconut pulp has better moisture resistance than regular fruit pulp. By comparing example 1 with examples 7 and 8, it can be seen that the stirring also influences the forming of the thick paste emulsion to a certain extent, and thus influences the properties of the sheets formed from the thick paste emulsion.
The specific embodiments described herein are merely illustrative of the spirit of the invention. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the invention as defined in the appended claims.
Claims (10)
1. A heating cigarette slice comprises water, adhesive, smoke agent, tobacco powder and wood pulp, and is characterized in that: the tea fruit pulp comprises tannin and tea saponin, and the animal oil comprises glyceride.
2. A heated rolled smoking sheet according to claim 1, wherein: the dosage of the animal fat is 3-5wt% of the dosage of the tea fruit pulp.
3. A heated smoking article according to claim 1, wherein: the heating cigarette sheet comprises, by mass, 10-60 parts of tobacco powder, 5-60 parts of tea fruit pulp, 10-40 parts of water, 0.2-5 parts of an adhesive, 10-60 parts of a smoke agent, 1-4 parts of wood pulp and 0.5-4 parts of animal fat.
4. A heated rolled smoking sheet according to claim 1, wherein: the tobacco powder is prepared by baking and crushing a mixture of fruit pulp and fermented tobacco leaves at 140-160 ℃.
5. A heated rolled smoking sheet according to claim 4, wherein: according to the mass parts, the tobacco powder comprises 10-99 parts of fermented tobacco leaves and 1-30 parts of fruit pulp.
6. A heated rolled smoking sheet according to claim 4, wherein: the fermented tobacco leaves are mixed fermentation products of tobacco leaves and cocoa pulp.
7. A heated rolled smoking sheet according to claim 4, wherein: the fruit pulp comprises coconut pulp.
8. A method of manufacturing a heated rolled smoking sheet according to any one of claims 1 to 7, wherein: the method comprises the following steps:
s1, uniformly mixing tobacco powder, tea fruit pulp, water, an adhesive, a smoke agent, wood pulp and animal fat according to the mass parts, and stirring at 50-60 ℃ to obtain thick pulp;
s2, uniformly spraying the thick slurry on a steel belt through a slit of tape casting equipment, forming and drying to obtain a sheet.
9. A method of manufacturing a heated smoking article according to claim 8, wherein: drying after molding until the water content is 7-12% to obtain the slice.
10. The method of manufacturing a heated cigarette sheet of claim 8, wherein: the tobacco powder is prepared by the following steps: mixing cocoa pulp and tobacco leaf, and fermenting at 40-50 deg.C; taking out the fermentation product, and baking at 90-110 deg.C until the water content is 10-20% to obtain fermented tobacco leaf; mixing the fermented tobacco leaves and the fruit pulp, baking at 140-160 ℃ until the moisture content is 4-7%, and then crushing and screening to obtain the tobacco powder.
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