CN103356400A - Soap-base facial cleanser and preparation method thereof - Google Patents
Soap-base facial cleanser and preparation method thereof Download PDFInfo
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- CN103356400A CN103356400A CN2013102964401A CN201310296440A CN103356400A CN 103356400 A CN103356400 A CN 103356400A CN 2013102964401 A CN2013102964401 A CN 2013102964401A CN 201310296440 A CN201310296440 A CN 201310296440A CN 103356400 A CN103356400 A CN 103356400A
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- soap base
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- cleaning cream
- facial cleaning
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Abstract
The invention discloses a soap-base facial cleanser and a preparation method thereof. The soap-base facial cleanser is mainly prepared from 30-35 wt.% of fatty acid, 15-20 wt.% of polyalcohol, 5.5-6.5 wt.% of potassium hydroxide, 2-4 wt.% of emulsifier, 3-5 wt.% of polyquaternary amine salt-7, 0.1-0.5 wt.% of guar hydroxypropyltrimonium chloride, 0.05-0.1 wt.% of ion chelator, 0.2-0.3 wt.% of essence and the balance of deionized water. The soap-base facial cleanser can generate abundant, fine, thick and stable foam, and can protect the skin.
Description
Technical field
The present invention relates to cosmetic composition and preparation method thereof, especially a kind of soap base facial cleaning cream and preparation method thereof.
Background technology
In clean the popular product, clean product of soap base class is more and more in the market, and not only there is ripe product in a lot of international major companies, and domestic a lot of daily chemical industries are also at clean product of soap base class of constantly releasing each conception of species.Clean product of soap base class has excellent washability, and smooth bath sense and salubrious wash rear skinfeel is subject to liking of Chinese Consumer's especially.
Part soap base facial cleaning cream foam is abundant but foam is larger and unstable in the market, and therefore foam easily disappears in washing process, causes cleaning effect poor, and skinfeel is bad.
Summary of the invention
First technical problem that the present invention will solve provides a kind of foam of skin of can protecting and enriches fine and closely woven stable soap base facial cleaning cream.
Second technical problem that the present invention will solve provides the method for the described soap base facial cleaning cream of preparation that a kind of production technology is easy to control.
For solving the problems of the technologies described above, the technical solution used in the present invention is specific as follows:
The invention provides a kind of soap base facial cleaning cream, described soap base facial cleaning cream is mainly made by fatty acid, polyhydric alcohol, potassium hydroxide, emulsifying agent, polyquaternary ammonium salt-7, guar hydroxypropyltrimonium chloride, ion chelating agent, essence and deionized water, and wherein following constituent content is expressed as:
Fatty acid 30～35wt.%
Polyhydric alcohol 15～20wt.%
Potassium hydroxide 5.5～6.5wt.%
Emulsifying agent 2～4wt.%
Polyquaternary ammonium salt-7 3～5wt.%
Guar hydroxypropyltrimonium chloride 0.1～0.5wt.%
Ion chelating agent 0.05 ~ 0.1wt.%
Essence 0.2～0.3wt.%.
Among the present invention, in the prescription of described soap base facial cleaning cream, except said components, can no longer add other components, also can add other components, antiseptic for example, described antiseptic can be methyl hydroxybenzoate, propylparaben etc., preferably methyl hydroxybenzoate and the 0.1～0.2wt.% propylparaben by 0.1～0.3wt.% forms.Described constituent content is take prescription (raw materials) gross weight as 100wt%.
Among the present invention, fatty acid and potassium hydroxide generation saponification are produced soap, have good clean result.Further, described fatty acid is selected from following a kind of or arbitrarily several combination: dodecoic acid, tetradecylic acid, stearic acid, stearic acid.Further, described fatty acid is selected from following several combination: dodecoic acid, tetradecylic acid, stearic acid, stearic acid.
Among the present invention, polyhydric alcohol provides low-temperature stability for facial cleaning cream and to the moistening effect of skin.Further, described polyhydric alcohol is selected from following a kind of or arbitrarily several combination: glycerol, 1,3 butylene glycol, PEG-400.Further, described polyhydric alcohol is selected from following three kinds combination: glycerol, 1,3 butylene glycol, PEG-400.
Among the present invention, add polyquaternary ammonium salt-7, can change the character of foam, make the size of foam, make foam finer and closely woven abundant; Add guar hydroxypropyltrimonium chloride, then can change the structure of foam, form layer protecting film at foam surface, make foam more stable difficult broken.
Among the present invention, described emulsifying agent is preferably the self emulsifying monoglyceride.
Among the present invention, the preferred EDTA-2Na of described ion chelating agent, it can the softening of water stable foam.
The preferred described soap base facial cleaning cream of the present invention is made by fatty acid, polyhydric alcohol, potassium hydroxide, emulsifying agent, polyquaternary ammonium salt-7, guar hydroxypropyltrimonium chloride, ion chelating agent, essence, methyl hydroxybenzoate, propylparaben and deionized water, and each constituent content is expressed as follows:
Fatty acid 30～35wt.%
Polyhydric alcohol 15～20wt.%
Potassium hydroxide 5.5～6.5wt.%
Emulsifying agent 2～4wt.%
Polyquaternary ammonium salt-7 3～5wt.%
Guar hydroxypropyltrimonium chloride 0.1～0.5wt.%
Ion chelating agent 0.05 ~ 0.1wt.%
Essence 0.2～0.3wt.%
Methyl hydroxybenzoate 0.1～0.3wt.%
Propylparaben 0.1～0.2wt.%
The deionized water surplus.
The present invention also provides a kind of preparation method of described soap base facial cleaning cream, and it may further comprise the steps:
A, ion chelating agent, polyhydric alcohol are added in the deionized water, then add KOH, be heated to 75 ~ 85 ℃, obtain water;
B: fatty acid, emulsifying agent are mixed and heated to 75 ~ 85 ℃, obtain oil phase;
C: water is added in the oil phase rapid stirring;
D: kept more than 80 ℃ the temperature saponification 40 ~ 55 minutes, simultaneously froth breaking;
E: add polyquaternary ammonium salt-7, guar hydroxypropyltrimonium chloride when being cooled to 55 ~ 60 ℃;
F: add essence when being cooled to 40 ~ 45 ℃;
G: keep 40 ~ 45 ℃ to stir 30 ~ 45 minutes, prepare discharging.
When described soap base facial cleaning cream also comprised antiseptic, described antiseptic prepared oil phase with fatty acid, emulsifying agent in step B.
Compared with prior art, beneficial effect of the present invention is:
(1) the present invention adds polyquaternary ammonium salt-7 and guar hydroxypropyltrimonium chloride in prescription, arrange in pairs or groups according to specific ratio by polyquaternary ammonium salt-7 and guar hydroxypropyltrimonium chloride, make the product foam very abundant and fine and closely woven stable, be not easy destroyed, thereby obtained the very abundant and unusual fine and closely woven stable soap base type facial cleaning cream product of foam of a kind of foam.Consumer can form the soft tough and tensile foam protective layer of one deck in use between hand and skin of face, both goed deep into the pore cleaning skin, avoids simultaneously hand skin to cause facial skin lesions because of friction.
(2) the preparation method technique of soap base facial cleaning cream of the present invention is simple, good operation, and material dispersion is even, produces more easy to control.
The specific embodiment
The following example is used for exemplary illustration the present invention, but the scope that does not limit the present invention in any way.
Embodiment 1:
A kind of foam of skin of can protecting enriches fine and closely woven stable soap base facial cleaning cream, takes by weighing as following weight percent material:
| Dodecoic acid | 5％ |
| Tetradecylic acid | 6％ |
| Stearic acid | 20％ |
| Stearic acid | 2％ |
| The self emulsifying monoglyceride | 2.5％ |
| Methyl hydroxybenzoate | 0.2％ |
| Propylparaben | 0.1％ |
| KOH | 6.1％ |
| PEG-400 | 12％ |
| Glycerol | 5％ |
| Polyquaternary ammonium salt-7(Guangzhou Tianci Advanced Materials Co., Ltd, M550) | 4％ |
| Guar hydroxypropyltrimonium chloride | 0.1% |
| 1,3 butylene glycol | 3％ |
| EDTA-2Na | 0.1％ |
| Essence | 0.3％ |
| Water | 34％ |
Respectively water and oil phase are added in the reactor, slowly be heated to 80 ℃, water is joined in the oil phase, rapid stirring, and kept more than 80 ℃ the temperature saponification 45 minutes, add polyquaternary ammonium salt-7 when being cooled to 60 ℃, be incubated 45 minutes, namely get foam and enrich fine and closely woven stable soap base facial cleaning cream.And detect according to industry standard QB/T 1645, test item is as follows: pH 5.5～11.0, heat-resisting (40 ± 1) ℃ keep 24h, return to after the room temperature without oil-water separation phenomenon, cold-resistant-5 ℃～-10 ℃ to keep 24h, return to after the room temperature without layering, coarse, metachromatism.
Embodiment 2:
A kind of foam of skin of can protecting enriches fine and closely woven stable soap base facial cleaning cream, takes by weighing as following weight percent material:
| Dodecoic acid | 6％ |
| Tetradecylic acid | 7.5％ |
| Stearic acid | 17％ |
| Stearic acid | 2％ |
| The self emulsifying monoglyceride | 2.5％ |
| Methyl hydroxybenzoate | 0.2％ |
| Propylparaben | 0.1％ |
| KOH | 6.2％ |
| PEG-400 | 12％ |
| Glycerol | 5％ |
| Polyquaternary ammonium salt-7 | 4％ |
| Guar hydroxypropyltrimonium chloride | 0.5% |
| 1,3 butylene glycol | 3％ |
| EDTA-2Na | 0.1％ |
| Essence | 0.3％ |
| Water | 34％ |
Respectively water and oil phase are added in the reactor, slowly be heated to 80 ℃, water is joined in the oil phase, rapid stirring, and kept more than 80 ℃ the temperature saponification 45 minutes, add polyquaternary ammonium salt-7 when being cooled to 60 ℃, be incubated 45 minutes, namely get foam and enrich fine and closely woven stable soap base facial cleaning cream.And detect according to industry standard QB/T 1645, test item is as follows: pH 5.5～11.0, heat-resisting (40 ± 1) ℃ keep 24h, return to after the room temperature without oil-water separation phenomenon, cold-resistant-5 ℃～-10 ℃ to keep 24h, return to after the room temperature without layering, coarse, metachromatism.
Embodiment 3:
A kind of foam of skin of can protecting enriches fine and closely woven stable soap base facial cleaning cream, takes by weighing as following weight percent material:
| Dodecoic acid | 5％ |
| Tetradecylic acid | 6％ |
| Stearic acid | 18％ |
| Stearic acid | 4％ |
| The self emulsifying monoglyceride | 2.5％ |
| Methyl hydroxybenzoate | 0.2％ |
| Propylparaben | 0.1％ |
| KOH | 6.1％ |
| PEG-400 | 12％ |
| Glycerol | 5％ |
| Polyquaternary ammonium salt-7 | 5％ |
| Guar hydroxypropyltrimonium chloride | 0.1% |
| 1,3 butylene glycol | 3％ |
| EDTA-2Na | 0.1％ |
| Essence | 0.3％ |
| Water | 33％ |
Respectively water and oil phase are added in the reactor, slowly be heated to 80 ℃, water is joined in the oil phase, rapid stirring, and kept more than 80 ℃ the temperature saponification 45 minutes, add polyquaternary ammonium salt-7 when being cooled to 60 ℃, be incubated 45 minutes, namely get foam and enrich fine and closely woven stable soap base facial cleaning cream.And detect according to industry standard QB/T 1645, test item is as follows: pH 5.5～11.0, heat-resisting (40 ± 1) ℃ keep 24h, return to after the room temperature without oil-water separation phenomenon, cold-resistant-5 ℃～-10 ℃ to keep 24h, return to after the room temperature without layering, coarse, metachromatism.
Claims (10)
1. soap base facial cleaning cream, it is characterized in that: described soap base facial cleaning cream is mainly made by fatty acid, polyhydric alcohol, potassium hydroxide, emulsifying agent, polyquaternary ammonium salt-7, guar hydroxypropyltrimonium chloride, ion chelating agent, essence and deionized water, and wherein following constituent content is expressed as:
Fatty acid 30～35wt.%
Polyhydric alcohol 15～20wt.%
Potassium hydroxide 5.5～6.5wt.%
Emulsifying agent 2～4wt.%
Polyquaternary ammonium salt-7 3～5wt.%
Guar hydroxypropyltrimonium chloride 0.1～0.5wt.%
Ion chelating agent 0.05 ~ 0.1wt.%
Essence 0.2～0.3wt.%.
2. soap base facial cleaning cream as claimed in claim 1, it is characterized in that: the raw materials of described soap base facial cleaning cream also comprises antiseptic.
3. soap base facial cleaning cream as claimed in claim 2, it is characterized in that: described antiseptic is the combination of methyl hydroxybenzoate and propylparaben, and wherein the Metagin ester content is 0.1～0.3wt.%, and propylparaben content is 0.1～0.2wt.%.
4. soap base facial cleaning cream as claimed in claim 1, it is characterized in that: described soap base facial cleaning cream is made by fatty acid, polyhydric alcohol, potassium hydroxide, emulsifying agent, polyquaternary ammonium salt-7, guar hydroxypropyltrimonium chloride, ion chelating agent, essence, methyl hydroxybenzoate, propylparaben and deionized water, and each constituent content is expressed as follows:
Fatty acid 30～35wt.%
Polyhydric alcohol 15～20wt.%
Potassium hydroxide 5.5～6.5wt.%
Emulsifying agent 2～4wt.%
Polyquaternary ammonium salt-7 3～5wt.%
Guar hydroxypropyltrimonium chloride 0.1～0.5wt.%
Ion chelating agent 0.05 ~ 0.1wt.%
Essence 0.2～0.3wt.%
Methyl hydroxybenzoate 0.1～0.3wt.%
Propylparaben 0.1～0.2wt.%
The deionized water surplus.
5. such as the described soap base facial cleaning cream of one of claim 1 ~ 4, it is characterized in that: described fatty acid is selected from following a kind of or arbitrarily several combination: dodecoic acid, tetradecylic acid, stearic acid, stearic acid; Described polyhydric alcohol is selected from following a kind of or arbitrarily several combination: glycerol, 1,3 butylene glycol, PEG-400.
6. such as the described soap base facial cleaning cream of one of claim 1 ~ 4, it is characterized in that: described fatty acid is selected from following several combination: dodecoic acid, tetradecylic acid, stearic acid, stearic acid; Described polyhydric alcohol is selected from following three kinds combination: glycerol, 1,3 butylene glycol, PEG-400.
7. such as the described soap base facial cleaning cream of one of claim 1 ~ 4, it is characterized in that: described emulsifying agent is the self emulsifying monoglyceride, and described ion chelating agent is EDTA-2Na.
8. soap base facial cleaning cream as claimed in claim 7, it is characterized in that: described fatty acid is selected from following several combination: dodecoic acid, tetradecylic acid, stearic acid, stearic acid; Described polyhydric alcohol is selected from following three kinds combination: glycerol, 1,3 butylene glycol, PEG-400.
9. the preparation method of a soap base facial cleaning cream as claimed in claim 1 is characterized in that described preparation method comprises the steps:
A, ion chelating agent, polyhydric alcohol are added in the deionized water, then add KOH, be heated to 75 ~ 85 ℃, obtain water;
B: fatty acid, emulsifying agent are mixed and heated to 75 ~ 85 ℃, obtain oil phase;
C: water is added in the oil phase rapid stirring;
D: kept more than 80 ℃ the temperature saponification 40 ~ 55 minutes, simultaneously froth breaking;
E: add polyquaternary ammonium salt-7, guar hydroxypropyltrimonium chloride when being cooled to 55 ~ 60 ℃;
F: add essence when being cooled to 40 ~ 45 ℃;
G: keep 40 ~ 45 ℃ to stir 30 ~ 45 minutes, prepare discharging.
10. the preparation method of soap base facial cleaning cream as claimed in claim 9, it is characterized in that: the raw materials of described soap base facial cleaning cream also comprises antiseptic, described antiseptic adds the preparation oil phase with fatty acid, emulsifying agent in step B.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103919772A (en) * | 2014-03-31 | 2014-07-16 | 上海鲁冠生物科技有限公司 | Bacteria-inhibiting and itching-relieving cream, preparation method and application thereof |
| CN104069026A (en) * | 2014-07-17 | 2014-10-01 | 广州丹奇日用化工厂有限公司 | Facial cleanser and preparation method |
| CN104629096A (en) * | 2014-07-23 | 2015-05-20 | 成都海麓生物科技有限公司 | Gel capable of preventing PM2.5 and other nasal allergens |
| CN108042394A (en) * | 2017-12-20 | 2018-05-18 | 广州玮弘祺生物科技有限公司 | A kind of Soap-base facial cleanser and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103919772A (en) * | 2014-03-31 | 2014-07-16 | 上海鲁冠生物科技有限公司 | Bacteria-inhibiting and itching-relieving cream, preparation method and application thereof |
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| CN104069026A (en) * | 2014-07-17 | 2014-10-01 | 广州丹奇日用化工厂有限公司 | Facial cleanser and preparation method |
| CN104629096A (en) * | 2014-07-23 | 2015-05-20 | 成都海麓生物科技有限公司 | Gel capable of preventing PM2.5 and other nasal allergens |
| CN108042394A (en) * | 2017-12-20 | 2018-05-18 | 广州玮弘祺生物科技有限公司 | A kind of Soap-base facial cleanser and preparation method thereof |
| CN108042394B (en) * | 2017-12-20 | 2020-12-15 | 广州玮弘祺生物科技有限公司 | Soap-based facial cleanser and preparation method thereof |
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