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CN102943396A - Dyeing technology of polyamide fibers - Google Patents

Dyeing technology of polyamide fibers Download PDF

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Publication number
CN102943396A
CN102943396A CN2012104271395A CN201210427139A CN102943396A CN 102943396 A CN102943396 A CN 102943396A CN 2012104271395 A CN2012104271395 A CN 2012104271395A CN 201210427139 A CN201210427139 A CN 201210427139A CN 102943396 A CN102943396 A CN 102943396A
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China
Prior art keywords
cloth
water
dye liquor
dragon
dyestuff
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Pending
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CN2012104271395A
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Chinese (zh)
Inventor
董林
曹光瑾
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Best Pacific Textile Ltd
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Best Pacific Textile Ltd
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Publication date
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Priority to CN2012104271395A priority Critical patent/CN102943396A/en
Publication of CN102943396A publication Critical patent/CN102943396A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a dyeing technology of polyamide fibers, comprising the following steps: (1) adding soda ash Na2CO3 in water until the pH value of the water is 8.8-9.2, adding the cloth in the water with the ratio of the cloth to the water being 1lg:10L, adding dyes telon yellow, telon blue, telon emerald blue to the water and mixing to form a dye liquor, and adding levelling agent to the dye liquor, wherein weight ratio of the telon yellow to the cloth is 0.045:1, the weight ratio of the telon blue to the cloth is 0.015:1, the weight ratio of the telon emerald blue is 0.24:1, and the weight ratio of the levelling agent to the cloth is 0.04:1; and (2) heating up the dye liquor to 70 DEG C, then adding acid-releasing agent to the dye liquor, wherein the ratio of the acid-releasing agent to the water is 0.4g:1L, and the acid-releasing agent is added to the dye liquor at a speed of 0.0067-0.008g/min to reduce the pH value of the dye liquor to 6.5. According to the invention, the technology dyes the cloth uniformly, and greatly reduces the cost of repair or rework.

Description

A kind of dyeing of nylon fibre
Technical field
The present invention relates to a kind of dyeing, specifically a kind of dyeing of nylon fibre.
Background technology
In recent years, increasingly mature along with polyamide fibre elastomer market, the nylon fabric product is more and more used.Because client's demand, nylon fabric can be dyed various colors according to actual needs.In the market the demand of the nylon fabric of bright-colored constantly increased, wherein demand is large especially for the nylon fabric of emerald green blue look.In the process to textile dyeing, need to dye any color, just need to adopt the ACID DYES of corresponding color.Wherein the uneven problem of more dyeing has appearred in ACID DYES with emerald green Lan Sewei representative when in use, causes the fabric quality of finished not high, affects market sales volume.This kind phenomenon is because colouring is too fast after dyestuff reaches the colouring condition, causes local colouring too much, thereby causes whole colouring uneven.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of certain technique of nylon fibre, and it is more even to paint, and has promoted the quality of finished product.
In order to solve the problems of the technologies described above, the present invention takes following technical scheme:
A kind of dyeing of nylon fibre may further comprise the steps:
(1) in water, adds soda ash Na 2CO 3Until the pH value of water is 8.8-9.2, add cloth in water, the proportion of this cloth and water is that 1 kilogram of KG:10 rises L, then adds yellow, day imperial blue and emerald green orchid of day dragon of dyestuff sky dragon in the water, water and dyestuff are mixed into dye liquor, dyestuff sky dragon is yellow counts 0.045:1 by weight with cloth, and the imperial indigo plant in dyestuff sky is 0.015:1 with cloth by weight percentage, and the emerald green orchid of dyestuff sky dragon and cloth are 0.24:1 by weight percentage, also be added with levelling agent in the dye liquor, this levelling agent and cloth are 0.01:1 by weight percentage;
(2) dye liquor is heated to 70 ℃ after, in dye liquor, add acid-releasing agent, the acid-releasing agent of adding and the proportion of water are that 0.4 gram G:1 rises L, join in the dye liquor with the speed of 0.0067-0.008 grams per minute, until the pH value of dye liquor drops to 6.5.
Behind the pH value 6.5 of described dye liquor, heating makes dye liquor be warming up to 95 ℃~98 ℃, and is incubated 30 minutes when temperature is 95 ℃~98 ℃.
The yellow model of dragon was M-5GL in described day, and a day imperial blue model is M-2R, and the model of day emerald green orchid of dragon is M-5G.
The invention solves traditional handicraft and paint too fast and colouring problem of non-uniform that cause, reach the effect of even dyeing, effectively promoted the quality of finished product, greatly reduce the repair rate of cloth and the cost of reforming, for enterprise has reduced production cost.
The specific embodiment
For the ease of those skilled in the art's understanding, the invention will be further described below in conjunction with accompanying drawing.
The present invention has disclosed a kind of dyeing of nylon fibre, may further comprise the steps:
(1) in water, adds soda ash Na 2CO 3Until the pH value of water is 8.8~9.2, in water, add cloth to be dyeed, the proportion of this cloth and water is that 1 kilogram of KG:10 rises L, then add yellow, day imperial blue and emerald green orchid of day dragon of dyestuff sky dragon in the water, water and dyestuff are mixed into dye liquor, dyestuff sky dragon is yellow counts 0.045:1 by weight with cloth, dyestuff sky dragon indigo plant is 0.015:1 with cloth by weight percentage, the emerald green orchid of dyestuff sky dragon is 0.24:1 with cloth by weight percentage, also be added with levelling agent in the dye liquor, this levelling agent and cloth are 0.01:1 by weight percentage; (2) dye liquor is heated to 70 ℃ after, in dye liquor, add acid-releasing agent, the acid-releasing agent of adding and the proportion of water are that 0.4 gram G:1 rises L, join in the dye liquor with the speed of 0.0067~0.008 grams per minute, until the pH value of dye liquor drops to 6.5.Namely be then to add 1 kilogram cloth in 10 liters water, add 0.1 kilogram cloth in the water of 1L, 5 liters water then adds 0.5 kilogram cloth.Equally, when 1 kilogram of the weight of cloth, the dyestuff sky yellow weight of dragon of adding is 0.045 kilogram, and day imperial indigo plant is 0.015 kilogram, and a day imperial emerald green orchid is 0.24 kilogram, and levelling agent is 0.01 kilogram.And mix reinforced according to such proportionate relationship.
Behind the pH value 6.5 of described dye liquor, heating makes dye liquor be warming up to 95 ℃~98 ℃, and is incubated 30 minutes when temperature is 95 ℃~98 ℃.The yellow model of it dragon is M-5GL, and the model of day dragon indigo plant is M-2R, and the emerald green blue model of day dragon is M-5G.Levelling agent and dyestuff sky dragon are blue, it dragon is yellow, a day imperial emerald green orchid is directly to buy on the market and gets final product, and dyestuff is REACTIVE DYES.For material as well known to those skilled in the art, be not described in detail at this.It imperial yellow M-2R is Telon Yellow M-5GL, and a day imperial blue M-2R is Telon Blue M-2R, and day emerald green blue M-5G of dragon is Telon Turquoise M-5G.
The below specifies with specific embodiment.
Embodiment one, adds first pure salty Na in the water of normal temperature (20 ℃~25 ℃) 2CO 3, making water pH value extremely is 8.8, then adds cloth to be dyeed in water, the proportion of this cloth and water is 1 kilogram: 10 liters, namely add the cloth of 1 kilopond in 10 liters the water.Then add in water that dyestuff sky dragon is yellow, it dragon is blue and day imperial emerald green orchid totally three kinds of dyestuffs, wherein dyestuff sky dragon is yellow counts 0.045:1 by weight with cloth, the imperial indigo plant in dyestuff sky is 0.015:1 with cloth by weight percentage, and the emerald green orchid of dyestuff sky dragon and cloth are 0.24:1 by weight percentage.The cloth that namely adds is 1 kilogram, and the dyestuff sky yellow weight of dragon that then adds is 0.045 kilogram, and the sky blue weight of dragon is 0.015 kilogram, and day blue weight of dragon kingfisher is 0.24 kilogram.Also be added with levelling agent in the dye liquor, this levelling agent and cloth are 0.01:1 by weight percentage, i.e. the corresponding levelling agent that adds 0.01 kilogram of 1 kilogram cloth.Then after dye liquor being heated to 70 ℃, add acid-releasing agent in dye liquor, the acid-releasing agent of adding and the proportion of water are that 0.4 gram G:1 rises L, join in the dye liquor with the speed of 0.0067 grams per minute, until the pH value of dye liquor drops to 6.5.The acid-releasing agent that namely adds 0.4 gram in 10 liters the water then adds 4 acid-releasing agents that restrain in 10 liters the water.After the pH value of dye liquor is down to 6.5, dye liquor is heated, make it be warmed up to 95 ℃, and under 95 ℃ temperature, kept 30 minutes.Then other subsequent treatment operations are the same with prior art, namely cool, draining etc., are known technology.Effectively traditional handicraft is too fast to the dyeing of dying cloth, and causes the uneven problem of dyeing.
Embodiment two, add first pure salty Na in the water of normal temperature (20 ℃~25 ℃) 2CO 3, making water pH value extremely is 9.0, then adds cloth to be dyeed in water, the proportion of this cloth and water is 1 kilogram: 10 liters, namely add the cloth of 1 kilopond in 10 liters the water.Then add in water that dyestuff sky dragon is yellow, it dragon is blue and day imperial emerald green orchid totally three kinds of dyestuffs, wherein dyestuff sky dragon is yellow counts 0.045:1 by weight with cloth, the imperial indigo plant in dyestuff sky is 0.015:1 with cloth by weight percentage, and the emerald green orchid of dyestuff sky dragon and cloth are 0.24:1 by weight percentage.The cloth that namely adds is 1 kilogram, and the dyestuff sky yellow weight of dragon that then adds is 0.045 kilogram, and the sky blue weight of dragon is 0.015 kilogram, and day blue weight of dragon kingfisher is 0.24 kilogram.Also be added with levelling agent in the dye liquor, this levelling agent and cloth are 0.01:1 by weight percentage, i.e. the corresponding levelling agent that adds 0.01 kilogram of 1 kilogram cloth.Then after dye liquor being heated to 70 ℃, add acid-releasing agent in dye liquor, the acid-releasing agent of adding and the proportion of water are that 0.4 gram G:1 rises L, join in the dye liquor with the speed of 0.0072 grams per minute, until the pH value of dye liquor drops to 6.5.The acid-releasing agent that namely adds 0.4 gram in 10 liters the water then adds 4 acid-releasing agents that restrain in 10 liters the water.After the pH value of dye liquor is down to 6.5, dye liquor is heated, make it be warmed up to 97 ℃, and under 97 ℃ temperature, kept 30 minutes.Then other subsequent treatment operations are the same with prior art, namely cool, draining etc., are known technology.Effectively traditional handicraft is too fast to the dyeing of dying cloth, and causes the uneven problem of dyeing.
Embodiment three, add first pure salty Na in the water of normal temperature (20 ℃~25 ℃) 2CO 3, making water pH value extremely is 9.2, then adds cloth to be dyeed in water, the proportion of this cloth and water is 1 kilogram: 10 liters, namely add the cloth of 1 kilopond in 10 liters the water.Then add in water that dyestuff sky dragon is yellow, it dragon is blue and day imperial emerald green orchid totally three kinds of dyestuffs, wherein dyestuff sky dragon is yellow counts 0.045:1 by weight with cloth, the imperial indigo plant in dyestuff sky is 0.015:1 with cloth by weight percentage, and the emerald green orchid of dyestuff sky dragon and cloth are 0.24:1 by weight percentage.The cloth that namely adds is 1 kilogram, and the dyestuff sky yellow weight of dragon that then adds is 0.045 kilogram, and the sky blue weight of dragon is 0.015 kilogram, and day blue weight of dragon kingfisher is 0.24 kilogram.Also be added with levelling agent in the dye liquor, this levelling agent and cloth are 0.01:1 by weight percentage, i.e. the corresponding levelling agent that adds 0.01 kilogram of 1 kilogram cloth.Then after dye liquor being heated to 70 ℃, add acid-releasing agent in dye liquor, the acid-releasing agent of adding and the proportion of water are that 0.4 gram G:1 rises L, join in the dye liquor with the speed of 0.008 grams per minute, until the pH value of dye liquor drops to 6.5.The acid-releasing agent that namely adds 0.4 gram in 10 liters the water then adds 4 acid-releasing agents that restrain in 10 liters the water.After the pH value of dye liquor is down to 6.5, dye liquor is heated, make it be warmed up to 98 ℃, and under 98 ℃ temperature, kept 30 minutes.Then other subsequent treatment operations are the same with prior art, namely cool, draining etc., are known technology.Effectively traditional handicraft is too fast to the dyeing of dying cloth, and causes the uneven problem of dyeing.

Claims (3)

1. the dyeing of a nylon fibre may further comprise the steps:
(1) in water, adds soda ash Na 2CO 3Until the pH value of water is 8.8-9.2, add cloth in water, the proportion of this cloth and water is 1 kilogram: 10 liters, then add yellow, day imperial blue and emerald green orchid of day dragon of dyestuff sky dragon in the water, water and dyestuff are mixed into dye liquor, dyestuff sky dragon is yellow counts 0.045:1 by weight with cloth, and the imperial indigo plant in dyestuff sky is 0.015:1 with cloth by weight percentage, and the emerald green orchid of dyestuff sky dragon and cloth are 0.24:1 by weight percentage, also be added with levelling agent in the dye liquor, this levelling agent and cloth are 0.01:1 by weight percentage;
(2) dye liquor is heated to 70 ℃ after, in dye liquor, add acid-releasing agent, the acid-releasing agent of adding and the proportion of water are 0.4 gram: 1 liter, join in the dye liquor with the speed of 0.0067-0.008 grams per minute, until the pH value of dye liquor drops to 6.5.
2. the dyeing of nylon fibre according to claim 1 is characterized in that: behind the pH value 6.5 of described dye liquor, heating makes dye liquor be warming up to 95 ℃~98 ℃, and insulation 30 minutes when temperature is 95 ℃~98 ℃.
3. the dyeing of nylon fibre according to claim 2 is characterized in that: the yellow model of dragon was M-5GL in described day, and the model that day dragon is blue is M-2R, and the emerald green blue model of day dragon is M-5G.
CN2012104271395A 2012-10-31 2012-10-31 Dyeing technology of polyamide fibers Pending CN102943396A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103669026A (en) * 2013-12-09 2014-03-26 常熟市梦迪安家饰用品有限公司 Polyamide fiber dyeing technology
CN105274876A (en) * 2015-11-20 2016-01-27 常熟市梦迪安家饰用品有限公司 Dyeing method of polyamide fibers
CN105887518A (en) * 2016-06-17 2016-08-24 优纤科技(丹东)有限公司 Dyeing method for nylon-56 fibers
CN107630367A (en) * 2017-10-26 2018-01-26 福建省宏港纺织科技有限公司 It is a kind of to be used to improve the heterochromatic technique of polyamide fibre lace cloth flower pattern net bottom

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5631352A (en) * 1994-06-20 1997-05-20 Ciba-Geigy Corporation Azodyes containing a bridge member based on diamino-substituted triazines
CN101446048A (en) * 2008-12-30 2009-06-03 上虞新晟化工工业有限公司 Continuous pad dyeing method for chinlon and blended fabric thereof
CN102199884A (en) * 2011-03-07 2011-09-28 浙江理工大学 Method for dip-dyeing polyamide/cotton (viscose) fabrics with acid or neutral and reactive dyes in one-bath way
CN102702787A (en) * 2012-03-27 2012-10-03 河北永泰柯瑞特化工有限公司 Acid dye composition for nylon dyeing

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5631352A (en) * 1994-06-20 1997-05-20 Ciba-Geigy Corporation Azodyes containing a bridge member based on diamino-substituted triazines
CN101446048A (en) * 2008-12-30 2009-06-03 上虞新晟化工工业有限公司 Continuous pad dyeing method for chinlon and blended fabric thereof
CN102199884A (en) * 2011-03-07 2011-09-28 浙江理工大学 Method for dip-dyeing polyamide/cotton (viscose) fabrics with acid or neutral and reactive dyes in one-bath way
CN102702787A (en) * 2012-03-27 2012-10-03 河北永泰柯瑞特化工有限公司 Acid dye composition for nylon dyeing

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103669026A (en) * 2013-12-09 2014-03-26 常熟市梦迪安家饰用品有限公司 Polyamide fiber dyeing technology
CN105274876A (en) * 2015-11-20 2016-01-27 常熟市梦迪安家饰用品有限公司 Dyeing method of polyamide fibers
CN105887518A (en) * 2016-06-17 2016-08-24 优纤科技(丹东)有限公司 Dyeing method for nylon-56 fibers
CN105887518B (en) * 2016-06-17 2017-11-03 优纤科技(丹东)有限公司 A kind of colouring method of the fiber of polyamide fibre 56
CN107630367A (en) * 2017-10-26 2018-01-26 福建省宏港纺织科技有限公司 It is a kind of to be used to improve the heterochromatic technique of polyamide fibre lace cloth flower pattern net bottom

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Application publication date: 20130227