CN100560859C - Natural fabric and polyamide fibre wet method transfer printing method - Google Patents
Natural fabric and polyamide fibre wet method transfer printing method Download PDFInfo
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- CN100560859C CN100560859C CNB2007100253293A CN200710025329A CN100560859C CN 100560859 C CN100560859 C CN 100560859C CN B2007100253293 A CNB2007100253293 A CN B2007100253293A CN 200710025329 A CN200710025329 A CN 200710025329A CN 100560859 C CN100560859 C CN 100560859C
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Abstract
The invention provides a kind of natural fabric and polyamide fibre wet method transfer printing method, key step comprises: 1, select acid dye inks or REACTIVE DYES printing ink for use; 2, printing: by the flower roller PET film or BOPP film surface are carried out stamp with the printing ink of selecting for use, make the transfer printing film; 3, transfer printing: natural fabric and polyamide fibre by maceration extract, are made printing thin film and institute prints lining again and pass through padding machine simultaneously and pressurize; 4, oven dry:, accompany the baking fixation to the lining oven dry that transfer printing finishes.Advantage of the present invention is: use this method rate of transform height, lining tinctorial yield height, lovely luster, fastness index are superior, low blowdown, environment-friendly water-saving, and technology is simple, production efficiency is high, cost is lower, has realized no paper transfer printing fully.
Description
Technical field
The present invention relates to a kind of dyeing method of fabric, particularly a kind of natural fabric and polyamide fibre wet method transfer printing method.
Background technology
In the prior art, China Patent No. 96108188.0 discloses a kind of transfer printing of natural fabric and has given finishing agent and printing technology.By natural fabric is given processing, close the hydroxyl of natural fabric, utilize the distillation principle of DISPERSE DYES, under hot conditions, finish transfer printing.The shortcoming of giving processing is to form thermoplastic film at the skin of natural fabric to admit DISPERSE DYES or natural fabric is carried out sex change, and this can make the moisture absorbing and sweat releasing of natural fabric, and the ventilative degradation that waits all has certain influence to the fastness and the feel of product.China Patent No. 200410041034.1 discloses a kind of transfer printing of natural fabric, paper coating isolating agent, water-soluble reactive colour print paste stamp, lining roll after the alkali with calico paper simultaneously by padding machine, the dyestuff on the paper dissociates out and to infiltrate face liber inner and painted.The shortcoming of water-soluble reactive colour paper transfer printing is that dyestuff and paper and isolating agent have certain affinity, and the not high printed color vividness that causes of the rate of transform is not high, and dark color and luster can not finely embody.
Summary of the invention
Goal of the invention: the objective of the invention is at the deficiencies in the prior art, the new method for transfer printing of natural fabric such as a kind of cotton and nylon fabric is provided, and the printing ink that uses REACTIVE DYES or ACID DYES to make carries out transfer printing respectively on natural fabric and nylon fabric.
Technical scheme: natural fabric of the present invention and polyamide fibre wet method transfer printing method is characterized in that this method may further comprise the steps:
1, selects acid dye inks or REACTIVE DYES printing ink for use.Wherein acid dye inks is used for real silk, wool, corium and nylon fiber lining.REACTIVE DYES printing ink is mainly used in cotton fabric.
2, printing: by the flower roller PET film or BOPP film surface are carried out stamp with the printing ink of selecting for use, make the transfer printing film.
3, transfer printing: to natural fabric or polyamide fibre dewing such as cottons, printing thin film and print lining are pressurizeed simultaneously through padding machine, the dye transfer on the film is spent type to the face liber fine structure and present printing.
4, oven dry: i.e. the lining oven dry that transfer printing is finished, accompany the baking fixation.
Wherein the colored roller described in the step 2 adopts computer carving plate-making.
Dewing described in the step 3 be instigate print lining and pass through maceration extract.The component of maceration extract and formulation by weight are: thickener 1-10%; Surfactant 1-10%; Cosolvent 1-3%; Alkaline agent 3-5%; All the other are water.Above thickener can be a modified starch ether, and surfactant can be a bleeding agent, and cosolvent can be a glycerine, and alkaline agent can be caustic soda and sodium silicate.Method for making is exactly above component to be mixed get final product.
The natural fabric of indication comprises fabrics such as cotton, fiber crops, real silk, silk flosssilk wadding, people cotton, wool in the step 3.
Oven dry described in the step 4, accompanying the baking temperature is the 100-180 degree.
REACTIVE DYES printing ink of the present invention or acid dye inks are the printing ink of being made by commercially available REACTIVE DYES or ACID DYES.
Specifically be, acid dye inks, it comprises following component and weight ratio: ACID DYES 15-20%, is connected material 20-30%, solvent 50-64%, defoamer 0.3-0.5%, levelling agent 0.3-0.5%.ACID DYES comprises highly acid dyestuff, weak acid dye, neutral dye, acidic complex dye, acid mordant dye.Connect material and select solid-state polyamide for use.Solvent is mainly selected nontoxic ethanol for use, and can add a small amount of low toxicity MEK, or DAA is regulated the rate of drying of printing ink.Defoamer can be a silicone defoaming agent, such as polysiloxane.Levelling agent can be the organosilicon levelling agent, such as polyether-modified polysiloxane.
The preparation method of acid dye inks is:
1, dyestuff is pre-dispersed: solvent (as ethanol) is placed agitator, at temperature 45-55 degree, slowly add bridging agent (as polyamide) during stirring at low speed, dissolve fully until bridging agent, add levelling agent, defoamer again, stir (approximately 5-10 minute), slowly add ACID DYES again, (mixing speed is brought up to about 1200-1500 rev/min in stirring, 30-45 minute), the test color slurry viscosity replenishes adding solvent (as ethanol), regulate viscosity to moderate (approximately 1300-1500 centipoise, i.e. 40 degree).
2, mill base grinds: the mill base that step 1 is prepared, place grinding in ball grinder, and keep grinding about 48-72 hour, make the mill base fineness be less than or equal to 1 micron.
3, configuration printing ink: step 2 gained printing ink is emitted, regulate viscosity to moderate (about 50 seconds, i.e. Zan Shi 2# cup, 25 spend) with the mixture of ethanol or ethanol and MEK or DAA.
REACTIVE DYES printing ink, it comprises following component and weight ratio: REACTIVE DYES 15-30%, is connected material 20-30%, solvent 40-63%, defoamer 0.3-0.5%, levelling agent 0.3-0.5%, pH value stabilization agent 0.5-1%.REACTIVE DYES is selected homemade K type REACTIVE DYES, M type REACTIVE DYES, the perhaps P of U.S. Huntsman Corporation type REACTIVE DYES for use.Connect material and select mandelic acid, acrylic acid alkyd or Abietyl modified alkyd for use.Solvent is mainly selected nontoxic ethanol for use, also can add the rate of drying of a spot of low poison solvent such as MEK, cyclohexanone adjusting printing ink.Defoamer can be silicone based or higher alcohols, such as polysiloxane.Levelling agent can be silicone based, such as polyether-modified polysiloxane.The agent of pH value stabilization is the mixture of organic acid and organic amine.
The preparation method of REACTIVE DYES printing ink is:
1, dyestuff is pre-dispersed: solvent (as ethanol) is placed agitator, at temperature 45-55 degree, slowly add during stirring at low speed and connect material (as the alkyd resins of modification), dissolve fully until bridging agent, add levelling agent, defoamer, the agent of pH value stabilization, stir (approximately 5-10 minute), add REACTIVE DYES again, (the mixer rotating speed is brought up to 1200-1500 rev/min in stirring, stirred 30-45 minute), test mill base viscosity replenishes adding solvent (as ethanol), regulate viscosity to moderate (approximately 1300-1500 centipoise, i.e. 40 degree).
2, mill base grinds: the mill base with step 1 gained, place grinding in ball grinder, and keep grinding 48-72 hour, make the mill base fineness be less than or equal to 1 micron.
3, preparation printing ink: gained printing ink in the step 2 is emitted, and with ethanol or ethanol and MEK, or the mixture of cyclohexanone is regulated modest viscosity (about 50 seconds, i.e. Zan Shi 2# cup, 25 degree).
Beneficial effect: the present invention compared with prior art, its remarkable advantage is: 1, select for use REACTIVE DYES, ACID DYES to make ink printing on the PET film, dyestuff and film do not have affinity, during transfer printing, rate of transform height.2, dye transfer is to lining, the tinctorial yield height, and lovely luster, the fastness index is superior.3, adopt the computer intaglio printing, the printing effect loyalty is embodied on the fabric, four color separation photograph effects, and dim colour transition level all can finely show.4, adopt REACTIVE DYES or ACID DYES stamp at the different natural fibres fabric, nylon fabric is adopted ACID DYES, better agree with fabric characteristics.The dye uptake height, COLOR FASTNESS is good.Therefore loose colour seldom reaches low blowdown, environment-friendly water-saving in the water-washing process.5, technology is simple, need not printing, and the stamp carrier gives processing, the production efficiency height, and cost is lower, energy efficiency.6, need not use paper, realize no paper transfer printing.Avoid a large amount of paper of traditional transfer printing, effectively reduced lumber consumption, reduced the waste water that produces because of papermaking in a large number simultaneously.
The specific embodiment
Embodiment 1～4 is the preparation acid dye inks.
Embodiment 1:
The component and the weight ratio of acid dye inks are: highly acid dyestuff 15%, polyamide 30%, ethanol 54%, machine silicon defoaming agent 0.5%, organosilicon levelling agent 0.5%.
Its preparation method is: ethanol is placed agitator, at temperature 55 degree, slowly add polyamide (solid-state polyamide during stirring at low speed, its molecular weight is between 500-9000), dissolve fully until resin, add organosilicon levelling agent, machine silicon defoaming agent again, stirred 10 minutes, slowly add ACID DYES again, mixing speed is brought up to 1500 rev/mins, stirred the test color slurry viscosity 45 minutes, replenish and add ethanol, adjusting viscosity to 1500 centipoise (40 degree).The mill base of gained is placed grinding in ball grinder, keep grinding 72 hours, make the mill base fineness be less than or equal to 1 micron.Gained printing ink is emitted, and with ethanol or ethanol and MEK, or the mixture of DAA is regulated viscosity to 50 second (Zan Shi 2# cup, 25 degree).
Embodiment 2:
The component of acid dye inks with weight ratio is: weak acid dye 20%, be connected material 20%, solvent 59.4%, defoamer 0.3%, levelling agent 0.3%.
Its preparation method is: ethanol is placed agitator, at temperature 45 degree, slowly add polyamide (forming) during stirring at low speed by dimerization vegetable fatty acids and the polycondensation of polyethylene polyamine class, dissolve fully until resin, add levelling agent, defoamer again, stirred 5 minutes, and slowly added ACID DYES again, mixing speed is brought up to 1200 rev/mins, stirred 30 minutes, the test color slurry viscosity replenishes adding ethanol, regulates viscosity to 1300-1500 centipoise (40 degree).The mill base of gained is placed grinding in ball grinder, keep grinding 48 hours, make the mill base fineness be less than or equal to 1 micron.Gained printing ink is emitted, and with ethanol or ethanol and MEK, or the mixture of DAA is regulated viscosity to 50 second (Zan Shi 2# cup, 25 degree).
Embodiment 3:
The component and the weight ratio of acid dye inks are: acidic complex dye 15%, polyamide 20.2%, solvent 64%, polysiloxane 0.4%, polyether-modified polysiloxane 0.4%.
Its preparation method is: solvent is placed agitator, at temperature 50 degree, slowly add polyamide during stirring at low speed, dissolve fully until resin, add polysiloxane, polyether-modified polysiloxane again, stirred 8 minutes, and slowly added ACID DYES again, mixing speed is brought up to 1400 rev/mins, stirred 40 minutes, the test color slurry viscosity replenishes adding ethanol, regulates viscosity to 1300-1500 centipoise (40 degree).The mill base of gained is placed grinding in ball grinder, keep grinding 60 hours, make the mill base fineness be less than or equal to 1 micron.Gained printing ink is emitted, and with ethanol or ethanol and MEK, or the mixture of DAA is regulated viscosity to 50 second (Zan Shi 2# cup, 25 degree).
Embodiment 4:
The component of acid dye inks with weight ratio is: acid mordant dye 19%, be connected material 30%, solvent 50%, defoamer 0.5%, levelling agent 0.5%.
Its preparation method is with embodiment 1.
Embodiment 5～8 is preparation REACTIVE DYES printing ink.
Embodiment 5:
The component and the weight proportion of REACTIVE DYES printing ink are: selecting homemade M type REACTIVE DYES for use is REACTIVE DYES 15%; Select for use acrylic acid alkyd for connecting material 30%; Selecting ethanol for use is solvent 53%; Selecting the higher alcohols defoamer for use is defoamer 0.5%; Selecting polyether-modified polysiloxane for use is levelling agent 0.5%; The mixture of selecting organic acid and organic amine for use is pH value stabilization agent 1%.
Its preparation method is: ethanol is placed agitator, at temperature 45-55 degree, slowly add the alkyd resins of modification during stirring at low speed, dissolve fully until resin, add levelling agent, defoamer, pH value stabilizing agent, stirred 5 minutes, and added REACTIVE DYES again, the mixer rotating speed is brought up to 1200-1500 rev/min, stirred 30 minutes, test mill base viscosity replenishes adding ethanol, and regulating viscosity is 1300-1500 centipoise (40 degree).The mill base of gained is placed grinding in ball grinder, keep grinding 48 hours, make the mill base fineness be less than or equal to 1 micron.Gained printing ink is emitted, and with ethanol or ethanol and MEK, or the mixture of cyclohexanone is regulated viscosity to 50 second (Zan Shi 2# cup, 25 degree).
Embodiment 6:
The component and the weight proportion of REACTIVE DYES printing ink are: selecting homemade K type REACTIVE DYES for use is REACTIVE DYES 30%; Selecting mandelic acid for use is to connect material 20%; Selecting ethanol for use is solvent 48%; Selecting polysiloxane for use is defoamer 0.5%; Selecting polyether-modified polysiloxane for use is levelling agent 0.5%; The mixture of selecting organic acid and organic amine for use is pH value stabilization agent 1%.
Its preparation method is: ethanol is placed agitator, at temperature 45-55 degree, slowly add the alkyd resins of modification during stirring at low speed, dissolve fully until resin, add levelling agent, defoamer, the agent of pH value stabilization, stirred 5 minutes, and added REACTIVE DYES again, the mixer rotating speed is brought up to 1200-1500 rev/min, stirred 30 minutes, test mill base viscosity replenishes adding ethanol, and regulating viscosity is 1300-1500 centipoise (40 degree).The mill base of gained is placed grinding in ball grinder, keep grinding 48 hours, make the mill base fineness be less than or equal to 1 micron.Gained printing ink is emitted, and with ethanol or ethanol and MEK, or the mixture of cyclohexanone is regulated viscosity to 50 second (Zan Shi 2# cup, 25 degree).
Embodiment 7:
The component and the weight proportion of REACTIVE DYES printing ink are: selecting the P of U.S. Huntsman Corporation type REACTIVE DYES for use is REACTIVE DYES 28.9%; Select for use Abietyl modified alkyd for connecting material 30%; Selecting ethanol for use is solvent 40%; Selecting polysiloxane for use is defoamer 0.3%; Selecting polyether-modified polysiloxane for use is levelling agent 0.3%; The mixture of selecting organic acid and organic amine for use is pH value stabilization agent 0.5%.
Its preparation method is with embodiment 1.
Embodiment 8:
The component and the weight proportion of REACTIVE DYES printing ink are: selecting the P of U.S. Huntsman Corporation type REACTIVE DYES for use is REACTIVE DYES 15.5%; Selecting alkyd resins for use is to connect material 20%; Selecting ethanol for use is solvent 63%; Selecting polysiloxane for use is defoamer 0.5%; Selecting polyether-modified polysiloxane for use is levelling agent 0.5%; The mixture of selecting organic acid and organic amine for use is pH value stabilization agent 0.5%.
Its preparation method is with embodiment 1.
Embodiment 9～11 is the preparation maceration extract.
Embodiment 9:
With percentage by weight is 1% modified starch ether, 1% bleeding agent, and 1% glycerine, 5% caustic soda and 92% water mix.
Embodiment 10:
With percentage by weight is 5% modified starch ether, 5% bleeding agent, and 3% glycerine, 3% sodium silicate and 84% water mix.
Embodiment 11:
With percentage by weight is 10% modified starch ether, 10% bleeding agent, and 2% glycerine, 3% sodium silicate and 75% water mix.
Embodiment 12～15 is natural fabric and polyamide fibre wet method transfer printing method.
Embodiment 12:
The acid dye inks of embodiment 1 preparation is carried out stamp by the flower roller to BOPP film surface, make the transfer printing film; With the maceration extract of silk fabric, the silk fabric after printing thin film and the dewing is pressurizeed simultaneously through padding machine by embodiment 9 preparation; Under 100 ℃,, accompany the baking fixation with the lining oven dry.
Embodiment 13:
The REACTIVE DYES printing ink of embodiment 6 preparations is carried out stamp by the flower roller to the PET film surface, make the transfer printing film; By maceration extract, the cotton fabric after printing thin film and the dewing is pressurizeed simultaneously through padding machine cotton fabric; Under 180 ℃,, accompany the baking fixation with the lining oven dry.
Embodiment 14:
The acid dye inks of embodiment 3 preparations is carried out stamp by the flower roller to PET film surface, make the transfer printing film; With the maceration extract of nylon fiber lining, the nylon fiber lining after printing thin film and the dewing is pressurizeed simultaneously through padding machine by embodiment 10 preparation; Under 140 ℃,, accompany the baking fixation with the lining oven dry.
Embodiment 15:
The REACTIVE DYES printing ink of embodiment 8 preparations is carried out stamp by the flower roller to the BOPP film surface, make the transfer printing film; By maceration extract, the cotton fabric after printing thin film and the dewing is pressurizeed simultaneously through padding machine cotton fabric; Under 160 ℃,, accompany the baking fixation with the lining oven dry.
Claims (6)
1, a kind of natural fabric and polyamide fibre wet method transfer printing method is characterized in that comprising the steps:
(1) selects acid dye inks or REACTIVE DYES printing ink for use;
(2) printing: by the flower roller PET film or BOPP film surface are carried out stamp with the printing ink of selecting for use, make the transfer printing film;
(3) transfer printing: natural fabric or polyamide fibre by maceration extract, are made printing thin film and institute prints lining again and pass through padding machine simultaneously and pressurize;
(4) oven dry:, accompany the baking fixation to the lining oven dry that transfer printing finishes;
Described acid dye inks comprises following component and weight ratio: ACID DYES 15-20%, is connected material 20-30%, solvent 50-64%, defoamer 0.3-0.5%, levelling agent 0.3-0.5%; Wherein, described connection material is solid-state polyamide, and described solvent is an ethanol;
Described REACTIVE DYES printing ink comprises following component and weight ratio: REACTIVE DYES 15-30%, is connected material 20-30%, solvent 40-63%, defoamer 0.3-0.5%, levelling agent 0.3-0.5%, pH value stabilization agent 0.5-1%; Wherein, described connection material is mandelic acid, acrylic acid alkyd or Abietyl modified alkyd, and described solvent is an ethanol.
2, natural fabric according to claim 1 and polyamide fibre wet method transfer printing method is characterized in that acid dye inks makes as follows: (1) dyestuff is pre-dispersed: solvent is placed agitator, at temperature 45-55 degree, slowly add during stirring at low speed and connect material, dissolve fully until bridging agent, add levelling agent, defoamer again, stir, slowly add ACID DYES again, stir, the test color slurry viscosity replenishes the adding solvent, regulate viscosity to 1300～1500 centipoises, 40 degree; (2) mill base grinds: with the prepared mill base of step (1), place grinding in ball grinder, make the mill base fineness be less than or equal to 1 micron; (3) configuration printing ink: step (2) gained printing ink is emitted, use ethanol, or the mixture of ethanol and MEK or DAA adjusting viscosity to 50 second, Zan Shi 2# cup, 25 spend.
3, natural fabric according to claim 1 and polyamide fibre wet method transfer printing method, it is characterized in that REACTIVE DYES printing ink makes as follows: (1) dyestuff is pre-dispersed: solvent is placed agitator, at temperature 45-55 degree, slowly add during stirring at low speed and connect material, until connecting material dissolving fully, add levelling agent, defoamer, the agent of pH value stabilization again, stir, add REACTIVE DYES again, stir, test mill base viscosity replenishes the adding solvent, regulate viscosity to 1300～1500 centipoises, 40 degree; (2) mill base grinds: with the prepared mill base of step (1), place grinding in ball grinder, make the mill base fineness be less than or equal to 1 micron; (3) preparation printing ink: gained printing ink in the step (2) is emitted, and with ethanol or ethanol and MEK, or the mixture of cyclohexanone is regulated viscosity to 50 second, Zan Shi 2# cup, 25 degree.
4, natural fabric according to claim 1 and polyamide fibre wet method transfer printing method is characterized in that the colored roller described in the step (2) adopts computer carving plate-making.
5, natural fabric according to claim 1 and polyamide fibre wet method transfer printing method is characterized in that the maceration extract described in the step (3) comprises following component and weight ratio: thickener 1-10%; Surfactant 1-10%; Cosolvent 1-3%; Alkaline agent 3-5%; All the other are water; Wherein, described thickener is a modified starch ether, and described surfactant is a bleeding agent.
6, natural fabric according to claim 1 and polyamide fibre wet method transfer printing method is characterized in that the oven dry described in the step (4), and accompanying the baking temperature is the 100-180 degree.
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| CNB2007100253293A CN100560859C (en) | 2007-07-24 | 2007-07-24 | Natural fabric and polyamide fibre wet method transfer printing method |
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| CNB2007100253293A CN100560859C (en) | 2007-07-24 | 2007-07-24 | Natural fabric and polyamide fibre wet method transfer printing method |
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| CN101105006A (en) | 2008-01-16 |
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