CN105854067B - The preparation method and chamomile core hip pad paper diaper of chamomile hip pad paper diaper core - Google Patents
The preparation method and chamomile core hip pad paper diaper of chamomile hip pad paper diaper core Download PDFInfo
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- CN105854067B CN105854067B CN201610177120.8A CN201610177120A CN105854067B CN 105854067 B CN105854067 B CN 105854067B CN 201610177120 A CN201610177120 A CN 201610177120A CN 105854067 B CN105854067 B CN 105854067B
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- 235000007866 Chamaemelum nobile Nutrition 0.000 title claims abstract description 79
- 235000007232 Matricaria chamomilla Nutrition 0.000 title claims abstract description 79
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 240000003538 Chamaemelum nobile Species 0.000 title claims abstract 20
- 238000000605 extraction Methods 0.000 claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 claims abstract description 20
- 239000011347 resin Substances 0.000 claims abstract description 18
- 229920005989 resin Polymers 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 54
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 41
- 239000000706 filtrate Substances 0.000 claims description 30
- 239000002904 solvent Substances 0.000 claims description 29
- 244000157790 Buglossoides arvense Species 0.000 claims description 27
- 235000004256 Buglossoides arvense Nutrition 0.000 claims description 27
- 235000019441 ethanol Nutrition 0.000 claims description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 12
- 239000012065 filter cake Substances 0.000 claims description 10
- 238000010992 reflux Methods 0.000 claims description 10
- 238000005292 vacuum distillation Methods 0.000 claims description 10
- 238000010792 warming Methods 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 7
- 229920002521 macromolecule Polymers 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 238000010521 absorption reaction Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 11
- 241000894006 Bacteria Species 0.000 abstract description 9
- 230000002401 inhibitory effect Effects 0.000 abstract description 8
- 201000004624 Dermatitis Diseases 0.000 abstract description 7
- 208000010668 atopic eczema Diseases 0.000 abstract description 7
- 206010061218 Inflammation Diseases 0.000 abstract description 5
- 230000004054 inflammatory process Effects 0.000 abstract description 5
- 230000003467 diminishing effect Effects 0.000 abstract description 4
- 244000005700 microbiome Species 0.000 abstract description 4
- 239000002250 absorbent Substances 0.000 abstract description 2
- 230000002745 absorbent Effects 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 abstract description 2
- 244000042664 Matricaria chamomilla Species 0.000 description 59
- 239000011162 core material Substances 0.000 description 36
- 210000002700 urine Anatomy 0.000 description 6
- 229920001661 Chitosan Polymers 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 239000004745 nonwoven fabric Substances 0.000 description 5
- 230000003385 bacteriostatic effect Effects 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- 244000025254 Cannabis sativa Species 0.000 description 2
- 241001573881 Corolla Species 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 210000004209 hair Anatomy 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000002344 surface layer Substances 0.000 description 2
- 241000270955 Achnatherum calamagrostis Species 0.000 description 1
- 235000017847 Anchusa officinalis Nutrition 0.000 description 1
- 241001072256 Boraginaceae Species 0.000 description 1
- 241001164374 Calyx Species 0.000 description 1
- 241000006479 Cyme Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 235000005206 Hibiscus Nutrition 0.000 description 1
- 235000007185 Hibiscus lunariifolius Nutrition 0.000 description 1
- 244000048199 Hibiscus mutabilis Species 0.000 description 1
- 235000003973 Hibiscus mutabilis Nutrition 0.000 description 1
- 244000284380 Hibiscus rosa sinensis Species 0.000 description 1
- 240000004050 Pentaglottis sempervirens Species 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
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- 239000003814 drug Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 210000000265 leukocyte Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
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- 230000000192 social effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/40—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/44—Medicaments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/46—Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/20—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
- A61L2300/30—Compounds of undetermined constitution extracted from natural sources, e.g. Aloe Vera
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/404—Biocides, antimicrobial agents, antiseptic agents
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
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- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- Hematology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Botany (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Zoology (AREA)
- Absorbent Articles And Supports Therefor (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of chamomile hip pad paper diaper cores and preparation method thereof and chamomile hip pad paper diaper, belong to paper diaper manufacturing technology field.Chamomile hip pad paper diaper core of the present invention includes following raw materials in terms of mass parts: 3-4 parts of camomile extract, 1-2 parts of Radix Arnebiae extract, 100-150 parts of hydroscopic high-molecular resin.The present invention is using the camomile extract and Radix Arnebiae extract for voluntarily researching and developing extraction, it is mixed with hydroscopic high-molecular resin, chamomile hip pad paper diaper core is made, the chamomile paper diaper core is compared with traditional core, it not only assigns paper diaper excellent absorbent properties, also assign the excellent inhibiting bacteria and diminishing inflammation of paper diaper and effect of releiving, there is excellent inhibiting effect to microorganism, it not only can effectively prevent eczema and red hip, has effects that hip pad, keep user safer, more comfortable, healthier, while also there is excellent permeance property.
Description
Technical field
The invention belongs to paper diaper manufacturing technology fields, and in particular to a kind of preparation side of chamomile hip pad paper diaper core
Method and chamomile core hip pad paper diaper.
Background technique
Paper diaper are mainly made of non-woven fabrics surface layer, guide layer, absorbed layer and counterdie, and the use of paper diaper at home
Steady increase of amount does not subtract, and paper diaper, not only as infant's special product, use scope is also gradually expanded, in health care
Industry and some special industries also have use.Paper diaper quality control in process of production and its stringent, total plate count by
To strict control, but still there are part paper diaper to cause paper diaper surface layer total plate count exceeded since raw material pollute；In addition,
Current paper diaper do not have anti-microbial property, use easily grow under urine environment for a long time because of the limitation of its material therefor
Endophytic bacteria, a problem that will lead to eczema, red hip appearance.
Also there is the relevant report of related antibacterial paper diaper in recent years, such as application No. is 201110431244.1 China specially
Benefit discloses a kind of Novel antibacterial paper diaper, is provided with the antibacterial layer of water soluble chitosan on built-in absorbed layer, when urine contacts
After the antibacterial layer of water soluble chitosan, water soluble chitosan solid particle dissolves immediately, to play bacteriostasis property, and is not meeting
To before urine, water soluble chitosan will not dissolve, volatilize, and cause to waste, but the bacteriostasis property of the paper diaper can be with urine
Increasing for liquid measure and weaken, and when urine excess, chitosan is dissolved in urine, can directly contact skin, therefore its city
Field, which is promoted, also will receive limitation；Application No. is 201510703430.4 Chinese patent, a kind of bacteriostatic solution and its system are disclosed
At paper diaper and paper diaper preparation method, assign nonwoven and non-woven fabrics is soaked in the bacteriostatic solution of preparation
The good biocidal property of cloth, but its application in paper diaper field will receive limitation, because containing there are many have in its bacteriostatic solution
Machine substance can remain on non-woven fabrics, although it can assign non-woven fabrics good biocidal property, it still has human skin
Certain adverse effect.
Therefore, there are biggish social effect and good market prospects to the research of paper diaper bacteria resistance function.
Summary of the invention
A kind of chamomile hip pad paper diaper core and its system are provided the purpose of the present invention is overcome the deficiencies in the prior art
Preparation Method and chamomile core hip pad paper diaper, the paper diaper pass through chamomile and the Radix Arnebiae extract for voluntarily researching and developing extraction, system
Core material is obtained, and assigns the excellent inhibiting bacteria and diminishing inflammation of paper diaper and effect of releiving, can effectively prevent eczema and red hip, there is shield
Stern effect.
Chamomile originates in Britain, and plantation is in Germany, France and Morocco.Chamomile have help for sleep, anti-inflammatory reducing internal heat
The effect of, it can be relieved inflammation and the pain symptom of patient, alleviation is had a sleepless night as caused by neurotic skin itch.China also has a large amount of
Cultivation, to be used as medicine and tea making.Simultaneously as chamomile has the manufacture of stimulation white blood cell, and then bacterium can be resisted to enhance
Immune system.
Asian puccoon, alias mountain Asian puccoon, Zi Dan, purple cottonrose hibiscus, it is small, blood, crow rank grass, alkanet, be Boraginaceae puccoon, it is more
Year sward sheet, up to 90 centimetres.Root is upright, cylindrical, slightly curved song, normal disagreement, crust puniceous.Stem is upright, it is single or on
Part discrimination, complete stool is by thick and stiff hair.Leaf alternate, stockless；The long round shape lanceolar of blade is about 6 centimetres, about 1.3 centimetres wide, apex
Point, base portion wedge shape, full edge, two sides is by strigose.The total shape of cyme, basidixed；Flower both sexes；Bract is lobate, two mask coarse wool；Flower
The short tubular of calyx, 5 drastic cracks, sliver are narrow tapering；Corolla white, corolla pipe is short, and apex 5 is split, and throat has 5 flakey appendages, base
Portion has hair, the function with clearing away heat,cooling blood and removing toxin promoting eruption.
The present invention voluntarily researches and develops camomile extract and Radix Arnebiae extract, and the two is compounded, and is applied to paper diaper
In, it to assign the excellent inhibiting bacteria and diminishing inflammation of paper diaper and effect of releiving, can effectively prevent eczema and red hip, there is good shield
Stern effect.
The present invention adopts the following technical scheme:
Chamomile hip pad paper diaper core, including following raw materials in terms of mass parts: 3-4 parts of camomile extract,
1-2 parts of Radix Arnebiae extract, 100-150 parts of hydroscopic high-molecular resin.
The production method of the chamomile hip pad paper diaper core, includes the following steps:
Step 1, the preparation of camomile extract:
A: choosing the chamomile that moisture content is 15%-20%, remove impurity and rhizome, after chamomile immersed into 40-50 DEG C of water
Middle 2-8min, is pulled out, and drip to the anhydrous droplet in chamomile surface is fallen；
B: being freeze-dried 10-15h under -30 to -20 DEG C, 9-15Pa for chamomile, after be crushed to 80-100 mesh；
C: using the mixture of ethyl alcohol and ethyl acetate as Extraction solvent, by ethyl alcohol, ethyl acetate with mass ratio 2:1-3:1
It is uniformly mixed, obtains Extraction solvent, Extraction solvent is warming up to 40-50 DEG C, it is molten that the smashed chamomile of step b is added to extraction
It in agent, is heated to flowing back with the heating rate of 0.5 DEG C/min, maintains the reflux for 5-6h, stop extracting, filter while hot, take filtrate, use
Ethyl acetate washs filter cake, merging filtrate；
D: vacuum distillation removes filtrate, obtains camomile extract；
Step 2, the preparation of Radix Arnebiae extract:
A: Asian puccoon is cleaned, and is cleaned with clear water, and sunning to moisture content is 8%-10%, after be switched to the segment of 1-2cm, it is spare；
B: being freeze-dried 5-10h under -25 to -20 DEG C, 10-15Pa for the Asian puccoon of segment, after be crushed to 100-150 mesh
Sieve, obtains Asian puccoon crushed material；
C: using ethyl alcohol as Extraction solvent, it is warming up to reflux, Asian puccoon crushed material obtained by step b, return stirring 8- is added
10h stops heating, is cooled to 50-55 DEG C, filters while hot, take filtrate, filter cake ethanol washing, merging filtrate；
D: vacuum distillation removes filtrate, obtains powdered Radix Arnebiae extract；
Macromolecule water uptake is added in camomile extract obtained by camomile extract obtained by step 1, step 2 by step 3
It is stirred evenly in resin, obtains mixture；
Step 4, by mixture obtained by step 3 by net wheel absorption, molding obtains chamomile hip pad paper diaper core.
Further, the production method of the chamomile hip pad paper diaper core, what is be wherein added in step 1 c mentions
It takes solvent and the mass ratio of chamomile is 10:1-15:1.
Further, the production method of the chamomile hip pad paper diaper core, the second being wherein added in step 2 c
The mass ratio of alcohol and Asian puccoon crushed material is 5:1-9:1.
The chamomile hip pad paper diaper made from the chamomile hip pad paper diaper core.
Compared with the prior art, the present invention has the following beneficial effects: the present invention is using the chamomile for voluntarily researching and developing extraction
Extract and Radix Arnebiae extract mix it with hydroscopic high-molecular resin, and chamomile hip pad paper diaper core, the chamomile is made
Paper diaper core not only assigns paper diaper excellent absorbent properties compared with traditional core, the also excellent suppression of imparting paper diaper
Bacterium anti-inflammatory and effect of releiving have excellent inhibiting effect to microorganism, not only can effectively prevent eczema and red hip, have shield
Stern effect keeps user safer, more comfortable, healthier, while also having excellent permeance property.
Specific embodiment
Below by specific embodiment, invention is further described in detail, but those skilled in the art will manage
Solution, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.Macromolecule used in the present invention
Water-absorbing resin is acrylic compounds water-absorbing resin.
Embodiment 1
Chamomile hip pad paper diaper core, including following raw materials in terms of mass parts: 3.5 parts of camomile extract,
1.5 parts of Radix Arnebiae extract, 120 parts of hydroscopic high-molecular resin.
The production method of the chamomile hip pad paper diaper core, includes the following steps:
Step 1, the preparation of camomile extract:
A: choosing the chamomile that moisture content is 15%-20%, remove impurity and rhizome, after chamomile is immersed in 45 DEG C of water
6min is pulled out, and drip to the anhydrous droplet in chamomile surface is fallen；
B: being freeze-dried 13h under -25 DEG C, 12Pa for chamomile, after be crushed to 90 meshes；
C: using the mixture of ethyl alcohol and ethyl acetate as Extraction solvent, ethyl alcohol, ethyl acetate are mixed with mass ratio 2.6:1
It closes uniformly, obtains Extraction solvent, Extraction solvent is warming up to 45 DEG C, the smashed chamomile of step b is added in Extraction solvent,
It is heated to flowing back with the heating rate of 0.5 DEG C/min, maintains the reflux for 5.5h, stop extracting, filter while hot, take filtrate, use acetic acid
Ethyl ester washs filter cake, merging filtrate, wherein the mass ratio of the Extraction solvent and chamomile that are added is 12:1；
D: vacuum distillation removes filtrate, obtains camomile extract；
Step 2, the preparation of Radix Arnebiae extract:
A: Asian puccoon is cleaned, and is cleaned with clear water, and sunning to moisture content is 9%, after be switched to the segment of 1.5cm, it is spare；
B: being freeze-dried 8h under -22 DEG C, 13Pa for the Asian puccoon of segment, after be crushed to and sieve with 100 mesh sieve, obtain Asian puccoon crushing
Object；
C: using ethyl alcohol as Extraction solvent, it is warming up to reflux, Asian puccoon crushed material obtained by step b is added, return stirring 9h stops
It only heats, is cooled to 52 DEG C, filters while hot, take filtrate, filter cake ethanol washing, merging filtrate, wherein the ethyl alcohol and purple of addition
The mass ratio that grass meal minces is 8:1；
D: vacuum distillation removes filtrate, obtains powdered Radix Arnebiae extract；
Macromolecule water uptake is added in camomile extract obtained by camomile extract obtained by step 1, step 2 by step 3
It is stirred evenly in resin, obtains mixture；
Step 4, by mixture obtained by step 3 by net wheel absorption, molding obtains chamomile hip pad paper diaper core.
The chamomile hip pad paper diaper made from the resulting chamomile hip pad paper diaper core of the present embodiment, the system of paper diaper
Make to be made of existing manufacture craft.
Embodiment 2
Chamomile hip pad paper diaper core, including following raw materials in terms of mass parts: 3 parts of camomile extract, purple
1 part of careless extract, 100 parts of hydroscopic high-molecular resin.
The production method of the chamomile hip pad paper diaper core, includes the following steps:
Step 1, the preparation of camomile extract:
A: choosing the chamomile that moisture content is 15%, removes impurity and rhizome, after chamomile immersed into 2min in 40 DEG C of water,
It pulls out, drip to the anhydrous droplet in chamomile surface is fallen；
B: being freeze-dried 10h under -30 DEG C, 9Pa for chamomile, after be crushed to 80 meshes；
C: using the mixture of ethyl alcohol and ethyl acetate as Extraction solvent, ethyl alcohol, ethyl acetate are mixed with mass ratio 2:1
Uniformly, Extraction solvent is obtained, Extraction solvent is warming up to 40 DEG C, the smashed chamomile of step b is added in Extraction solvent, with
The heating rate of 0.5 DEG C/min is heated to flowing back, and maintains the reflux for 5h, stops extracting, filters while hot, take filtrate, use ethyl acetate
Wash filter cake, merging filtrate；The mass ratio of the Extraction solvent and chamomile that are wherein added is 10:1；
D: vacuum distillation removes filtrate, obtains camomile extract；
Step 2, the preparation of Radix Arnebiae extract:
A: Asian puccoon is cleaned, and is cleaned with clear water, and sunning to moisture content is 8%, after be switched to the segment of 1cm, it is spare；
B: being freeze-dried 5h under -25 DEG C, 10Pa for the Asian puccoon of segment, after be crushed to and sieve with 100 mesh sieve, obtain Asian puccoon crushing
Object；
C: using ethyl alcohol as Extraction solvent, it is warming up to reflux, Asian puccoon crushed material obtained by step b is added, return stirring 8h stops
It only heats, is cooled to 50 DEG C, filters while hot, take filtrate, filter cake ethanol washing, merging filtrate；The ethyl alcohol and purple being wherein added
The mass ratio that grass meal minces is 5:1；
D: vacuum distillation removes filtrate, obtains powdered Radix Arnebiae extract；
Macromolecule water uptake is added in camomile extract obtained by camomile extract obtained by step 1, step 2 by step 3
It is stirred evenly in resin, obtains mixture；
Step 4, by mixture obtained by step 3 by net wheel absorption, molding obtains chamomile hip pad paper diaper core.
The chamomile hip pad paper diaper made from the resulting chamomile hip pad paper diaper core of the present embodiment.The system of paper diaper
Make to be made of existing manufacture craft.
Embodiment 3
Chamomile hip pad paper diaper core, including following raw materials in terms of mass parts: 4 parts of camomile extract, purple
2 parts of careless extract, 150 parts of hydroscopic high-molecular resin.
The production method of the chamomile hip pad paper diaper core, includes the following steps:
Step 1, the preparation of camomile extract:
A: choosing the chamomile that moisture content is 20%, removes impurity and rhizome, after chamomile immersed into 8min in 50 DEG C of water,
It pulls out, drip to the anhydrous droplet in chamomile surface is fallen；
B: being freeze-dried 15h under -20 DEG C, 15Pa for chamomile, after be crushed to and sieve with 100 mesh sieve；
C: using the mixture of ethyl alcohol and ethyl acetate as Extraction solvent, ethyl alcohol, ethyl acetate are mixed with mass ratio 3:1
Uniformly, Extraction solvent is obtained, Extraction solvent is warming up to 50 DEG C, the smashed chamomile of step b is added in Extraction solvent, with
The heating rate of 0.5 DEG C/min is heated to flowing back, and maintains the reflux for 6h, stops extracting, filters while hot, take filtrate, use ethyl acetate
Wash filter cake, merging filtrate；The mass ratio of the Extraction solvent and chamomile that are wherein added is 15:1；
D: vacuum distillation removes filtrate, obtains camomile extract；
Step 2, the preparation of Radix Arnebiae extract:
A: Asian puccoon is cleaned, and is cleaned with clear water, and sunning to moisture content is 10%, after be switched to the segment of 2cm, it is spare；
B: being freeze-dried 10h under -20 DEG C, 15Pa for the Asian puccoon of segment, after be crushed to 150 meshes, obtain Asian puccoon crushing
Object；
C: using ethyl alcohol as Extraction solvent, being warming up to reflux, is added Asian puccoon crushed material obtained by step b, return stirring 10h,
Stop heating, is cooled to 55 DEG C, filters while hot, take filtrate, filter cake ethanol washing, merging filtrate；The ethyl alcohol that is wherein added with
The mass ratio of Asian puccoon crushed material is 9:1
D: vacuum distillation removes filtrate, obtains powdered Radix Arnebiae extract；
Macromolecule water uptake is added in camomile extract obtained by camomile extract obtained by step 1, step 2 by step 3
It is stirred evenly in resin, obtains mixture；
Step 4, by mixture obtained by step 3 by net wheel absorption, molding obtains chamomile hip pad paper diaper core.
The chamomile hip pad paper diaper made from the resulting chamomile hip pad paper diaper core of the present embodiment.The system of paper diaper
Make to be made of existing manufacture craft.
Reference examples 1
The paper diaper of the reference examples are also made using existing manufacture craft, the difference with paper diaper produced by the present invention
It is to be not added with camomile extract in paper diaper core.Paper diaper core includes the following original according to mass fraction meter simultaneously
Material: 1.5 parts of Radix Arnebiae extract, 120 parts of hydroscopic high-molecular resin.
Reference examples 2
The paper diaper of the reference examples are also made using existing manufacture craft, the difference with paper diaper produced by the present invention
It is that the camomile extract added in paper diaper core is commercially available camomile extract and is wherein not added with Radix Arnebiae extract, together
When paper diaper core include following raw materials in terms of mass parts: 3.5 parts of commercially available camomile extract, hydroscopic high-molecular resin
120 parts.Current existing core manufacture craft can also be used in the method that the production method of paper diaper core can refer to embodiment 1.
1 to 3 gained hip pad paper diaper of embodiment, 1 to 2 gained paper diaper of reference examples are subjected to performance detection, it is as a result as follows
Shown in table 1:
1 performance detection data of table
As seen from the above table, there is good permeance property using paper diaper made from 1 to 3 gained core of the embodiment of the present invention
And comfort, pH are in neutrality substantially, and it is nonirritant to user's hip, it can effective hip pad；Paper diaper tool of the invention simultaneously
There is good inhibiting bacteria and diminishing inflammation, there is good inhibiting effect to microorganism, can effectively prevent eczema and red hip, have and relax
Slow effect；And the paper diaper of common commercially available camomile extract are used, though having certain biocidal property, it is to microorganism
Inhibiting effect it is weaker, although bacterium and fungus colony sum within the specified scope, paper diaper more of the present invention compared to still partially
If do not paid attention to replacing in time, there are still paper diaper total plate count is exceeded, the peace of injury is brought to skin in use for height
Full hidden danger, meanwhile, its pH of the paper diaper of reference examples 2 is higher, and permeance property is also poor；In contrast, as reference examples 1 are i.e. common
Paper diaper, comprehensive performance is poor.In short, the camomile extract voluntarily developed and Asian puccoon are mentioned according to the method for the present invention
It takes object to compound with hydroscopic high-molecular resin, is applied in paper diaper core, paper diaper obtained have good antibacterial disappear
Scorching, the prevention hip pads performance such as eczema and red hip makes the safer environmental protection of paper diaper obtained, more comfortably, healthier.
Claims (4)
1. the production method of chamomile hip pad paper diaper core, includes the following steps:
Step 1, the preparation of camomile extract:
A: choosing the chamomile that moisture content is 15%-20%, remove impurity and rhizome, after chamomile is immersed in 40-50 DEG C of water
2-8min is pulled out, and drip to the anhydrous droplet in chamomile surface is fallen；
B: being freeze-dried 10-15h under -30 to -20 DEG C, 9-15Pa for chamomile, after be crushed to 80-100 mesh；
C: using the mixture of ethyl alcohol and ethyl acetate as Extraction solvent, ethyl alcohol, ethyl acetate are mixed with mass ratio 2:1-3:1
Uniformly, Extraction solvent is obtained, Extraction solvent is warming up to 40-50 DEG C, the smashed chamomile of step b is added to Extraction solvent
In, it is heated to flowing back with the heating rate of 0.5 DEG C/min, maintains the reflux for 5-6h, stop extracting, filter while hot, take filtrate, use second
Acetoacetic ester washs filter cake, merging filtrate；
D: vacuum distillation removes filtrate, obtains camomile extract；
Step 2, the preparation of Radix Arnebiae extract:
A: Asian puccoon is cleaned, and is cleaned with clear water, and sunning to moisture content is 8%-10%, after be switched to the segment of 1-2cm, it is spare；
B: being freeze-dried 5-10h under -25 to -20 DEG C, 10-15Pa for the Asian puccoon of segment, after be crushed to 100-150 mesh,
Obtain Asian puccoon crushed material；
C: using ethyl alcohol as Extraction solvent, it is warming up to reflux, Asian puccoon crushed material obtained by step b is added, return stirring 8-10h stops
It only heats, is cooled to 50-55 DEG C, filters while hot, take filtrate, filter cake ethanol washing, merging filtrate；
D: vacuum distillation removes filtrate, obtains powdered Radix Arnebiae extract；
Macromolecule water uptake is added in powdered Radix Arnebiae extract obtained by camomile extract obtained by step 1, step 2 by step 3
It is stirred evenly in resin, obtains mixture；
Step 4, by mixture obtained by step 3 by net wheel absorption, molding obtains chamomile hip pad paper diaper core；
The chamomile hip pad paper diaper core, including following raw materials in terms of mass parts: 3-4 parts of camomile extract,
1-2 parts of Radix Arnebiae extract, 100-150 parts of hydroscopic high-molecular resin.
2. the production method of chamomile hip pad paper diaper core according to claim 1, which is characterized in that in step 1 c
The Extraction solvent of addition and the mass ratio of chamomile are 10:1-15:1.
3. the production method of chamomile hip pad paper diaper core according to claim 1, which is characterized in that in step 2 c
The ethyl alcohol of addition and the mass ratio of Asian puccoon crushed material are 5:1-9:1.
4. a kind of chamomile hip pad paper diaper comprising chamomile hip pad paper diaper core made of claim 1 the method.
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| CN106267311B (en) * | 2016-08-31 | 2020-04-10 | 西藏宇妥文化发展有限公司 | Water-absorbing composition and preparation method and application thereof |
| CN106267307A (en) * | 2016-08-31 | 2017-01-04 | 西藏宇妥文化发展有限公司 | A kind of compositions with water sorption and preparation method thereof and purposes |
| CN112336906A (en) * | 2019-08-08 | 2021-02-09 | 佛山市顺德区州福慈鑫无纺布有限公司 | Plant essence hip-protecting cream |
| CN110433323A (en) * | 2019-08-21 | 2019-11-12 | 东莞苏氏卫生用品有限公司 | A kind of super absorbent resin containing functional skin care ingredient, preparation method and disposable absorbent article |
| CN110694097A (en) * | 2019-09-18 | 2020-01-17 | 泉州佩吉酷贸易有限公司 | Plant chip for paper diaper and preparation method of paper diaper |
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| CN102440871A (en) * | 2011-12-21 | 2012-05-09 | 刘杰 | Novel antibacterial diaper |
| CN103409990A (en) * | 2013-08-02 | 2013-11-27 | 东华大学 | Finishing agent used for infant red butt hygiene care as well as preparation method and application thereof |
| CN105168206A (en) * | 2015-10-23 | 2015-12-23 | 杨超 | Antibacterial solution, paper diaper prepared through antibacterial solution and preparation method for paper diaper |
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|---|---|---|---|---|
| CN102440871A (en) * | 2011-12-21 | 2012-05-09 | 刘杰 | Novel antibacterial diaper |
| CN103409990A (en) * | 2013-08-02 | 2013-11-27 | 东华大学 | Finishing agent used for infant red butt hygiene care as well as preparation method and application thereof |
| CN105168206A (en) * | 2015-10-23 | 2015-12-23 | 杨超 | Antibacterial solution, paper diaper prepared through antibacterial solution and preparation method for paper diaper |
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Address after: 362200 Hengmei building, Shangzhai village, Yonghe Town, Jinjiang City, Quanzhou City, Fujian Province Patentee after: Fujian slug care products Co.,Ltd. Address before: 362200 Hengmei building, Shangzhai village, Yonghe Town, Jinjiang City, Quanzhou City, Fujian Province Patentee before: FUJIAN BITICHONG BABY PRODUCTS CO.,LTD. |
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Application publication date: 20160817 Assignee: Fujian Quanzhou gulite Biotechnology Research Institute Co.,Ltd. Assignor: Fujian slug care products Co.,Ltd. Contract record no.: X2024980007252 Denomination of invention: Preparation method of chamomile hip protecting diaper core and chamomile core protecting diaper core Granted publication date: 20190326 License type: Common License Record date: 20240626 |
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