CN105559132A - Preparation method and application of functional reconstituted tobacco - Google Patents
Preparation method and application of functional reconstituted tobacco Download PDFInfo
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- CN105559132A CN105559132A CN201610031290.5A CN201610031290A CN105559132A CN 105559132 A CN105559132 A CN 105559132A CN 201610031290 A CN201610031290 A CN 201610031290A CN 105559132 A CN105559132 A CN 105559132A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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Abstract
The invention discloses a preparation method and application of functional reconstituted tobacco. The preparation method includes the following steps that 1, tobacco waste is subjected to soaking extraction and solid-liquid separation to obtain a tobacco powder extraction solution and tobacco powder dregs; 2, tobacco stems are subjected to soaking extraction and separation to obtain a stem extraction solution and stem dregs; 3, the tobacco powder dregs and stem dreg fibers are mixed, wood pulp fibers are added, and the mixture is prepared into pulp; 4, non-tobacco matter is smashed and screened, the screened non-tobacco matter is added into the pulp, the non-tobacco matter and the pulp are mixed evenly, and the pulp is prepared into a substrate in a papermaking mode; or the screened non-tobacco matter is added into the pulp in the pulp papermaking process; 5, a stem concentrated solution, a tobacco powder concentrated solution and spice are blended to obtain a coating solution; 6, the substrate is coated with the coating solution, dried and sliced to obtain tobacco slices. According to the preparation method, the non-tobacco matter is smashed and then added into the pulp, then papermaking is carried out, high-temperature treatment of the non-tobacco matter is not needed, the preparation method is suitable for many types of raw materials, the characteristic aroma of the non-tobacco matter is kept to the maximum degree, and the quality of the tobacco slices is improved.
Description
Technical field
The invention belongs to technical field of tobacco, be specifically related to a kind of preparation method and application of functional form reconstituted tobacco.
Background technology
Reconstituted tobacco, the characteristic such as also known as reconstituted tobacoo, homogeneous tobacco leaf or recombination tobacco leaf, local Filling power is high, have good burning performance, releasing content of coke tar is low, substitute with reconstituted tobacco or pipe tobacco that Some substitute is traditional to prepare cigarette be one of effective means of Tar.
The process adopting paper process to prepare reconstituted tobacco generally includes tobacco material immersion, extraction, using after extract is concentrated as coating fluid, the steps such as the slag charge after immersion carries out that defibrination is manufactured paper with pulp are prepared into paper substrate, and coating solution is obtained reconstituted tobacco after paper substrate drying.In the higher extraction of temperature and the process such as concentrated, in tobacco material, a part can volatilize to suction taste and the contributive material of fragrance, decompose, transform.Thus there is the defects such as fragrance shortcoming and pungent sense aggravation in the reconstituted tobacco causing paper process to prepare, affects its sense organ suction quality.
Application number is that 2014105533996 tangerine grass are prepared in the method for functional form reconstituted tobacco, non-tobacco material tangerine grass is added in reconstituted tobacco, tangerine grass instead of the wood pulp cellulose in reconstituted tobacco paper substrate, but, there is following shortcoming in this invention: 1, have higher selective to non-cigarette material, some are not easily pulled an oar and can not apply in the method at the non-cigarette material of the volatile foaming of enrichment process; 2, non-cigarette material extract is in concentration process, and under long-time high temperature (60-80 DEG C), fragrance matter can change, and changes its original style and features; 3, non-cigarette material is after existing method process, and larger change occurs the physical arrangement of plant itself, is unfavorable for the maintenance of style and features.
Application number is the patent of invention of 2014108393456, after orange skin being made the powder of suitable particulate, in coating process, add orange skin powder to paper substrate, improve the properties of reconstituted tobacco, be applied to more scientific for the active ingredient of orange skin efficiently in the preparation of reconstituted tobacco.But there is following drawback in this invention: 1, orange skin powder adds in paper substrate in the process of coating, be only applicable to the interpolation of a small amount of orange skin powder, because, if the amount of orange skin powder is more, be attached on paper substrate through coating, when after coating fluid drying, orange skin powder is then easy to split away off from paper substrate, falls slag serious; 2, orange skin powder is attached on paper substrate through coating, because orange skin powder and coating fluid can not ensure to mix, then there will be the phenomenon that orange skin powder crawling on paper substrate is even, affects the quality stability of product; 3, this invention is only applicable in reconstituted tobacco, add orange skin powder, can not be applicable to other non-cigarette material, so, the method scope of application critical constraints of this invention.
In a word, in reconstituted tobacco, add the powder of non-cigarette material, original style and features of non-cigarette material can be kept, but there is the defect easily falling slag in the product produced, if use adhesive to be fixed non-cigarette material, the suction taste of use on thin slice of adhesive produces certain impact; Meanwhile, the non-cigarette material that Same Way is suitable for is single, has larger limitation.
Summary of the invention
The present invention, in order to solve the technical problem existed in prior art, provides a kind of preparation method and application of functional form reconstituted tobacco.
To achieve these goals, the technical solution used in the present invention is as follows:
A preparation method for functional form reconstituted tobacco, comprises the steps:
1) tobacco leaf dead meal is obtained offal extract and residue through immersion extraction, Separation of Solid and Liquid;
2) offal is obtained stalk extract and stalk slag after soaking extraction, being separated;
3) stalk slag is obtained stalk slag silk through fiber uncoiling machine solution fibre;
4) by residue and the mixing of stalk slag silk, add wood pulp cellulose, make slurry;
5) non-cigarette material pulverized, screen, the non-cigarette material after screening is joined in slurry and mixes, base in blocks that slurry is manufactured paper with pulp; Maybe the non-cigarette material after screening is added in slurry in process manufactured paper with pulp by slurry;
6) obtain obstructing concentrate by concentrated for stalk extract, obtain offal concentrate by concentrated for offal extract;
7) stalk concentrate, offal concentrate, spices are allocated to obtain coating fluid;
8) by coating solution on substrate, drying, section make reconstituted tobacoo.
Join in slurry after being pulverized by non-cigarette material and mix, base in blocks of then being manufactured paper with pulp by slurry, can be evenly distributed on non-cigarette material powder in sheet base, increase the active force between non-cigarette material powder and other materials, effectively reduce slag rate.Non-cigarette material does not need, through the immersion extraction process in early stage, can keep original physiological structure and style and features preferably, go for various non-cigarette material.Meanwhile, owing to being directly distributed in by powder in sheet base, the material that those are not easy to be extracted can be retained, make style more natural.
Preferably, step 1) in, the mass ratio of tobacco leaf dead meal and soak is 1:6-1:12.
Preferably, described soak is water, and the temperature of soaking extraction is 60-90 DEG C, and the time of soaking extraction is 20-50min.
Preferably, step 2) in, the soak that offal soaks extraction is water, and the time of soaking extraction is 20-50min, and the temperature of soaking extraction is 60-90 DEG C.
Preferably, step 4) in, the mass fraction that the wood pulp cellulose added accounts for mixture entirety is 5%-15%.Wood pulp cellulose plays increases sheet base wet strength, improves the tensile index of sheet base, tear index, air permeability, absorbability.
Preferably, step 5) in, the granularity of non-cigarette material after pulverizing, screening is 80-100 order.
When the granularity of non-cigarette material powder is 80-100 order, non-cigarette material powder can mix with slurries, and after base in blocks of manufacturing paper with pulp, combine closely between non-cigarette material powder and other materials of paper substrate, effectively reduce slag rate, and make non-cigarette material be uniformly distributed in sheet base, effectively improve the quality stability of product.
Preferably, step 5) in, non-cigarette material powder is 10%-60% at the mass percent of obtained reconstituted tobacoo.
Preferably, step 6) and step 7) in the concentration of concentrate be 35%-45%.
Preferably, step 7) in, the absolute dry mass of stalk concentrate and offal concentrate is than being 2:8-6:4.
Preferably, described non-cigarette material is the non-cigarette material of the non-cigarette material of wooden class and plant flowers, leaf class.
Preferred further, the non-cigarette material of described wooden class is agalloch eaglewood or Radix Glycyrrhizae, and plant flowers, leaf class material are mugwort leaf or chrysanthemum.
Preferably, step 8) in, the spreading rate of coating fluid is 30%-45%.
Reconstituted tobacco prepared by the preparation method of above-mentioned functions type reconstituted tobacco.
The preparation method of above-mentioned functions type reconstituted tobacco is preparing the application in reconstituted tobacco.
Beneficial effect of the present invention is:
1, the present invention adds in slurry after non-cigarette material can being pulverized, then manufactured paper with pulp by slurry, the method can not carry out high-temperature process to non-cigarette material, and applicable raw materials kind is extensive, the characteristic perfume of non-cigarette material can be kept to greatest extent, improve the quality of reconstituted tobacoo;
2, non-cigarette material is contrasted and tobacco material jointly extracts, concentrates, the process of slurrying, solve non-tobacco raw-material component concentration process volatilize bring feature perfume change problem, solve a part of non-cigarette material extract simultaneously and cannot concentrate thus cause it can not be applied to the problem of reconstituted tobacoo product;
3, non-cigarette material powder adds in slurries, and the granularity controlling non-cigarette material powder is at 80-100 order, makes non-cigarette material mix in the slurry, adds the active force between non-cigarette material powder and slurry, efficiently solve slag rate high, non-cigarette material powder scatters uneven problem.
Accompanying drawing explanation
Fig. 1 is process chart of the present invention.
Detailed description of the invention
Below in conjunction with drawings and Examples, the invention will be further described.
Embodiment 1
As shown in Figure 1, a kind of preparation method of functional form reconstituted tobacco, comprises the steps:
1) tobacco leaf dead meal is added clear water by the amount that solid-to-liquid ratio is 1:8, the temperature of soaking extraction is 85 DEG C, and the time of soaking extraction is 30min, to obtaining mixing offal extract and residue after compound Separation of Solid and Liquid;
2) offal is added clear water by the amount that solid-to-liquid ratio is 1:8, the temperature of soaking extraction is 85 DEG C, and the time of soaking extraction is 30min, to obtaining stem extracting solution and stalk slag after compound Separation of Solid and Liquid;
3) stalk slag is obtained stalk slag silk through fiber uncoiling machine solution fibre;
4) by step 1) in residue and step 3) in stalk slag silk mixing after, add the wood pulp cellulose of mass fraction 10%, mixture is carried out defibrination, the beating degree of slurry is 28 ° of SR, and concentration is 3%;
5) mugwort leaf is pulverized, screening, powder size is 80 orders, and the mugwort leaf powder after screening is joined step 4 according to slurry absolute dry mass 40%) in mix in the slurry that obtains, base in blocks that slurry is manufactured paper with pulp; Maybe the mugwort leaf powder after screening is added in slurry in process manufactured paper with pulp by slurry;
6) by step 1) in the offal extract that obtains through filtration, purification, offal extract after purification is through evaporation and concentration, concentrate concentration after concentrated is 40%, by step 2) in stalk liquid carry out filtration, purification, stalk liquid after purification is through evaporation and concentration, and the concentrate concentration after concentrated is 40%; Offal concentrate and stalk concentrate are mixed than for 6:4 according to absolute dry mass, adding spices is deployed into coating fluid;
7) by coating solution to step 5) on the sheet base that obtains, drying, section make reconstituted tobacoo.
To smoke panel test experiment
By the reconstituted tobacco chopping of preparation, ratio according to 20% adds in cigarette composition puts into climatic chamber inner equilibrium 48h, make cigarette, as sample sets, and will the cigarette of reconstituted tobacco do not added as a control group, by sample sets and control group random number, the group of smokeing panel test be made up of the member of smoking possessing qualification of smokeing panel test carries out sensory evaluating smoking.
Effect assessment
Smoking result shows: compared with control group, and the cigarette adding the reconstituted tobacco prepared with the inventive method has obvious mugwort leaf odor characteristic, comfortable taste, natural fusion fragrant with cigarette.
Mugwort leaf together can not extract with tobacco leaf dead meal, concentrated.Reason is that mixed extract foaming boiling is severe in concentration process, and foam is pumped with vacuum, and mixed extract can not concentrate.
Fall the experiment of slag rate
By the reconstituted tobacco of preparation, put into climatic chamber inner equilibrium 48h, as sample sets, take 20g sample, carry out vibrations 10min shaking in sieve, be separated with sheet by powder, take the quality that residue is large stretch of, slag rate is fallen in calculating.
Fall slag rate=(M
just-M
surplus)/M
just
M
justfor the quality of initial sample, M
surplusfor remaining the quality of large stretch of sample.
The slag rate of falling of sample sets is 1 ‰.
Embodiment 2
As shown in Figure 1, a kind of preparation method of functional form reconstituted tobacco, comprises the steps:
1) tobacco leaf dead meal is added clear water by the amount that solid-to-liquid ratio is 1:6, the temperature of soaking extraction is 65 DEG C, and the time of soaking extraction is 50min, to obtaining mixing offal extract and residue after compound Separation of Solid and Liquid;
2) offal is added clear water by the amount that solid-to-liquid ratio is 1:8, the temperature of soaking extraction is 90 DEG C, and the time of soaking extraction is 20min, to obtaining stem extracting solution and stalk slag after compound Separation of Solid and Liquid;
3) stalk slag is obtained stalk slag silk through fiber uncoiling machine solution fibre;
4) by step 1) in residue and step 3) in stalk slag silk mixing after, add the wood pulp cellulose of mass fraction 15%, mixture is carried out defibrination, the beating degree of slurry is 28 ° of SR, and concentration is 3%;
5) agalloch eaglewood is pulverized, screening, powder size is 80 orders, and the agalloch eaglewood powder after screening is joined step 4 according to slurry absolute dry mass 60%) in mix in the slurry that obtains, base in blocks that slurry is manufactured paper with pulp; Maybe the agalloch eaglewood powder after screening is added in slurry in process manufactured paper with pulp by slurry;
6) by step 1) in the offal extract that obtains through filtration, purification, offal extract after purification is through evaporation and concentration, concentrate concentration after concentrated is 45%, by step 2) in stalk liquid carry out filtration, purification, stalk liquid after purification is through evaporation and concentration, and the concentrate concentration after concentrated is 35%; Offal concentrate and stalk concentrate are mixed than for 2:8 according to absolute dry mass, adding spices is deployed into coating fluid;
7) by coating solution to step 5) on the sheet base that obtains, drying, section make reconstituted tobacoo.
To smoke panel test experiment
By the reconstituted tobacco chopping of preparation, ratio according to 10% adds in cigarette composition puts into climatic chamber inner equilibrium 48h, make cigarette, as sample sets, and will the cigarette of reconstituted tobacco do not added as a control group, by sample sets and control group random number, the group of smokeing panel test be made up of the member of smoking possessing qualification of smokeing panel test carries out sensory evaluating smoking.
Agalloch eaglewood together can not extract with tobacco leaf dead meal, concentrated.Reason is mainly oil-soluble at the flavor matter of agalloch eaglewood, and Extraction medium is water, can not effectively effectively extract the aroma component in agalloch eaglewood.
Effect assessment
Smoking result shows: compared with control group, and the cigarette adding the reconstituted tobacco prepared with the inventive method has obvious agalloch eaglewood odor characteristic, comfortable taste, natural fusion fragrant with cigarette.
Carry out the test of slag rate by identical method, the slag rate of falling of sample sets is 1.2 ‰.
Embodiment 3
As shown in Figure 1, a kind of preparation method of functional form reconstituted tobacco, comprises the steps:
1) tobacco leaf dead meal is added clear water by the amount that solid-to-liquid ratio is 1:12, the temperature of soaking extraction is 75 DEG C, and the time of soaking extraction is 50min, to obtaining mixing offal extract and residue after compound Separation of Solid and Liquid;
2) offal is added clear water by the amount that solid-to-liquid ratio is 1:10, the temperature of soaking extraction is 60 DEG C, and the time of soaking extraction is 50min, to obtaining stem extracting solution and stalk slag after compound Separation of Solid and Liquid;
3) stalk slag is obtained stalk slag silk through fiber uncoiling machine solution fibre;
4) by step 1) in residue and step 3) in stalk slag silk mixing after, add the wood pulp cellulose of mass fraction 5%, mixture is carried out defibrination, the beating degree of slurry is 28 ° of SR, and concentration is 3%;
5) chrysanthemum and Radix Glycyrrhizae are pulverized respectively, screened, powder size is 80 orders, be that 7:3 mixes by the chrysanthemum powder after screening and Radix Glycyrrhizae powder according to mass ratio, then mixed-powder is joined step 4 according to slurry absolute dry mass 30%) in mix in the slurry that obtains, base in blocks that slurry is manufactured paper with pulp; Or mixed-powder is added in slurry in process manufactured paper with pulp by slurry;
6) by step 1) in the offal extract that obtains through filtration, purification, offal extract after purification is through evaporation and concentration, concentrate concentration after concentrated is 45%, by step 2) in stalk liquid carry out filtration, purification, stalk liquid after purification is through evaporation and concentration, and the concentrate concentration after concentrated is 35%; Offal concentrate and stalk concentrate are mixed than for 1:1 according to absolute dry mass, adding spices is deployed into coating fluid;
7) by coating solution to step 5) on the sheet base that obtains, drying, section make reconstituted tobacoo.
To smoke panel test experiment
By the reconstituted tobacco chopping of preparation, put into climatic chamber inner equilibrium 24h, make cigarette, as sample sets, and so that chrysanthemum powder, Radix Glycyrrhizae powder are together extracted the obtained cigarette of the reconstituted tobacco for preparing as a control group through soaking with tobacco leaf dead meal, by sample sets and control group random number, the group of smokeing panel test be made up of the member of smoking possessing qualification of smokeing panel test carries out sensory evaluating smoking.Effect assessment
Smoking result shows: compared with control group, the cigarette adding the reconstituted tobacco prepared with the inventive method has obvious Scent of Chrysanthemum feature, comfortable taste, natural fusion fragrant with cigarette, control sample Scent of Chrysanthemum feature is not obvious, and Scent of Chrysanthemum comparatively sample sets is slightly different.
Carry out the test of slag rate by identical method, the slag rate of falling of sample sets is 0.9 ‰.
Visible, method of the present invention goes for multiple non-cigarette material, has a wide range of applications, and can not affect the local flavor of non-cigarette material, and when efficiently solving non-cigarette material powder interpolation in prior art, the reconstituted tobacco caused falls the high drawback of slag rate.
By reference to the accompanying drawings the specific embodiment of the present invention is described although above-mentioned; but the restriction not to invention protection domain; one of ordinary skill in the art should be understood that; on the basis of technical scheme of the present invention, those skilled in the art do not need to pay various amendment or distortion that creative work can make still in protection scope of the present invention.
Claims (10)
1. a preparation method for functional form reconstituted tobacco, is characterized in that: comprise the steps:
1) tobacco leaf dead meal is obtained offal extract and residue through immersion extraction, Separation of Solid and Liquid;
2) offal is obtained stalk extract and stalk slag after soaking extraction, being separated;
3) stalk slag is obtained stalk slag silk through fiber uncoiling machine solution fibre;
4) by residue and the mixing of stalk slag silk, add wood pulp cellulose, make slurry;
5) non-cigarette material pulverized, screen, the non-cigarette material after screening is joined in slurry and mixes, base in blocks that slurry is manufactured paper with pulp; Maybe the non-cigarette material after screening is added in slurry in process manufactured paper with pulp by slurry;
6) obtain obstructing concentrate by concentrated for stalk extract, obtain offal concentrate by concentrated for offal extract;
7) stalk concentrate, offal concentrate, spices are allocated to obtain coating fluid;
8) by coating solution on substrate, drying, section make reconstituted tobacoo.
2. preparation method according to claim 1, is characterized in that: step 1) in, the mass ratio of tobacco leaf dead meal and soak is 1:6-1:12;
Or soak is water, the temperature of soaking extraction is 60-90 DEG C, and the time of soaking extraction is 20-50min.
3. preparation method according to claim 1, is characterized in that: step 2) in, the soak that offal soaks extraction is water, and the time of soaking extraction is 20-50min, and the temperature of soaking extraction is 60-90 DEG C.
4. preparation method according to claim 1, is characterized in that: step 4) in, the mass fraction that the wood pulp cellulose added accounts for mixture entirety is 5%-15%.
5. preparation method according to claim 1, is characterized in that: step 5) in, the granularity of non-cigarette material after pulverizing, screening is 80-100 order;
Or non-cigarette material powder mass percent is in the slurry 10%-60%.
6. preparation method according to claim 1, is characterized in that: step 6) and step 7) in the concentration of concentrate be 35%-45%, the absolute dry mass of stalk concentrate and offal concentrate is than being 2:8-6:4.
7. preparation method according to claim 1, is characterized in that: described non-cigarette material is the non-cigarette material of the non-cigarette material of wooden class and plant flowers, leaf class;
Preferably, the non-cigarette material of described wooden class is agalloch eaglewood or Radix Glycyrrhizae, and plant flowers, leaf class material are mugwort leaf or chrysanthemum.
8. preparation method according to claim 1, is characterized in that: step 8) in, the spreading rate of coating fluid is 30%-45%.
9. the reconstituted tobacco prepared of the preparation method of the arbitrary described functional form reconstituted tobacco of claim 1-8.
10. the preparation method of the arbitrary described functional form reconstituted tobacco of claim 1-8 is preparing the application in reconstituted tobacco.
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