CN105168038A - Aurea helianthus flower mud facial mask and preparation method therefor - Google Patents
Aurea helianthus flower mud facial mask and preparation method therefor Download PDFInfo
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Abstract
The invention discloses an aurea helianthus flower mud facial mask and a preparation method therefor. The facial mask comprises the following raw materials, by weight, 20-30% of aurea helianthus flowers, 20-30% of luffa flowers, 5-8% of propylene glycol, 0.3-0.7% of carbomer, 1.0-1.5% of triethanolamine, 0.05-0.1% of EUXYL K300 and 0.002-0.005% of citral, the balance being luffa stem nutritious water. The preparation method for the facial mask comprises the following steps: firstly, luffa stem nutritious water is disinfected and filtered for stand-by; secondly, flowers are crushed and stirred into mud for stand-by; thirdly, carbomer is subjected to swelling in the luffa stem nutritious water; fourthly, a carbomer gel matrix is prepared; fifthly, citral is dissolved in propylene glycol, then the luffa stem nutritious water is added, and a solution I is obtained; sixthly, the solution I and the flower mud are added in the gel matrix, then EUXYL K300 is added, the mixture is stirred and mixed uniformly, and an aurea helianthus flower mud facial mask is obtained. The facial mask has whitening and moisture retention fuctions and has no side effects.
Description
Technical field
The invention belongs to a kind of plant puree facial film of cosmetic technical field, relate to a kind of Hibiscus manihot L. flower mud facial film and preparation method thereof particularly.
Background technology
Way mask sheet being spread on face comes from the external treatment of medicine, is one of conventional cosmetic skin care methods.After using facial film, skin seems clearly smooth, pure white delicacy, this is because facial film can produce affinity with skin, along with the drying gradually of facial film after coating, face temperature raises, blood circulation is accelerated, skin-tightening and tension force are strengthened, and the sebum of skin secretion and moisture reverse osmosis, in horny layer, make epidermis cell softness unfold, pore instinct is opened, and the effective ingredient in facial film infiltrates skin and is absorbed.Again because facial film tightly can be affixed with skin, when knowing facial film, in the aging cutin on skin, pore, deep layer dirt is stripped leukorrhagia, makes skin totally pure and fresh.At present, more as the facial film of facial film mud excipient using mineral on market, but have no and grow using Ramulus Luffae the facial film that water makes as preparation solvent as excipient with the serosity of Hibiscus manihot L. flower and Fructus Luffae flower.
The special product plant at mansion, Shuande is recited as in " mansion, Shuande will " of Hibiscus manihot L. once between Ming Dynasty constitution ancestor one-tenth year.1984, during National Agricultural resource investigation, confirmed as extinction plant because not finding Hibiscus manihot L. by biosphere.In August, 2003, the Chinese Academy of Agricultural Sciences's institute is Qiu Xian's Late Cambrian Hibiscus manihot L. in Hebei, and because of the biological effect that it is peculiar, at home and abroad the market such as flowers, food, medicine, health product and chemical circles causes strong repercussion rapidly.Gold Hibiscus manihot L. has another name called vegetable Furong, golden Hibisci Mutabilis, is annual herb plant, is Malvaceae, belongs to together with Abelmoschus manihot （L.） Medic.Its taste is cold, sweet, nontoxic, and the general florescence, every strain bloomed 30 ~ 60 in 7 ~ JIUYUE, and spend large as bowl, corolla is golden yellow.Flower of Hibiscus manihot L dietotherapeutic, Compendium of Material Medica records its energy heat clearing away, removing heat from blood, removing toxic substances, and itself is nontoxic.Take orally and cure mainly five types of stranguria, edema, external can be controlled soup and scald." praise and help book on Chinese herbal medicine " is recorded it and can be controlled all malignant boil.
Modern technologies are analyzed, containing flavonoid glycoside, complete protein, high polysaccharide glue, dietary fiber, trace element-selenium, zinc, multiple non-saponifiable matter etc. in Hibiscus manihot L. flower.Have experiment to prove, natural flavone content decades of times more contour than Semen Ginkgo, Semen sojae atricolor in flower of Hibiscus manihot L, it has the effects such as heat clearing away, dampness removing, antiinflammatory, removing toxic substances, analgesia; The Proteinaceous structure of the vitamin E energy stabilizing cell membrane contained by it, promote the normal development of muscle and keep the elasticity of skin, skin directly can be helped after vitamin E enters Skin Cell to the infringement of free radical resisting, ultraviolet and pollutant, prevent skin from following the string until aging because of some chronic or stealthy injuries.Some bibliographical informations, the total flavone glucoside extract of Hibiscus manihot L. has obvious inhibitory action to tyrosinase activity, and tryrosinase is a kind of main enzyme in melanin production process, when its activity inhibited, melanocyte produces melanic ability will correspondingly be reduced, and namely reaches the effect of whitening.
In sum, be the facial film that primary raw material makes with Hibiscus manihot L. flower, there is skin-care effects such as maintaining elasticity of skin, help skin antioxidation, defying age and promotion whitening.
Luffa cucurbitaceous plant, its sweet in the mouth is put down, and Flos Luffae contains several amino acids, has heat-clearing and toxic substances removing, antiinflammatory pathogenic fire purging, only throat pain, disappears and be tired of effects such as quenching the thirst.Containing β-paddy Zi alcohol, oleanolic acid and Luffa saponin in its male flower.Oleanolic acid has whitening function, and Luffa saponin has life lengthening, the acquisition promoting memory, consolidation and reproduction effect, can Glycerin, treatment scald etc.β-paddy Zi alcohol, except reducing the total cholesterol level in blood, also has the effects such as antiinflammatory, Tumor suppression, suppression cyclomastopathy and immunity moderation system.
In sum, there is the antiinflammatory of help skin, the fat anti-acne that disappears with the facial film that Flos Luffae flower is primary raw material making, suppress the effect such as cutaneous tumor and whitening.
Ramulus Luffae is grown water and is had another name called loofah bleeding sap, sky Luo Shui etc., contain nature moisturizing factor in Ramulus Luffae taste water, let out root acid, catalase, superoxide dismutase, multiple-microorganism and trace element, moisture of skin can be supplemented, remove the activity etc. of unnecessary free radical, inhibiting bacteria and diminishing inflammation, restraint of tyrosinase, help to moisturize the skin, whitening and antioxidation.Ramulus Luffae grows the moisture that water contains 98.7 ~ 99.3%.Result of study shows, Ramulus Luffae grows glassware for drinking water the excellent skin-care effect such as moisturizing, whitening.In addition, it possesses enough moisture, can be used as the solvent of preparation facial film.
General Chinese herbal medicine facial film mostly is powder face pack, namely Chinese herbal medicine is pulverized and sieved subpackage, faces used time use water furnishing pulpous state and be coated on face.Such facial film usually easily blocks pore, not easily completely clean.Separately, in Chinese herbal medicine, some effective ingredient is not because dissolving dispersion well without emulsifying, therefore can not play its due skin care effect.
Summary of the invention
Object of the present invention is exactly the deficiency that will overcome the existence of above-mentioned prior art, provides a kind of Hibiscus manihot L. flower mud facial film and preparation method thereof, has skin-care effects such as maintaining elasticity of skin, help skin antioxidation, defying age and promotion whitening.
For achieving the above object, technical scheme of the present invention is achieved in that a kind of Hibiscus manihot L. flower mud facial film, and it is prepared from primarily of the raw material of following percetage by weight, and wherein the percetage by weight of each component raw material is as follows:
Hibiscus manihot L. flower: 20 ~ 30%, Fructus Luffae flower: 20 ~ 30%, propylene glycol: 5 ~ 8%, carbomer: 0.3 ~ 0.7%, triethanolamine: 1.0 ~ 1.5%, EUXYLK300:0.05 ~ 0.1%, citral: 0.002 ~ 0.005%, surplus is that Ramulus Luffae grows water.
Preferably, described facial film is prepared from primarily of the raw material of following percetage by weight, and wherein the percetage by weight of each component raw material is as follows:
Hibiscus manihot L. flower: 22 ~ 25%, Fructus Luffae flower: 22 ~ 25%, propylene glycol: 5 ~ 8%, carbomer: 0.3 ~ 0.5%, triethanolamine: 1.0 ~ 1.5%, EUXYLK300:0.05 ~ 0.1%, citral: 0.002 ~ 0.005%, surplus is that Ramulus Luffae grows water.
As more preferably scheme, described facial film is prepared from primarily of the raw material of following percetage by weight, and wherein the percetage by weight of each component raw material is as follows:
Hibiscus manihot L. flower: 22.5%, Fructus Luffae flower: 22.5%, propylene glycol: 5%, carbomer: 0.5%, triethanolamine: 1.5%, EUXYLK300:0.05%, citral: 0.004%, surplus is that Ramulus Luffae grows water.
Preferably, described carbomer is carbomer U20.Carbomer U20 is the cross-linked copolymer of acrylate and alkyl acrylate, there is thickening, suspension, stable emulsion system, function such as regulation and control water and active substance release etc., it can increase the denseness of flower serosity, make facial film demonstrate desirable figuration effect, be unlikely to when being coated on face to drip, the phenomenon such as flowing; The effective ingredient rapid dispersion that flower of Hibiscus manihot L, Flos Luffae are grown in water around Ramulus Luffae can be suspended in gel-type vehicle by it, is uniformly distributed in face everywhere, thus produces slim and graceful sprawling sense and clearly feel, and effectively improves the organoleptic properties of facial film.
The preparation method of above-mentioned Hibiscus manihot L. flower mud facial film, comprises the steps:
1) Ramulus Luffae is grown water by after ultraviolet ray sterilizer sterilization and metre filter, be placed in disinfecting container stand-by;
2) Hibiscus manihot L. flower is become muddy with Fructus Luffae flower crushing, stirring, stand-by;
3) by carbomer step 1) process after Ramulus Luffae grow water fully swelling, hold over night;
4) triethanolamine is joined step 3) in the swelling carbomer solution that obtains, stir and obtain clear gel substrate;
5), after citral being dissolved in propylene glycol, step 1 is added) Ramulus Luffae after process grows in water, obtains solution I;
6) by step 5) obtained solution I and step 2) obtained flower serosity joins step 4) in obtained gel-type vehicle, then EUXYLK300 is added under constantly stirring, be uniformly mixed and both obtain Hibiscus manihot L. flower mud facial film.
Preferably, described step 1) in the filter element precision of filter that uses be 0.2 μm.
Preferably, described step 3) in Ramulus Luffae used grow water and be heated to 50 ~ 60 DEG C in advance
The present invention selects triethanolamine to make carbomer resin molecule obtain significant expansion stretching, extension, thus increases the denseness of system, makes facial film keep faintly acid pH=6.3 ~ 6.8 simultaneously, ensures the skin effect of facial film.
The present invention selects propylene glycol, and propylene glycol is efficient moisture-retention agent, emulsifying agent, stabilizing agent and dermal osmosis accelerator, during it can make the multiple volatile oil in Hibiscus manihot L. flower and Fructus Luffae flower better be soluble in the aqueous phase; It can delay some compositions hydrolysis in flower and Ramulus Luffae taste water, increases its stability; Propylene glycol also has moisture-keeping function, can make facial film in long term storage, keep not drying shrinkage, have good infiltration function, and the active component can guided in flower and Ramulus Luffae taste water infiltrates among skin in a larger amount, strengthens skin-protecting function.
The citral system fruit type edible essence that the present invention selects, can make product of the present invention have the sensory effects making us clearly being suitable for.
The composite component antiseptic of the EUXYLK300 system that the present invention selects.EUXYLK300 is formed by several composite in phenoxyethanol, methyl hydroxybenzoate, butyl hydroxybenzoate, ethyl hydroxybenzoate, propyl hydroxybenzoate, oxybenzene isobutyl ester, commercially.Not release formaldehyde, has broad-spectrum sterilization effect to antibacterial, yeast and mycete, and its applicable PH scope is large, gentle non-stimulated, is applicable to sun-proof, is usually used in the special cosmetics such as eye and child care products.
It is all that Wuhan Lang Bao Science and Technology Ltd. produces in Hong Beiyuan planting base, Caidian District, Wuhan City that the flower of Hibiscus manihot L used in the present invention, Flos Luffae and Ramulus Luffae grow water.
The present invention has the following advantages:
(1) the present invention adopts Hibiscus manihot L. flower, Fructus Luffae flower and Ramulus Luffae to grow water as main function raw material, the natural organic characteristic that Hibiscus manihot L. flower, Fructus Luffae flower and Ramulus Luffae grow water etc. can be given prominence to, give full play to the skin-protecting functions such as its moisturizing, whitening, antiinflammatory, antiallergic, promotion cutaneous circulation and aging resistance;
(2) the present invention is primarily of plant tissue composition itself, but has used the modern manufacturing technologies such as thickening, suspension, emulsifying because of it, and the effective ingredient that Hibiscus manihot L. flower, Fructus Luffae flower and Ramulus Luffae grow water etc. can be evenly dispersed in system; Under the guiding of transdermal enhancer, skin can be infiltered in time and play skin care effect, be stranded in pore without dust granules again;
(3) raw material that the present invention is used is all nontoxic, has no side effect, and safe and feasible meets cosmetics manufacture requirements.
Accompanying drawing explanation
Fig. 1: Hibiscus manihot L. flower mud facial film performance of keeping humidity test pattern;
Fig. 2: the active comparison diagram of Hibiscus manihot L. flower mud facial film restraint of tyrosinase.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1
1) take Hibiscus manihot L. flower: 22.5%, Fructus Luffae flower: 22.5%, propylene glycol: 5%, carbomer: 0.5%, triethanolamine: 1.5%, EUXYLK300:0.05%, citral: 0.002%, surplus is that Ramulus Luffae grows water;
2) Ramulus Luffae is grown water to be sterilized by ultraviolet ray sterilizer with 1200mL/h speed, then be the metre filter of 0.2 μm by filter element precision, be placed in disinfecting container stand-by;
3) pluck fresh Hibiscus manihot L. flower and Fructus Luffae flower, clean and drain, removing stem branch, crushing, stirring becomes muddy;
4) Ramulus Luffae after sterilization, filtration is grown water and be heated to 55 DEG C in advance, carbomer Ramulus Luffae is grown in water fully swelling, hold over night;
5) triethanolamine is joined in swelling carbomer solution, stir and obtain clear gel substrate;
6) citral is dissolved in propylene glycol, join Ramulus Luffae and grow in water, obtain solution I;
7) solution I and flower mud are slowly joined in gel-type vehicle, then add EUXYLK300 under constantly stirring, be uniformly mixed and both obtain Hibiscus manihot L. flower mud facial film.
Embodiment 2
1) take Hibiscus manihot L. flower: 25%, Fructus Luffae flower: 25%, propylene glycol: 8%, carbomer: 0.7%, triethanolamine: 1.5%, EUXYLK300:0.08%, citral: 0.004%, surplus is that Ramulus Luffae grows water;
2) Ramulus Luffae is grown water to be sterilized by ultraviolet ray sterilizer with 1200mL/h speed, then be the metre filter of 0.2 μm by filter element precision, be placed in disinfecting container stand-by;
3) pluck fresh Hibiscus manihot L. flower and Fructus Luffae flower, clean and drain, removing stem branch, crushing, stirring becomes muddy;
4) Ramulus Luffae after sterilization, filtration is grown water and be heated to 55 DEG C in advance, carbomer Ramulus Luffae is grown in water fully swelling, hold over night;
5) triethanolamine is joined in swelling carbomer solution, stir and obtain clear gel substrate;
6) citral is dissolved in propylene glycol, join Ramulus Luffae and grow in water, obtain solution I;
7) solution I and flower mud are slowly joined in gel-type vehicle, then add EUXYLK300 under constantly stirring, be uniformly mixed and both obtain Hibiscus manihot L. flower mud facial film.
Embodiment 3
1) take Hibiscus manihot L. flower: 20%, Fructus Luffae flower: 20%, propylene glycol: 6%, carbomer: 0.3%, triethanolamine: 1.0%, EUXYLK300:0.1%, citral: 0.005%, surplus is that Ramulus Luffae grows water;
2) Ramulus Luffae is grown water to be sterilized by ultraviolet ray sterilizer with 1200mL/h speed, then be the metre filter of 0.2 μm by filter element precision, be placed in disinfecting container stand-by;
3) pluck fresh Hibiscus manihot L. flower and Fructus Luffae flower, clean and drain, removing stem branch, crushing, stirring becomes muddy;
4) Ramulus Luffae after sterilization, filtration is grown water and be heated to 50 DEG C in advance, carbomer Ramulus Luffae is grown in water fully swelling, hold over night;
5) triethanolamine is joined in swelling carbomer solution, stir and obtain clear gel substrate;
6) citral is dissolved in propylene glycol, join Ramulus Luffae and grow in water, obtain solution I;
7) solution I and flower mud are slowly joined in gel-type vehicle, then add EUXYLK300 under constantly stirring, be uniformly mixed and both obtain Hibiscus manihot L. flower mud facial film.
Embodiment 4
1) take Hibiscus manihot L. flower: 30%, Fructus Luffae flower: 30%, propylene glycol: 8%, carbomer: 0.5%, triethanolamine: 1.3%, EUXYLK300:0.08%, citral: 0.005%, surplus is that Ramulus Luffae grows water;
2) Ramulus Luffae is grown water to be sterilized by ultraviolet ray sterilizer with 1200mL/h speed, then be the metre filter of 0.2 μm by filter element precision, be placed in disinfecting container stand-by;
3) pluck fresh Hibiscus manihot L. flower and Fructus Luffae flower, clean and drain, removing stem branch, crushing, stirring becomes muddy;
4) Ramulus Luffae after sterilization, filtration is grown water and be heated to 60 DEG C in advance, carbomer Ramulus Luffae is grown in water fully swelling, hold over night;
5) triethanolamine is joined in swelling carbomer solution, stir and obtain clear gel substrate;
6) citral is dissolved in propylene glycol, join Ramulus Luffae and grow in water, obtain solution I;
7) solution I and flower mud are slowly joined in gel-type vehicle, then add EUXYLK300 under constantly stirring, be uniformly mixed and both obtain Hibiscus manihot L. flower mud facial film.
1, cutaneous safety test:
According to " safety evaluation of cosmetics progresses and methods " (GB7919-87) relevant regulations, skin wound repair test is carried out to the present invention.
The healthy men and women experimenter 70 of Stochastic choice, experimenter to ethanol and medical proof fabric without allergies.
To inside the left forearm of volunteer from ancon 4cm place first with clear water clean wipe dry, then get facial film of the present invention divide on skin 2.5 × 2.5cm square, thickness is about 0.5cm.Then apply gently with gauze piece, then cover with one deck oilpaper, paste with medical proof fabric fixing.Open gauze after 1h, observe change of skin, analyze according to table 1 skin wound repair evaluation criterion.
Table 1 skin wound repair evaluation criterion
Table 2 Hibiscus manihot L. flower mud facial film skin wound repair test result
Above-mentioned result of the test shows, in the experimenter, only have 3 people visible erythema reluctantly, the visible erythema of 1 people, positive rate is only 5.7%; In the experimenter, only have 2 people visible edema reluctantly, positive rate is only 2.9%, and the safety of the present invention to skin is excellent.
2, the mensuration of performance of keeping humidity
Keep the moisture content of skin, can skin elasticity be increased, make skin eubolism, reduce the generation of wrinkle and mottle.Under normal conditions, the water content normal value at people's different skin position is as follows:
| Skin part | Cheek portion | Forehead | Eyelid | The palm of the hand | The back of the hand | Wrist |
| Water content | 30～50％ | 30～50％ | 40～50％ | 40～55％ | 30～50％ | 35～40％ |
The digital skin water tester (SkinDetectorSD) that this experiment adopts Ai Beimei Science and Technology Ltd. of Shenzhen to produce specifies skin part to test to experimenter, and SD system adopts the high accuracy skin moisture tester of Bioelectrical impedance analysis technology.By test probe flicking after the tested person skin part several seconds, namely its LCD display demonstrates the instant water content percent of skin.
Select moisturizing test volunteer 60, the age in 20-45 year between, be divided into three groups at random.Difference, under the environment of room temperature about 25 DEG C, relative humidity 50%, first with inside clean water cleaning left finesse, is then treated that test agent evenly divides into 3 × 3cm square by experimenter respectively.First group is applied normal saline gauze at appointment skin part; Second group of substrate facial film of specifying skin part application not grow water containing flower mud and Ramulus Luffae; 3rd group at appointment skin part application facial film of the present invention.After 30min, remove each determinand.In 0,30,60,90, the period such as 120min tests the cutaneous application place of three groups of experimenters respectively with SD, obtain skin moisture content, each group of digital average value of surveying be analyzed.Test result is shown in Fig. 1.
Test result shows, and normal saline is without moisture-keeping function, and the substrate facial film not containing flower mud and rattan taste water has certain moisture-keeping function, but moisture-keeping function is not lasting; Facial film of the present invention has significant moisturizing usefulness, and after 120min skin moisture content still within ideal value.
3, whitening function test
The primary raw material manufacturing the black pigment of skin is tyrosine, and tryrosinase is the major rate-limiting enzyme that tyrosine changes melanocyte into, and when tyrosinase activity is suppressed, melanocyte produces Melanogenic ability can corresponding decline.In other words, restraint of tyrosinase activity can play the effect of skin whitening.
As follows to the whitening function testing procedure of facial film of the present invention:
Prepare tryrosinase liquid: get fresh intact Rhizoma Solani tuber osi clean after in 4 DEG C of pre-cooling 4 hours, peeling, be cut into about 1.3cm
2fourth shape, in-20 DEG C of freeze overnight, phosphate buffer is added in the ratio of 1:1 (W/V) after taking out, homogenate is made with tissue mashing machine, by 3 layers of filtered through gauze, filtrate is again in the centrifugal 10min of 4000r/min, and supernatant is the tryrosinase crude enzyme liquid of gained, in 4 DEG C of preservations, be finished in 2 hours.
Test solution is treated in preparation: accurately take facial film 40mg of the present invention, fully stir, centrifugal filtration, get supernatant with 100ml deionized water, obtain 0.4mg/ml and treat test solution.
Prepare positive control solution: accurately take ascorbic acid (Vc) 40mg, dissolve with sodium phosphate buffer (PH6.8,0.1mol/L), be mixed with the solution of 0.4mg/ml.
Prepare TYR reagent: accurately take TYR 90.595mg, add several concentrated hydrochloric acid, after slight fever is dissolved completely, add water number 10ml, be neutralized to neutrality with sodium hydroxide, be settled to 100ml, make TYR solution concentration be 5mol/L.
This experiment take deionized water as negative control, with 0.4mg/mlVc solution for positive control, total reaction volume is 2ml, and wherein tryrosinase crude extract 0.5ml, 0.1mol/L phosphate buffer (PH6.8) 0.5ml, adds deionized water 1.0ml in blank tube; Treat to treat test solution 0.5ml in test solution pipe.TYR solution 0.5ml; Vc solution 0.5ml, TYR solution 0.5ml in positive control pipe.
Concrete test process: first by TYR solution and phosphate buffer mixing, 30 DEG C of temperature bath 10min, then add liquid to be measured and tryrosinase crude extract.Continue the bath of difference temperature 30min, 60min, 120min in 30 DEG C of water-baths.Be then reference with blank tube, measure the absorbance of each tube reaction liquid under spectrophotometer 475mm wavelength.Using negative control group as reference, get the mean of three parallel sample, calculate respectively with following formula and treat that test solution and Vc solution are to the suppression ratio of tyrosinase activity, and mapping is analyzed.
Inhibitory activity against tyrosinase %=[(A-B)/A] × 100
Wherein: A: the absorbance of negative control group, B: the absorbance of experimental group.Suppression ratio is high show the inhibition strength of tyrosinase activity high.
Restraint of tyrosinase activity experiment the results are shown in Figure 2.This experimental result shows, Vc extends in time, and the function of its restraint of tyrosinase activity lowers gradually, and the function of facial film restraint of tyrosinase activity of the present invention first increases, and then reduces gradually.Generally speaking, Vc and facial film of the present invention all have the effect of restraint of tyrosinase activity.
4, quality control standards (QCS)
(1) with reference to the content measuring total flavone glucoside in facial film of the present invention in the Pharmacopoeia of the People's Republic of China (version in 2012) I about total flavone glucoside content assaying method, measurement result is labelled amount ± 5%.
(2) physical behavior inspection: product colour of the present invention is yellow green, translucent plant pureed, homogeneous, has the fragrant of slight Hibiscus manihot L. and Fructus Luffae mixing.Spreading property is good, is coated on skin non-stimulated; Removing in 15 ~ 20 minutes, skin seems that water is tender, fine and smooth, smooth.
(3) health chemical testing: lead, hydrargyrum, arsenic are no more than " cosmetics health specification " required standard that Ministry of Public Health is issued.
(4) microorganism detection: the clump count such as total plate count, excrement colibacillus group, bacillus pyocyaneus, staphylococcus aureus, yeast, mycete is no more than the required standard of " the cosmetics health specification " that Ministry of Public Health is issued.
(5) toxicology test: repeatedly Skin Irritation Test, acute ocular irritation test meet national standard;
(6) packing instructions: meet country about the relevant regulations such as " cosmetics inspection rule (QB/T1684) ", " cosmetic product packaging external appearance requires (QB/T1685) " and " Metrolgy Inspection of Products in Prepackages rule (JJF1070-2000) ", the packaging material of direct contact product are accomplished nontoxic, aseptic.
Claims (7)
1. a Hibiscus manihot L. flower mud facial film, it is characterized in that: it is prepared from primarily of the raw material of following percetage by weight, wherein the percetage by weight of each component raw material is as follows:
Hibiscus manihot L. flower: 20 ~ 30%, Fructus Luffae flower: 20 ~ 30%, propylene glycol: 5 ~ 8%, carbomer: 0.3 ~ 0.7%, triethanolamine: 1.0 ~ 1.5%, EUXYLK300:0.05 ~ 0.1%, citral: 0.002 ~ 0.005%, surplus is that Ramulus Luffae grows water.
2. Hibiscus manihot L. flower mud facial film according to claim 1, it is characterized in that: it is prepared from primarily of the raw material of following percetage by weight, wherein the percetage by weight of each component raw material is as follows:
Hibiscus manihot L. flower: 22 ~ 25%, Fructus Luffae flower: 22 ~ 25%, propylene glycol: 5 ~ 8%, carbomer: 0.3 ~ 0.5%, triethanolamine: 1.0 ~ 1.5%, EUXYLK300:0.05 ~ 0.1%, citral: 0.002 ~ 0.005%, surplus is that Ramulus Luffae grows water.
3. Hibiscus manihot L. flower mud facial film according to claim 1, it is characterized in that: it is prepared from primarily of the raw material of following percetage by weight, wherein the percetage by weight of each component raw material is as follows:
Hibiscus manihot L. flower: 22.5%, Fructus Luffae flower: 22.5%, propylene glycol: 5%, carbomer: 0.5%, triethanolamine: 1.5%, EUXYLK300:0.05%, citral: 0.004%, surplus is that Ramulus Luffae grows water.
4. Hibiscus manihot L. flower mud facial film according to claim 1, is characterized in that: described carbomer is carbomer U20.
5. a preparation method for Hibiscus manihot L. flower mud facial film described in claim 1, it is characterized in that, the method comprises the steps:
1) Ramulus Luffae is grown water by after ultraviolet ray sterilizer sterilization and metre filter, be placed in disinfecting container stand-by;
2) Hibiscus manihot L. flower is become muddy with Fructus Luffae flower crushing, stirring, stand-by;
3) by carbomer step 1) process after Ramulus Luffae grow water fully swelling, hold over night;
4) triethanolamine is joined step 3) in the swelling carbomer solution that obtains, stir and obtain clear gel substrate;
5), after citral being dissolved in propylene glycol, step 1 is added) Ramulus Luffae after process grows in water, obtains solution I;
6) by step 5) obtained solution I and step 2) obtained flower serosity joins step 4) in obtained gel-type vehicle, under constantly stirring, add EUXYLK300, be uniformly mixed and both obtain Hibiscus manihot L. flower mud facial film.
6. the preparation method of Hibiscus manihot L. flower mud facial film according to claim 4, is characterized in that: described step 1) in the filter element precision of filter that uses be 0.2 μm.
7. the preparation method of Hibiscus manihot L. flower mud facial film according to claim 4, is characterized in that: described step 3) in Ramulus Luffae used grow water and be heated to 50 ~ 60 DEG C in advance.
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Cited By (9)
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| CN106063925A (en) * | 2016-07-22 | 2016-11-02 | 许备占 | Wild Hibisci Mutabilis pet skin medicine for external use |
| CN106074238A (en) * | 2016-06-14 | 2016-11-09 | 广州暨南生物医药研究开发基地有限公司 | A kind of golden flower certain herbaceous plants with big flowers whitening and spot eliminating cream and preparation method thereof |
| CN106109369A (en) * | 2016-06-21 | 2016-11-16 | 广州暨南生物医药研究开发基地有限公司 | A kind of anti-wrinkle composition containing Hibiscus manihot L. and anti-wrinkle cream thereof |
| CN107362108A (en) * | 2017-09-26 | 2017-11-21 | 深圳聚源宝鼎农业生物科技产业发展有限公司 | A kind of Golden flower facial mask and preparation method thereof |
| KR101857528B1 (en) * | 2016-07-01 | 2018-05-15 | 에스케이바이오랜드 주식회사 | Cosmetic composition with the extract of Aurea Helianthus for skin-whitening |
| CN105853287B (en) * | 2016-05-03 | 2018-08-28 | 广州暨南生物医药研究开发基地有限公司 | A kind of Golden flower moisturizing essence and preparation method thereof |
| CN111150696A (en) * | 2020-02-24 | 2020-05-15 | 林淑娴 | After-sun repair emulsion and preparation method thereof |
| CN112516020A (en) * | 2020-11-26 | 2021-03-19 | 江西真美生物科技有限公司 | Luffa flower hydrolat and preparation method and application thereof |
| KR20220083398A (en) * | 2020-12-11 | 2022-06-20 | 동의대학교 산학협력단 | Skin anti-pollution composition containing aurea helianthus extract |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105853287B (en) * | 2016-05-03 | 2018-08-28 | 广州暨南生物医药研究开发基地有限公司 | A kind of Golden flower moisturizing essence and preparation method thereof |
| CN106074238B (en) * | 2016-06-14 | 2019-01-18 | 广州暨南生物医药研究开发基地有限公司 | A kind of Golden flower whitening and spot eliminating cream and preparation method thereof |
| CN106074238A (en) * | 2016-06-14 | 2016-11-09 | 广州暨南生物医药研究开发基地有限公司 | A kind of golden flower certain herbaceous plants with big flowers whitening and spot eliminating cream and preparation method thereof |
| CN106109369A (en) * | 2016-06-21 | 2016-11-16 | 广州暨南生物医药研究开发基地有限公司 | A kind of anti-wrinkle composition containing Hibiscus manihot L. and anti-wrinkle cream thereof |
| CN106109369B (en) * | 2016-06-21 | 2018-12-11 | 广州暨南生物医药研究开发基地有限公司 | A kind of anti-wrinkle composition and its anti-wrinkle cream containing Golden flower |
| KR101857528B1 (en) * | 2016-07-01 | 2018-05-15 | 에스케이바이오랜드 주식회사 | Cosmetic composition with the extract of Aurea Helianthus for skin-whitening |
| CN106063925A (en) * | 2016-07-22 | 2016-11-02 | 许备占 | Wild Hibisci Mutabilis pet skin medicine for external use |
| CN107362108A (en) * | 2017-09-26 | 2017-11-21 | 深圳聚源宝鼎农业生物科技产业发展有限公司 | A kind of Golden flower facial mask and preparation method thereof |
| CN111150696A (en) * | 2020-02-24 | 2020-05-15 | 林淑娴 | After-sun repair emulsion and preparation method thereof |
| CN111150696B (en) * | 2020-02-24 | 2021-03-12 | 深圳天和圆实业有限公司 | After-sun repair emulsion and preparation method thereof |
| CN112516020A (en) * | 2020-11-26 | 2021-03-19 | 江西真美生物科技有限公司 | Luffa flower hydrolat and preparation method and application thereof |
| KR20220083398A (en) * | 2020-12-11 | 2022-06-20 | 동의대학교 산학협력단 | Skin anti-pollution composition containing aurea helianthus extract |
| KR102544880B1 (en) | 2020-12-11 | 2023-06-16 | 동의대학교 산학협력단 | Skin anti-pollution composition containing aurea helianthus extract |
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