CN105012225A - Beauty and skincare enzyme liquid and application thereof - Google Patents
Beauty and skincare enzyme liquid and application thereof Download PDFInfo
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Abstract
The invention provides a beauty and skincare enzyme liquid and an application thereof. The beauty and skincare enzyme liquid is prepared from the following raw materials in parts by weight: 1-10 parts of malt, 5-10 parts of yeast and 0.1-3 parts of effective raw materials, wherein the effective raw materials are selected from 4-10 of the following components: ginseng, peach kernel, apricot kernel, poria cocos, coix seed, wolfberry fruit, licorice root, scutellaria baicalensis root, puerarin, rhodiola rosea root, bletilla striata root, burdock root, rose, dandelion, tea leaf, lophatherum gracile, centella leaf, chrysanthemum, gardenia, purslane, scabish, hop and herba leonuri. An enzyme mask essence liquid containing the beauty and skincare enzyme liquid is capable of helping activation of skin cells, promoting metabolism, effectively repairing aged skin, improving the antioxidant ability, increasing the moisture content of the skin and locking water and moisturizing in a long-acting manner, and plays a nourishing role when moisturizing, so that the skin is smooth and elastic.
Description
Technical field
The present invention relates to cosmetics manufacture field, specifically, relate to a kind of beauty and skin care enzyme liquid and application thereof.
Background technology
Ferment, be a kind of be made up of aminoacid there is special bioactive material, be maintain body normal function, digest food, the required material of one of the vital movements such as repair tissue.Ferment can bring vigor for Skin Cell, accelerates its metabolism, also has decompose removal effect to dirt, dead cell.Ferment can promote normal cell proliferation and damaged cell regeneration, makes cellular-restoring healthy, skin high resilience, and makes skin keep moistening for a long time.Therefore, ferment becomes the emerging cosmetic industry additive of a class.
Application number be 20141045118.X application discloses a kind of ferment facial mask essence with moisturizing whitening function, wherein add ferment stock solution 4 ~ 6 parts.Described ferment stock solution is formed by fruit natural fermentation, and after fermentation ends, namely elimination marc obtains ferment stock solution, and sterile filling is for subsequent use.Sweat takes natural fermentation, easy pollution microbes, and fermented quality is unstable, is not easy to realize industrialized standardization and produces.Do not clearly state microbial treatments mode in ferment stock solution.
Day by day be subject to today of popular favor at facial film class cosmetics, needing badly provides one can activating skin cells, enhances metabolism, effectively repairs aged skin, and improve oxidation resistance simultaneously, increase the facial mask essence of skin water content.
Summary of the invention
In order to solve problems of the prior art, the object of this invention is to provide a kind of beauty and skin care enzyme liquid and application thereof.
In order to realize the object of the invention, first the present invention provides a kind of beauty and skin care enzyme liquid, and its raw material comprises: Fructus Hordei Germinatus, yeast and both effectiveness raw material; Described both effectiveness raw material is selected from four kinds to ten kinds in following component: Radix Ginseng, Semen Persicae, Semen Armeniacae Amarum, Poria, Semen Coicis, FRUCTUS LYCII, licorice, scutellariae,radix, Radix Puerariae, root of Rhodiola sachalinensis, Pseudobulbus Bletillae (Rhizoma Bletillae) root, Radix Arctii, Flos Rosae Rugosae, Herba Taraxaci, Folium Camelliae sinensis, Herba Lophatheri, accumulated snow blade of grass, Flos Chrysanthemi, Flos Gardeniae, Herba Portulacae, Radix Oenotherae erythrosepalae, Flos lupuli (Flos Humuli Lupuli), Herba Leonuri.
As preferably, described both effectiveness raw material is selected from five kinds to seven kinds in said components.
Further, its raw material comprises according to parts by weight: 1 ~ 10 part, Fructus Hordei Germinatus, 5 ~ 10 parts, yeast, both effectiveness raw material often plant 0.1 ~ 3 part.As preferably, described both effectiveness raw material often plants 0.1 ~ 1 part.
Further, the preparation method of described beauty and skin care enzyme liquid comprises the steps:
(1) both effectiveness raw material is mixed, add the water soaking of its dry weight 10 ~ 20 times relatively or boil, obtaining lixiviating solution after filtration, obtain feed liquid I;
Particularly, in raw material, Radix Ginseng, Semen Persicae, Semen Armeniacae Amarum, Poria, Semen Coicis, FRUCTUS LYCII, licorice, scutellariae,radix, Radix Puerariae, root of Rhodiola sachalinensis, Pseudobulbus Bletillae (Rhizoma Bletillae) root, Radix Arctii etc. are when preparing lixiviating solution, add its dry weight 10 ~ 20 times of water, soak 2 ~ 6 hours, boil 20 ~ 40min, filter to obtain a lixiviating solution, repeat lixiviate and once obtain secondary lixiviating solution, control to boil intensity lower than 10%.In raw material, Flos Rosae Rugosae, Herba Taraxaci, Folium Camelliae sinensis, Herba Lophatheri, accumulated snow blade of grass, Flos Chrysanthemi, Flos Gardeniae, Herba Portulacae, Radix Oenotherae erythrosepalae, Flos lupuli (Flos Humuli Lupuli), Herba Leonuri etc. are when preparing lixiviating solution, add its dry weight 10 ~ 20 times of water, 70 ~ 90 DEG C of constant temperature soak 20 ~ 40min, filter to obtain a lixiviating solution, repeat lixiviate and once obtain secondary lixiviating solution.Mix all lixiviating solution and obtain feed liquid I;
(2) Fructus Hordei Germinatus is pulverized, after crossing 10 ~ 50 mesh sieves, add sacchariferous equipment, add the water of Fructus Hordei Germinatus dry weight 2 ~ 4 times, stage temperature reaction to iodine shows completely, and add more than 80 DEG C hot water wash grain filter 23s, each water consumption is 1 ~ 2 times of Fructus Hordei Germinatus dry weight, merging filtrate, obtains feed liquid II;
(3) feed liquid I and feed liquid II are squeezed into fermentation tank, be warmed up to 120 DEG C, sterilizing 30min;
(4) after sterilizing terminates, cooling feed liquid to 25 ~ 30 DEG C, access yeast;
(5) pass into clean compressed air, 25 ~ 30 DEG C, 100 ~ 1000rpm stirs fermentation 24 ~ 72 hours;
(6) after fermentation ends, fermentation liquid is centrifugal, collect fermented supernatant fluid and precipitate respectively;
(7) in precipitate, add the step 6 of its weight in wet base 2 ~ 6 times) gained fermented supernatant fluid, carry out low temperature cell breakage after dispersion mixing, after broken, liquid obtains the molten born of the same parents' thing of yeast through centrifuging and taking supernatant;
(8) by step (6) remaining fermented supernatant fluid and the molten born of the same parents' thing mixing of step (7) gained yeast, filter through the degerming microfiltration systems of film, collect bacteria-free filtrate, be described beauty and skin care enzyme liquid.
Wherein, the stage temperature reaction of step (2) is specially: heat up 45 ~ 50 DEG C of insulation 30min, is warmed up to 62 ~ 65 DEG C of insulation 40min, is warmed up to 70 ~ 72 DEG C and shows completely to iodine.
Wherein, the low temperature cell breakage of step (7) is specially: adopt low-temperature ultrahigh-pressure continuous flow cell disintegrating machine to carry out cell breakage.
Wherein, the centrifugal condition of step (6) and step (7) is 8000 ~ 12000rpm.
Further, used yeast bacterium is Pichia sp. (Pichia sp.) and candida valida (Candida valida).As preferably, in used yeast bacterium, Pichia sp. (Pichia sp.) and candida valida (Candida valida) mix in the ratio of 1:2 ~ 2:1.
Beauty and skin care enzyme liquid provided by the invention can be used as functional component and is used for being made into cosmetics.
Invention further provides a kind of ferment facial mask essence, containing aforementioned beauty and skin care enzyme liquid in described ferment facial mask essence, the mass percent of described beauty and skin care enzyme liquid is 5 ~ 15%.
As preferably, the mass percent of described beauty and skin care enzyme liquid is 10%.
Further, described ferment facial mask essence, according to weight percent meter, comprises following composition: water 70 ~ 90%; Beauty and skin care enzyme liquid 5 ~ 15%; Glycerol 2 ~ 4%; Radix Ginseng extract 1 ~ 3%; Butanediol 0.5 ~ 3%; Trehalose 0.5 ~ 3%; Hyaluronate sodium 0.02 ~ 0.2; Pantothenylol 0.5 ~ 1.0%; Tocopherol 0.1 ~ 0.5%, allantoin 0.2 ~ 0.5%, arbutin 0.2 ~ 1%; Cremophor RH40 0.3 ~ 1.5%; Carbomer 0.1 ~ 0.3%; Glycerol polymethacrylates 0.1 ~ 0.5%; Sodium hydroxide 0.01 ~ 0.05%; Methylisothiazolinone 0.005 ~ 0.01%; Iodine propilolic alcohol butyl mephenesin Carbamate 0.005 ~ 0.02%.
Beneficial effect of the present invention is:
Containing abundant aminoacid, oligopeptide, vitamin, mineral, ferment and various plants extract component in beauty and skin care enzyme liquid provided by the invention.Plant extraction liquid, through the Fermentation of microorganism, not only remains the nutritional labeling of itself, also add the nutritional labeling that microbial metabolic products brings, as vitamin, aminoacid, polypeptide, enzyme etc.Under enzyme microb zymolysis, some nutritive effect compositions of plant extract become micromolecule from macromole, as proteolysis has become aminoacid, the nonabsorbable composition of skin script are become Absorbable rod composition.These compositions are the nature moisturizing factor in skin, high and easily absorbed with skin affinity.These compositions have the hydrophilic groups such as a lot of amino, hydroxyl, carboxyl, and have very strong combination with water, while entering cell, portability large quantity of moisture enters cell, and moisture can be locked in cell and have moisture-keeping functions.
Ferment in beauty and skin care enzyme liquid can clear up skin surface rubbish, as the impurity in cell surface, intercellular lipid, the horny layer being blocked in rubbish in follicular orifice, sweat gland, sebaceous gland and overaging, for the input of moisture and nutrient substance is cleared away the obstacles.Along with the increase of skin water absorption, after the complete hydration of horny layer is swelling, osmotic absorption ability increases, ferment can by absorption deeply to skin layers, and scavenger cell metabolism dirt, clears up from profound level, the small circulation of unobstructed skin, makes skin obtain sufficient nutrition and moisture.Ferment in beauty and skin care enzyme liquid and micromolecule nutrient substance can not only provide abundanter nutrient substance for skin cell metabolism, and with the functional components such as pantothenylol, vitamin E, hyaluronate sodium, arbutin, allantoin, Radix Ginseng extract with the use of, these nutrition compositions will be promoted to go deep at the bottom of flesh and improve absorbing power at the bottom of its flesh, strengthening its efficacy.
The beauty and skin care enzyme liquid provided in the present invention, form through the preferred specified microorganisms fermentation of Based Intelligent Control, sweat safety is controlled, and tunning is pollution-free, non-stimulated, safety is high.Serial K cryogenic treatment measure is have employed after enzyme liquid fermentation ends, release somatic cells Dissolve things inside, add enzyme liquid nutritional labeling, while guaranteeing enzyme liquid bioactive ingredients effectiveness, remove wherein microorganism, make its quality meet " cosmetics health specification " related request.Simultaneously, carry out acute oral toxicity test, acute dermal toxicity test, skin irritation/corrosion test, acute ocular zest/corrosion test according to " cosmetics health specification ", result shows that this beauty and skin care enzyme liquid is nontoxic, nonirritant, non-corrosiveness.
The beauty and skin care enzyme liquid provided in the present invention, production technology is simple, with short production cycle, is convenient to artificial intelligence control, can carries out large-scale standardized production, applied range.
Ferment facial mask essence provided by the invention can help activating skin cells, enhances metabolism, effectively repairs aged skin, improve oxidation resistance, increase skin water content, the moisturizing of long-acting lock water, while moisturizing, play nourishing effect, make skin smooth and high resilience.
Detailed description of the invention
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1 beauty and skin care enzyme liquid and preparation method thereof
Beauty and skin care enzyme liquid raw material, according to parts by weight, comprises following component: 2 parts, Fructus Hordei Germinatus, Radix Ginseng 0.1 part, Semen Persicae 0.5 part, Semen Coicis 1 part, Folium Camelliae sinensis 0.8 part, 5 parts, yeast.
Beauty and skin care enzyme liquid preparation method comprises the steps:
(1) needed raw material Radix Ginseng, Semen Persicae, Semen Coicis and Folium Camelliae sinensis is weighed respectively in proportion, cleaning remove impurity.Mixing Radix Ginseng, Semen Persicae, Semen Coicis, add its dry weight 20 times of water, soak 4 hours, boil 30min, filter to obtain a lixiviating solution, repeats lixiviate and once obtain secondary lixiviating solution, controls to boil intensity lower than 10%.In Folium Camelliae sinensis, add the water of its dry weight 15 times, 80 DEG C of constant temperature soak 30min, filter to obtain a lixiviating solution, repeat lixiviate and once obtain secondary lixiviating solution.Mix all lixiviating solution and obtain feed liquid I.
(2) required dried malt is weighed in proportion, cleaning remove impurity, pulverize, after crossing 10 ~ 50 mesh sieves, add sacchariferous equipment, add the water of Fructus Hordei Germinatus dry weight 4 times, heat up 50 DEG C of insulation 30min, be warmed up to 65 DEG C of insulation 40min, be warmed up to 70 to iodine and show completely, add more than 80 DEG C hot water wash grain filter 23s, each water consumption is 1 times of Fructus Hordei Germinatus dry weight, and merging filtrate obtains feed liquid II.
(3) feed liquid I and feed liquid II are squeezed into fermentation tank, be warmed up to 120 DEG C, sterilizing 30min.
(4) after sterilizing terminates, cooling feed liquid to 30 DEG C, access yeast.Used yeast bacterium is Pichia sp. (Pichia sp.) and candida valida (Candida valida).Yeast activation culture is aseptically, yeast is inoculated in sterilizing malt extract medium, 30 DEG C, and 150rpm cultivates 36 hours, and yeast count reaches 10
8individual/more than ml.Pichia sp. (Pichiasp.) and candida valida (Candida valida) inoculative proportion are 1:1.
(5) pass into clean compressed air, 30 DEG C, 120rpm stirs fermentation 36 hours.
(6) the online centrifugal fermentation liquid of 10000rpm after fermentation ends, collects fermented supernatant fluid and precipitate respectively.
(7) in precipitate, add above-mentioned 6 of its weight in wet base 6 times) described supernatant, carries out cell breakage with low-temperature ultrahigh-pressure continuous flow cell disintegrating machine after disperseing mixing, after broken, liquid is centrifugal through 10000rpm, and eliminating precipitation is got supernatant and obtained the molten born of the same parents' thing of yeast.
(8) by above-mentioned (6) remaining fermented supernatant fluid and the molten born of the same parents' thing mixing of above-mentioned (7) gained yeast, filter through the degerming microfiltration systems of film, collect bacteria-free filtrate and obtain beauty and skin care enzyme liquid.
Carry out acute oral toxicity test, acute dermal toxicity test, skin irritation/corrosion test, acute ocular zest/corrosion test according to " cosmetics health specification " to beauty and skin care enzyme liquid prepared by the present embodiment, result shows that this beauty and skin care enzyme liquid is nontoxic, nonirritant, non-corrosiveness.
Entrust domestic authoritative institution to carry out proteomic image analysis detection to beauty and skin care enzyme liquid prepared by the present embodiment, result shows in beauty and skin care enzyme liquid prepared by the present embodiment main containing the various enzymes shown in table 1.
The enzyme contained in table 1 beauty and skin care enzyme liquid
Embodiment 2 beauty and skin care enzyme liquid and preparation method thereof
Beauty and skin care enzyme liquid raw material, according to parts by weight, comprises following component: 5 parts, Fructus Hordei Germinatus, Pseudobulbus Bletillae (Rhizoma Bletillae) root 0.6 part, 1 part, Semen Armeniacae Amarum, root of Rhodiola sachalinensis 0.2 part, Herba Taraxaci 0.8 part, Herba Centellae 1.0 parts, 10 parts, yeast.
Beauty and skin care enzyme liquid preparation method comprises the steps:
(1) needed raw material Pseudobulbus Bletillae (Rhizoma Bletillae) root, Semen Armeniacae Amarum, root of Rhodiola sachalinensis, Herba Taraxaci, Herba Centellae is weighed respectively in proportion, cleaning remove impurity.The mixing Pseudobulbus Bletillae (Rhizoma Bletillae), Semen Armeniacae Amarum and root of Rhodiola sachalinensis, add the water of its dry weight 15 times, soak 4 hours, boil 35min, filter to obtain a lixiviating solution, repeats lixiviate and once obtain secondary lixiviating solution, controls to boil intensity lower than 10%.Mixing Herba Taraxaci and Herba Centellae, add the water of its dry weight 10 times, and 75 DEG C of constant temperature soak 40min, filter to obtain a lixiviating solution, repeats lixiviate and once obtain secondary lixiviating solution.Mix all lixiviating solution and obtain feed liquid I.
(2) required dried malt is weighed in proportion, cleaning remove impurity, pulverize, after crossing 10 ~ 50 mesh sieves, add sacchariferous equipment, add the water of Fructus Hordei Germinatus dry weight 3 times, heat up 45 DEG C of insulation 30min, be warmed up to 62 DEG C of insulation 40min, be warmed up to 72 DEG C and show completely to iodine, add more than 80 DEG C hot water wash grain filter 23s, each water consumption is 2 times of Fructus Hordei Germinatus dry weight, and merging filtrate obtains feed liquid II.
(3) feed liquid I and feed liquid II are squeezed into fermentation tank, be warmed up to 120 DEG C, sterilizing 30min.
(4) after sterilizing terminates, cooling feed liquid to 28 DEG C, access yeast.Used yeast bacterium is Pichia sp. (Pichia sp.) and candida valida (Candida valida).Yeast activation culture is aseptically, yeast is inoculated in sterilizing malt extract medium, 30 DEG C, and 150rpm cultivates 36 hours, and yeast count reaches 10
8individual/more than ml.Pichia sp. (Pichiasp.) and candida valida (Candida valida) inoculative proportion are 2:1.
(5) pass into clean compressed air, 28 DEG C, 500rpm stirs fermentation 30 hours.
(6) the online centrifugal fermentation liquid of 12000rpm after fermentation ends, collects fermented supernatant fluid and precipitate respectively.
(7) in precipitate, add above-mentioned (6) described supernatant of its weight in wet base 5 times, cell breakage is carried out with low-temperature ultrahigh-pressure continuous flow cell disintegrating machine after dispersion mixing, after broken, liquid is centrifugal through 12000rpm, and eliminating precipitation is got supernatant and obtained the molten born of the same parents' thing of yeast.
(8) by above-mentioned (6) remaining fermented supernatant fluid and the molten born of the same parents' thing mixing of above-mentioned (7) gained yeast, filter through the degerming microfiltration systems of film, collect bacteria-free filtrate and obtain beauty and skin care enzyme liquid.
Carry out acute oral toxicity test, acute dermal toxicity test, skin irritation/corrosion test, acute ocular zest/corrosion test according to " cosmetics health specification " to beauty and skin care enzyme liquid prepared by the present embodiment, result shows that this beauty and skin care enzyme liquid is nontoxic, nonirritant, non-corrosiveness.
Embodiment 3 beauty and skin care enzyme liquid and preparation method thereof
The difference of the present embodiment and embodiment 1 is:
Beauty and skin care enzyme liquid raw material, according to parts by weight, comprises following component: 8 parts, Fructus Hordei Germinatus, scutellariae,radix 1.0 parts, 0.5 part, Poria, FRUCTUS LYCII 0.3 part, Herba Portulacae 1.0 parts, Radix Oenotherae erythrosepalae 0.8 part, Herba Lophatheri 0.5 part, 8 parts, yeast.
Carry out acute oral toxicity test, acute dermal toxicity test, skin irritation/corrosion test, acute ocular zest/corrosion test according to " cosmetics health specification " to beauty and skin care enzyme liquid prepared by the present embodiment, result shows that this beauty and skin care enzyme liquid is nontoxic, nonirritant, non-corrosiveness.
Embodiment 4 ferment facial mask essence and preparation method thereof
Ferment facial mask essence is prepared raw materials used as shown in table 2.
Table 2 ferment facial mask essence is prepared raw materials used
| Composition | Consumption (part) |
| Water | 76.813 |
| Beauty and skin care enzyme liquid prepared by embodiment 1 | 15 |
| Radix Ginseng extract | 1 |
| Pantothenylol | 0.6 |
| Hyaluronate sodium | 0.03 |
| Trehalose | 1 |
| Butanediol | 2 |
| Glycerol | 2 |
| Tocopherol | 0.1 |
| Allantoin | 0.5 |
| Arbutin | 0.2 |
| Cremophor RH40 | 0.3 |
| Carbomer | 0.1 |
| Glycerol polymethacrylates | 0.3 |
| Sodium hydroxide | 0.04 |
| Methylisothiazolinone | 0.01 |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.007 |
Ferment facial mask essence preparation method is as follows:
(1) weigh deionized water in proportion and squeeze into emulsifying pot, open and stir, drop into load weighted carbomer, be stirred to and dissolve completely, add sodium hydroxide solution and regulate pH to 5 ~ 7.Then add load weighted trehalose, glycerol, butanediol, allantoin, arbutin successively, often add a component and add next component again after dissolving completely, after adding, be stirred to complete clear homogeneous.
(2) weigh deionized water in proportion, add load weighted hyaluronate sodium, be stirred to and dissolve completely, then add above-mentioned (1) gained solution.Open and stir and homogenizing, be warming up to 80 DEG C, insulated and stirred 30min, make each component fully dissolve mixing.
(3) cooling is opened, above-mentioned (2) gained solution temperature is down to 40 DEG C, add load weighted glycerol polymethacrylates, pantothenylol, Methylisothiazolinone and iodine propilolic alcohol butyl mephenesin Carbamate successively, stir homogenizing and each component is dissolved completely.
(4) by load weighted tocopherol and Cremophor RH40 mixing, be uniformly mixed to homogeneous transparent, add above-mentioned (3) gained solution.
(5) in above-mentioned (4) gained solution, load weighted beauty and skin care enzyme liquid and Radix Ginseng extract is added successively, stirring and evenly mixing.Sampling carries out the inspection of semifinished product, qualified rear discharging fill.End product quality meets QB/T 2872 " facial film " related request.
Embodiment 5 ferment facial mask essence and preparation method thereof
Ferment facial mask essence is prepared raw materials used as shown in table 3.
Table 3 ferment facial mask essence is prepared raw materials used
| Composition | Consumption (part) |
| Water | 80.412 |
| Beauty and skin care enzyme liquid prepared by embodiment 2 | 10 |
| Radix Ginseng extract | 2 |
| Pantothenylol | 1.0 |
| Hyaluronate sodium | 0.04 |
| Trehalose | 0.5 |
| Butanediol | 1 |
| Glycerol | 3 |
| Tocopherol | 0.2 |
| Allantoin | 0.3 |
| Arbutin | 0.6 |
| Cremophor RH40 | 0.6 |
| Carbomer | 0.2 |
| Glycerol polymethacrylates | 0.1 |
| Sodium hydroxide | 0.03 |
| Methylisothiazolinone | 0.008 |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.01 |
Ferment facial mask essence preparation method is as follows:
(1) weigh deionized water in proportion and squeeze into emulsifying pot, open and stir, drop into load weighted carbomer, be stirred to and dissolve completely, add sodium hydroxide solution and regulate pH to 5 ~ 7.Then add load weighted trehalose, glycerol, butanediol, allantoin, arbutin successively, often add a component and add next component again after dissolving completely, after adding, be stirred to complete clear homogeneous.
(2) weigh deionized water in proportion, add load weighted hyaluronate sodium, be stirred to and dissolve completely, then add above-mentioned (1) gained solution.Open and stir and homogenizing, be warming up to 80 DEG C, insulated and stirred 30min, make each component fully dissolve mixing.
(3) cooling is opened, above-mentioned (2) gained solution temperature is down to 45 DEG C, add load weighted glycerol polymethacrylates, pantothenylol, Methylisothiazolinone and iodine propilolic alcohol butyl mephenesin Carbamate successively, stir homogenizing and each component is dissolved completely.
(4) by load weighted tocopherol and Cremophor RH40 mixing, stirring and dissolving, to homogeneous transparent, adds above-mentioned (3) gained solution.
(5) in above-mentioned (4) gained solution, load weighted beauty and skin care enzyme liquid and Radix Ginseng extract is added successively, stirring and evenly mixing.Sampling carries out the inspection of semifinished product, qualified rear discharging fill.End product quality meets QB/T 2872 " facial film " related request.
Embodiment 6 ferment facial mask essence and preparation method thereof
The difference of the present embodiment and embodiment 4 is: beauty and skin care enzyme liquid embodiment 1 prepared replaces with beauty and skin care enzyme liquid prepared by embodiment 3.
Experimental example 1
Ferment facial mask essence embodiment 4 ~ 6 prepared coordinates facial mask cloth compatible to be with it prepared into mask, respectively each through 100 20-50 year without about 2 months on probation of the women of skin allergy history, within every 4 days 1, paste, amount to 15 subsides.Requirement washes one's face after clean, by facial film mulching on the face, takes off facial film, pat massage skin gently after 15 ~ 20 minutes, essence is all absorbed, and clear water carries out operational maintenance after cleaning.Trial employment period occurs without any allergic phenomena.On probation terminate after, more than 95 parts triers think that skin makes moderate progress than before, and it is tender moistening, smooth and flexible to become water.
Embodiment 7 ~ 12 ferment facial mask essence and preparation method thereof
Embodiment 7 ~ 12 is with the difference of embodiment 4: the consumption of beauty and skin care enzyme liquid is replaced with 0,2%, 5%, 8%, 10%, 20%, and the part of change makes total amount be consistent by regulating the consumption of water.
Comparative example 1
Coordinate facial mask cloth compatible to be with it prepared into mask facial mask essence described in embodiment 4 and embodiment 7-12, each through 50 20 ~ 50 years old women without skin allergy history about 2 months on probation respectively, within every 4 days 1, paste, total 15 subsides.Requirement washes one's face after clean, by facial film mulching on the face, takes off facial film, pat massage skin gently after 15 ~ 20 minutes, essence is all absorbed, and clear water carries out operational maintenance after cleaning.Carry out result of use satisfaction investigation to trier after end on probation, result is as shown in table 4 below:
Table 4 facial film result of use satisfaction investigation result
During average mark >=4, facial film result of use satisfaction at least reaches the level of " very well ", namely reaches test acceptable level.When differing≤0.2 between average mark, result of use is considered as, without significant change, being namely considered as same level.
According to facial mask essence result of use satisfaction average mark, in conjunction with beauty and skin care enzyme liquid economical benefit, it is 5 ~ 15% that selected beauty and skin care enzyme liquid adds concentration range, when wherein concentration is 10%, result of use is obviously better than 5% and 8%, suitable with 15%, and use cost is lower than 15%, therefore 10% is regarded as beauty and skin care enzyme liquid the best interpolation concentration.
Facial mask essence result of use satisfaction average mark adds in concentration 0 ~ 10% at beauty and skin care enzyme liquid and increases fast along with the increase of beauty and skin care enzyme liquid concentration, add in concentration 10% ~ 20% without significant change at beauty and skin care enzyme liquid, show that facial mask essence result of use and beauty and skin care enzyme liquid add concentration relevant, affect particularly evident when low concentration, high concentration has no significant effect, and this is main relevant to beauty and skin care enzyme liquid effective efficiency constituent concentration in facial mask essence.During low concentration, functional component can not meet needed for skin metabolism, and action effect increases with functional component concentration and increases, once functional component concentration is increased to and is enough to meet skin cell metabolism and takes, its action effect will without significant change.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (9)
1. a beauty and skin care enzyme liquid, is characterized in that, its raw material comprises: Fructus Hordei Germinatus, yeast and both effectiveness raw material; Described both effectiveness raw material is selected from four kinds to ten kinds in following component: Radix Ginseng, Semen Persicae, Semen Armeniacae Amarum, Poria, Semen Coicis, FRUCTUS LYCII, licorice, scutellariae,radix, Radix Puerariae, root of Rhodiola sachalinensis, Pseudobulbus Bletillae (Rhizoma Bletillae) root, Radix Arctii, Flos Rosae Rugosae, Herba Taraxaci, Folium Camelliae sinensis, Herba Lophatheri, accumulated snow blade of grass, Flos Chrysanthemi, Flos Gardeniae, Herba Portulacae, Radix Oenotherae erythrosepalae, Flos lupuli (Flos Humuli Lupuli), Herba Leonuri.
2. beauty and skin care enzyme liquid according to claim 1, is characterized in that, its raw material comprises according to parts by weight: 1 ~ 10 part, Fructus Hordei Germinatus, 5 ~ 10 parts, yeast, both effectiveness raw material often plant 0.1 ~ 3 part.
3. beauty and skin care enzyme liquid according to claim 1 and 2, it is characterized in that, its preparation method comprises the steps:
(1) both effectiveness raw material is mixed, add the water soaking of its dry weight 10 ~ 20 times relatively or boil, obtaining lixiviating solution after filtration, obtain feed liquid I;
(2) Fructus Hordei Germinatus is pulverized, after crossing 10 ~ 50 mesh sieves, add sacchariferous equipment, add the water of Fructus Hordei Germinatus dry weight 2 ~ 4 times, stage temperature reaction to iodine shows completely, and add more than 80 DEG C hot water wash grain filter 23s, each water consumption is 1 ~ 2 times of Fructus Hordei Germinatus dry weight, merging filtrate, obtains feed liquid II;
(3) feed liquid I and feed liquid II are squeezed into fermentation tank, be warmed up to 120 DEG C, sterilizing 30min;
(4) after sterilizing terminates, cooling feed liquid to 25 ~ 30 DEG C, access yeast;
(5) pass into clean compressed air, 25 ~ 30 DEG C, 100 ~ 1000rpm stirs fermentation 24 ~ 72 hours;
(6) after fermentation ends, fermentation liquid is centrifugal, collect fermented supernatant fluid and precipitate respectively;
(7) in precipitate, add the step 6 of its weight in wet base 2 ~ 6 times) gained fermented supernatant fluid, carry out low temperature cell breakage after dispersion mixing, after broken, liquid obtains the molten born of the same parents' thing of yeast through centrifuging and taking supernatant;
(8) by step (6) remaining fermented supernatant fluid and the molten born of the same parents' thing mixing of step (7) gained yeast, filter through the degerming microfiltration systems of film, collect bacteria-free filtrate, be described beauty and skin care enzyme liquid.
4. beauty and skin care enzyme liquid according to claim 3, is characterized in that, the low temperature cell breakage of step (7) is specially: adopt low-temperature ultrahigh-pressure continuous flow cell disintegrating machine to carry out cell breakage.
5. beauty and skin care enzyme liquid according to claim 3, is characterized in that, the centrifugal condition of step (6) and step (7) is 8000 ~ 12000rpm.
6. beauty and skin care enzyme liquid according to claim 1 and 2, is characterized in that, used yeast bacterium is Pichia sp. and candida valida.
7. a ferment facial mask essence, is characterized in that, containing the beauty and skin care enzyme liquid described in any one of claim 1 ~ 6 in described ferment facial mask essence, the mass percent of described beauty and skin care enzyme liquid is 5 ~ 15%.
8. ferment facial mask essence according to claim 7, is characterized in that, the mass percent of described beauty and skin care enzyme liquid is 10%.
9. ferment facial mask essence according to claim 7, is characterized in that, described ferment facial mask essence, according to weight percent meter, comprises following composition: water 70 ~ 90%; Beauty and skin care enzyme liquid 5 ~ 15%; Glycerol 2 ~ 4%; Radix Ginseng extract 1 ~ 3%; Butanediol 0.5 ~ 3%; Trehalose 0.5 ~ 3%; Hyaluronate sodium 0.02 ~ 0.2; Pantothenylol 0.5 ~ 1.0%; Tocopherol 0.1 ~ 0.5%, allantoin 0.2 ~ 0.5%, arbutin 0.2 ~ 1%; Cremophor RH40 0.3 ~ 1.5%; Carbomer 0.1 ~ 0.3%; Glycerol polymethacrylates 0.1 ~ 0.5%; Sodium hydroxide 0.01 ~ 0.05%; Methylisothiazolinone 0.005 ~ 0.01%; Iodine propilolic alcohol butyl mephenesin Carbamate 0.005 ~ 0.02%.
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