Astm C1293.35962
Astm C1293.35962
Astm C1293.35962
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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the recommended container. Alternative storage containers cement either by analysis or by obtaining a mill run certificate
must contain the required depth of water. When reporting from the cement manufacturer. Add NaOH to the concrete
results, note the use of an alternative container, if one is used, mixing water so as to increase the alkali content of the mixture,
together with documentation proving compliance with the expressed as Na2O equivalent, to 1.25 % by mass of cement
above. (see Note 3).
NOTE 1—Polypropylene geotextile fabric or blotting paper are suitable NOTE 3—The value of 1.25 % Na2O equivalent by mass of cement has
materials for use as the wick. been chosen to accelerate the process of expansion rather than to
reproduce field conditions. At the 420 kg/m3 cement content, this
5.3 The storage environment necessary to maintain the 38.0 corresponds to an alkali level of 5.25 kg/m3 .
°C reaction accelerating storage temperature consistently and
homogeneously is described in 5.3.1. 7.2 Aggregates:
5.3.1 Recommended Environment—The recommended stor- 7.2.1 To evaluate the reactivity of a coarse aggregate, use a
age environment is a sealed space insulated so as to minimize nonreactive fine aggregate. A nonreactive fine aggregate is
heat loss. Provide a fan for air circulation so the maximum defined as an aggregate that develops an expansion in the
variation in temperature measured within 250 mm of the top accelerated mortar bar, (see Test Method C1260) of less than
and bottom of the space does not exceed 2.0 °C. Provide an 0.10 % at 14 days (see X1.6 for interpretation of expansion
insulated entry door with adequate seals so as to minimize heat data). Use a fine aggregate meeting Specification C33 with a
loss. Racks for storing containers within the space are not to be fineness modulus of 2.7 6 0.2.
closer than 30 mm to the sides of the enclosure and are to be 7.2.2 To evaluate the reactivity of a fine aggregate, use a
perforated so as to provide air flow. Provide an automatically nonreactive coarse aggregate. Prepare the nonreactive coarse
controlled heat source to maintain the temperature at 38.0 6 aggregate according to 7.2.3.6 A nonreactive coarse aggregate
2.0 °C (see Note 2). Record the ambient temperature and its is defined as an aggregate that develops an expansion in the
variation within the space to ensure compliance. accelerated mortar bar (see Test Method C1260) of less than
0.10 % at 14 days (see X1.6 for interpretation of expansion
NOTE 2—It has been found to be good practice to monitor the efficiency data). Use a coarse aggregate meeting Specification C33. Test
of the storage environment by placing thermocouples inside dummy
concrete specimens inside a dummy container within the storage area. The
the fine aggregate using the grading as delivered to the
storage room described in Test Method C227 generally will be satisfac- laboratory.
tory. 7.2.3 Sieve the coarse aggregate and recombine in accor-
5.3.2 Alternative Storage Environment—Use of an alterna- dance with the requirements in Table 1. Select the Table 1
tive storage environment is permitted. Confirm the efficiency grading based on the as-received grading of the sample. Coarse
of the alternative storage container with an alkali-reactive aggregate fractions larger than 19.0-mm sieve are not to be
aggregate of known expansion characteristics.6 The expansion tested as such. When petrographic examination using Guide
efficiency is confirmed when expansions at one year obtained C295 reveals that the material making up the size fraction
using the alternative storage environment are within 10 % of larger than the 19.0-mm sieve is of such a composition and
those obtained using the recommended environment. When lithology that no difference should be expected compared with
reporting the results, note the use of an alternative storage the smaller size material, then no further attention need be paid
environment, if one is utilized, together with documentation to the larger sizes. If petrographic examination suggests the
proving compliance with the above. larger size material to have a different reactivity, the material
should be studied for its effect in concrete according to one of
6. Reagents the other alternative procedures described herein:
6.1 Sodium Hydroxide (NaOH)—USP or technical grade 7.2.3.1 Proportional Testing—Crush material larger than the
may be used. (Warning—Before using NaOH, review: (1) the 19.0-mm sieve to pass the 19.0-mm sieve. The crushing
safety precautions for using NaOH; (2) first aid for burns; and operation shall be performed in a manner that minimizes
(3) the emergency response to spills as described in the production of material passing the 4.75-mm sieve. Grade this
manufacturers Material Safety Data Sheet or other reliable crushed material per the Table 1 grading, and add to the
safety literature. NaOH can cause severe burns and injury to original mass of graded aggregate produced in 7.2.3 such that
unprotected skin and eyes. Always use suitable personal the ratio of crushed, graded, oversize aggregate to total graded
protective equipment including: full-face shields, rubber aggregate equals the ratio of material retained on the 19.0-mm
aprons, and gloves impervious to NaOH (Check periodically sieve to the total material retained above the 4.75-mm sieve
for pinholes.).) (See Note 4).
6.2 Water: NOTE 4—For example, if the material retained on the 19-mm sieve
formed 25 % of the total material retained above the 4.75-mm sieve, then
6.2.1 Use potable tap water for mixing and storage.
7. Materials
TABLE 1 Grading Requirement
7.1 Cement—Use a cement meeting the requirements for a Sieve Size Mass Fraction
Type I Portland cement as specified in Specification C150. The Passing Retained Coarse Intermediate
cement must have a total alkali content of 0.9 6 0.1 % Na2O 19.0-mm 12.5-mm 1⁄ 3 ...
12.5-mm 9.5-mm 1⁄ 3 1 ⁄2
equivalent (Na2O equivalent is calculated as percent Na2O + 9.5-mm 4.75-mm 1⁄ 3 1 ⁄2
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the mass of crushed and returned oversize material shall form 25 % of the 2 3 39.997/61.98 5 1.291; (1)
total graded aggregate. Amount of NaOH required in Example A:
7.2.3.2 Separated Size Testing—Crush material larger than 1.47 3 1.291 5 1.898 kg/m 3 (2)
the 19.0-mm sieve to pass the 19.0-mm sieve, grade that Example B (20 % of cement is replaced
material as per Table 1 and test in concrete as a separate by pozzolan)
Cementitious materials = 420 kg
aggregate. content of 1 m3 concrete
7.3 Concrete Mixture Proportions—Proportion the concrete Cement content of = 420 kg × 0.8
concrete (20 % by mass pozzolan)
mixture to the following requirements: = 336 kg
7.3.1 Cementitious Materials Content—420 6 10 kg/m.3 Amount of alkali in the concrete = 336 kg × 0.90 %
= 3.02 kg
7.3.1.1 When evaluating the susceptibility of an aggregate Specified amount of alkali in concrete = 336 kg × 1.25 %
to expansive alkali-silica reaction, use cement as 100 % of the = 4.20 kg
cementitious material. Amount of alkali to be added to concrete = 4.20 kg – 3.02 kg
= 1.18 kg
7.3.1.2 When evaluating combinations of aggregate with
pozzolan or slag, replace cement with the desired amount of The difference (1.18 kg) is the amount of alkali, expressed as Na2O
equivalent, to be added to the mix water.
pozzolan or slag on a percent by mass basis. Amount of NaOH required for Example B:
7.3.2 Coarse Aggregate Content—Use a dry mass of coarse
aggregate per unit volume of concrete equal to 0.70 6 0.02 of 1.18 3 1.291 5 1.523 kg/m 3 (3)
its dry-rodded bulk density as determined by Test Method 8. Sampling
C29/C29M for all classes of aggregates (for example, low
density, normal, and high density). 8.1 Obtain the aggregate sample in accordance with Practice
7.3.3 Water-Cementitious Materials Ratio (w/cm)— D75 and reduce it to test portion size in accordance with
Maintain w/cm in the range of 0.42 to 0.45 by mass. Adjust the Practice C702.
w/cm within this range to give sufficient workability to permit 9. Specimen Preparation
satisfactory compaction of the concrete in the molds. If
necessary to obtain sufficient workability within the specified 9.1 Mixing Concrete:
w/cm range, use of a high-range water reducer (HRWR), 9.1.1 General—Mix concrete in accordance with the stan-
meeting the requirements of Specification C494/C494M Type dard practice for making and curing concrete test specimens in
F is permitted. If, within the specified w/cm range, specimens the laboratory as described in Practice C192/C192M.
representative of the concrete mixture cannot be fabricated due 9.1.2 Slump—Measure the slump of each batch of concrete
to excessive bleeding or segregation, the use of a viscosity- immediately after mixing in accordance with Test Method
modifying admixture (VMA) is permitted. Report the w/cm C143/C143M.
ratio used and the amount, if any, of HRWR or VMA. 9.1.3 Yield, and Air Content—Determine the yield, and air
content of each batch of concrete in accordance with Test
7.3.4 Admixture (NaOH)—Dissolve in the mixing water and
Method C138/C138M. Concrete used for slump, yield, and air
add as required to bring the alkali content of the concrete
content tests may be returned to the mixing pan and remixed
mixture, expressed as Na2Oe = % Na2O + 0.658× % K2O, up
into the batch.
to 1.25 % by mass of cement (see Note 5). Use no other
admixture in the concrete except as permitted in the section on 9.2 Prepare three specimens of the type required for con-
Water-Cementitious Materials Ratio. crete in Test Method C157/C157M from one batch of concrete
(see Note 6).
NOTE 5—Example calculations for determining the amount of NaOH to
be added to the mixing water to increase the alkali content of the cement NOTE 6—It has been found useful to cast an additional (4th) prism that
from 0.90 % to 1.25 %: can be removed from the test and used for petrographic examination at any
Example A (Cement Only) time.
Cementitious materials = 420 kg 9.3 Initial Conditioning—Cure, store, and remove molds in
content of 1 m3 concrete
Cement content of concrete = 420 kg accordance with Test Method C157/C157M.
Amount of alkali in the concrete = 420 kg × 0.90 %
= 3.78 kg 10. Procedure
Specified amount of alkali in concrete = 420 kg × 1.25 %
= 5.25 kg 10.1 Initial Comparator Reading—Follow the procedure of
Amount of alkali to be added to concrete = 5.25 kg − 3.78 kg Test Method C157/C157M, except do not place in saturated
= 1.47 kg
lime water. Make initial length reading at the time of removal
The difference (1.47 kg) is the amount of alkali, expressed as Na2O from the mold at an age of 23.5 6 0.5 h. Thereafter, keep the
equivalent, to be added to the mix water. Factor to convert Na2O to specimens at 38.0 6 2 °C in storage containers in accordance
NaOH: with 5.2.
since
(Na2O + H2O → 2 NaOH) 10.2 Subsequent Comparator Readings—Stand the speci-
Compound Molecular Weight men on end. Specimens shall not be in contact with water in the
Na2O 61.98
NaOH 39.997
reservoir within the storage container. Seal the container and
place container in a 38.0 6 2 °C storage environment. At no
Conversion factor: time should the storage container be in contact with the walls
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or floor of the 38.0 6 2 °C storage environment and there shall 12.1.8 The w/cm based on saturated, surface dry (SSD)
be an adequate flow of air around the container. aggregates,
10.2.1 When the specimens are 7 days old, take a compara- 12.1.9 The slump, with mass yield and air content of the
tor reading after removal of the container and contents from the concrete batched,
storage environment according to 10.2.2. Subsequent readings 12.1.10 The average length change in percent at each
are required at the ages of 28 and 56 days, as well as 3, 6, 9, reading of the prisms along with the individual length change
and 12 months when testing an aggregate for susceptibility to in percentage for each prism,
expansive alkali-silica reaction and additionally at 18 and 24 12.1.11 Any significant features revealed by examination of
months when testing combinations of aggregates with pozzo- the concrete prisms either during the test or at the end of the
lans or slag. Additional readings beyond those required for the test (for example, cracks, gel formation, or peripheral reaction
specific application are suggested at 6-month intervals. rims on aggregate particles), and
10.2.2 Remove the containers holding the prisms from the 12.1.12 Type of storage container and 38.0 6 2.0 °C storage
38.0 6 2.0 °C temperature environment and place in a moist environment used to store the concrete prisms if they differ
cabinet or moist room that is in compliance with Specification from those specified in 5.2.1 and 5.3.1.
C511 for a period 16 6 4 h before reading.
13. Precision and Bias
10.3 Fabricate all specimens placed in a given storage
13.1 Multi-Laboratory Precision:
container at the same time so that all specimens in that
13.1.1 Average Expansion Less Than 0.014 %—The multi-
container are due for comparator reading at the same time.
laboratory standard deviation of a single test result (mean of
10.4 Identify the specimens so as to place the specimens in measurements of three prisms) for average expansion less than
the comparator with the same end up. After the comparator 0.014 % has been found to be 0.0032 % (CSA A23.2-14A).4
reading of the prism, replace the specimen in the storage Therefore, results of two properly conducted tests in different
container but invert the upper end as compared with the laboratories on the same aggregate should not differ by more
previous storage period. In this way the prisms are not stored than 0.009 %, nineteen times out of twenty.
through two consecutive storage periods with the same ends 13.1.2 Average Expansion Greater Than 0.014 %—The
up. multi-laboratory coefficient of variation of a single test result
(mean of measurements of three prisms) for average expansion
11. Calculation greater than 0.014 % has been found to be 23 % (CSA
11.1 Calculate the change in length between the initial A23.2-14A).4 Therefore, results of two properly conducted
comparator reading of the specimen and the comparator tests in different laboratories on the same aggregate should not
reading at each time interval to the nearest 0.001 % of the differ from each other by more than 65 % of their average,
effective gage length and record as the length change of the nineteen times out of twenty.
prism for that period. Calculate the average length change in 13.2 Within-Laboratory Precision:
percentage for the group of prisms at the age. 13.2.1 Average Expansion Less Than 0.02 %—For average
11.2 Data from at least three bars must be available at any expansions of less than 0.02 %, the multi-specimen, within-
age to constitute a valid test at that age. laboratory standard deviation has been found to be 0.0025 %
(CSA A23.2-14A). Therefore, the range (difference between
12. Report highest and lowest) of the three individual prism measurements
12.1 Report the following information: used in calculating an average test result should not exceed
12.1.1 Type and source of coarse and fine aggregates, and 0.008 %, nineteen times out of twenty.
the coarse aggregate grading used, 13.2.2 Average Expansion Greater Than 0.02 %—For aver-
12.1.2 Type and source of portland cement, age expansions of more than 0.02 %, the multi-specimen,
12.1.3 The alkali content of the cement as percent potas- within-laboratory coefficient of variation has been found to be
sium oxide (K2O), sodium oxide (Na2O), and calculated 12 % (CSA A23.2-14A). Therefore, the range (difference
percent NaOe, between highest and lowest) of the three individual prism
12.1.4 Type, source, and amount (percent by mass of measurements used in calculating an average test result should
cementitious material) of any pozzolan or slag used, not exceed 40 % of the average, nineteen times out of twenty.
12.1.5 The amount, if any, of high-range water reducer or 13.3 Bias—Since there is no accepted reference material for
viscosity-modifying admixture used, determining the bias of this test method, no statement is being
12.1.6 Concrete mixture proportions based on SSD made.
aggregates, and corrected for yield,
12.1.7 The amount of sodium hydroxide (NaOH) added to 14. Keywords
the mixing water, expressed as percent sodium oxide (Na2O) 14.1 aggregate; alkali-silica reactivity; concrete; length
equivalent by mass of the cement, change ; pozzolan; slag
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APPENDIX
(Nonmandatory Information)
X1.1 The question of whether or not criteria based on the Method C1260. It is recommended that the relevant proce-
results obtained using this test method should be used for dure(s) be performed concurrently with this test method and
acceptance of materials for use as concrete aggregate will be any discrepancies between the results explained. Care should
dealt with, if deemed appropriate, in Specification C33. be exercised in the interpretation of these other test method
results (9-14).
X1.2 Work has been reported from which it may be inferred
that an aggregate might reasonably be classified as potentially X1.6 The use of this test method should especially be
deleteriously reactive if the average expansion of three con- considered when other test methods may be inadequate. Some
crete specimens is equal to or greater than 0.04 % at one year examples of such problems are as follows: The potential
(7) (CSA A23.2-27A-00 Table 1). reactivity of various varieties of quartz may not be accurately
determined by Test Method C227 since the test method may
X1.3 It is reasonable to conclude that the amount of produce a false-negative result (3). False-negative results are
pozzolan or slag used in combination with an aggregate is at possible with a number of aggregates such as slow-late
least the minimum needed to prevent excessive expansion in expanding argillaceous greywackes, strained quartz and micro-
field concrete if the average expansion is less than 0.04 % at crystalline quartz associated with strained quartz (3,4,13).
two years (CSA A23.2-28A-02). False-negative results are also possible due to storage condi-
tions (9), reactive aggregate levels far above or below pessi-
X1.4 A history of satisfactory field performance in concrete mum (3) or insufficient alkali to accelerate the test (3). The
is the best method of evaluating the potential for an aggregate potential reactivity of various varieties of quartz may not be
to cause premature deterioration of concrete due to alkali-silica accurately determined by Test Method C1260 since the test
reaction. When field performance of an aggregate in concrete is method may produce a false-positive result with a number of
to be accepted, the following conditions should be met (8): marginally reactive aggregates (13). Test Method C1260 may
X1.4.1 The cement content and alkali content of the cement also give a false-negative result with aggregates suspected of
should be the same or higher in the field concrete than is containing deleterious strained quartz (14).
proposed in the new structure.
X1.7 If the data generated with other test methods and
X1.4.2 The concrete examined should be at least 10 years supplemented with information from this test method judge an
old. aggregate to be “not potentially deleteriously alkali-silica
X1.4.3 The exposure conditions of the field concrete should reactive,” no restrictions are usually required with the use of
be at least as severe as those in the proposed structure. that aggregate in order to protect against expansion due to
alkali-silica reaction (7) (see Note X1.1).
X1.5 This test method supplements the results of other test
X1.8 Additional interlaboratory testing data is provided in
methods. The results of the other test methods are usually
Ref (15).
reported before the results of this test method are available. NOTE X1.1—In critical structures such as those used for nuclear
Standards that this test method supplements include: Test containment or large dams, where slight expansions cannot be tolerated, a
Method C227, Guide C295, Test Method C289, and Test lower expansion limit may be required.
REFERENCES
(1) Diamond, S., “Alkali Reactions in Concrete-Pore Solution Effects,” (5) Rogers, C. A., and Hooton, R. D., “Comparison Between Laboratory
Proceedings, 6th International Conference on Alkali-Aggregate Re- and Field Expansion of Alkali-Carbonate Reactive Concrete,”
action in Concrete, Copenhagen, Denmark, 1983, pp. 155–166. Proceedings, 9th International Conference on Alkali-Aggregate Re-
(2) Diamond, S., “ASR—Another Look at Mechanisms,” Proceedings, action in Concrete, Concrete Society, Slough, U.K., 1992, pp.
8th International Conference on Alkali-Aggregate Reaction, Kyoto, 877–884.
Japan, 1989, pp. 83–94. (6) Rogers, C. A., “General Information on Standard Alkali-Reactive
(3) Grattan-Bellew, P. E., “Test Methods and Criteria for Evaluating the Aggregates from Ontario, Canada,” Ontario Ministry of
Potential Reactivity of Aggregates,” Proceedings, 8th International Transportation, Engineering Materials Office, 1988, p. 59.
Conference on Alkali-Aggregate Reaction, Kyoto, Japan, 1989, pp. (7) Grattan-Bellew, P. E., “Reevaluation of Standard Mortar Bar and
279–294. Concrete Prism Tests,” Materiaux et Constructions, Vol 16, No. 94,
(4) Grattan-Bellew, P. E., “Microcrystalline Quartz, Undulatory Extinc- 1983, pp. 243–250.
tion and Alkali-Silica Reaction,” Proceedings, 9th International Con- (8) British Cement Association, “The Diagnosis of Alkali-silica
ference on Alkali-Aggregate Reaction in Concrete, Concrete Society, Reaction,” British Cement Association, Crowthorne, Berks, RG1
Slough, U.K., 1992, pp. 383–394. 6YS, United Kingdom, Second edition, 1992.
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C1293 − 08b (2015)
(9) Rogers, C. A., and Hooton, R. D., “Reduction in Mortar and Concrete Various Parameters on the Test Results, Cement and Concrete
Expansion with Reactive Aggregates Due to Leaching,” Cement, Research, Vol 21, 1991, pp. 853–862.
Concrete and Aggregates, CCAGDP, Vol 13, 1991, pp. 42–49. (13) Hooton, R. D., “New Aggregate Alkali-Reactivity Test Methods,”
(10) Bérubé, M. A., and Fournier, B., “Accelerated Test Methods for Ontario Ministry of Transportation, Research and Development
Alkali-Aggregate Reactivity,” Advances in Concrete Technology, Branch Report MAT-91-14, November, 1991.
Malhotra, V. M., ed., Canada Communication Group, Ottawa, 1992, (14) Kerrick, D. M., and Hooton, R. D., “ASR of Concrete Aggregate
pp. 583–627. Quarried from a Fault Zone: Results and Petrographic Interpretation
(11) Sorrentino, D., Clément, J. Y., and Goldberg, J. M., “A New of Accelerated Mortar Bar Test,” Cement and Concrete Research,
Approach to Characterize the Chemical Reactivity of the Vol 22, 1992, pp. 949–960.
Aggregates,” Proceedings, 9th International Conference on Alkali-
(15) Fournier, B. and Malhotra, V.M., “Interlaboratory Study on the CSA
Aggregate Reaction in Concrete, Concrete Society, Slough, U.K.,
A 23.2-14A Concrete Prism Test for Alkali-Silica Reactivity in
1992, pp. 1009–1016.
Concrete”, Proceedings, 10th International Conference on Alkali-
(12) Fournier, B., and Bérubé, M. A., “Application of the NBRI Accel-
erated Mortar Bar Test to Siliceous Carbonate Aggregates Produced Aggregate Reaction in Concrete”, CSIRO, Melbourne, Australia,
in the St. Lawrence Lowlands (Quebec, Canada), Part 1: Influence of 1996, pp. 302-309.
SUMMARY OF CHANGES
Committee C09 has identified the location of selected changes to this test method since the last issue,
C1293 – 08a, that may impact the use of this test method. (Approved December 1, 2008)
Committee C09 has identified the location of selected changes to this test method since the last issue,
C1293 – 08, that may impact the use of this test method. (Approved February 1, 2008)
(1) Revised 1.2, 5.1, 7.2.3, and 7.2.3.1. (4) Removed all informational inch-pound units throughout to
(2) Added new 12.1.13 and Note 4. conform to ASTM Form and Style.
(3) Revised Table 1.
Committee C09 has identified the location of selected changes to this test method since the last issue,
C1293 – 06, that may impact the use of this test method. (Approved January 15, 2008)
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