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Micromass GCT Classic Site Preparation Guide

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Waters GCT
Site Preparation Guide

715000574, REV. E PAGE 1 OF 24


Notice
©2013 WATERS CORPORATION. PRINTED IN THE UNITED STATES OF AMERICA. ALL RIGHTS
RESERVED. THIS BOOK OR PARTS THEREOF MAY NOT BE REPRODUCED IN ANY FORM WITHOUT THE
WRITTEN PERMISSION OF THE PUBLISHER.
Waters, The Science of What’s Possible and Connections INSIGHT are registered trademarks of Waters
Corporation.
GCT is a trademark of Waters Corporation.
Swagelok is a registered trademark of Swagelok Company.
All other trademarks are the sole property of their respective owners.

715000574, REV. E PAGE 2 OF 24


Table of Contents
Introduction .................................................................................................................. 4

Responsibilities ............................................................................................................. 4

Storage ......................................................................................................................... 5

Unpacking and Moving .................................................................................................. 5

Lifting Equipment .......................................................................................................... 6

Space Requirements ..................................................................................................... 7


Instrument ................................................................................................................ 7
Rotary Pump .............................................................................................................. 7
GC System ................................................................................................................ 7
Data System .............................................................................................................. 8
Connections INSIGHT® Installation Requirements ........................................................... 8
Electrical Safety ............................................................................................................ 8
Power Requirements ..................................................................................................... 8
Power Supply ............................................................................................................. 8
Electrical Transformers .............................................................................................. 10
System Plug Options ................................................................................................. 10
Uninterruptible Power Supply ..................................................................................... 12
Water Supplies ............................................................................................................ 13

Environmental Requirements ...................................................................................... 14


Safety Recommendations .......................................................................................... 14
Positioning ............................................................................................................... 14
Ventilation ............................................................................................................... 14
Temperature ............................................................................................................ 14
Humidity ................................................................................................................. 14
Altitude ................................................................................................................... 15
Vibration ................................................................................................................. 15
Magnetic Fields ........................................................................................................ 15
Radio Emissions ....................................................................................................... 15
Gases and Regulators ................................................................................................. 15
Soft Vent Gas .......................................................................................................... 15
Compressed Air ........................................................................................................ 15
GC Carrier Gas ......................................................................................................... 15
CI Reagent Gas ........................................................................................................ 16
Exhaust Outlets ........................................................................................................... 16
Rotary Pump Exhaust ................................................................................................ 16
Test Samples ............................................................................................................... 17
Solvents .................................................................................................................. 18
Cleaning Equipment .................................................................................................... 18

Summary of Fittings .................................................................................................... 18

GCT Site Preparation Checklist .................................................................................... 19

Applications Survey .................................................................................................... 24

715000574, REV. E PAGE 3 OF 24


Introduction
This document describes the recommended environmental conditions, power supplies, gas
supplies and water supplies that are required for the operation of the Waters GCT™. Operating the
instrument in conformance with these conditions will enable the instrument to achieve its optimum
performance.

Responsibilities
Warning: Observe Good Laboratory Practice (GLP) at all times, particularly when
working with hazardous materials, and consult the safety representative
for your organization regarding its protocols for handling such materials.

Warning: Safety glasses must be worn at all times when working with
hazardous materials and pressurized fluidics.

A Waters engineer will be responsible for installing and commissioning the system to ensure that
the instrument is properly installed and operational. The laboratory must be prepared in advance
to allow the engineer to carry out the installation efficiently. A site preparation checklist is included
at the end of this document for you to fill in and return to Waters when the laboratory is ready.

Important: The installation of the system cannot begin until the checklist has been completed
and returned.

The duration of the installation may vary, depending on the number of instrument options being
installed. The site preparation checklist should be completed as accurately as possible to help
minimize the installation time.

A major part of system installation is a series of tests which are used to evaluate the instrument
under specific operating conditions. The actual test result obtained, is recorded in the Installation
Checklist or Instrument Qualification Workbook, whichever is appropriate.

Important: An operator who has been designated to be responsible for the normal use and
upkeep of the instrument should be present during the installation.

The operator will assist with the instrument tests during the installation; this allows the operator
to be trained in the basic system operation. If there are foreseen periods when the intended
operator cannot be present, please notify us in advance; this will enable us to schedule the
installation for a more convenient time.

The instrument is supplied with a DB5-MS 30 m GC column. Please contact your Waters sales
representative if you wish Waters to supply any additional columns.

If you have any questions regarding the information in this document or any particular site
problems, please contact your local Waters sales representative. If necessary we will arrange to
carry out a site survey.

715000574, REV. E PAGE 4 OF 24


Storage
The following storage conditions are required prior to installation:

• Unopened shipping crates

• Crates stored away from heavy machinery such as compressors or generators, which
generate excessive floor vibration

• Storage area temperature 0 to 40 °C (32 to 104 °F) and humidity <80%, non-condensing

Contact your local Waters representative if you need further advice regarding storage conditions.

Unpacking and Moving


The instrument is delivered in several palletized cartons and crates. Their sizes may vary
dependent on instrument specification and optional accessories.

It is a warranty condition that the shipping crates are unpacked only when the Waters engineer is
present.

If possible, provide an electrical screwdriver or drill with screwdriver attachment to assist with
opening the crates. At the end of the installation, it is the customer’s responsibility to dispose of
the crates and packaging.

It is essential that the instrument is not bumped or jolted during unpacking or any subsequent
transport. If the instrument needs to be transported across an uneven surface, the instrument
must be carried on a forklift truck or trolley.

Doorways must be at least 600 mm (24 in.) wide. Elevators and corridors (including corners) must
be sufficiently wide for maneuvering of the instrument. Special handling arrangements may be
necessary if access to the laboratory is via a staircase.

715000574, REV. E PAGE 5 OF 24


Lifting Equipment
Once unpacked, the instrument weights are approximately as shown in Table 1:

Table 1: Instrument weights

GCT 100 kg (220 lbs)

Data system
50 kg (110 lbs)
(computer, monitor and optional printer*)

Rotary Pump 22 kg (50 lbs)

Total Weight 172 kg (380 lbs)

Warning: The instrument must only be lifted using lifting equipment capable of raising the
instrument's weight safely. The instrument must not be lifted manually.

Important: It is essential that you provide suitable equipment for lifting the instrument. The
installation cannot be implemented unless this equipment is made available.

Do not attempt to unpack the shipping crate until the Waters engineer is present.
The engineer will require assistance lifting and positioning the equipment.

Caution: Do not attempt to lift the instrument by the front moulded cover, the probe, the GC
interface or the source housing.

A forklift truck or A-frame hoist is recommended for lifting and transporting the instrument.
The instrument is fitted with a lifting harness, which must be used to lift the instrument from the
shipping crate onto the bench.

As a general guide, before undertaking any lifting, lowering or moving of the instrument:
• Assess the risk of injury.
• Take action to eliminate the risk.

If some risk still exists:

• Plan the operation in advance and in conjunction with the Waters engineer when they
arrive on site.
• Use trained personnel where necessary.
• Adhere to appropriate country and/or company regulations.

715000574, REV. E PAGE 6 OF 24


Space Requirements

Instrument
The GCT mass spectrometer has a width of 567 mm (22.3 in), a length of 790 mm (31.3 in), and
a height of 450 mm (17.7 in). The instrument is mounted on four supporting feet.

The GCT may be installed on any flat surface. Allow the following minimum clearances around the
instrument for service access and ventilation (Figure 1):

• 200 mm (8 in) at the back or the front of the instrument (to allow the instrument to be
pulled forward), for servicing the electronics unit.
• 200 mm (8 in) behind the bench to allow for the bend radius of the vacuum pipes.
• 250 mm (10 in) on the right hand side of the instrument if a GC is fitted.
• 450 mm (18 in) between the GC and the GCT instrument if a solids probe is to be used.

A suggested bench layout for the GCT, data system, and GC is shown in Figure 1.
600 mm (23.6 in.)

200 mm
(7.9 in.)

200 mm (7.9 in.)


Rotary pump Bend radius for hoses

Data System

567 mm
750 mm (22.3 in.)
(29.5 in.)

200 mm (7.9 in.)

1500 mm (59.0 in.) 1380 mm (54.3 in.)

250 mm (9.8 in.)


Or
450 mm (17.7 in.) With probe
Figure 1 - Suggested Bench Layout for the GCT System

Rotary Pump
The rotary pump should be positioned either behind or underneath the instrument, and within 1 m
(39 in) of the rear of the instrument chassis. It is recommended the rotary pump be elevated 150
to 200 mm (6 to 8 in) above the floor to provide easy access during routine maintenance (e.g.
changing the pump oil).

GC System
Ensure that there is sufficient space to the right of the GCT to allow the GC to be pulled clear of
the GC interface line.

715000574, REV. E PAGE 7 OF 24


Data System
The data system may either be positioned beside the mass spectrometer or placed on a separate
bench (available as an option).

The data system must be located within 5 m (16 ft) of the mass spectrometer to enable the
communication cables to be fitted. The communication and power cables supplied with the
instrument, data system and the rotary pump are all 2 m (6.5 ft) long.

Warning: To avoid damage to and/or risk of electric shock and fire,


the data system and any ancillary equipment must not
be exposed to dripping or splashing liquids nor should
objects filled with liquid, such as solvent bottles, be
placed on them.

Connections INSIGHT® Installation Requirements


Installation of the Waters Connections INSIGHT software (Intelligent Services that provide
real-time system monitoring and notification), requires the following:

• An active Internet connection (direct, or through a firewall or proxy server)

• SSL (secure sockets layer) port 443 to be activated

Note: Connections INSIGHT software directly communicates with the Waters Enterprise
Server using 128-bit data encryption. For further information see Connections
INSIGHT Frequently Asked Questions (p/n 720001131EN).

Electrical Safety
The GCT complies with the International Safety Standard IEC 61010-1:2001 and meets the
European Low Voltage Directive 2006/95/EC by means of European Harmonized Standard
EN 61010-1:2001.

For installations in Australia and New Zealand, the building installation must comply with AS3000:
electrical installations for Australia and New Zealand.

The instrument is suitable for use in environments categorized as Pollution Degree 2 and
Over-voltage Category II.

Power Requirements

Power Supply
The GCT requires two grounded (earthed) power sockets, one for the GCT and one for the rotary
pump. The maximum current consumption of the GCT is 6.0 A. The power supply sockets should
be located within 2 m (6.5 ft) of the instrument. Do not position the equipment so that it is
difficult to disconnect the mains cable.

For customer-supplied GCs, an outlet conforming to the Manufacturer’s requirements must be


supplied. If the GC is ordered from Waters, a fast heating HP6890 is supplied, which requires
220 to 250 V, 50 to 60 Hz at 13 A.

715000574, REV. E PAGE 8 OF 24


The data system typically requires two power sockets located adjacent to the Xevo TQD for the
MassLynx PC and monitor. Further outlets may be required for optional equipment, such as a printer.
Do not position the equipment so that it is difficult to disconnect the mains cable.

Important: Mains voltage fluctuations must not exceed ±10%.

The power requirements for the equipment are summarized in Table 2:

Table 2: Summary of Power Requirements

Maximum Supply Fuse /


Nominal Typical Power Power
Equipment Operating Circuit-Breaker
Voltage Range Consumption Connection
Voltage Range Rating

100 to 240 V IEC 60320 C14


GCT 90 to 264 V 13 to 16 A 1.2 kW
50/60 Hz receptacle

110 to 120 V
100 to132 V 13 to 16 A 300 W
RV3 Rotary 60 Hz IEC 60320 C14
Pump 220 to 240 V receptacle
180 to 253 V - -
50 Hz

220 to 240 V IEC 60320 C20


GC HP6890 180 to 253 V 13 to 16 A 3.0 kW
50 Hz receptacle

Important: Voltage supply stability is critical for instrument operation, the power supply
voltage must fall within the ranges specified in Table 2 at all times to avoid the risk
of instrument failure.

The supplies must be fused or fitted with circuit-breakers of the specified ratings, in accordance
with local regulations.

The mains supply must not have brown-outs/surges greater than ±10%, and must not exceed the
specified maximum operating range, for more than 0.3 sec. Transient voltage drops to half
nominal voltage or less must have a duration of less than 20 msec.

On pump start-up, currents of up to 32 A may be drawn for up to a second, due to the initial
pump loading. It is recommended that time delay fuses and circuit-breakers are used to prevent
nuisance tripping.

The backing pump is normally in continuous operation; it is recommended that the system be
installed such that the supply cannot be inadvertently switched off.

It is also recommended that additional protection is provided for the instrument by means of:

• Residual Current Devices (RCD’s) for UK and European markets


• Ground Fault Circuit Interrupters (GFCI’s) for the Rest of the World

715000574, REV. E PAGE 9 OF 24


Electrical Transformers
If there is a possibility that the supply voltages will not meet the specified operating range under all
conditions, a transformer must be used to change the primary supply voltage to the specified range.
Mains conditioners/stabilizers are also available as an optional accessory. Contact Waters with
advance notification if power supply problems are likely to be experienced and for additional advice.

In the case of instruments fitted with a transformer, the RCD/GFCI must be fitted on the primary
(supply) side of the transformer.

If your order includes a nitrogen generator and the mains supply is known to run continuously at
voltages less than 220 V, Waters and Peak Scientific recommend fitting one of the following
transformers between the generator and mains supply.

Caution: Running nitrogen generators continuously at voltages less than 220 V is not
recommended and extended periods at these extremes can affect the operation
and life of the generator.

Table 3: Nitrogen Generator Transformer Options

Model Type 06-3100 06-3110

View

208 volt AC to 230 volt AC 115 volt AC to 230 volt AC


Description
boost transformer boost transformer

System Plug Options


The system plug options are shown in Table 4. The instrument is shipped with the plugs that were
requested at the point of order. The user must provide appropriate sockets for the relevant type of
plug used. If the available sockets are incompatible with the plugs supplied, the customer must
supply appropriate cord sets for the instrument and pumps. The cord sets must comply with local
regulations.

Computer equipment is typically rated at 100 to 120 V / 220 to 240 V, 50/60 Hz. In some cases,
it may be necessary to set the appropriate voltage using a voltage selector switch before
connecting the equipment to the power supply. For full details, refer to the instructions provided
with the equipment.

Note: If ancillary equipment is to be installed (for example, compressors) additional


power outlets, possibly requiring 3-phase supplies, may be needed. Such
supplemental needs must be confirmed with the local Waters agent prior to the
start of the installation.

715000574, REV. E PAGE 10 OF 24


Table 4: Power Cords Supplied by Waters

Plug Option Plug Type System Components

US/Canada (125 V)

5-15P Data System


(UL817 and CSA C.22.2) Rotary Pump

US/Canada (250 V)

L6-15P Mass Spectrometer


(UL817 and CSA C.22.2) Nitrogen Generator

UK

3-pin
(BS1363)

Europe

2-pin
(CEE7) Data System
Mass Spectrometer
Rotary Pump
Denmark Nitrogen Generator

3-pin
(Afsnit 107-2-D1)

Australia

3-pin
(AS/NZS 3112)

China

GB2099
Data System
(10 A version)

China
Mass Spectrometer
GB2099
Rotary Pump
(16 A version)
Nitrogen Generator

715000574, REV. E PAGE 11 OF 24


Uninterruptible Power Supply
To prevent instabilities in local mains power impacting system reliability and performance, Waters
recommends the use of an uninterruptible power supply (UPS). In support of this recommendation,
Waters supplies UPS units that have been specifically configured and evaluated for use with
Waters MS systems. Your local Waters field sales representative can provide further details.

These UPS units step up single-phase line voltage to 230 V AC, provide power conditioning and
protection for the MS system.

For North America, the UPS system requires one L6-30 (30 amp) wall socket. In other areas, the
UPS system will typically connect to your laboratory mains power using the standard MS
instrument power cord and wall socket required for your system. See Table 2 and Table 4.

305 mm
838 mm (33 in.) (12 in.)

813 mm
(32 in.)

Side View Front View

Figure 2 - Approximate maximum dimensions of the UPS

715000574, REV. E PAGE 12 OF 24


Water Supplies
Cooling water must be provided, either from a reliable mains water supply, with the outlet going
to a suitable drain, or from an optional recirculating chiller.

One water inlet and one water outlet are required for the instrument. Reinforced flexible hose
10 mm ID should be used. A 5 m (16 ft) length is supplied with the instrument. The mains water
supply requirements are as follows:

Table 5: Water Supply Requirements

Parameter Value

Inlet Temperature 15 to 20 °C (59 to 68 °F)

Flow Rate 1 L/min at 20 °C (68 °F)

If mains water supplies are used, suitable in-line filters are required to remove particulate matter
and prevent blockage of the water pipes.

The water may be supplied by a recirculating chiller with the specifications shown in Table 6.

Table 6: Chiller Specifications

Parameter Value

Heat Dissipation into System 320 W at 20 °C (68 °F)

Temperature Stability ± 2 °C (± 3.6 °F)

Minimum Reservoir Volume 2L

Minimum Supply Pressure 10 psi (outlet at atmospheric pressure)

Maximum Supply Pressure 40 psi

These specifications assume that the outlet water temperature is no more than 30 °C (86 °F).

Note: Do not use an inlet water temperature of less than 15 °C (59 °F), as this may lead
to the formation of condensation on exposed pipe work.

Note: Operation above 2000 m (6500 ft) altitude may adversely affect the cooling of the
system.

715000574, REV. E PAGE 13 OF 24


Environmental Requirements
Safety Recommendations
The user should be aware of potential chemical hazards. In particular, the user should assess the
risks associated with gases and solvents which could be vented into the laboratory.

Warning: The active exhaust vent must provide a minimum vacuum of 2 millibar
below atmospheric pressure (negative pressure). It must be capable of
supporting a maximum instrument exhaust gas load of 2000 L/hour.

Warning: Exhaust venting must comply with all local safety and environmental
regulations. The ANSI/AIHA Z9.2-2001 standard for “Fundamentals
governing the design and operation of local exhaust ventilation systems”
provides guidance on compliant exhaust systems.

Positioning
It is recommended that the instrument be installed in an air-conditioned laboratory, in a draft free
position, away from excessive amounts of dust and out of direct sunlight. Air-conditioning units
should not be positioned directly above the mass spectrometer.

Ventilation
The maximum overall heat dissipation into the room from the instrument and pump is
approximately 1.2 kW. This figure does not take into account ancillary equipment such as GC
systems. Air conditioning systems may have to be installed or upgraded to accommodate
additional heat load into the room when these systems are installed.

Caution: Waters recommends using a forced air exchange system in the laboratory; refer to
local safety regulations for examples of exchange rates required for hazardous
substances.

Temperature
The ambient temperature range required for normal operation is 15 to 30 °C (59 to 86 °F).

The optimum temperature range is 19 to 22 °C (66 to 72 °F).

Short-term (1.5 h) variations should be no more than ±2 °C (3.6 °F).

The ambient temperature range for operation must not exceed 5 to 40 °C (41 to 104 °F),
otherwise the performance will be reduced and the instrument may fail.

Humidity
The relative humidity must not exceed 70% for temperatures up to 31 °C (88 °F).

At higher temperatures, the maximum humidity allowed decreases linearly to 50% at 40 °C


(104 °F).

715000574, REV. E PAGE 14 OF 24


Altitude
The recommended maximum operating altitude is 2000 m (6500 ft).

Vibration
The instrument should not be placed close to heavy machines such as compressors and
generators, which may generate excessive floor vibration.

Magnetic Fields
The instrument must be positioned away from magnetic fields of greater than 10 Gauss, such as
those generated by NMR spectrometers or magnetic sector mass spectrometers.

Radio Emissions
The instrument should not be placed within a Radio Frequency (RF) field of greater than 1.0 V/m.

Possible sources of RF emission include RF-linked alarm systems, Local Area Networks (LANs),
mobile telephones and hand-held transmitters.

Gases and Regulators

Soft Vent Gas


A supply of clean, dry, inert gas at 0.35 bar (5 psi) is recommended for venting the instrument.
This will ensure fast pump-down and conditioning times.

Compressed Air
Compressed air at 7 bar (100 psi) is required for operating the instrument.

GC Carrier Gas
Caution: Ensure that there are no soldered or brazed joints in the line, as these may result
in contamination of the instrument with tin or lead oxide. Any joints in the nitrogen
line must be compression fittings.

Dry ultra high purity helium (99.999% or better, with less than 1 ppm H2O) is required. A Supelco
OMI2 purifier fitted with suitable shut-off valves is recommended. This may improve performance
with some analytes and increase column life.

Gases must be connected using clean 1/8 in chemically cleaned copper or medical grade stainless
steel tubing (not supplied) and checked for leaks under pressure. All gases must be regulated up
to 7 bar (100 psi) maximum; the pressure depends on the GC and current application.

715000574, REV. E PAGE 15 OF 24


CI Reagent Gas
Caution: Ensure that there are no soldered or brazed joints in the gas line, as these may
result in contamination of the instrument with tin or lead oxide. Any joints in the
nitrogen line must be compression fittings.

For CI operation, methane, ammonia, and isobutane are recommended. Methane is required for
the installation procedure. Gases should be of a high purity (≥99.9%).

Gases must be connected using clean 1/8 in chemically cleaned copper or medical grade stainless
steel tubing (not supplied) and checked for leaks under pressure. All gases must be regulated at
0.7 bar (10 psi), [2.1 bar (30 psi) maximum]. Stainless steel pipe is required if ammonia is used.

A needle shut-off valve (Swagelok SS-OVS2 or similar) between the CI gas regulator and the CI
gas tubing is highly recommended to protect the diaphragm of the regulator when purging the
external CI gas inlet.

For additional GC options, such as Cryo cooling and FID, additional gases and regulators may be
required. Please contact your Agilent representative for details.

Exhaust Outlets
Note: Refer to the exhaust warnings in the Environmental Requirements section on
page 14 for additional exhaust information.

Rotary Pump Exhaust


The rotary pump exhaust gases must be vented to the atmosphere outside the laboratory via a
user-supplied fume hood or industrial vent. The exhaust may be connected to an existing
laboratory vent carrying gases from other sources.

Five meters (16 ft) of 12 mm ID PVC tubing is supplied. If this length is insufficient, the user must
supply an adapter and tubing with an internal diameter of at least 51 mm (2 in.) for the extra
distance to the vent point.

Note: The fume hood/industrial vent must be equipped with an extraction fan system to
enable adequate displacement of the exhaust gases.

715000574, REV. E PAGE 16 OF 24


Test Samples

Warning: Hazardous samples must be handled with care and in a manner that
conforms to the manufacturers’ guidelines.

Test samples are required for verifying the operation of instruments at the time of installation;
they are also used for routine operations such as tuning and mass calibration. The compounds that
are used for testing the GCT are listed in Table 7.

Table 7: Samples required for system testing

Ionization probe*
Ionization Mode

Desorption

Desorption
Ionization

Ionization

Chemical
Chemical
Electron

probe*
Mode*

Mode*
Field

Field
Sample Supplier Code

Heptacosa (FC 43) Sigma H5262     

Hexachlorobenzene Aldrich 171050 

Benzophenone Sigma B3634 

Octafluoronapthalene Aldrich 248061 

2,4,6 Tris(trifluoromethyl)-1,3,5-
Fluorochem 001549   
triazine

Chloropentafluorobenzene Fluorochem 002833   

Hexadecane Aldrich H6703 

Caffeine Sigma C0750 

Cholesterol Aldrich 362794 

Xylene Aldrich 277642  

Acetone Aldrich 270725  

Pentafluorobenzene Fluka 76710  

Hexafluorobenzene Aldrich 302856  

Methyl stearate Sigma S5376 

Perfluorotrimethylcyclohexane Fluorochem 007171  

* Option

Note: The samples listed in Table 7 are not supplied with the instrument and should be
purchased by the customer prior to installation. Contact your local Water’s Sales
representative if you need assistance obtaining the necessary compounds
(www.waters.com).

Note: If your laboratory practices require full sample certification documentation, Waters
Analytical Standards and Reagents provide ready-to-use reference materials and
reagents that are fully traceable and certified (www.waters.com).

Important: The Waters engineer will not be carrying test samples to the installation.

715000574, REV. E PAGE 17 OF 24


Solvents
GC-grade hexane is required to dissolve and dilute the samples.

Note: The hexane must be supplied by the customer.

Facilities for making up test samples must be made available.

Cleaning Equipment
An ultrasonic bath is required for the routine cleaning of instrument parts. The bath must be at
least 300 mm x 150 mm x 100 mm deep (12 in. x 6 in. x 4 in.).

Caution: Surfactants must not be used for cleaning glassware or other components. Refer to
®
the document Controlling Contamination in Ultra Performance LC /MS and
HPLC/MS Systems (p/n 715001307), located in the Support area of the Waters
website (www.waters.com).

Surfactant-free glass vessels are required in which to place instrument components for cleaning.
These vessels must be made available for use at the time of installation. The vessels must have a
diameter of at least 120 mm (5 in.) and be approximately 120 mm (5 in.) high.

Summary of Fittings
Table 8 shows a summary of the waste and gas connections for the installation of the GCT.

Table 8: Summary of the Fittings Required

Fittings on the Items Supplied Items to be supplied


system with instrument by the customer
Rotary Pump 5 m (16 ft) PVC tube,
12 mm OD tail pipe Industrial vent or fume hood.
Exhaust 12 mm ID
Connection to clean water supply and
5 m (16 ft)
return.
Water Supply 2 x 10 mm OD nozzles reinforced hose,
2 x 10 mm OD nozzles required
10 mm ID
if using mains water.
Compressed Air 4 mm push-in 5 m (16 ft) hose, Connection to
Supply fitting 4 mm OD compressed air supply.
4 mm push-in 5 m (16 ft) hose, Connection to soft vent gas supply at
Inert Soft Vent Gas
fitting 4 mm OD 1 bar (14 psi).
1
1 /8 inch OD stainless steel or copper
/8 inch fitting
GC Oven - tubing to regulated gas supply.
(Swagelok type)
Regulator adapter should be 1/8 inch.
1
/8 inch OD stainless steel or copper
1 tubing to regulated gas supply.
CI Option /8 inch fitting
- Regulator adapter should be 1/8 inch.
Gas Connection (Swagelok type)
(Needle shut-off valve also
recommended).
1
1 /8 inch OD stainless steel or copper
FID Option /8 inch fitting
- tubing to regulated gas supply.
Gas Connection (Swagelok type)
Regulator adapter should be 1/8 inch.

715000574, REV. E PAGE 18 OF 24


GCT Site Preparation Checklist
This checklist must be completed and returned to Waters when all the amenities are available.

Note: If any items are on order, please indicate this on the checklist and include the
anticipated arrival date.

Note: It is the customer’s responsibility to ensure that all the correct laboratory supplies
are present. If you need any additional information or have difficulties acquiring
parts or samples, please contact your local Waters Sales representative.

Access (see page 5)


The instrument will be located on the ground floor/basement/___ floor (delete as appropriate) ...... 
All elevators, staircases, corridors and doorways through which the instrument must pass are
adequate to allow easy access to the laboratory ....................................................................... 
Bench/Floor Space (see page 7)
Adequate bench or floor space is available for the system .......................................................... 
Connections INSIGHT® Installation Requirements (see page 8)
If you are planning to install Waters Connections INSIGHT software, an Internet connection is
available .............................................................................................................................. 
Power Supply (see page 8)
An appropriate number of outlets are available and they meet the stipulated power requirements ..... 
Water Supply (see page 13)
The local water supply meets the stated conditions and will be used ............................................ 
A water chiller will be used ..................................................................................................... 

Chiller type: ___________________________________

Positioning / Ventilation (see page 14)


There is no direct air conditioning flow onto the instrument ........................................................ 
Temperature (see page 14)
The room temperature is always between 5 and 40 °C (41 to 104 °F) and normally
between 15 and 30 °C (59 to 86 °F) ........................................................................................ 
Humidity (see page 14)
The humidity is as specified, and never exceeds 70% ................................................................ 
Altitude (see page 15)
The site is below 2000 m ....................................................................................................... 

715000574, REV. E PAGE 19 OF 24


Floor Vibration (see page 15)
The site is free from known vibration ....................................................................................... 
Magnetic Fields (see page 15)
The site is free from magnetic fields of greater than 10 Gauss .................................................... 
Radio Emissions (see page 15)
The RF field strength is less than 1 V/m ................................................................................... 
Gases and Regulators (see page 15)
Dry, ≥99.999% purity helium gas is available, regulated at 7 bar (100 psi) with a
1

/8 in fitting for GC/MS ...........................................................................................................

Methane gas is available, regulated at 2 bar (30 psi) with a / in fitting for all CI options .............. 
1
8

Needle shut-off valve for CI options (recommended) is available ................................................. 

Compressed air supply is available, at 7 bar (100 psi) with a fitting for a 4 mm hose (supplied) ..... 

Clean, dry, inert gas is available, at 0.35 bar (5 psi) with a fitting a for a 4 mm hose
(supplied) ............................................................................................................................ 
Rotary Pump Exhaust (see page 16)
A suitable outlet is available for the rotary pump exhaust .......................................................... 
GC System (see page 7)
The GC was purchased with the GCT mass spectrometer ........................................................... 
or

The GC will be supplied by the customer .................................................................................. 


GC make and model: _____________________________

The GC system is already on site and commissioned ................................................................. 


or

The GC system is scheduled to be commissioned on: dd______ / mm ______ / yy______ ............ 

715000574, REV. E PAGE 20 OF 24


Ancillary Equipment
If you plan to use any other equipment with the system (e.g. Gilson Autosampler; UV Detector),
please give details below.

Already
Make / Type Model To be commissioned on
commissioned

Test Samples (see page 17)


All samples required for the installation are available ................................................................. 
Solvents (see page 18)
Solvents and a balance are available ....................................................................................... 
Sample Preparation Equipment (see page 18)
Sample preparation equipment, as specified in this document, is available ................................... 
Cleaning (see page 18)

An ultrasonic bath is available ................................................................................................
Vessels for cleaning components are available .......................................................................... 

715000574, REV. E PAGE 21 OF 24


I confirm all supplies are now available and all specified environmental conditions have
been met*.

During the installation, the user intends to be available for demonstration and training by the
Waters engineer:

At all times ........................................................................................................................... 

Approximately _______% of the time ...................................................................................... 

Not at all .............................................................................................................................. 

During the likely period of installation, the following dates are NOT convenient:

___________________________________________

Signed: ___________________________________________

*Important: If an authorized Waters service engineer arrives on site to begin installation work
and can not complete the installation due to lack of facilities (i.e. lifting equipment,
power, water, test samples, laboratory readiness), costs incurred will be charged to
the customer.

715000574, REV. E PAGE 22 OF 24


Please complete the following sections in block letters:

Name ________________________________________________

Position ________________________________________________

Organization ________________________________________________

Street ________________________________________________

City ________________________________________________

ZIP/Postcode ________________________________________________

Country ________________________________________________

Telephone ________________________________________________

Fax ________________________________________________

E Mail ________________________________________________

Important: The installation of your system cannot begin until pages 19 through 24 of this
document have been fully completed and returned to the Mass Spectrometer Sales
Support Representative at your local Waters office.

715000574, REV. E PAGE 23 OF 24


Applications Survey
As part of our commitment to provide greater customer service, we have found it necessary to
obtain a little more information concerning our user base.

We would be grateful if you could take the time to complete the following questions to provide us
with some information about how the instrument will be used.

This information will enable us to inform you of relevant current application notes and seminars
and allows us to identify common interest groups so that we can promote cross transfer of
information between customers.

What is your scientific field?


(e.g. pharmaceutical, environmental, general, etc.)

_______________________________________________________________________

_______________________________________________________________________

Which classes of compounds will be analyzed?


(e.g. carbohydrate, peptides, pesticides, etc.)

_______________________________________________________________________

_______________________________________________________________________

What is your application area?


(e.g. quantitation, purity analysis, structural determination, etc.)

_______________________________________________________________________

_______________________________________________________________________

Our sales team often requires reference sites for specific applications.
Would you be willing to be used as a contact reference site for prospective customers?

_______________________________________________________________________

_______________________________________________________________________

715000574, REV. E PAGE 24 OF 24

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