Product Manual For Cymoxanil + Mancozeb Wettable Powder According To IS: 15601:2005

PM/ IS 15601/1/June 2019
PRODUCT MANUAL FOR

CYMOXANIL + MANCOZEB WETTABLE POWDER
According to IS: 15601:2005
This Product Manual shall be used as reference material by all Regional/Branch Offices & licensees
to ensure coherence of practice and transparency in operation of certification under Scheme-I of
Bureau of Indian Standards (Conformity Assessment) Regulations, 2018 for various products. The
document may also be used by prospective applicants desirous of obtaining BIS certification
licence/certificate.
1. Product : IS 15601:2005
CYMOXANIL+MANCOZEB WETTABLE
Title :
POWDER
No. of Amendments : NIL
2. Sampling Guidelines:
Cymoxanil technical shall confirm to IS 15600
Mancozeb technical shall confirm to IS 8707 Each
a) Raw material : lot shall be accompanied with test certificate from
manufacturer, or a sample shall be tested in
house/independent lab
b) Grouping guidelines : NA
c) Sample Size : 500 gm.
3. List of Test Equipment : Please refer ANNEX – A
Scheme of Inspection
4. : Please refer ANNEX – B
and Testing
5. Possible tests in a day :
i) Physical tests (Description Cl. 3.2.1)
ii) Sieving requirement (Cl. 3.2.2)
iii) Wettability (Clause 3.2.4)
iv) Acidity (Cl. 3.2.2)
v) Alkalinity (Cl. 3.3.3)
6. Scope of the Licence :
Licence is granted to use Standard Mark as per IS 15601:2005 with the following
scope:-
Name of the product CYMOXANIL……%+MANCOZEB…..% WETTABLE

POWDER
BUREAU OF INDIAN STANDARDS

Manak Bhawan, 9, Bahadur Shah Zafar Marg,
New Delhi – 110002
PM/ IS 15601/1/June 2019
Annex –A
TO PRODUCT MANUAL FOR
List of Test Equipment
Sr. No. Test Equipment Tests used in with Clause

Reference
1 Visual
Description as per Cl 3.2.1
2 Test Sieve (as per IS 460 (Part 1) Sieving requirement (3.2.2)

Pressure Assembly
Beaker, Rubber Hose
Weighing balance
3 Beaker Suspensibility (3.2.3)
Pressure Assembly
Graduated Cylinder
Glass tube,
Calcium Chloride anhydrous
Magnesium Chloride Hexahydrate
Balance
Waterbath
4 Beaker Wettability (3.2.4)
Weighing balance
Calcium Chloride anhydrous
Magnesium Chloride Hexahydrate
5 a)High Performance Liquid Chramatograph, equipped Determination of Cymoxanil
with a constant flow pump, -constant content., (Cl. 3.3.1)
temperature column compartment, sample injector
capable of injecting 25 pl aliquots, a 254 m wavelength
Ultraviolet detector. And a recorder (digital integrator or
other data handling device) is used for this
determination.
b)Analytical balance
c) Microliter syringe 25 microliter
D) Filtering apparatus for sample and standard solution.
e) Ultrasonic bath.
f) Standard glassware.
g) Acetonitrile, HPLC grade.
h) HPLC Grade Water
i)Acetanilide of known purity.
j) Cymoxanil of known purity.
k) Ortho Phosphoric Acid, HPLC grade,
85 percent.
PM/ IS 15601/1/June 2019
6 a) Balance (analytical) 0.1mg Determination of Mancozeb
b) Carbon disulphide assembly.(Figures 1,2,3 and 4 of content.,(Cl. 3.3.1)
IS).
c) Glass vial (Dia 8-12 mm, height 20-25 mm)
d) Ware sirculation system (as per A-2.2.3 of IS)
e) Vacuum pump.pump.
f) Acetic acid , 30 % solution.
g) Iodine, 0.1 N solution.
h) Lead acetate, 10 percent solution.
i) Phenolphthalein indicator – 0.5 percent ethanolic
solution.
j) Potassium hydroxide, 2 N methanolic solution
k) Starch indicator
l) Sulphuric acid, 1.1 N solution
7 a) Methyl red indicatorsolution-aqueous - one percent Test for acidity.,(Cl. 3.3.2)

( mlu ).
b) Bromocresol purple indicator solution - one percent
(m/v) in ethyl alcohol.
c) Standard sodium hydruxide solution - 0·05 N
d) Standard hydrochloric acid - 0·05 N.
8 a) Methyl red indicater solution - aqueous, one Test for alkalinity.,(Cl. 3.3.3)
percent ( mlo ).
b) Bromocresol purple indicator solution - one percent
(mlv) in ethyl alcohol.
c) Standard hydrochloric acid - 0·05 N.
d) Standard sodium hydroxide solution - 0·05 N.
PM/ IS 15601/1/June 2019
ANNEX - B
TO PRODUCT MANUAL FOR
(SCHEME OF INSPECTION AND TESTING)
1. LABORATORY - A laboratory shall be maintained which shall be suitably equipped (as per the
requirement given in column 2 of Table 1) and staffed, where different tests given in the
specification shall be carried out in accordance with the methods given in the specification.
1.1 The manufacturer shall prepare a calibration plan for the test equipments.
2. TEST RECORDS – The manufacturer shall maintain test records for the tests carried out to
establish conformity.
3. PACKING AND MARKING – The Standard Mark, as given in the Schedule of the licence,
shall be printed/stencilled on each container of Cymoxanil +Mancozeb Wettable Powder, provided
always that the product so marked conform to every requirement of the specification.
3.1 Packing and marking shall be done as per the provision of IS 15601:2005. In addition, the
following details shall be mentioned on each container/package:-
a) BIS Licence No. CM/L--------.

b) BIS website details i.e. –“For details of BIS certification please visit www.bis.gov.in”.
4. CONTROL UNIT – For the purpose of this Scheme, the entire quantity of
Cymoxanil+Mancozeb Wettable Powder taken from the same consignment of raw materials, finally
blended in a blender at a time in one operation shall constitute one control unit.
5. LEVELS OF CONTROL - The tests as indicated in column 1 of Table 1 and the levels of
control in column 3 of Table 1, shall be carried out on the whole production of the factory which is
covered by this plan and appropriate records maintained in accordance with paragraph 2 above.
5.1 All the production which conforms to the Indian Standards and covered by the licence shall be
marked with Standard Mark.
6. REJECTIONS – Disposal of non-conforming product shall be done in such a way so as to

ensure that there is no violation of provisions of BIS Act, 2016.
PM/ IS 15601/1/June 2019
Table 1 (Levels of Control)

(Scheme of Inspection and Testing)
(1) (2) (3)

Test Details Test equipment Recommended Levels of Control
Cl. Requirement Test Methods requirement No. of Sample Frequency Remarks
R: required (or)S:
Sub-contracting
Reference Clause permitted
3.2.1 Description 3.2.1 IS 15601 R One Each Control Unit
3.2.2 Seiving Requirement 11.1 IS 6940 R One Each Control Unit
3.2.3 Suspensibility 11.2 IS 6940 R One Each Control Unit
3.2.4 Wettability 11.4 IS 6940 R One Each Control Unit
3.3.1 Cymoxanil content Annex A IS 15600 R Two Each Control Unit
Mancozeb content Annex A IS 8707 R Two Each Control Unit
3.3.2 Acidity 11.3.2 IS 6940 R One Each Control Unit
3.3.3 Alakalinity 11.3.3 IS 6940 R One Each Control Unit
Note-1: Sub- contracting is permitted to a laboratory recognized by the Bureau or Government laboratories empanelled by the Bureau
Note-2: The control Unit and levels of control as decided by the Bureau are obligatory, to which the licensee shall comply with.
OR
Levels of control given in column 3 are only recommendatory in nature. The manufacturer may define the control and submit his own levels of
control in column 3 with proper justification for approval by BO Head.

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PM/ IS 15601/1/June 2019

PRODUCT MANUAL FOR

Name of the product CYMOXANIL……%+MANCOZEB…..% WETTABLE

BUREAU OF INDIAN STANDARDS

Sr. No. Test Equipment Tests used in with Clause

2 Test Sieve (as per IS 460 (Part 1) Sieving requirement (3.2.2)

7 a) Methyl red indicatorsolution-aqueous - one percent Test for acidity.,(Cl. 3.3.2)

a) BIS Licence No. CM/L--------.

6. REJECTIONS – Disposal of non-conforming product shall be done in such a way so as to

Table 1 (Levels of Control)

(1) (2) (3)

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