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Optical Mineralogy: Lab 14 - Fall, 2012 Biaxial Interference Figures

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Optical Mineralogy

Lab 14 – Fall, 2012


Biaxial Interference Figures

1
Biaxial Sign: Bxa Figures
• To determine the optic sign of a biaxial
mineral from a BXA figure, position the
isogyres so that the melatopes are in the NE
and SW quadrants
• There should be an area near the melatopes
that shows a 1o gray interference color
• Observe this area as you insert the 550nm
or 1o red compensator

2
Biaxial Sign: Bxa Figures
• If the 1o gray area in
region between the
two isogyres turns
yellow, the mineral is
biaxial positive
• If the 1o gray area
inside of both the
isogyres turns yellow
the mineral is biaxial
negative
3
Biaxial Sign: Centered OA
Figures
• Optic axis figures probably provide the easiest
method for determination of optic sign because
grains with an orientation that would produce an
OA figure are perhaps the easiest to find
• Place the isogyre so that the inside of the isogyre
is in the NE quadrant
• Find the area that shows 1o gray close to the
melatope
• Observe this area as the 550 nm compensator plate
is inserted
4
Biaxial Sign: Centered OA
Figures
• If the area outside of
the isogyre turns
yellow, the mineral is
biaxial positive
• If the area inside the
isogyre turns yellow,
the mineral is biaxial
negative

5
Biaxial Sign: Off-Centered
Bxa or OA Figures
• Probably even easier to locate are off-
centered OA or BXA interference figures
• Position the isogyre so that it fits best in
either the NE or SW quadrant
• Observe the gray area near the melatope and
note the color change on insertion of the
550 nm compensator

6
Biaxial Sign: Off-Centered
Bxa or OA Figures
• If the gray area outside
the isogyre turns
yellow, the mineral is
biaxial positive
• If the gray area outside
isogyre turns blue and
the gray area inside
the isogyre turns
yellow, the mineral is
biaxial negative
7
Estimation of 2V
• Precise determination of 2V can only be
made by determining the 3 principal
refractive indices of the mineral
• 2V can be estimated from Bxa and OA
figures using the diagrams shown here

8
2V Estimation: Bxa Figure
• For a BXA figure the distance between the
melatopes is proportional to the 2V angle
• To estimate the 2V from a BXA figure, it is
necessary to know the numerical aperture (N.A.)
of the objective lens used to observe the
interference figure
• The microscopes in our labs have an N.A. of
between 0.65 and 0.85

9
2V Estimation: Bxa
Figure
• The diagram shown here
gives a visual estimate of the
2V angle for objective lenses
with these two values of N.A.
for a mineral with a b
refractive index of 1.6

10
2V Estimation: Bxa Figure
• Remember that if the 2V is 0o the mineral is
uniaxial, and would thus show the uniaxial
interference figure
• The separation of the isogyres or melatopes
increases with 2V and the isogyres
eventually go outside of the field of view
for a 2V of 50o with the smaller N.A., and
about 60o for the larger N.A
11
2V Estimation: Bxa Figure
• Since the maximum 2V
that can be observed for a
Bxa figure depends on the
b refractive index, the
chart shown here may be
useful to obtain more
precise estimates if the b
refractive index is known
As b increases, the maximum or can be measured
observable 2V decreases

12
2V Estimation: OA Figure
• 2V estimates can be made
on an optic axis figure by
noting the curvature of the
isogyres and referring to
the diagram shown here
• Note that the curvature is
most for low values of 2V
and decreases to where the
isogyre essentially forms a
straight line across the
field of view for a 2V of
90o
13

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