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WO2009080974A3 - Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles - Google Patents

Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles Download PDF

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Publication number
WO2009080974A3
WO2009080974A3 PCT/FR2008/052251 FR2008052251W WO2009080974A3 WO 2009080974 A3 WO2009080974 A3 WO 2009080974A3 FR 2008052251 W FR2008052251 W FR 2008052251W WO 2009080974 A3 WO2009080974 A3 WO 2009080974A3
Authority
WO
WIPO (PCT)
Prior art keywords
mineral nanoparticles
polymer material
transparent polymer
preparing
nanoparticles
Prior art date
Application number
PCT/FR2008/052251
Other languages
French (fr)
Other versions
WO2009080974A2 (en
Inventor
Virginie Boucher
Alexandra Roos
Sophie Duquesne
Serge Bourbigot
Laure Meynie
Karine Cavalier
Didier Sy
Marc Lacroix
Original Assignee
Essilor Int
Ecole Nale Sup Artes Metiers
Renault Sa
Solvay
Virginie Boucher
Alexandra Roos
Sophie Duquesne
Serge Bourbigot
Laure Meynie
Karine Cavalier
Didier Sy
Marc Lacroix
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=39493572&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO2009080974(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Essilor Int, Ecole Nale Sup Artes Metiers, Renault Sa, Solvay, Virginie Boucher, Alexandra Roos, Sophie Duquesne, Serge Bourbigot, Laure Meynie, Karine Cavalier, Didier Sy, Marc Lacroix filed Critical Essilor Int
Priority to EP08865864.6A priority Critical patent/EP2220146B1/en
Priority to KR1020107015540A priority patent/KR101662650B1/en
Priority to KR1020157033529A priority patent/KR20150140850A/en
Priority to BRPI0820881A priority patent/BRPI0820881A8/en
Priority to US12/746,011 priority patent/US9284422B2/en
Priority to JP2010537493A priority patent/JP5551080B2/en
Priority to CN2008801203044A priority patent/CN101896539B/en
Publication of WO2009080974A2 publication Critical patent/WO2009080974A2/en
Publication of WO2009080974A3 publication Critical patent/WO2009080974A3/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/20Compounding polymers with additives, e.g. colouring
    • C08J3/22Compounding polymers with additives, e.g. colouring using masterbatch techniques
    • C08J3/226Compounding polymers with additives, e.g. colouring using masterbatch techniques using a polymer as a carrier
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/005Reinforced macromolecular compounds with nanosized materials, e.g. nanoparticles, nanofibres, nanotubes, nanowires, nanorods or nanolayered materials
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L69/00Compositions of polycarbonates; Compositions of derivatives of polycarbonates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2369/00Characterised by the use of polycarbonates; Derivatives of polycarbonates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2425/00Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2433/00Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2469/00Characterised by the use of polycarbonates; Derivatives of polycarbonates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24Acids; Salts thereof
    • C08K3/26Carbonates; Bicarbonates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/0008Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
    • C08K5/005Stabilisers against oxidation, heat, light, ozone
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L25/00Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
    • C08L25/02Homopolymers or copolymers of hydrocarbons
    • C08L25/04Homopolymers or copolymers of styrene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L33/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • C08L33/04Homopolymers or copolymers of esters
    • C08L33/06Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, which oxygen atoms are present only as part of the carboxyl radical
    • C08L33/10Homopolymers or copolymers of methacrylic acid esters
    • C08L33/12Homopolymers or copolymers of methyl methacrylate

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • General Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Instrument Panels (AREA)
  • Non-Portable Lighting Devices Or Systems Thereof (AREA)
  • Optics & Photonics (AREA)

Abstract

The present invention relates to a method of preparing a transparent polymer material, comprising the following steps: i) mineral nanoparticles, chosen from alkaline-earth metal carbonate, alkaline-earth metal sulphate, metal oxide, metalloid oxide and siloxane nanoparticles, are mixed with a composition A comprising at least one thermoplastic polymer in the molten state chosen from polycarbonate (PC), polystyrene (PS) and polymethyl methacrylate (PMMA), in order to obtain a masterbatch, the mixture resulting from step i) comprising at least 25% and at most 75% by weight of said mineral nanoparticles; and ii) the masterbatch obtained from i) is mixed with a composition B comprising a thermoplastic polycarbonate matrix (mPC) in the molten state, so as to obtain a transparent polymer material comprising at most 10% by weight of said mineral nanoparticles, preferably at most 5% by weight of said mineral nanoparticles.
PCT/FR2008/052251 2007-12-13 2008-12-09 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles WO2009080974A2 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
EP08865864.6A EP2220146B1 (en) 2007-12-13 2008-12-09 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles
KR1020107015540A KR101662650B1 (en) 2007-12-13 2008-12-09 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles
KR1020157033529A KR20150140850A (en) 2007-12-13 2008-12-09 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles
BRPI0820881A BRPI0820881A8 (en) 2007-12-13 2008-12-09 PREPARATION PROCESS OF A TRANSPARENT POLYMER MATERIAL
US12/746,011 US9284422B2 (en) 2007-12-13 2008-12-09 Method of preparing a transparent polumer material comprising a thermoplastic polycarbonate and mineral nanoparticles
JP2010537493A JP5551080B2 (en) 2007-12-13 2008-12-09 Method for producing transparent polymer material containing thermoplastic polycarbonate and inorganic nanoparticles
CN2008801203044A CN101896539B (en) 2007-12-13 2008-12-09 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0759808A FR2925060B1 (en) 2007-12-13 2007-12-13 PROCESS FOR PREPARING TRANSPARENT POLYMER MATERIAL COMPRISING THERMOPLASTIC POLYCARBONATE AND MINERAL NANOPARTICLES
FR0759808 2007-12-13

Publications (2)

Publication Number Publication Date
WO2009080974A2 WO2009080974A2 (en) 2009-07-02
WO2009080974A3 true WO2009080974A3 (en) 2009-08-20

Family

ID=39493572

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2008/052251 WO2009080974A2 (en) 2007-12-13 2008-12-09 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles

Country Status (8)

Country Link
US (1) US9284422B2 (en)
EP (1) EP2220146B1 (en)
JP (1) JP5551080B2 (en)
KR (2) KR20150140850A (en)
CN (1) CN101896539B (en)
BR (1) BRPI0820881A8 (en)
FR (1) FR2925060B1 (en)
WO (1) WO2009080974A2 (en)

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US8173739B2 (en) * 2008-04-15 2012-05-08 Suncolor Corporation Optical polymeric composition and method of making same
FR2939441B1 (en) * 2008-12-08 2010-12-24 Solvay PROCESS FOR THE PREPARATION OF A TRANSPARENT POLYMER MATERIAL COMPRISING MINERAL NANOPARTICLES HAVING A FORM FACT STRICTLY GREATER THAN 1.0
CN101831129A (en) * 2010-03-31 2010-09-15 江苏华天通科技有限公司 Preparation method of electric welding lens containing transition metal oxide nano-material
CN101824192B (en) * 2010-05-11 2012-01-04 宁波力达得为高分子科技有限公司 Modified polystyrene material and preparation method thereof
JP2013107933A (en) * 2011-11-17 2013-06-06 Denki Kagaku Kogyo Kk Resin composition for optical molded article, method for producing the same and optical molded article
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US8691915B2 (en) 2012-04-23 2014-04-08 Sabic Innovative Plastics Ip B.V. Copolymers and polymer blends having improved refractive indices
EP2970096B1 (en) 2013-03-15 2018-08-08 SABIC Global Technologies B.V. Process for purification of diphenyl carbonate for the manufacturing of high quality polycarbonate
EP2778186B1 (en) 2013-03-15 2017-07-12 SABIC Global Technologies B.V. Production of a polycarbonate with limited metal residuals
CN106929941A (en) * 2015-12-31 2017-07-07 上海水星家用纺织品股份有限公司 The fabric that the preparation method and the fiber of stalactite Chinese medicine mineral fibres are prepared
CN107033756A (en) * 2017-04-13 2017-08-11 四川圣典节能服务有限公司 A kind of frosted coating of LED lampshade
EP3676350A1 (en) * 2017-08-29 2020-07-08 SABIC Global Technologies B.V. Quantum dot compositions including polycarbonate and acrylic blends and methods of manufacture
CN108359231A (en) * 2018-02-09 2018-08-03 天津德迈特汽车零部件有限公司 Plastic lens and preparation method thereof
CN114230998A (en) * 2021-09-17 2022-03-25 无锡德塑新材料科技有限公司 PC/PS/PMMA ternary alloy material and preparation method thereof
CN113817304A (en) * 2021-09-18 2021-12-21 金旸(厦门)新材料科技有限公司 Composite nano silicon dioxide modified PC/ABS alloy material and preparation method thereof

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Also Published As

Publication number Publication date
KR20100131418A (en) 2010-12-15
FR2925060A1 (en) 2009-06-19
CN101896539B (en) 2013-06-12
EP2220146B1 (en) 2018-09-05
US9284422B2 (en) 2016-03-15
JP5551080B2 (en) 2014-07-16
BRPI0820881A2 (en) 2015-06-16
KR20150140850A (en) 2015-12-16
JP2011506667A (en) 2011-03-03
US20110034588A1 (en) 2011-02-10
WO2009080974A2 (en) 2009-07-02
FR2925060B1 (en) 2012-12-21
KR101662650B1 (en) 2016-10-05
EP2220146A2 (en) 2010-08-25
BRPI0820881A8 (en) 2018-08-14
CN101896539A (en) 2010-11-24

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