Nothing Special   »   [go: up one dir, main page]

US3259538A - Comprehensive pulping system for producing paper pulp - Google Patents

Comprehensive pulping system for producing paper pulp Download PDF

Info

Publication number
US3259538A
US3259538A US274419A US27441963A US3259538A US 3259538 A US3259538 A US 3259538A US 274419 A US274419 A US 274419A US 27441963 A US27441963 A US 27441963A US 3259538 A US3259538 A US 3259538A
Authority
US
United States
Prior art keywords
pulp
liquor
tank
washer
digester
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US274419A
Inventor
Auxilius P Schnyder
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lummus Technology LLC
Original Assignee
Lummus Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lummus Co filed Critical Lummus Co
Priority to US274419A priority Critical patent/US3259538A/en
Application granted granted Critical
Publication of US3259538A publication Critical patent/US3259538A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • D21C3/24Continuous processes

Definitions

  • This present invention relates to an improved method and apparatus for the delignification of cellulosic materials to prepare cellulosic fibers and, more particularly,
  • the chips are initially deaerated in a feed tank maintained under vacuum and submerged in liquor therein to form a slurry of suitable consistency.
  • the slurry is then pumped to an i-mpregnator where the chips are impregnated with cooking liquor by being subjected to successive, incrementally increasing hydraulic pressures.
  • the chip slurry is passed to a digester, and excess liquor is recycled to the feed tank. After digestion, the chips are washed within the digester.
  • a high temperature liquor of high solids concentration is separated from the pulp in the initial washing within the digester.
  • the pulp is discharged into a blow tank provided with means to enable improved heat recovery and condensing of flash steam within the blow tank.
  • the pulp is then further washed in vacuum type washers.
  • a portion of the steam flashed in the blow tank is passed to the headers of the vacuum type washers to minimize air infiltration and foaming.
  • the waste liquor is sent to conventional multiple-effect evaporators for concentration prior to smelting.
  • a primary object of the present invention is to provide an improved comprehensive pulping system.
  • Another object of the present invention is to provide an improved continuous process for delignifying cellulosic material to pulp of high quality and yield.
  • Another object of the present invention is to provide an improved continuous process for delignifying cellulosic material including .a method of washing digested pulp within a continuous digester.
  • Still another object of the present invention is to provide an improved continuous process for delignifying cellulosic material including improved tank discharge means for submerging cellulosic material within cooking liquor to form a slurry of suitable pumping consistency.
  • a further object of the present invention is to provide an improved continuous process for delignifying cellulosic material including a continuous digester of novel structure enabling .an initial washing operation to be carried out within the digester.
  • a still further object of the present invention is to provide an improved continuous process for delignifying cellulosic material including means to recover heat from the pulp and liquor leaving the digester.
  • FIGURES la and 1b together show a schematic flow diagram illustrating one embodiment of the comprehensive pulping system
  • FIGURE 2 is a vertical sectional view through a portion of the vacuum tank and chip submergence means of FIGURE 1a;
  • FIGURE 3 is a horizontal cross sectional view on the line 33 of FIGURE la through the washing zone.
  • FIGURE 4 is an enlarged cross-sectional view of a drainage member of the washer taken along the lines 4-4 of FIGURE 3.
  • wood chips or like cellulosic material are passed from a main chip silo including a vibration hammer 12 into a vibrating feeder device 14 'or other suitable chip metering device and introduced into a vacuum tank 16.
  • Liquor in line 18 comprised of a solution of fresh cooking liquor and recirculated liquor, is introduced into tank 16 as will be explained more fully hereinafter.
  • Suitable liquid level control means may be provided to maintain the liquor level in tank 16 within the desired range so that only .a portion of the body of chips within tan-k 16 is below the level of the liquor.
  • Air is withdrawn from the tank 16 through vacuum line 20 and pump '22.
  • the chips, after being subjected to the vacuum are gradually submerged beneath the level of the cooking liquor within tank 16. This gradual submergence is also effective to displace air from the pores of the chips.
  • FIGURE 2 The slurry discharge mechanism of tank 16 is best shown in FIGURE 2.
  • An annular housing 24 is rigidly secured to a flange 26 of the side walls 28 of vessel 16. Suitable support means 29 are welded or otherwise fastened to side walls 28 above housing 24. Housing 24 is also rigidly secured to the bottom wall 30 of tank 16.
  • a hollow chip deflecting member 32 having an essentially conic-a1 upper surface projects upwardly through the center of bottom wall 30. Member 32 is provided with opposed openings 34 and with a gear housing 36 mounted interiorly thereof by suitable support elements 38.
  • Casing 40 is rotatably positioned Within housing 24 by means of an annular gear ring 42 driven by gear 44, a shaft 46 extending through bottom wall 30, and a motor 48.
  • Screw conveyors 50 are mounted above and adjacent to the slightly tapering inner surface of bottom Wall 30. Screw conveyors 50 extend at their outer ends through apertures in casing 40 and are secured to roller members 52 which support the lower end of casing 40 above the upper surface of bottom wall 30. At their inner ends, screw conveyors 50 are secured to bevel gears 54 within gear housing 36. A motor 56 having a drive shaft 58 extending through suitable bearing means into housing 36 is provided with a drive gear 60 engaging gears 54 for rotating screw conveyors 50. Screw conveyors 50 are provided with screw threads of progressively increasing height to facilitate movement of the slurry through apertures 34 land into a discharge conduit 62.
  • the screw conveyors 50 slowly rotate about the axis of vessel ⁇ 16 by means of mot-or 48 and gears 42 and 44, so that the entire bottom of vessel 16 is swept by conveyors 50 to prevent stagnation of the chips within vessel 16.
  • the slurry in conduit 62 is passed to transfer pump 64 and is pumped through the line 66 to an irnpregnator, generally designated by reference numeral 68, which is preferably of the type shown in my copending application entitled Pressure Impregnation Device S.'N. 274,422 filed April 22, 1963 now Patent No. 3,215,591, which is incorporated herein by reference.
  • a bypass line is connected from pump 64 to liquor line 18.
  • the impregnator 68 consists of a stationary outer casing and an inner revolving barrel assembly including a plurality of open ended tubular members constituting chip receiving passageways. Impregnator-68 is shown in a developed view of FIGURE la to better illustrate its function.
  • the slurry in line 66 i introduced through an inlet port 72 in the stationary casing into a tubular member present at the inlet station.
  • a corresponding port 74 in the top of the stationary outer casing is provided with a screen to prevent chip passage therethrough while allowing excess liquor to be recycled in line 76 to liquor supply line 18.
  • the member will be filled with chips.
  • the rotor assembly is then cyclically rotated to bring a tubular member filled only with liquor to the inlet station and to move the chip-filled tubular member into alignment with port 78.
  • Port 78 is supplied with a higher pressure liquor through line 80 by pump 82, and line 81 leading from liquor supply line 18.
  • the chips are subjected to successively increasing hydraulic impregnating pressure when in alignment with ports 84 and 86 which are supplied with high pressure liquor through lines 88 and 90, respectively, by pump 92 connected to liquor supply line 18 by line 91.
  • the filled tubular member is moved to a discharge station in alignment with the ports 94 and 96.
  • Port 94 is supplied with liquor through line 98 to flush chips out of the tubular member through discharge port 96 into line 100 as a chipliquor slurry.
  • the chips are uniformly impregnated by subjecting the chips to a high hydraulic pressure several times that of the standard cooking pressure. Additionally, by limiting the volume of chips subjected to successively higher hydraulic pressure stages with a final pressure in the order of 600 p.s. i.g., rapid impregnation of the chip may be effected.
  • the slurry in line 100 is introduced into a chip drainage device 102 of known construction including a tapering, perforated internal screen member containing a screw conveyor. Liquor in excess of that required for digestion is passed through the screen member and is recycled through line 104, pump 106 and heat exchanger 108 to line 98 and port 94 of the impregnator 68.
  • This external heating cycle is described more fully in my aforementioned copending application.
  • the chips are now passed from strainer 102 through line 110 into a digester 112 corresponding in size and hape to a standard digester.
  • the digester 112 is provided with a conventional access manhole 128 and vent line 122.
  • Steam at a pressure of p.s.i.g. is introduced into the digester 112 through steam line 124 to elfect digestion of the chips in non-submergence.
  • the chips may be digested while submerged in cooking liquor by supplying the entire heating requirements by the recycled liquor passing through heat exchanger 108.
  • a combination of steam and heated cooking liquor is also contemplated to supply the heating requirements for effecting delignification of the cellulosic material.
  • the chips are delignified to pulp during passage downwardly through the digester 112, and the residence time is regulated by suitable control means (not shown) to insure substantially complete digestion.
  • Recycled liquor in line 126 is introduced into the digested pulp in the lower portion of digester 112 to dilute the suspension to a consistency of from about 1% to about 3%.
  • the pulp is passed through a conduit 116 to a washer 118.
  • a suitable agitator 128 may be provided in conduit 116 to insure good pulp dispersion within the chip liquor suspension.
  • the suspension is passed upwardly through washer 118 which. includes a plurality of perforated liquor drainage members 130.
  • Drainage members 130 preferably extend in a saw-tooth offset fashion transversely from one side to the other of an internal perforated drainage cylinder 132 provided within Washer 118.
  • the drainage cylinder .132 is in communication with the ends of drain age members 130.
  • Drainage members 130 preferably consist of support pipes secured to the walls of drainage cylinder 132 which support a mesh or other similar perforated wall portions.
  • the apexes of members 130 are preferably imperforated V-shaped troughs and serve as drain troughs which discharge the liquor into perforated cylinder 132. Liquor is removed from the dilute suspension through members 130 and cylinder 132.
  • a drainage member 130 is illustrated having perforations 131 along the side walls and having an imperforated V-shaped trough 133.
  • the consistency of the pulp is increased to about 10% to about 12% at the top of washer 118 where the pulp is skimmed off by a scraper 134 and passed via line 135 into a launder 136.
  • the liquor removed by means of members 130 and cylinder 132 is introduced into a spent liquor tank 138 through line 140 at a temperature below the cooking temperature, for example, between about 250 F. to about 300 F. with a high concentration of dissolved solids.
  • a portion of the liquor in tank 138 is pa sed through line 142 by pump 144 to be introduced through line 126 into digester leg portion 114.
  • the remainder of the spent liquor is passed through line 146 to multiple-effect evapor-ators (not shown) for concentration and subsequent smelting, as is conventional in the art.
  • Steam liberated in tank 138 is vented through line 148 to heat exchanger 150 to preheat makeup cooking liquor in line 18.
  • the pulp in launder 136 is passed through blow line 152 provided with a blow valve 154 into a small cyclone 156 at the inlet to a blow tank 158.
  • Cyclone 156 distributes the stock in a thin sheet for tangential discharge through line 160 into blow tank 158 to facilitate the liberation of steam from the stock with minimum fibre entrainment.
  • Flash steam is liberated from the blown stock and is passed upwardly into a comically-shaped funnel 162 wherein the steam is condensed by contact with cooling water introduced through line 164 and discharged in spray form through a perforated plate 166. Steam condensate and cooling water is removed from the funnel 162 through line 167 and is passed into an accumulator tank 168.
  • Blow tank 158 also receives condensate from the heat exchanger 150 through line 170.
  • Blow tank 158 additionally functions as a stock storage vessel balancing digester operations with final washing operations in vacuum washers 172 and 174.
  • Accumulator 168 is provided with an external liquor circuit including line 180, heat eychanger 182, lines 184, 186, 188 and pump 190.
  • a temperature responsive flow control valve 192 is provided in bypass line 186 to regulate the flow of water to heat exchanger 182 through line 180, and the temperature of incoming fresh water supplied to heat exchanger 182 through line 194. From heat exchanger 182, the fresh water is passed through line 196 to a heat exchanger 198 in vent line 178.
  • the heated water is passed through line 200 to a hot water storage tank 202 from which water is removed to process as desired through line 204 by pump 206.
  • a portion of the incoming fresh Water in line 194 may be introduced dirlecly into the accumulator 168 through lines 208 and From accumulator 168, water is passed through line 210 by pump 212 to line 164 and perforated plate 166 for condensing flash steam as previously described. Water is also withdrawn from accumulator 168 through line 214 by pump 216 and is passed through line 218 to vacuum washer 174 as will be discussed hereinafter.
  • Pulp diluted to a suitable consistency in blow tank 158 is withdrawn through line 230 and is passed through line 232 to a pressurized pulp screen assembly 234.
  • Screen assembly 234 further refines the stock and returns oversized fibre masses to blow tank 158 through line 236.
  • the stock from screen assembly 234 is passed through line 238 to an inlet box 240 adjacent vacuum washer 172.
  • the stock is taken up on a conventional perforated drum 242 and sprayed with :a wash medium from spray head 244.
  • the wash medium is supplied to spray head 244 from the third stage vacuum washer 174 through line 246.
  • Liquor and wash medium drain through perforated drum 242 and are removed by line 248 to a washer liquor seal tank 250 which is provided with a baflie 252 and a vent line 254.
  • a portion of the liquor in tank 250 is removed through line 256 and passed by pump 258 through lines 260 and 126 to digester 112.
  • the remainder of the liquor in tank 250 is passed through line 262 by pump 264 and is passed through line 266 to blow tank 158 to dilute the stock therein, or through line 268 for admixture with the diluted pulp in line 230 being introduced into the screen assembly 234 through line 232.
  • the pulp stock from vacuum washer 172 is discharged into a trough 27 0 for treatment to break up sheeted pulp.
  • the pulp is diluted in trough 270 with liquor supplied from a liquor seal tank 272 through line 274, pump 276, and lines 278 and 280.
  • the diluted pulp in trough 270 is acted upon by blades 282 and is passed to the rotating perforated drum 284 of vacuum washer 174.
  • the pulp is washed by water supplied to a spray head 286 through line 218 from accumulator 168.
  • the wash water passes through the perforations of drum 284 and is removed by line 288 to the liquor seal tank 272 provided with suitable baflles 290 and a vent 292.
  • the pulp which has now undergone a three-stage washing is discharged from cylinder 284 into hopper 294 for further processing.
  • Spray heads 244 and 286 of vacuum Washers 172 and 174, respectively, are enclosed within housings 296 and 298, respectively. Housings 296 and 298 are supplied with flash steam from blow tank 158 through line 300 under control of valve 302 to essentially prevent foaming at vacuum washers 172 and 174 and their sea-l tanks 250 and 272 by eliminating air infiltration.
  • a process for digesting cellulosic material comprising vacuum deaerating said material, submerging said material in liquor forming a slurry of pumpable consistency, impregnating said material by subjecting the material to progressively increasing hydraulic pressures, introducing the impregnated material into a digester, digesting said impregnated material to pulp in non-submergence in the presence of steam, diluting the pulp within the digester with additional liquor, transferring the diluted pulp to a Washer, washing the diluted pulp in said Washer, removing liquor from the diluted pulp substantially at the cooking temperature, introducing the washed pulp a a thin stream into a blow tank, condensing the steam within the blow tank by direct contact with cooling water, passing the steam condensate and cooling Water to an accumulator tank, vacuum washing the pulp removed from said blow tank in a vacuum washer having a wash liquid sprayer, returning liquor from the vacuum washing step to said blow tank, and injecting steam from said blow tank into a header surrounding the wash liquid sprayer of the vacuum washer
  • a process for digesting cellulosic material comprising vacuum deaerating said material, submerging said material in liquor forming a slurry of pumpable consistency, impregnating said material by subjecting the material to progressively increasing hydraulic pressures, introducing the impregnated material into a digester, continuously digesting said impregnated material to pulp in said digester, diluting the pulp within said digester, removing liquor from the pulp substantially at the cooking temperature,
  • a process for digesting cellulosic material comprising deaerating said material, impregnating said material, introducing said material into a digester, digesting said material to pulp, diluting the pulp within the digester with additional liquor, transferring the diluted pulp to a Washer, washing the diluted pulp in said washer, removing liquor from the diluted pulp, introducing the washed pulp into a blow tank, vacuum washing the pulp removed from said blow tank in a plurality of vacuum washers, each having a wash liquid sprayer, returning liquor from the vacuum washing step to said blow tank, and injecting steam formed in said blow tank into headers surrounding the wash liquid sprayers.
  • Apparatus for treating wood chips or the like comprising a substantially upright tank, an annular housing rigidly secured to the bottom of said tank and closed off by a bottom wall, a hollow chip deflecting member having an essentially conical upper surface projecting above said bottom wall substantially in the center thereof, said deflecting member being provided with openings into the interior thereof, gear means mounted within the interior of said deflecting member, a casing rotatably positioned within said housing, drive gear means for rotating said casing, and a plurality of screw conveyors mounted at the outer ends thereof upon said casing and at the other ends thereof being adapted to convey chips through said openings into the interior of said deflecting member.
  • Apparatus for treating wood chips or the like comprising a substantially upright tank, an annular housing rigidly secured to the bottom of said tank and closed off by a bottom wall, a hollow chip deflecting member having an essentially conical upper surface projecting above said bottom wall substantially in the center thereof, said deflecting member being provided with opposed openings to the interior thereof, gear means mounted within the interior of said deflecting member, a casing rotatably positioned within said housing and provided with an annular gear ring, drive gear means cooperating with said gear ring, a plurality of screw conveyors mounted adjacent to the upper surface of said bottom wall with their outer ends mounted upon said casing and with their inner ends extending through said openings in said deflecting member, means to rotate said screw conveyors to convey chips through said openings into the interior of said deflecting member, and a discharge conduit in communication with the interior of said deflecting member.
  • Apparatus for pulping cellulosic material which comprises: tank means to submerge said cellulosic material in cooking liquor to form a slurry of said cellulosic material and said liquor; a first conduit means; an impregnator for receiving said slurry in fluid communication with said tank means through said first conduit means, said impregnator including means to progressively increase the hydraulic pressure of said slurry; a digester; a liquor supply means for diluting said pulp leaving said digester; a second conduit means; a washer in fluid communication with said digester through said second conduit means for receiving diluted pulp, said washer having a plurality of perforated drainage members extending trans versely across said washer in a saw-toothed arrangement; and a third conduit means for withdrawing liquor out of said washer from said drainage members.
  • Apparatus for pulping cellulosic material which comprises: tank means to submerge said cellulosic material in cooking liquor to form a slurry of said cellulosic material and said liquor; a first conduit means; an impregnat-or for receiving said slurry in fluid communication with said tank means through said first conduit means, said impregnator including means to progressively in crease the hydraulic pressure of said slurry; a digester; a liquor supply means for diluting said pulp leaving said digester; a second conduit means; a washer in fluid communication with said digester through said second conduit means for receiving diluted pulp, said washer having a plurality of perforated drainage members extending transversely across said washer in a saw-toothed arrangement; and a third conduit means for withdrawing liquor out of said washer from said drainage members; a fourth conduit means; a blow tank for receiving discharge pulp from said washer through said fourth conduit means; and condensing means including cooling water spray means within said blow tank to condense steam flashed by entry of
  • An apparatus for digesting cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said digester; means to introduce liquor into a lower region of said digester to dilute digested pulp; conduit means; a washer in fluid communication with said digester through said conduit means for receiving diluted pulp, said washer including a p1u rality of drainage members spaced in a staggered arrangement, each drainage member including essentially V- shaped imperforated bottom portions and perforated side wall portions, said imperforated bottom portions constituting drainage troughs for liquor passing through the side wall portion; and means to remove washed pulp from the top of said washer.
  • An apparatus for digesting cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said digester; means to introduce liquor into the lower portion of said digester to dilute digested pulp; conduit means, a washer in fluid communication with said digester through said conduit means for receiving diluted pulp, said washer including a plurality of drainage members spaced in staggered arrangement, each drainage member including essentially V- shaped imperforated bottom portions and perforated side wall portions, said imperforated bottom portions constituting drainage troughs for liquor passing through said side wall portions, an annular perforated drainage cylinder within said washer in fluid communication with 8 the drainage troughs of said drainage members; and means to remove wash pulp from the top of said washer.
  • An apparatus for digesting cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said.digester, means to supply steam into said digester to effect delignification of the cellulosic material; means to introduce liquor into the lower portion of said digester to dilute delignified pulp; conduit means; a washer in fluid communication with said digester through said conduit means for receiving diluted pulp, said washer including a plurality of drainage members spaced in a staggered arrangement, each drainage member including essentially V-shaped imperforated bottom portions and perforated side wall portions, said imperforated bottom portions constituting drainage troughs for liquor passing through said side wall portions; and means to remove wash pulp from the upper portion of said washer.
  • An apparatus for delignifying cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said digester; means to supply steam to said digester to effect delignification of the cellulosic material; means to introduce liquor into a lower portion of said digester to dilute the delignified pulp; conduit means; a washer in fluid communication with said digester through said conduit means to receive diluted pulp, said washer including a plurality of drainage members spaced in a staggered arrangement, each drainage member including essentially V-shaped imperforated bottom portions and perforated side wall portions, said imperforated portions constituting drainage troughs for liquor passing through the side wall portions; an annular perforated drainage cylinder positioned within said washer in fluid communication with the drainage trough of said drainage members; and means to remove washed pulp from the upper portion of said Washer.

Landscapes

  • Paper (AREA)

Description

y 1956 A. P. SCHNYDER 3,259,538
COMPREHENSIVE PULPING SYSTEM FOR PRODUCING PAPER PULP 5 Sheets-Sheet 1 9 a 9 Q u.
O (I) (D N (D 3 s E r-- qo P INVENTOR Q AUXILIUS P. SCHNYDER BY fr izflgezzsa@et/ ATTORNEY July 5, 1966 A. P. SCHNYDER 3,259,533
COMPREHENSIVE PULPING SYSTEM FOR PRODUCING PAPER PULP Filed April 22, 1963 5 Sheets-Sheet 2 INVENTOR AUXILIUS P. SCHNYDER July 5, 1966 A. P. SCHNYDER COMPREHENSIVE PULPING SYSTEM FOR PRODUCING PAPER PULP 5 Sheets-Sheet 5 Filed April 22, 1963 N OE INVENTOR AUXILI us P. SCHNYDER BY W ATTORNEY United States Patent 3,259,538 COMPREHENSIVE PULPING SYSTEM FOR PRUDUCENG PAPER PULP Auxilius P. chnyder, Bogota, N..I., assignor to The Lummus Company, New York, N.Y., a corporation of Delaware Filed Apr. 22, 1963, Ser. No. 274,419 12 Claims. (Cl. 162-19) This present invention relates to an improved method and apparatus for the delignification of cellulosic materials to prepare cellulosic fibers and, more particularly,
to a comprehensive, continuous system for treating cellulosic material which extends from a raw chip supply source through discharge of the washed pulp for final processing.
In accordance with a preferred embodiment of the present invention, the chips are initially deaerated in a feed tank maintained under vacuum and submerged in liquor therein to form a slurry of suitable consistency. The slurry is then pumped to an i-mpregnator where the chips are impregnated with cooking liquor by being subjected to successive, incrementally increasing hydraulic pressures. From the impregnator, the chip slurry is passed to a digester, and excess liquor is recycled to the feed tank. After digestion, the chips are washed within the digester. A high temperature liquor of high solids concentration is separated from the pulp in the initial washing within the digester. The pulp is discharged into a blow tank provided with means to enable improved heat recovery and condensing of flash steam within the blow tank. The pulp is then further washed in vacuum type washers. A portion of the steam flashed in the blow tank is passed to the headers of the vacuum type washers to minimize air infiltration and foaming. The waste liquor is sent to conventional multiple-effect evaporators for concentration prior to smelting.
A primary object of the present invention is to provide an improved comprehensive pulping system.
Another object of the present invention is to provide an improved continuous process for delignifying cellulosic material to pulp of high quality and yield.
Another object of the present invention is to provide an improved continuous process for delignifying cellulosic material including .a method of washing digested pulp within a continuous digester.
Still another object of the present invention is to provide an improved continuous process for delignifying cellulosic material including improved tank discharge means for submerging cellulosic material within cooking liquor to form a slurry of suitable pumping consistency.
A further object of the present invention is to provide an improved continuous process for delignifying cellulosic material including a continuous digester of novel structure enabling .an initial washing operation to be carried out within the digester.
A still further object of the present invention is to provide an improved continuous process for delignifying cellulosic material including means to recover heat from the pulp and liquor leaving the digester.
These and other objects, features and advantages of the present invention will become more apparent from the following description taken in conjunction with accompanying drawings wherein:
FIGURES la and 1b together show a schematic flow diagram illustrating one embodiment of the comprehensive pulping system;
FIGURE 2 is a vertical sectional view through a portion of the vacuum tank and chip submergence means of FIGURE 1a;
FIGURE 3 is a horizontal cross sectional view on the line 33 of FIGURE la through the washing zone; and
FIGURE 4 is an enlarged cross-sectional view of a drainage member of the washer taken along the lines 4-4 of FIGURE 3.
Referring now to the drawings, and more particularly to FIGURE la, wood chips or like cellulosic material are passed from a main chip silo including a vibration hammer 12 into a vibrating feeder device 14 'or other suitable chip metering device and introduced into a vacuum tank 16. Liquor in line 18, comprised of a solution of fresh cooking liquor and recirculated liquor, is introduced into tank 16 as will be explained more fully hereinafter. Suitable liquid level control means (not shown) may be provided to maintain the liquor level in tank 16 within the desired range so that only .a portion of the body of chips within tan-k 16 is below the level of the liquor. Air is withdrawn from the tank 16 through vacuum line 20 and pump '22. The chips, after being subjected to the vacuum, are gradually submerged beneath the level of the cooking liquor within tank 16. This gradual submergence is also effective to displace air from the pores of the chips.
The slurry discharge mechanism of tank 16 is best shown in FIGURE 2. An annular housing 24 is rigidly secured to a flange 26 of the side walls 28 of vessel 16. Suitable support means 29 are welded or otherwise fastened to side walls 28 above housing 24. Housing 24 is also rigidly secured to the bottom wall 30 of tank 16. A hollow chip deflecting member 32 having an essentially conic-a1 upper surface projects upwardly through the center of bottom wall 30. Member 32 is provided with opposed openings 34 and with a gear housing 36 mounted interiorly thereof by suitable support elements 38. Casing 40 is rotatably positioned Within housing 24 by means of an annular gear ring 42 driven by gear 44, a shaft 46 extending through bottom wall 30, and a motor 48.
Opposed screw conveyors 50 are mounted above and adjacent to the slightly tapering inner surface of bottom Wall 30. Screw conveyors 50 extend at their outer ends through apertures in casing 40 and are secured to roller members 52 which support the lower end of casing 40 above the upper surface of bottom wall 30. At their inner ends, screw conveyors 50 are secured to bevel gears 54 within gear housing 36. A motor 56 having a drive shaft 58 extending through suitable bearing means into housing 36 is provided with a drive gear 60 engaging gears 54 for rotating screw conveyors 50. Screw conveyors 50 are provided with screw threads of progressively increasing height to facilitate movement of the slurry through apertures 34 land into a discharge conduit 62. In addition to rotation about their own axes, the screw conveyors 50 slowly rotate about the axis of vessel \16 by means of mot-or 48 and gears 42 and 44, so that the entire bottom of vessel 16 is swept by conveyors 50 to prevent stagnation of the chips within vessel 16.
Referring to FIG-UR'E la, the slurry in conduit 62 is passed to transfer pump 64 and is pumped through the line 66 to an irnpregnator, generally designated by reference numeral 68, which is preferably of the type shown in my copending application entitled Pressure Impregnation Device S.'N. 274,422 filed April 22, 1963 now Patent No. 3,215,591, which is incorporated herein by reference. A bypass line is connected from pump 64 to liquor line 18.
As set forth more fully in my copending application,
the impregnator 68 consists of a stationary outer casing and an inner revolving barrel assembly including a plurality of open ended tubular members constituting chip receiving passageways. Impregnator-68 is shown in a developed view of FIGURE la to better illustrate its function. The slurry in line 66 i introduced through an inlet port 72 in the stationary casing into a tubular member present at the inlet station. A corresponding port 74 in the top of the stationary outer casing is provided with a screen to prevent chip passage therethrough while allowing excess liquor to be recycled in line 76 to liquor supply line 18. During the residence period of a tubular member in alignment with ports 72 and 74, the member will be filled with chips.
The rotor assembly is then cyclically rotated to bring a tubular member filled only with liquor to the inlet station and to move the chip-filled tubular member into alignment with port 78. Port 78 is supplied with a higher pressure liquor through line 80 by pump 82, and line 81 leading from liquor supply line 18. Similarly, the chips are subjected to successively increasing hydraulic impregnating pressure when in alignment with ports 84 and 86 which are supplied with high pressure liquor through lines 88 and 90, respectively, by pump 92 connected to liquor supply line 18 by line 91. Upon the next cyclical rotation of the rotor assembly, the filled tubular member is moved to a discharge station in alignment with the ports 94 and 96. Port 94 is supplied with liquor through line 98 to flush chips out of the tubular member through discharge port 96 into line 100 as a chipliquor slurry. During passage through impregnator 68, the chips are uniformly impregnated by subjecting the chips to a high hydraulic pressure several times that of the standard cooking pressure. Additionally, by limiting the volume of chips subjected to successively higher hydraulic pressure stages with a final pressure in the order of 600 p.s. i.g., rapid impregnation of the chip may be effected.
The slurry in line 100 is introduced into a chip drainage device 102 of known construction including a tapering, perforated internal screen member containing a screw conveyor. Liquor in excess of that required for digestion is passed through the screen member and is recycled through line 104, pump 106 and heat exchanger 108 to line 98 and port 94 of the impregnator 68. This external heating cycle is described more fully in my aforementioned copending application.
The chips are now passed from strainer 102 through line 110 into a digester 112 corresponding in size and hape to a standard digester. The digester 112 is provided with a conventional access manhole 128 and vent line 122. Steam at a pressure of p.s.i.g. is introduced into the digester 112 through steam line 124 to elfect digestion of the chips in non-submergence. The chips may be digested while submerged in cooking liquor by supplying the entire heating requirements by the recycled liquor passing through heat exchanger 108. A combination of steam and heated cooking liquor is also contemplated to supply the heating requirements for effecting delignification of the cellulosic material.
The chips are delignified to pulp during passage downwardly through the digester 112, and the residence time is regulated by suitable control means (not shown) to insure substantially complete digestion. Recycled liquor in line 126, as more fully hereinafter described, is introduced into the digested pulp in the lower portion of digester 112 to dilute the suspension to a consistency of from about 1% to about 3%. The pulp is passed through a conduit 116 to a washer 118. A suitable agitator 128 may be provided in conduit 116 to insure good pulp dispersion within the chip liquor suspension.
The suspension is passed upwardly through washer 118 which. includes a plurality of perforated liquor drainage members 130. Drainage members 130 preferably extend in a saw-tooth offset fashion transversely from one side to the other of an internal perforated drainage cylinder 132 provided within Washer 118. The drainage cylinder .132 is in communication with the ends of drain age members 130. Drainage members 130 preferably consist of support pipes secured to the walls of drainage cylinder 132 which support a mesh or other similar perforated wall portions. The apexes of members 130 are preferably imperforated V-shaped troughs and serve as drain troughs which discharge the liquor into perforated cylinder 132. Liquor is removed from the dilute suspension through members 130 and cylinder 132. In FIG- URE 4, a drainage member 130 is illustrated having perforations 131 along the side walls and having an imperforated V-shaped trough 133. The consistency of the pulp is increased to about 10% to about 12% at the top of washer 118 where the pulp is skimmed off by a scraper 134 and passed via line 135 into a launder 136.
The liquor removed by means of members 130 and cylinder 132 is introduced into a spent liquor tank 138 through line 140 at a temperature below the cooking temperature, for example, between about 250 F. to about 300 F. with a high concentration of dissolved solids. A portion of the liquor in tank 138 is pa sed through line 142 by pump 144 to be introduced through line 126 into digester leg portion 114. The remainder of the spent liquor is passed through line 146 to multiple-effect evapor-ators (not shown) for concentration and subsequent smelting, as is conventional in the art. However, since the liquor is recovered at a higher temperature than in prior art installations, an improved overall heat recovery is achieved. Steam liberated in tank 138 is vented through line 148 to heat exchanger 150 to preheat makeup cooking liquor in line 18.
The pulp in launder 136 is passed through blow line 152 provided with a blow valve 154 into a small cyclone 156 at the inlet to a blow tank 158. Cyclone 156 distributes the stock in a thin sheet for tangential discharge through line 160 into blow tank 158 to facilitate the liberation of steam from the stock with minimum fibre entrainment.
Flash steam is liberated from the blown stock and is passed upwardly into a comically-shaped funnel 162 wherein the steam is condensed by contact with cooling water introduced through line 164 and discharged in spray form through a perforated plate 166. Steam condensate and cooling water is removed from the funnel 162 through line 167 and is passed into an accumulator tank 168. Blow tank 158 also receives condensate from the heat exchanger 150 through line 170. Blow tank 158 additionally functions as a stock storage vessel balancing digester operations with final washing operations in vacuum washers 172 and 174.
Accumulator 168 is provided with an external liquor circuit including line 180, heat eychanger 182, lines 184, 186, 188 and pump 190. A temperature responsive flow control valve 192 is provided in bypass line 186 to regulate the flow of water to heat exchanger 182 through line 180, and the temperature of incoming fresh water supplied to heat exchanger 182 through line 194. From heat exchanger 182, the fresh water is passed through line 196 to a heat exchanger 198 in vent line 178. The heated water is passed through line 200 to a hot water storage tank 202 from which water is removed to process as desired through line 204 by pump 206. A portion of the incoming fresh Water in line 194 may be introduced dirlecly into the accumulator 168 through lines 208 and From accumulator 168, water is passed through line 210 by pump 212 to line 164 and perforated plate 166 for condensing flash steam as previously described. Water is also withdrawn from accumulator 168 through line 214 by pump 216 and is passed through line 218 to vacuum washer 174 as will be discussed hereinafter.
Pulp diluted to a suitable consistency in blow tank 158 is withdrawn through line 230 and is passed through line 232 to a pressurized pulp screen assembly 234. Screen assembly 234 further refines the stock and returns oversized fibre masses to blow tank 158 through line 236. The stock from screen assembly 234 is passed through line 238 to an inlet box 240 adjacent vacuum washer 172. The stock is taken up on a conventional perforated drum 242 and sprayed with :a wash medium from spray head 244. The wash medium is supplied to spray head 244 from the third stage vacuum washer 174 through line 246. Liquor and wash medium drain through perforated drum 242 and are removed by line 248 to a washer liquor seal tank 250 which is provided with a baflie 252 and a vent line 254. A portion of the liquor in tank 250 is removed through line 256 and passed by pump 258 through lines 260 and 126 to digester 112. The remainder of the liquor in tank 250 is passed through line 262 by pump 264 and is passed through line 266 to blow tank 158 to dilute the stock therein, or through line 268 for admixture with the diluted pulp in line 230 being introduced into the screen assembly 234 through line 232.
The pulp stock from vacuum washer 172 is discharged into a trough 27 0 for treatment to break up sheeted pulp. The pulp is diluted in trough 270 with liquor supplied from a liquor seal tank 272 through line 274, pump 276, and lines 278 and 280. The diluted pulp in trough 270 is acted upon by blades 282 and is passed to the rotating perforated drum 284 of vacuum washer 174. Here the pulp is washed by water supplied to a spray head 286 through line 218 from accumulator 168. The wash water passes through the perforations of drum 284 and is removed by line 288 to the liquor seal tank 272 provided with suitable baflles 290 and a vent 292. The pulp which has now undergone a three-stage washing is discharged from cylinder 284 into hopper 294 for further processing.
Spray heads 244 and 286 of vacuum Washers 172 and 174, respectively, are enclosed within housings 296 and 298, respectively. Housings 296 and 298 are supplied with flash steam from blow tank 158 through line 300 under control of valve 302 to essentially prevent foaming at vacuum washers 172 and 174 and their sea- l tanks 250 and 272 by eliminating air infiltration.
While I have shown and described several embodiments in accordance with the present invention, it is understood that the same is not limited thereto, but is susceptible of many changes and modifications within the spirit and scope thereof, and I, therefore, do not Wish to be limited to the details shown and described herein, but intend to cover all such changes and modifications as are encompassed by the scope of the appended claims.
I claim:
1. A process for digesting cellulosic material comprising vacuum deaerating said material, submerging said material in liquor forming a slurry of pumpable consistency, impregnating said material by subjecting the material to progressively increasing hydraulic pressures, introducing the impregnated material into a digester, digesting said impregnated material to pulp in non-submergence in the presence of steam, diluting the pulp within the digester with additional liquor, transferring the diluted pulp to a Washer, washing the diluted pulp in said Washer, removing liquor from the diluted pulp substantially at the cooking temperature, introducing the washed pulp a a thin stream into a blow tank, condensing the steam within the blow tank by direct contact with cooling water, passing the steam condensate and cooling Water to an accumulator tank, vacuum washing the pulp removed from said blow tank in a vacuum washer having a wash liquid sprayer, returning liquor from the vacuum washing step to said blow tank, and injecting steam from said blow tank into a header surrounding the wash liquid sprayer of the vacuum washer.
2. A process for digesting cellulosic material comprising vacuum deaerating said material, submerging said material in liquor forming a slurry of pumpable consistency, impregnating said material by subjecting the material to progressively increasing hydraulic pressures, introducing the impregnated material into a digester, continuously digesting said impregnated material to pulp in said digester, diluting the pulp within said digester, removing liquor from the pulp substantially at the cooking temperature,
introducing the pulp into a blow tank, condensing the steam Within said blow tank by direct contact with cooling water, passing the steam condensate and cooling water to an accumulator tank, vacuum washing the pulp removed from said blow tank in a vacuum washer having a wash liquid sprayer, returning liquor from the vacuum washing step to said blow tank, and injecting steam from said blow tank into a region surrounding the wash liquid sprayer of the vacuum washer.
3. In a process for digesting cellulosic material comprising deaerating said material, impregnating said material, introducing said material into a digester, digesting, said material to pulp, introducing the pulp into a blow tank, vacuum washing the pulp removed from said blow tank in a vacuum Washer having a wash liquid sprayer, the improvement which comprises returning liquor from the vacuum washing step to said blow tank, and injecting steam formed in said blow tank into a header surrounding the wash liquid sprayer.
4. A process for digesting cellulosic material comprising deaerating said material, impregnating said material, introducing said material into a digester, digesting said material to pulp, diluting the pulp within the digester with additional liquor, transferring the diluted pulp to a Washer, washing the diluted pulp in said washer, removing liquor from the diluted pulp, introducing the washed pulp into a blow tank, vacuum washing the pulp removed from said blow tank in a plurality of vacuum washers, each having a wash liquid sprayer, returning liquor from the vacuum washing step to said blow tank, and injecting steam formed in said blow tank into headers surrounding the wash liquid sprayers.
5. Apparatus for treating wood chips or the like, comprising a substantially upright tank, an annular housing rigidly secured to the bottom of said tank and closed off by a bottom wall, a hollow chip deflecting member having an essentially conical upper surface projecting above said bottom wall substantially in the center thereof, said deflecting member being provided with openings into the interior thereof, gear means mounted within the interior of said deflecting member, a casing rotatably positioned within said housing, drive gear means for rotating said casing, and a plurality of screw conveyors mounted at the outer ends thereof upon said casing and at the other ends thereof being adapted to convey chips through said openings into the interior of said deflecting member.
6. Apparatus for treating wood chips or the like, comprising a substantially upright tank, an annular housing rigidly secured to the bottom of said tank and closed off by a bottom wall, a hollow chip deflecting member having an essentially conical upper surface projecting above said bottom wall substantially in the center thereof, said deflecting member being provided with opposed openings to the interior thereof, gear means mounted within the interior of said deflecting member, a casing rotatably positioned within said housing and provided with an annular gear ring, drive gear means cooperating with said gear ring, a plurality of screw conveyors mounted adjacent to the upper surface of said bottom wall with their outer ends mounted upon said casing and with their inner ends extending through said openings in said deflecting member, means to rotate said screw conveyors to convey chips through said openings into the interior of said deflecting member, and a discharge conduit in communication with the interior of said deflecting member.
7. Apparatus for pulping cellulosic material which comprises: tank means to submerge said cellulosic material in cooking liquor to form a slurry of said cellulosic material and said liquor; a first conduit means; an impregnator for receiving said slurry in fluid communication with said tank means through said first conduit means, said impregnator including means to progressively increase the hydraulic pressure of said slurry; a digester; a liquor supply means for diluting said pulp leaving said digester; a second conduit means; a washer in fluid communication with said digester through said second conduit means for receiving diluted pulp, said washer having a plurality of perforated drainage members extending trans versely across said washer in a saw-toothed arrangement; and a third conduit means for withdrawing liquor out of said washer from said drainage members.
8. Apparatus for pulping cellulosic material which comprises: tank means to submerge said cellulosic material in cooking liquor to form a slurry of said cellulosic material and said liquor; a first conduit means; an impregnat-or for receiving said slurry in fluid communication with said tank means through said first conduit means, said impregnator including means to progressively in crease the hydraulic pressure of said slurry; a digester; a liquor supply means for diluting said pulp leaving said digester; a second conduit means; a washer in fluid communication with said digester through said second conduit means for receiving diluted pulp, said washer having a plurality of perforated drainage members extending transversely across said washer in a saw-toothed arrangement; and a third conduit means for withdrawing liquor out of said washer from said drainage members; a fourth conduit means; a blow tank for receiving discharge pulp from said washer through said fourth conduit means; and condensing means including cooling water spray means within said blow tank to condense steam flashed by entry of the pulp into said blow tank.
9. An apparatus for digesting cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said digester; means to introduce liquor into a lower region of said digester to dilute digested pulp; conduit means; a washer in fluid communication with said digester through said conduit means for receiving diluted pulp, said washer including a p1u rality of drainage members spaced in a staggered arrangement, each drainage member including essentially V- shaped imperforated bottom portions and perforated side wall portions, said imperforated bottom portions constituting drainage troughs for liquor passing through the side wall portion; and means to remove washed pulp from the top of said washer.
10. An apparatus for digesting cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said digester; means to introduce liquor into the lower portion of said digester to dilute digested pulp; conduit means, a washer in fluid communication with said digester through said conduit means for receiving diluted pulp, said washer including a plurality of drainage members spaced in staggered arrangement, each drainage member including essentially V- shaped imperforated bottom portions and perforated side wall portions, said imperforated bottom portions constituting drainage troughs for liquor passing through said side wall portions, an annular perforated drainage cylinder within said washer in fluid communication with 8 the drainage troughs of said drainage members; and means to remove wash pulp from the top of said washer.
11. An apparatus for digesting cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said.digester, means to supply steam into said digester to effect delignification of the cellulosic material; means to introduce liquor into the lower portion of said digester to dilute delignified pulp; conduit means; a washer in fluid communication with said digester through said conduit means for receiving diluted pulp, said washer including a plurality of drainage members spaced in a staggered arrangement, each drainage member including essentially V-shaped imperforated bottom portions and perforated side wall portions, said imperforated bottom portions constituting drainage troughs for liquor passing through said side wall portions; and means to remove wash pulp from the upper portion of said washer.
12. An apparatus for delignifying cellulosic material which comprises: a digester; means to supply cellulosic material and cooking liquor into said digester; means to supply steam to said digester to effect delignification of the cellulosic material; means to introduce liquor into a lower portion of said digester to dilute the delignified pulp; conduit means; a washer in fluid communication with said digester through said conduit means to receive diluted pulp, said washer including a plurality of drainage members spaced in a staggered arrangement, each drainage member including essentially V-shaped imperforated bottom portions and perforated side wall portions, said imperforated portions constituting drainage troughs for liquor passing through the side wall portions; an annular perforated drainage cylinder positioned within said washer in fluid communication with the drainage trough of said drainage members; and means to remove washed pulp from the upper portion of said Washer.
References Cited by the Examiner UNITED TATES PATENTS 2,969,156 1/1961 Miller et a1. 214-1782 2,999,784 9/1961 Hullman 162-19 3,050,201 8/1962 Humphrey 214-17.82 3,061,007 10/1962 Rich 162-237 3,081,820 3/ 1963 Schnyder 162-246 3,085,624 4/1963 Horstman 162-237 3,165,436 1/1965 Bennett et a1. 162-19 FOREIGN PATENTS 175,783 8/1953 Austria.
852,892 11/1939 France. 1,078,667 5/1954 France.
DONALL H. SYLVESTER, Primary Examiner.
J. H. NEWSOME, Assistant Examiner.

Claims (2)

1. A PROCESS FOR DIGESTING CELLULOSIC MATERIAL COMPRISING VACUUM DEAERATING SAID MATERIL, SUBMEGING SAID MATERIAL IN LIQUOR FORMING A SLURRY OF PUMPABLE CONSISTENCY IMPREGNATING SAID MATERIAL BY SUBJECTING THE MATERIAL TO PROGRESSIVELY INCREASING HYDRAULIC PRESSURES, INTRODUCING THE IMPREGNATED MATERIAL INTO A DIGESTER, DIGESTING SAID IMPREGNATED MATERIAL TO PULP IN NON-SUBMERGENCE IN THE PRESENCE OF STEAM, DURING THE PULP WITHIN THE DIGESTER WITH ADITIONAL LIQUOR, TRANSFERRING THE DILUTED PULP TO A WASHER, WASHING THE DILUTED PULP IN AAID WASHER, REMOVING LIQUOR FROM THE DILUTED PULP SUBSTANTIALLY AT THE COOKING TEMPERATURE, INTRODUCING THE WASHED PULP AS A THIN STREAM INTO A BLOW TANK, CONDENSING THE STREAM WITH IN THE BLOW TANK B DIRECT CONTACT WITH COOLING WATER, PASSING THE STREAM CONDENSED AND COOLING WATER TO AN ACCUMULATOR TANK, VACUUM WASHING THE PULP REMOVED FROM SAID BLOW TANK, IN A VACUUM WASHER HAVING A WASH LIQUID SPRAYER,RETURNING LIQUOR FROM THE VACUUM WASHING STEP TO SAID BLOW TANK, AND INJECTING STREAM FROM SAID LIQUID SPRAYER OF THE VACUUM WASHER.
5. APPARATUS FOR TREATING WOOD CHIPS OR THE LIKE, COMPRISING A SUBSTANTIALLY UPRIGHT TANK, AN ANNULAR HOUSING RIGIDLY SECURED TO THE BOTTOM OF SAID TANK AND CLOSED OFF BY A BOTTOM WALL, A HOLLOW CHIP DEFLECTING MEMBER HAVING AN ESSENTIALLY CONICAL UPPER SURFACE PROJECTING ABOVE SAID BOTTOM WALL SUBSTANTIALLY IN THE CENTER THEREOF, SAID DEFFECTING MEMBER BEING PROVIDED WITH OPENINGS INTO THE INTERIOR THEREOF, GEAR MEANS MOUNTED WITHIN THE INTERIOR OF SAID DEFFECTING MEMBER, A CASING ROTATABLE POSITIONED WITHIN SAID HOUSING, DRIVE GEAR MEANS FOR ROTATING SAID CASING, AND A PLURALITY OF SCREW CONVEYORS MOUNTED AT THE OUTER ENDS THERREOF UPON SAID CASING AND IN THE OTHER ENDS THEREOF BEING ADAPTED TO CONVEY CHIPS THROUGH SAID OPENINGS INTO THE INTERIOR OF SAID DEFFECTING MEMBER.
US274419A 1963-04-22 1963-04-22 Comprehensive pulping system for producing paper pulp Expired - Lifetime US3259538A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US274419A US3259538A (en) 1963-04-22 1963-04-22 Comprehensive pulping system for producing paper pulp

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US274419A US3259538A (en) 1963-04-22 1963-04-22 Comprehensive pulping system for producing paper pulp

Publications (1)

Publication Number Publication Date
US3259538A true US3259538A (en) 1966-07-05

Family

ID=23048119

Family Applications (1)

Application Number Title Priority Date Filing Date
US274419A Expired - Lifetime US3259538A (en) 1963-04-22 1963-04-22 Comprehensive pulping system for producing paper pulp

Country Status (1)

Country Link
US (1) US3259538A (en)

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3513994A (en) * 1968-09-27 1970-05-26 Clay Equipment Corp Bottom discharge silo construction
US3525665A (en) * 1965-10-22 1970-08-25 Lummus Co Method of transferring impregnated wood chips from an impregnating vessel to a digester
US3532232A (en) * 1968-12-09 1970-10-06 Eugene G Sukup Apparatus for evenly evacuating grain from a grain drying bin
US3595487A (en) * 1968-04-08 1971-07-27 Howard Bidwell Method of automating the operation of paper stock preparation processing apparatus
US3908839A (en) * 1972-10-16 1975-09-30 Jean Menaut Silo and means for removing particulate material therefrom
US4063654A (en) * 1975-08-11 1977-12-20 Shivvers Charles C Sweep auger apparatus
US4103788A (en) * 1977-06-23 1978-08-01 Sutton William H Apparatus for discharging from a silo
US4183706A (en) * 1979-01-26 1980-01-15 William Jackson Agitator for storage bin unloaders
US5203968A (en) * 1988-04-13 1993-04-20 A. Ahlstrom Corporation Apparatus for treating fiber suspensions having rotatable liquid permeable treatment ducts
US5207870A (en) * 1988-02-08 1993-05-04 Osmo Aho Process and equipment for pretreatment of cellulosic raw material
US5221434A (en) * 1988-04-13 1993-06-22 A. Ahlstrom Corporation Method for treating fiber suspensions
WO2010110724A1 (en) * 2009-03-26 2010-09-30 Metso Fiber Karlstad Ab Method and arrangement for wash after completed digestion in a continuous digester for the production of cellulose pulp
WO2011078775A1 (en) * 2009-12-23 2011-06-30 Metso Paper Sweden Ab Method and arrangement for improving a washing step after completed cooking in a continuous digester
WO2015183162A1 (en) * 2014-05-26 2015-12-03 Skandia Elevator Ab Grain sweep
WO2016068783A1 (en) * 2014-10-31 2016-05-06 Valmet Ab Method and arrangement for discharge dilution

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR852892A (en) * 1938-11-09 1940-03-05 Maschb Scholz & Co Method and device for the continuous cooking of fibrous cellulosic material, rubber, cut roots, etc., attacked by hot liquid under pressure
AT175783B (en) * 1949-10-22 1953-08-10 Phrix Werke Ag Method and apparatus for the continuous cooking of cellulosic material
FR1078667A (en) * 1953-04-08 1954-11-22 Continuous pulp manufacturing improvements
US2969156A (en) * 1956-05-09 1961-01-24 Miller Hofft Inc Unloader for circular silos
US2999784A (en) * 1957-07-10 1961-09-12 Escher Wyss Gmbh Process and apparatus for the treatment of fibrous materials in the production of cellulose or semi-cellulose
US3050201A (en) * 1960-08-29 1962-08-21 Frederick H Humphrey Apparatus for unloading materials from containers
US3061007A (en) * 1961-01-24 1962-10-30 Improved Machinery Inc Continuous pulping apparatus
US3081820A (en) * 1958-01-16 1963-03-19 Lummus Co Pulp preparation
US3085624A (en) * 1959-11-30 1963-04-16 Bauer Bros Co Continuous digester
US3165436A (en) * 1961-09-11 1965-01-12 Lummus Co Continuous impregnating and pulping process

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR852892A (en) * 1938-11-09 1940-03-05 Maschb Scholz & Co Method and device for the continuous cooking of fibrous cellulosic material, rubber, cut roots, etc., attacked by hot liquid under pressure
AT175783B (en) * 1949-10-22 1953-08-10 Phrix Werke Ag Method and apparatus for the continuous cooking of cellulosic material
FR1078667A (en) * 1953-04-08 1954-11-22 Continuous pulp manufacturing improvements
US2969156A (en) * 1956-05-09 1961-01-24 Miller Hofft Inc Unloader for circular silos
US2999784A (en) * 1957-07-10 1961-09-12 Escher Wyss Gmbh Process and apparatus for the treatment of fibrous materials in the production of cellulose or semi-cellulose
US3081820A (en) * 1958-01-16 1963-03-19 Lummus Co Pulp preparation
US3085624A (en) * 1959-11-30 1963-04-16 Bauer Bros Co Continuous digester
US3050201A (en) * 1960-08-29 1962-08-21 Frederick H Humphrey Apparatus for unloading materials from containers
US3061007A (en) * 1961-01-24 1962-10-30 Improved Machinery Inc Continuous pulping apparatus
US3165436A (en) * 1961-09-11 1965-01-12 Lummus Co Continuous impregnating and pulping process

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3525665A (en) * 1965-10-22 1970-08-25 Lummus Co Method of transferring impregnated wood chips from an impregnating vessel to a digester
US3595487A (en) * 1968-04-08 1971-07-27 Howard Bidwell Method of automating the operation of paper stock preparation processing apparatus
US3513994A (en) * 1968-09-27 1970-05-26 Clay Equipment Corp Bottom discharge silo construction
US3532232A (en) * 1968-12-09 1970-10-06 Eugene G Sukup Apparatus for evenly evacuating grain from a grain drying bin
US3908839A (en) * 1972-10-16 1975-09-30 Jean Menaut Silo and means for removing particulate material therefrom
US4063654A (en) * 1975-08-11 1977-12-20 Shivvers Charles C Sweep auger apparatus
US4103788A (en) * 1977-06-23 1978-08-01 Sutton William H Apparatus for discharging from a silo
US4183706A (en) * 1979-01-26 1980-01-15 William Jackson Agitator for storage bin unloaders
US5207870A (en) * 1988-02-08 1993-05-04 Osmo Aho Process and equipment for pretreatment of cellulosic raw material
US5203968A (en) * 1988-04-13 1993-04-20 A. Ahlstrom Corporation Apparatus for treating fiber suspensions having rotatable liquid permeable treatment ducts
US5221434A (en) * 1988-04-13 1993-06-22 A. Ahlstrom Corporation Method for treating fiber suspensions
WO2010110724A1 (en) * 2009-03-26 2010-09-30 Metso Fiber Karlstad Ab Method and arrangement for wash after completed digestion in a continuous digester for the production of cellulose pulp
WO2011078775A1 (en) * 2009-12-23 2011-06-30 Metso Paper Sweden Ab Method and arrangement for improving a washing step after completed cooking in a continuous digester
US8366876B2 (en) 2009-12-23 2013-02-05 Metso Paper Sweden Ab Method and arrangement for improving a washing step after completed cooking in a continuous digester
WO2015183162A1 (en) * 2014-05-26 2015-12-03 Skandia Elevator Ab Grain sweep
US10238042B2 (en) 2014-05-26 2019-03-26 Skandia Elevator Ab Grain sweep
WO2016068783A1 (en) * 2014-10-31 2016-05-06 Valmet Ab Method and arrangement for discharge dilution

Similar Documents

Publication Publication Date Title
US3259538A (en) Comprehensive pulping system for producing paper pulp
CA1245011A (en) Countercurrent acid hydrolysis
US3532594A (en) Method of digesting cellulosic material in steam phase
US4274913A (en) Process for producing alkali pulp
US3298899A (en) Method and arrangement for washing and cooling at the outlet end of a continuous cellulose digester
US2359543A (en) Apparatus for continuous digestion of fibrous material
US3007839A (en) Method and plant for continuous cellulose digestion
US1843466A (en) Paper manufacture
US1982130A (en) Chemical treatment process for pulp manufacture
US2474862A (en) Process and apparatus for continuous digestion of fibrous materials
US4123318A (en) Three-vessel treatment system
US6159338A (en) Supply of washing liquid in a fractionating multi-stage washer
US2999785A (en) Method and plant for washing of cellulosic pulp under overpressure
US2534324A (en) Process for separating cooking liquor from pulp
US3579420A (en) Sieve device in an upright cylindrical container for continuous flow of cellulosic material
US3258390A (en) Method and apparatus for maintaining a water balance during impregnation and digestion of cellulosic material
US4608122A (en) Method for washing a paper fiber on a belt washer using a sonic frequency disturbance
US4539827A (en) Belt washing improvements
NO145592B (en) A sealing head.
US1954012A (en) Manufacture of cellulose and the like
US3681192A (en) Sluice feeders for introducing finely divided chips into vessels under pressure
WO1989012716A1 (en) Process and apparatus for the manufacture of pulp for paper, board, fiberboard and similar products
US2769710A (en) Process for the continuous treatment of vegetable fibers
EP0782642B1 (en) Method and apparatus for the continuous production of cellulosic pulp
US2711359A (en) Bleaching plant and method of bleaching cellulose pulp