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US2372605A - Method and apparatus for making solid objects from metal powder - Google Patents

Method and apparatus for making solid objects from metal powder Download PDF

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Publication number
US2372605A
US2372605A US417806A US41780641A US2372605A US 2372605 A US2372605 A US 2372605A US 417806 A US417806 A US 417806A US 41780641 A US41780641 A US 41780641A US 2372605 A US2372605 A US 2372605A
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Prior art keywords
powder
rams
current
die
particles
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US417806A
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Walter F Ross
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Fellows Gear Shaper Co
Jones and Lamson Machine Co
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Fellows Gear Shaper Co
Jones and Lamson Machine Co
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B30PRESSES
    • B30BPRESSES IN GENERAL
    • B30B11/00Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
    • B30B11/02Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses using a ram exerting pressure on the material in a moulding space
    • B30B11/04Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses using a ram exerting pressure on the material in a moulding space co-operating with a fixed mould
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously

Definitions

  • the present invention relates to the subject generically known as powder metallurgy. It is more particularly concerned with that phase of the art which consists in consolidating metallic powders into coherent objects by simultaneous application of heat and pressure.
  • the heat treatment is carried on at a temperature high enough to cause fusion and flow of the ingredient of lower melting point.
  • the primary object of this invention is to provide a commercial machine adapted to supply this need.
  • Objects contributory to the foregoing are to regulate and control the temperature, amount and timing of heat input during pressing; to regulate the intensity of pressure loading applied to the powder mass or briquette; and to apply shock or impact loading in conjunction with constant, or squeeze, loading, or independently.
  • Further objects, which are preferred but not obligatory, are to eflect a precompression, without heating, of the powder in the same die or mold in which hot compression is effected; to deliver automatically measured quantities of powder to the die or mold, and to carry out the steps of loading the mold, precompressing the powder, hot pressing the briquette, and electing the finished product in an automatic sequence of operations.
  • Fig. 1 is a central vertical section of the machine, showing the hot pressing elements thereof in elevation;
  • Fig. 2 is a side view of the machine as seen from the right of Fig. 1;
  • Fig. 3 is a sectional view of the hot pressing equipment in a plane parallel to that of Fig. l, and shown on a larger scale;
  • Fig. 4 is a partial plan view of the machine
  • Fig. 5 is a horizontal section taken on line 5-5 of Figs. 1 and 2;
  • Fig. 6 is a detail sectional view taken on line 6-6 of Fig. 1 and shown on a larger scale;
  • Fig. 7 is a vertical sectional view taken approximately on line 1-7 of Figs. 1 and 5;
  • Fig. 8 is a horizontal section taken on line 88 of Fig. 7;
  • Fig. 9 is a partial section and partial plan view of the powder metering and feeding ele ment of the machine taken on line -9 of Fig. "5';
  • Fig. 10 is a diagram of electrical circuits controlling the operation of the machine.
  • the operative instruments of the machine are mounted and supported by a frame structure of any convenient construction, here shown as horizontal plates it, ii, 52 and I3 spaced apart, one above another, by spacing sleeves l4 located at suitable positions, and tied together by rods 85 passing through holes in the plates and through the sleeves E i, and on the ends of which nuts it are threaded above the top plate in and beenath the bottom plate 53.
  • This structure rests on a base, a portion of which is indicated in Figs. 1 and 2 as an I beam M.
  • a turret 48 containing four dies i9, which is indexed to bring each die successively into each of four different positions; a hopper 20 for containing powder; a metering head 2i; precompression plungers 22 and 23; main pressing bars or rods 2% and 25 carrying plungers or rams 26 and 27, respectively; an ejector 28; mechanisms for operating these several instruments in proper sequence; and means for causing flow of electric current between the main pressure plungers through the powder in suificient volume to heat the powder by electric resistance to welding temperature.
  • and a guide 29 for the upper precompression plunger 22 are all supported on or provided in a bracket 30 supported on and in the frame plate II.
  • the metering head is secured to a shaft 32, rotatable in a bearing 33 in the bracket 30, and contains a number of passages 34 arranged to be placed in succession, by rotation of the head, beneath the outlet 35 of the hopper. Passages 34 extend throughout the depth of the metering head and are obstructed at their lower ends by the supporting surface of bracket 30. Adjacent to one of the stopping locations of these passages, a conduit 36 passes through the bracket 30 and into the side of the plunger guideway 29 for conducting powder to that molding die which is alined with plungers 22 and 23.
  • Blocks 3 are adjusted by screws 38 and 39 to protrude more or less into the metering passages or cavities 34 for regulating the volume of the charges.
  • a ratchet 40 is keyed to shaft 32 and is operated by a pawl 4
  • a guide 44 for the lower precompression plunger 23 is mounted in a bracket 45, supported on the frame plate I2, in vertical alinement with the guide 29, beneath the turret l8 and in alinement with one of the stopping positions of the dies l9.
  • a seal 46 is mounted on guide 44 and cameos closely surrounds the plunger 23 to exclude metal dust from the guide.
  • Plunger 22 is connected by a pivot pin 41 with a lever 48 pivoted at 49 to a link 50, which in turn. is pivoted at 5! to a bracket 52 on the frame plate M.
  • This lever is coupled by a connecting rod 53 with a crank pin 54 carried by a cam shaft 55 which rotates in a bracket 56 secured to the under side of plate ll.
  • Plunger 23 is coupled by a pivot 51 with a lever 58, which is suspended from bracket 45 by a link 59.
  • a rod 50 is coupled at one end to lever 58 and at its other end to a lever 6
  • a spring 63 reacts between a. portion of bracket 45 and a shoulder 64 on the rod 60, holding a cam follower portion of lever 6i against a cam 65 on cam shaft 55.
  • the cam shaft is rotated by an electric motor 66 which drives a shaft 61 through belt transmission 68, said shaft 61 being contained in a bearing in bracket 56 and carrying a worm 69 meshing with a worm wheel 10 on the cam shaft.
  • Cam 43 which rotates the metering head, is likewise secured to shaft 55.
  • a rod or core pin H for providing such an opening is mounted to travel endwise through the plunger 23, which has a central bore for the purpose, and to enter a recess 12 in the plunger 22.
  • This core pin is coupled by a pin and slot connection with a lever 13 which is pivoted at 14 to a bracket 15, (said bracket being secured to the under side of frame plate l2), and the other arm of which is coupled by a link 16 with a lever 11 mounted beside the lever 6
  • a spring I! is suspended from an anchorage on bracket 45 and connected to lever I3, exerting force thereon to hold a cam follower portion of lever 11 against a cam IS on cam shaft 55.
  • cams and the crank pin 54 are suitably timed to cause withdrawal of the plungers from turret [8 prior to indexing movement of the latter and then, in the following order, advance plunger 23 into the lower end of the contiguous die l9, project the core rod 'II from the plunger, turn the metering head to deliver a. quantity of powder into the die, and advance plunger 22 so as to exert a pressure against the mass of powder resting on the lower plunger. Sumcient pressure is thus exerted to cause the powder briquette to remain in the die while traveling to the main pressing position.
  • the core rod l I may be removed, and solid plungers substituted for the recessed plunger 22 and tubular plunger 23.
  • the ejector 28 which is above the turret in alinement with the final position of the dies, is likewise operated by the cam shaft 55. It is carried by the lower end of a bar 80, which is movable endwise through guide passages in the frame plates [0 and II and is normally held above the turret by a spring 8
  • the main pressing action is performed when the die reaches the rearmost position shown in Figs. 5 and 8.
  • the plunger (or ram-carrying) rods 24 and 25 are forced toward one another with a powerful squeezing action by toggle linkages. These linkages are alike for both plungers. That for the upper plunger consists of double links 85 and 86 pivoted to a yoke 91, links 89 and B9 pivoted to a collar 90, and knuckle pins I, connecting links 85 and 88 together, and 92 connecting link 86 to link 89.
  • Yoke 81 surounds the plunger rod 24 and is anchored to the frame.
  • the anchorage here shown is a sleeve 93 supported in frame plate I and'through which the rod 24 is movable, the yoke being confined with provision for limited rocking movement, between said plate and a shoulder 94 on sleeve 93.
  • Collar 90 surrounds the plunger rod and grasps it frictionally with sufiicient force to raise the rod when the knuckle pins are moved apart to break the toggles, while permitting slip of the rod under the hammer impulsion later described.
  • Adjustable means to maintain the described clutching eflect after wear may be used. This collar impels the rod, when the toggles are straightened, by thrusting against a shoulder 95 on the rod.
  • of one toggle is connected by a link 96 with a pivot pin 91 carried by a rocker 98 which is supported rotatably in a bracket 99 suspended from the frame plate I0.
  • the other toggle knuckle 92 is connected by two links, I00 and II, which embrace the rod or bar 24, with pivot pins I02 and I03 mounted in alinement with each other at the diametrically opposite side of rocker 99 from the pivot 92'.
  • Identical toggle links I04, I05, I06 and I01 are connected to a yoke I08 (which is conflnedbetween the bottom frame plate I3 and the shoulder I09), and a collar IIO which surrounds rod 25 and thrusts against a shoulder III thereon.
  • the knuckle pins of the latter toggle are connected by an inner link II 2 and two outer embracing links H3 with pins H4, H5 at diametrically opposite sides, of a rocker II6 which is pivotally mounted on a bracket I I7 secured to the bottom plate I3.
  • the two rockers 98 and 6 are operated by connecting rods H8 and H9 from crank pins I and I2I' on a crank disk I22, the connecting rods being coupled with the rockers by pivots I20a and I'2Ia.
  • the several links and pivots are arranged so that, when crank pin I20 is on dead center with respect to connecting rod M8, the pivots 91, I02 and I 03 are on dead center with respect to the links 96, I00 and II", respectively, and ram 26 is fully advanced.
  • crank pin I2I, connecting rod II9, the pivots H4 and 5, links H2 and H3, and ram 21 The throw of the cranks I20 and I2I and the displacement of the toggle links are made sufiicient to withdraw the rams wholly from the turret I8.
  • crank pins I20 and I2I are preferably nonsymetrical with respect to the axis of the crank disk and their respective connecting rods, in such manner that one crank pin approaches its dead center in advance of the other. Assuming that the pin I2I is the one in advance, this pfii will reach and pass dead center while the crank pin I20 is approaching dead center, if their rotation is carried so far. Hence the rams, after entering the die, travel at unequal speeds and the mass of powder confined between them is shifted along the die while being compressed; at least during the final stages of compression. If the pin I2! is moved beyond dead center through a small angle while the pin I20 is coming near dead center, there will be a slight movement of both plungers in the same direction at the same time.
  • Crank disk I22 is mounted on a shaft I29 rotatable in a bracket I24 on the frame plate I2.
  • This shaft is driven by a reversible electric motor I25 (secured to frame plate I2) which, for convenience, may be called the main motor, through a belt or chain I26, 8.
  • a reversible electric motor I25 secured to frame plate I2
  • main motor through a belt or chain I26
  • one of the rams is provided with a projecting rod to hold the passage open while pressure is applied; as shown in Fig. 3 with respect to ram 26.
  • Such rod may be made of non-conductive material or of metal electrically insulated from one, or both rams. It is, of course, omitted, and rams with closed ends employed, when solid articles are made.
  • the rams or plungers 26 and 21 are the terminals of an electric welding circuit through which electric current of low voltage and high amperage is delivered to heat the metal powder, by the electrical resistance of the powder, to a temperature at which the particles are soft enough to be readily deformable, and will unite. They are of form and dimensions such that they may enter and fit closely but slidingly in the dies.
  • Ram 26 is formed with an enlargement I34 back of its terminal extremity and with a flange I35 and centering lip I36 at its opposite end to bear on and embrace the end of plunger rod 24. It is secured to the plunger rod by a screw I31 and is insulated from the rod by sleeves and washers of insulating material, all comprehensively desigated I38.
  • Ram 21 is correspondingly formed and is secured to and insulated from the plunger rod 25 by duplicates of the same means, designated by the same reference characters.
  • Electrodes I39 and I40 surround the enlarged portion I34 of the respective rams with good electrical contact and a water tight fit. They are internally cored to provide chambers I through which water or other cooling fluid may be passed to keep the rams at a low temperature. They are connected by means of laminated flexible conductors I42 and I43 with the secondary winding of a high current transformer I44.
  • the dies I9 are each constructed of a series of rings in tandem arrangement and accurate alinement, supported in a shell or casing I45 by insulating material I46 which insulates them electrically from the shell.
  • the rings may also be insulated from each other by thin washers of mica or the like to prevent a short circuit through them; but this is not of vital importance, for reasons later set forth, and each die may be made of a single solid piece.
  • Such rings may be made of hard and tough metal finished internally to exact prescribed dimensions with polished surfaces.
  • the several die casings I45 are provided with an inner flange at one end and a lock at the other end to retain the insulation I46, between which and the rams are air spaces wide enough to prevent leakage of current.
  • the briquette is further subjected to shock or impact loading applied by a hammer I48 to the ram 26 through the plunger rod 24.
  • This hammer is mounted to slide on a guide I49 mounted on the uppermost frame plate, and is arranged to move in alinement with the plunger rod 24 and to impinge on a cap piece I50 secured to the upper end of said rod. It is coupled by a pin and slot connection I5I with a lever I52 which is pivoted at I53 to a bracket I54 secured to the top plate.
  • An electric motor I55 which may be called the hammer motor, actuates the hammer through a train consisting of belt I56, pulley I51, shaft I58, worm I59, worm gear I60, shaft I6I, change gears I62 and I63, shaft I64 and cam I65, cooperatively arranged as clearly shown in Figs. 1 and 4.
  • This cam is located beneath the lever I52 and engages a projection I66 on the lever. In the form here shown, it is provided with a continuous rise through 360 of arc and a sharp drop, whereby it is adapted to raise the hammer, and permit descent of the hammer by gravity, once during each revolution.
  • I may use a cam designed to cause more than one hammer stroke during each revolution, or to cause a greater or less drop of the hammer than that here indicated, Or to efiect a series of hammer blows of progressively increasing force as the compression proceeds; or provide means for applying force other than gravity to the hammer.
  • I may cause the hammer to deliver as many blows as desired during or after the advance of the rams. Any desired timing of the shock impacts with the pressure loading may be practised.
  • Indexing of the turret I 8 is efiected by an electric motor I61 under control of the pressure mechanism.
  • Motor I61 which may be called. the indexing motor, drives a pulley I68 on shaft I69 by a belt I10.
  • Shaft I68 carries a worm I1I meshing with a worm gear I12 on the shaft I13, which turns in a bearing formed in a part of the bracket I24, and to which the turret is secured.
  • Shaft I69 carries also a gear I14 which drives an index plate I15 through a compound gear I16, I11, of which one element meshes with gear I14 and the other with teeth on the circumference of the index plate.
  • the index plate includes a flange I18 having a single notch arranged to be entered by the toe of a locking dog I19 which is mounted on a pivot I80.
  • An arm I8I forms a structural part of the dog I19 and extends to the opposite side of pivot I80 therefrom.
  • a spring I82 is connected to arm I8I and acts so as normally to hold the dog in locking engagement with the index plate.
  • a striker I83 is connected to arm Hit by a pivot I84 and is weighted so that it bears against a stop pin I85. It projects into the path of a cam projection I86 on the circumference of crank disk I22, and has a beveled face arranged to be engaged with the beveled advancing face of cam I86 during the rotation of the crank disk in the direction which causes separation of the pressing rams.
  • the direction referred to is clockwise and is indicated by the arrow A.
  • Arm I8I controls a switch I81 in the circuit of the indexing motor, (further shown diagrammatically in Fig. 10).
  • the arrangement of these parts is such that the initial movement imparted to the arm I8I closes the switch contacts, thereby energizing the motor I61, and thereafter the dog i fully withdrawn from the index plate.
  • spring I82 holds the dog against the index plate ready to reenter the notch in the latter when the plate has made a complete revolution.
  • cam I86 displaces the striker in passing it without moving the lever.
  • the cam is adjustable and is set to start the indexing action after the rams have withdraw from the turret and before the crank disk has come to the end of its clockwise rotation.
  • the gearing I14I15 which drives the index plate is in ratio to the worm gearing I1I--I12 such that it turns the index plate through a complete rotation while the turret is turned through a quarter rotation; i. e., from one stopping place to the next.
  • the dog enters the notch in flange I18 and the arm I8I opens the switch I81, causing the indexing motor to stop.
  • crank disk I22 coacting with limit switches I90 and I9I respectively, in a switch box I92, (Figs. 1 and 2).
  • limit switches are interconnected with the switch contact I81 as electric interlocks so as to prevent advance of the compression rams, after their retraction to permit indexing of the turret, until the indexing movement has been completed.
  • Suitable electrical connections for the purpose are shown in the diagram, Fig. 10. It may be noted that in this diagram the crank disk I22 is in the position occupied when the rams are withdrawn, whereas Figs. 1-3 show the condition where the rams are fully advanced into a. die.
  • All of these cam elements may be adjusted, or shifted to different positions, along the circumference of the crank disk in order to control and regulate the extent of penetration of the rams into the dies, short of or up to the limit established by the toggle linkages.
  • the intensity of pressure loading on the charges of powder may be thus regulated, in conjunction with regulation of the quantity of powder, or the dimensions of the briquette, placed in the die.
  • An important part of the invention consists in methods of applying electric heating current, in conjunction with application of mechanical force, to the powder mass or briquette, and in means for carrying such methods into effect.
  • the methods referred to include the steps of de livering heating current intermittently in impulses of shorter or longer duration, varying the intensity of the current thus delivered, and regulating the number, intensity and duration of current impulses according to the character of the material undergoing the consolidating treatment.
  • the effect of the current of high amperage and low voltage is to heat the particles of the powder to a condition of plasticity at their points of contact.
  • the particles of powder are in contact with one another at a comparatively few points of relatively narrow area. Resistance to flow of current from particle to particle is therefore very great, and is greatest at the points of contact which have the least area.
  • These points are quickly brought to the plastic condition in which they join together cohesively and are sufliciently ductile to be readily deformed by the pressure. Such deformation enlarges the contact areas and causes the interparticles resistance to be diminished.
  • repeated impulses of current and continued pressure application, or repeated hammer blows a progressive and irregular deformation of the particles occurs as the narrow contact areas become wider and the particles approach mutual conformity .of shape.
  • the method of applying current in brief impulses is of advantage over continuously passing current through the material, in a number of respects. It enables the heating effects to be accurately controlled. It avoids any serious heating of the die member even though the latter be continuously conductive and thus capable of furnishing shunt paths for the current. Due to the short duration of current flow during each impulse, the powder particles are heated to welding temperature at their contact points while the die is not heated obiectionably. It enables the optimum treatment for any particular material or mixture of materials to be determined and accurately duplicated in treating successive powder masses of like composition.
  • the heat input and temperature may be easily and exactly controlled and adjusted to the characteristics of the metal operated on.
  • metals become plastic.
  • the plastic range varies with diflerent metals, but with most metals its lower limit is at a temperature considerably below the melting point. However, in some cases the plastic range is very narrow and close to the melting point. It is necessary to maintain the metal in the plastic range While pressing for, if the metal melts, due to too great an input of heat or to the die being too highly heated, it acquires the undesirable properties of cast metal upon cooling. There would also be a tendency for the metal to adhere to the die walls or the rams.
  • Fig. 10 Metals that are not heated to the plastic stage have low strength, both in tension and compression, low density, and poor structure. They are liable to change their dimensions in unpredictable methods referred to is shown diagrammatically in Fig. 10.
  • P represents the primary
  • S the secondary, windings of the high current transformer I.
  • the primary winding is tapped at various points and such tapping points are connected electrically with removable contact buttons I99 on a tap selector I94.
  • a contact arm I9! is connected in the circuit and is arranged to pass from one contact button to the next in succession in time with the rotation of the crank disk I22.
  • crank shaft I29 It may be carried by the crank shaft I29, or may be driven therefrom by intermediate gearing so as to turn through a larger or smaller arc than that through which the crank disk tums, if desired.
  • the several contact buttons may be connected to any desired ones of the tapping points, so as to put different fractions of the primary winding in the circuit in any desired order.
  • any of these contacts may be removed and wholly omitted, or others may be substituted for them.-
  • the capacity for adjustmentand variation in these respects makes it possible to apply any desired number of current impulses during the cycle, to make such impulses longer or shorter, to make them of equal or unequal strength, and to apply relatively stronger or weaker current impulses in any desired sequence.
  • thecurrent may be progressively incremd or decreased as the interparticle resistance diminishes with widened areas of contact, or an impulse of low strength may be administered between strong impulses, and vice versa.
  • a device for interrupting the transformer circuit in time with the movement of the selector arm is associated with the selector.
  • This device comprises a cam I96 rotated in synchronism with the arm I and having projections I9'I arranged to open a face plate interlock I98 in circuit with a line contact switch I99.
  • the projections I9'I are adjustable and removable for substitution of others subtending larger or smaller angles, to correspond with the spacing and extent of the selector contacts I93. They are located so as to open the switch I99 just before the selector arm leaves any one of the contacts I93 so as to avoid arcing and to prevent the transformer circuit from being closed whenever the selector arm bridges across two contacts.
  • This device is timed also to insure that there will be no current in the electrodeswhen the rams are being retracted from the die.
  • the diagram further shows a starting switch 299 for the motor 96 of the measuring and precompresslon means, (called for convenience the loading motor), and a switch or interlock 29I for controlling the hammer motor I55.
  • This interlock is shown as operated by a cam 292 on the crank shaft I23, which may be suitably designed to start and stop the hammer motor once or a number or times during the persistence of the continuous pressure loading.
  • the diagram further shows main reversing switches 293 and 294 for the main motor I25; main switches 295, 296 and 29'! for the loading motor, indexing motor and hammer motor, respectively; auxiliary starting devices for these several motors; and a time relay 298 in connection with the main motor switch 293 and the interlock I99.
  • this time relay is to delay reversal of the main motor after the rams have been pressed together, for such length of time as may be prescribed for hammering or persistence of the squeezing pressure and heating effect. Holding circuits are also provided in order to insure continual supply of current to the main motor. But as the details of the electrical circuits and connections are not of the essence of the. invention, but are within the field of electrical engineering design and may be widely varied, it is unnecessary to describe them here.
  • the intermittent impact loading applied by blows of the hammer supplements the progressive pressure loading and brings the particles more rapidly into conformity with one another. It overcomes the tendency of the particles to form bridges or arches which, in some circumstances, prevent consolidation of powder masses in their central portions.
  • the current is interrupted when the hammer blows are struck, so that lines of magnetic force, which cause bridging efiect, then disappear.
  • the hammer action may be continued after the end of the pressing operation, or may be applied only at the end of that operation, or not at all.
  • the precompression step performed by the plungers 22 and 23 may be omitted and the powder may be loaded in a loose condition into the dies when in. the final compressing location.
  • Preliminary compression is desirable, as it brings the particles into a relation to one another which promotes and hastens the heating efiect under the electric current.
  • Any powders which have suflicient conductivity to permit current flow, and suflicient resistance to be heated to ductility when in contact at a limited number of points of small area, may be treated by the procedure here described. It is particularly effective, however, with the harder and more resistant metals, such as iron, iron alloys, and still harder metals and alloys. Powder mixtures of metals and non-metallic substances may likewise be converted into finished products of considerable strength, provided enough metal is present to afford conductive paths for the current.
  • the phase of the invention which comprises heating simultaneously with pressure application is not limited exclusively to the production of a heating efiect by electrical resistance, or even to heating the powder while in the die itself.
  • the heating efiect may be obtained by induction, i. e., concentration of lines of magnetic force by high frequency current passed through coils surrounding the dies.
  • powder briquettes previously heated to high temperature, may be placed in the dies while in loading position, and then compressed and forged by the rams in the forging position.
  • Products of many different forms and dimensions may be made according to the procedure here described by the selection of dies and complemental plungers and rams of appropriate forms and dimensions. Gears, other machine elements, armor piercing projectiles for artillery and small arms, and many other articles may be thus made.
  • the resulting pieces are substantially without voids, have a density closely approximating the density of the constituent particles, and a perlection of dimensions and surface finish exceeding that obtainable by any method of casting. Products too hard to be finished economically by metal cutting tools may be thus made with an accuracy closely approximating that obtainable by the most accurate machining or grinding operations.
  • An apparatus for hot pressing metal powder comprising a die, rams arranged to confine a mass of powder in said die, a source of electric current in circuit connection with said rams for producing a flow of current from one ram to the other through the metal powder between them, means for exerting pressure loading on one of said rams and advancing the same toward the other, and means for varying the intensity of the current during the advance of one ram toward the other.
  • An apparatus for hot pressing metal powder comprising a die, rams arranged to confine a mass of powder in said die, a source of electric current in circuit connection with said rams for producing a flow of current from one ram to the other through the metal powder between them.
  • An apparatus for hot pressing metal powder comprising a die, rams arranged to confine a mass of powder in said die, a source of electric current in circuit connection with said rams for producing a flow of current from one ram to the other through the metal powder between them, means for exerting pressure loading on one of said rams and advancing the same toward the other, means for repeatedly applying impact loading to one of said rams simultaneously with the exertion of such pressure loading, and means for interrupting the current while the impact loadings are applied and causing current flow between the repetitions of the impact loading.
  • a powder compressing apparatus comprising a molding die, rams disposed to enter said die from opposite ends thereof, plungers carrying said rams, toggle linkages mounted for operation to exert pressure on said plungers, each in the direction toward the other, and common operating means coupled to both said linkages for bringing them toward the maximum pressureexerting condition simultaneously, one of said plungers being connected with its toggle linkage with capability for movement independently thereof in the direction of the pressure application exerted by said linkage, and means for applying impact loading to said plunger during persistence of the pressure exerted by the linkage.
  • a powder compressing apparatus comprising a molding die, rams disposed to enter said die from opposite ends thereof, toggle linkages mounted for operation to exert pressure on said rams, each in the direction toward the other, common operating means coupled to both said linkages for bringing them toward the maximum pressure-exerting condition simultaneously, one of said rams being movable independently of its toggle linkage in the direction of the pressure application exerted by said linkage, a hammer disposed for operation to apply impact loading to the last named ram in the same direction, and means correlated with said operating means to actuate said hammer for the purpose set forth while the associated toggle linkage is in pressure exerting condition.
  • a powder compressing apparatus comprising a molding die, rams disposed to enter said die from opposite ends thereof, toggle linkages mounted for operation to exert pressure on said rams, each toward the other, correlated cranks cooperatively related with the respective toggle linkages to cause approach of the toggles toward straightened condition while the cranks approach their dead center locations, one of said cranks being in advance of the other whereby to approach dead center sooner than the other.
  • the method of transforming metal powder into solid articles which consists in placing a charge of metal powder in a die, advancing a ram into the die, applying pressure of progressively increasing intensity to the ram, passing a current of electricity through the mass of powder under compression in suflicient quantity to cause heating and softening of the particles of powder at their points of mutual contact, and altering the amount of current so passing while the powder is under compression.
  • the method of bonding discrete metal particles into a cohesive body which consists in placing a mass of such particles in a closed space, exerting progressively increasing pressure on the particles so confined, passing an electric current of intensity suflicient to make the particles plastic at their points of mutual contact, through the mass, in a series of intermittent impulses during the progress of the pressing action, superimposing on the continuous pressure loading a succession of impact loadings, and timing the impact loading with the intermittent current application to cause occurrence of the impacts when there is no current passing through the mass.

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Description

arch 27, 1945. 055 2,372,605
METHOD AND APPARATUS FOR MAKING SOLID OBJECT FROM METAL POWDER Filed Nov. 4, 1941 5 Sheets-Sheet l /f/ M M 04 //z M M 7 W. F. ROSS March 27, 1945.
METHOD AND APPARATUS FOR MAKING SOLID OBJECTS FROM METAL POWDER Filed Nov. 4, 1941 5 Sheets-Sheet 2 v d/W V M MU March 27, 1945. E o 2,372,605
METHOD AND APPARATUS FOR MAKING SOLID OBJECTS FROM METAL POWDER Filed NOV. 4, 1941 5 Shets-Sheet 3 m Imllllllll I a M 11 V f" I 4.012% g V?" W A,
arch 27, w E oss 2,372,605
METHOD AND APPARATUS FOR MAKING SOLID OBJECTS FROM METAL POWDER Filed Nov. 4, 1941 5 Sheets-Sheet 4 W. F. ROSS METHOD AND APPARATUS FOR MAKING SOLID OBJECT S FROM METAL POWDER Filed NOV. 4, 1941 5 Sheets-Sheet 5 I k R S s g g atented Mar. 27, 1945 METHOD AND APPARATUS FOR MAKING SOLID OBJECTS FROM METAL POWDER Walter F. Ross, Detroit, Mich, assignor to The Fellows Gear Shape: Company and to Jones & Lamson Machine Company, both of Springfield, Vt, and both corporations of Vermont Application November 4, 1941, Serial No. 417,806
12 Claims.
The present invention relates to the subject generically known as powder metallurgy. It is more particularly concerned with that phase of the art which consists in consolidating metallic powders into coherent objects by simultaneous application of heat and pressure.
Heretofore the development of powder metallurgy in commercial practice has been mainly along the lines of the so called cold press process, according to which quantities of metal powder are pressed cold in a mold under pressure, sometimes aided by binding material, suflicient to produce a metal powder compact or briquette which can be handled, but is not strong enough for use. The briquette so made is then sintered, i. e., heated to a degree suflicient to cause permanent adhesion to one another of the particles at their points of mutual contact. In the case of some products, notably the hard cemented carbides, where a powder mixture containing difierent metals, one of which has a lower melting point than others, is used, the heat treatment is carried on at a temperature high enough to cause fusion and flow of the ingredient of lower melting point.
Except in the case of very soft metals which are readily deformable under pressure, cold compression does not close up the voids between the particles, wherefore pieces which are slntered without fusion are permanently porous. Such porosity, while of advantage in certain circumstances, as where absorption of oil for lubrication occurs, is an objection where maximum density, strength and wear resisting properties are desired. Thus the cold press process is not satisfactory for molding powders of iron, iron alloys, and other metals and alloys of comparable hardness because it does not produce a sufiiciently close approach to the true theoretical density of the metal in the finished product. Pressures up to 200,000 pounds per square inch have been found necessary with certain ferrous powders-in order to obtain products having a reasonable density. Obviously, to compress pieces of any considerable dimensions with such an intensity of pressure would require extremely large, heavy and expensive presses; in some cases far beyond the limits of practicability and, in any case, involving a great capital investment.
But if the metal could be suiliciently heated to soften the particles, simultaneously with the application of pressure, a comparable density could be obtained with pressures in the order of one tenth those required in the cold pressing method, and products of density approximating the true density of the metal could be made by application of practicable pressures.
There is a crying need at the present time for a practical means for hot pressing ferrous and other powders which are highly resistant to deformation when cold. Many articles in the technical literature point to the great advantages incident to hot pressing in comparison with cold pressing. But no practical commercial means has yet been devised, to the best of my knowledge, whereby metal powder masses may be heated and compressed to a density approximating that of the forged metal, rapidly, and at the same time molded to finshed form and dimensions.
The primary object of this invention is to provide a commercial machine adapted to supply this need. Objects contributory to the foregoing are to regulate and control the temperature, amount and timing of heat input during pressing; to regulate the intensity of pressure loading applied to the powder mass or briquette; and to apply shock or impact loading in conjunction with constant, or squeeze, loading, or independently. Further objects, which are preferred but not obligatory, are to eflect a precompression, without heating, of the powder in the same die or mold in which hot compression is effected; to deliver automatically measured quantities of powder to the die or mold, and to carry out the steps of loading the mold, precompressing the powder, hot pressing the briquette, and electing the finished product in an automatic sequence of operations.
Illustrative means capable of accomplishing the foregoing objects are shown in the drawings and described in the following specification.
In the drawings,
Fig. 1 is a central vertical section of the machine, showing the hot pressing elements thereof in elevation;
Fig. 2 is a side view of the machine as seen from the right of Fig. 1;
Fig. 3 is a sectional view of the hot pressing equipment in a plane parallel to that of Fig. l, and shown on a larger scale;
Fig. 4 is a partial plan view of the machine;
Fig. 5 is a horizontal section taken on line 5-5 of Figs. 1 and 2;
Fig. 6 is a detail sectional view taken on line 6-6 of Fig. 1 and shown on a larger scale;
Fig. 7 is a vertical sectional view taken approximately on line 1-7 of Figs. 1 and 5;
Fig. 8 is a horizontal section taken on line 88 of Fig. 7;
Fig. 9 is a partial section and partial plan view of the powder metering and feeding ele ment of the machine taken on line -9 of Fig. "5';
Fig. 10 is a diagram of electrical circuits controlling the operation of the machine.
' Like reference characters designate the same parts wherever they occur in all the figures.
The operative instruments of the machine are mounted and supported by a frame structure of any convenient construction, here shown as horizontal plates it, ii, 52 and I3 spaced apart, one above another, by spacing sleeves l4 located at suitable positions, and tied together by rods 85 passing through holes in the plates and through the sleeves E i, and on the ends of which nuts it are threaded above the top plate in and beenath the bottom plate 53. This structure rests on a base, a portion of which is indicated in Figs. 1 and 2 as an I beam M.
In the organization of the machine for automatically furnishing measured quantities of powder, precompressing the powder, uniting the powder into a solid body under pressure, and ejecting the finished product, there is provided a turret 48 containing four dies i9, which is indexed to bring each die successively into each of four different positions; a hopper 20 for containing powder; a metering head 2i; precompression plungers 22 and 23; main pressing bars or rods 2% and 25 carrying plungers or rams 26 and 27, respectively; an ejector 28; mechanisms for operating these several instruments in proper sequence; and means for causing flow of electric current between the main pressure plungers through the powder in suificient volume to heat the powder by electric resistance to welding temperature. These instrumentalities are taken up for further description in detail in the approximate order of their sequence of operations on the material, rather than in the order of their importance to the invention.
The powder hopper 20, metering head 2| and a guide 29 for the upper precompression plunger 22 are all supported on or provided in a bracket 30 supported on and in the frame plate II. The metering head is secured to a shaft 32, rotatable in a bearing 33 in the bracket 30, and contains a number of passages 34 arranged to be placed in succession, by rotation of the head, beneath the outlet 35 of the hopper. Passages 34 extend throughout the depth of the metering head and are obstructed at their lower ends by the supporting surface of bracket 30. Adjacent to one of the stopping locations of these passages, a conduit 36 passes through the bracket 30 and into the side of the plunger guideway 29 for conducting powder to that molding die which is alined with plungers 22 and 23. Blocks 3?! are adjusted by screws 38 and 39 to protrude more or less into the metering passages or cavities 34 for regulating the volume of the charges. A ratchet 40 is keyed to shaft 32 and is operated by a pawl 4|, carried by a bar 42 which slides in a guideway in a portion of the bracket 30, and a cam 43, to turn the metering head intermittently, whereby the passages are brought into register with the hopper outlet and the conduit 36 successively.
A guide 44 for the lower precompression plunger 23 is mounted in a bracket 45, supported on the frame plate I2, in vertical alinement with the guide 29, beneath the turret l8 and in alinement with one of the stopping positions of the dies l9. A seal 46 is mounted on guide 44 and cameos closely surrounds the plunger 23 to exclude metal dust from the guide.
Plunger 22 is connected by a pivot pin 41 with a lever 48 pivoted at 49 to a link 50, which in turn. is pivoted at 5! to a bracket 52 on the frame plate M. This lever is coupled by a connecting rod 53 with a crank pin 54 carried by a cam shaft 55 which rotates in a bracket 56 secured to the under side of plate ll. Plunger 23 is coupled by a pivot 51 with a lever 58, which is suspended from bracket 45 by a link 59. A rod 50 is coupled at one end to lever 58 and at its other end to a lever 6| which is pivoted at 62 to the bracket 56. A spring 63 reacts between a. portion of bracket 45 and a shoulder 64 on the rod 60, holding a cam follower portion of lever 6i against a cam 65 on cam shaft 55.
The cam shaft is rotated by an electric motor 66 which drives a shaft 61 through belt transmission 68, said shaft 61 being contained in a bearing in bracket 56 and carrying a worm 69 meshing with a worm wheel 10 on the cam shaft. Cam 43, which rotates the metering head, is likewise secured to shaft 55.
The equipment here illustrated is adapted to mold pieces with central openings. A rod or core pin H for providing such an opening is mounted to travel endwise through the plunger 23, which has a central bore for the purpose, and to enter a recess 12 in the plunger 22. This core pin is coupled by a pin and slot connection with a lever 13 which is pivoted at 14 to a bracket 15, (said bracket being secured to the under side of frame plate l2), and the other arm of which is coupled by a link 16 with a lever 11 mounted beside the lever 6| on pivot pin 62. A spring I! is suspended from an anchorage on bracket 45 and connected to lever I3, exerting force thereon to hold a cam follower portion of lever 11 against a cam IS on cam shaft 55.
These several cams and the crank pin 54 are suitably timed to cause withdrawal of the plungers from turret [8 prior to indexing movement of the latter and then, in the following order, advance plunger 23 into the lower end of the contiguous die l9, project the core rod 'II from the plunger, turn the metering head to deliver a. quantity of powder into the die, and advance plunger 22 so as to exert a pressure against the mass of powder resting on the lower plunger. Sumcient pressure is thus exerted to cause the powder briquette to remain in the die while traveling to the main pressing position. When pieces without apertures are made, the core rod l I may be removed, and solid plungers substituted for the recessed plunger 22 and tubular plunger 23.
The ejector 28, which is above the turret in alinement with the final position of the dies, is likewise operated by the cam shaft 55. It is carried by the lower end of a bar 80, which is movable endwise through guide passages in the frame plates [0 and II and is normally held above the turret by a spring 8|. It carries a. collar 82 in position to receive the impingement of a finger 83 carried by the cam shaft which is suitably located and proportioned to depress the ejector, while the camshaft turns counter-clockwise with respect to Fig. '7, far enough to displace the finished article from the subjacent die into a. conduit or receptacle 84.
The main pressing action is performed when the die reaches the rearmost position shown in Figs. 5 and 8. The plunger (or ram-carrying) rods 24 and 25 are forced toward one another with a powerful squeezing action by toggle linkages. These linkages are alike for both plungers. That for the upper plunger consists of double links 85 and 86 pivoted to a yoke 91, links 89 and B9 pivoted to a collar 90, and knuckle pins I, connecting links 85 and 88 together, and 92 connecting link 86 to link 89. Yoke 81 surounds the plunger rod 24 and is anchored to the frame. The anchorage here shown is a sleeve 93 supported in frame plate I and'through which the rod 24 is movable, the yoke being confined with provision for limited rocking movement, between said plate and a shoulder 94 on sleeve 93. Collar 90 surrounds the plunger rod and grasps it frictionally with sufiicient force to raise the rod when the knuckle pins are moved apart to break the toggles, while permitting slip of the rod under the hammer impulsion later described. Adjustable means to maintain the described clutching eflect after wear may be used. This collar impels the rod, when the toggles are straightened, by thrusting against a shoulder 95 on the rod.
The knuckle pin 9| of one toggle is connected by a link 96 with a pivot pin 91 carried by a rocker 98 which is supported rotatably in a bracket 99 suspended from the frame plate I0. The other toggle knuckle 92 is connected by two links, I00 and II, which embrace the rod or bar 24, with pivot pins I02 and I03 mounted in alinement with each other at the diametrically opposite side of rocker 99 from the pivot 92'.
Identical toggle links I04, I05, I06 and I01 are connected to a yoke I08 (which is conflnedbetween the bottom frame plate I3 and the shoulder I09), and a collar IIO which surrounds rod 25 and thrusts against a shoulder III thereon. The knuckle pins of the latter toggle are connected by an inner link II 2 and two outer embracing links H3 with pins H4, H5 at diametrically opposite sides, of a rocker II6 which is pivotally mounted on a bracket I I7 secured to the bottom plate I3.
The two rockers 98 and 6 are operated by connecting rods H8 and H9 from crank pins I and I2I' on a crank disk I22, the connecting rods being coupled with the rockers by pivots I20a and I'2Ia. The several links and pivots are arranged so that, when crank pin I20 is on dead center with respect to connecting rod M8, the pivots 91, I02 and I 03 are on dead center with respect to the links 96, I00 and II", respectively, and ram 26 is fully advanced. The same conditions exist with respect to crank pin I2I, connecting rod II9, the pivots H4 and 5, links H2 and H3, and ram 21. The throw of the cranks I20 and I2I and the displacement of the toggle links are made sufiicient to withdraw the rams wholly from the turret I8.
The crank pins I20 and I2I are preferably nonsymetrical with respect to the axis of the crank disk and their respective connecting rods, in such manner that one crank pin approaches its dead center in advance of the other. Assuming that the pin I2I is the one in advance, this pfii will reach and pass dead center while the crank pin I20 is approaching dead center, if their rotation is carried so far. Hence the rams, after entering the die, travel at unequal speeds and the mass of powder confined between them is shifted along the die while being compressed; at least during the final stages of compression. If the pin I2! is moved beyond dead center through a small angle while the pin I20 is coming near dead center, there will be a slight movement of both plungers in the same direction at the same time.
Owing to the different speeds of the rams, there is less tendency for the compressed mass to seize on the die than there would be if it were compressed equally from both ends at equal speeds toward a fixed central position; and when the rams are thereafter moved in the same direction as above described, the likelihood of seizing is further reduced.
Crank disk I22 is mounted on a shaft I29 rotatable in a bracket I24 on the frame plate I2. This shaft is driven by a reversible electric motor I25 (secured to frame plate I2) which, for convenience, may be called the main motor, through a belt or chain I26, 8. sprocket I21 on a shaft I28, change gears I29 and I30, secured respectively to said shaft and to a shaft III, a worm I32 on shaft I 3|, and a worm gear I33 meshing with worm I32 and secured to shaft I23.
When pieces with through passages are made, one of the rams is provided with a projecting rod to hold the passage open while pressure is applied; as shown in Fig. 3 with respect to ram 26. Such rod may be made of non-conductive material or of metal electrically insulated from one, or both rams. It is, of course, omitted, and rams with closed ends employed, when solid articles are made.
The rams or plungers 26 and 21 are the terminals of an electric welding circuit through which electric current of low voltage and high amperage is delivered to heat the metal powder, by the electrical resistance of the powder, to a temperature at which the particles are soft enough to be readily deformable, and will unite. They are of form and dimensions such that they may enter and fit closely but slidingly in the dies. Ram 26 is formed with an enlargement I34 back of its terminal extremity and with a flange I35 and centering lip I36 at its opposite end to bear on and embrace the end of plunger rod 24. It is secured to the plunger rod by a screw I31 and is insulated from the rod by sleeves and washers of insulating material, all comprehensively desigated I38. Ram 21 is correspondingly formed and is secured to and insulated from the plunger rod 25 by duplicates of the same means, designated by the same reference characters.
Electrodes I39 and I40 surround the enlarged portion I34 of the respective rams with good electrical contact and a water tight fit. They are internally cored to provide chambers I through which water or other cooling fluid may be passed to keep the rams at a low temperature. They are connected by means of laminated flexible conductors I42 and I43 with the secondary winding of a high current transformer I44.
The dies I9 are each constructed of a series of rings in tandem arrangement and accurate alinement, supported in a shell or casing I45 by insulating material I46 which insulates them electrically from the shell. The rings may also be insulated from each other by thin washers of mica or the like to prevent a short circuit through them; but this is not of vital importance, for reasons later set forth, and each die may be made of a single solid piece. Such rings may be made of hard and tough metal finished internally to exact prescribed dimensions with polished surfaces. The several die casings I45 are provided with an inner flange at one end and a lock at the other end to retain the insulation I46, between which and the rams are air spaces wide enough to prevent leakage of current. They are fitted in suitably located holes extending through the turret and are secured therein by set screws In addition to the pressure or squeeze loading, to which the metal powder briquette is subjected through the agency of the toggle linkages previously described, the briquette is further subjected to shock or impact loading applied by a hammer I48 to the ram 26 through the plunger rod 24. This hammer is mounted to slide on a guide I49 mounted on the uppermost frame plate, and is arranged to move in alinement with the plunger rod 24 and to impinge on a cap piece I50 secured to the upper end of said rod. It is coupled by a pin and slot connection I5I with a lever I52 which is pivoted at I53 to a bracket I54 secured to the top plate. An electric motor I55, which may be called the hammer motor, actuates the hammer through a train consisting of belt I56, pulley I51, shaft I58, worm I59, worm gear I60, shaft I6I, change gears I62 and I63, shaft I64 and cam I65, cooperatively arranged as clearly shown in Figs. 1 and 4. This cam is located beneath the lever I52 and engages a projection I66 on the lever. In the form here shown, it is provided with a continuous rise through 360 of arc and a sharp drop, whereby it is adapted to raise the hammer, and permit descent of the hammer by gravity, once during each revolution.
This, however, is but one of several types of means which may be used for the purpose. For instance, I may use a cam designed to cause more than one hammer stroke during each revolution, or to cause a greater or less drop of the hammer than that here indicated, Or to efiect a series of hammer blows of progressively increasing force as the compression proceeds; or provide means for applying force other than gravity to the hammer. And by use of appropriate change gears I62--I63, and timing means for starting and stopping motor 155, I may cause the hammer to deliver as many blows as desired during or after the advance of the rams. Any desired timing of the shock impacts with the pressure loading may be practised.
Indexing of the turret I 8 is efiected by an electric motor I61 under control of the pressure mechanism. Motor I61, which may be called. the indexing motor, drives a pulley I68 on shaft I69 by a belt I10. Shaft I68 carries a worm I1I meshing with a worm gear I12 on the shaft I13, which turns in a bearing formed in a part of the bracket I24, and to which the turret is secured. Shaft I69 carries also a gear I14 which drives an index plate I15 through a compound gear I16, I11, of which one element meshes with gear I14 and the other with teeth on the circumference of the index plate. The index plate includes a flange I18 having a single notch arranged to be entered by the toe of a locking dog I19 which is mounted on a pivot I80. These parts are all cooperatively supported by rigid portions of the bracket I28.
An arm I8I forms a structural part of the dog I19 and extends to the opposite side of pivot I80 therefrom. A spring I82 is connected to arm I8I and acts so as normally to hold the dog in locking engagement with the index plate.
A striker I83 is connected to arm Hit by a pivot I84 and is weighted so that it bears against a stop pin I85. It projects into the path of a cam projection I86 on the circumference of crank disk I22, and has a beveled face arranged to be engaged with the beveled advancing face of cam I86 during the rotation of the crank disk in the direction which causes separation of the pressing rams. In the illustrated machine, as seen in Fig. 1, the direction referred to is clockwise and is indicated by the arrow A. When such engagement occurs, the cam projection is rising and the striker is blocked by the stop pin I85, so that arm I 8| is displaced to the left, and dog I19 to the right, of the position shown in Fig. 1. Arm I8I controls a switch I81 in the circuit of the indexing motor, (further shown diagrammatically in Fig. 10). The arrangement of these parts is such that the initial movement imparted to the arm I8I closes the switch contacts, thereby energizing the motor I61, and thereafter the dog i fully withdrawn from the index plate. After cam I86 passes the striker, spring I82 holds the dog against the index plate ready to reenter the notch in the latter when the plate has made a complete revolution. 0n the reverse rotation of the crank disk, cam I86 displaces the striker in passing it without moving the lever. The cam is adjustable and is set to start the indexing action after the rams have withdraw from the turret and before the crank disk has come to the end of its clockwise rotation.
It will be understood that the gearing I14I15 which drives the index plate is in ratio to the worm gearing I1I--I12 such that it turns the index plate through a complete rotation while the turret is turned through a quarter rotation; i. e., from one stopping place to the next. On the completion of such rotation of the index plate, the dog enters the notch in flange I18 and the arm I8I opens the switch I81, causing the indexing motor to stop.
The reversals and driving of the main motor I25 in opposite directions are controlled by cam projections I88 and I89 on the circumference of crank disk I22 coacting with limit switches I90 and I9I respectively, in a switch box I92, (Figs. 1 and 2). These limit switches are interconnected with the switch contact I81 as electric interlocks so as to prevent advance of the compression rams, after their retraction to permit indexing of the turret, until the indexing movement has been completed. Suitable electrical connections for the purpose are shown in the diagram, Fig. 10. It may be noted that in this diagram the crank disk I22 is in the position occupied when the rams are withdrawn, whereas Figs. 1-3 show the condition where the rams are fully advanced into a. die.
All of these cam elements may be adjusted, or shifted to different positions, along the circumference of the crank disk in order to control and regulate the extent of penetration of the rams into the dies, short of or up to the limit established by the toggle linkages. The intensity of pressure loading on the charges of powder may be thus regulated, in conjunction with regulation of the quantity of powder, or the dimensions of the briquette, placed in the die.
An important part of the invention consists in methods of applying electric heating current, in conjunction with application of mechanical force, to the powder mass or briquette, and in means for carrying such methods into effect. The methods referred to include the steps of de livering heating current intermittently in impulses of shorter or longer duration, varying the intensity of the current thus delivered, and regulating the number, intensity and duration of current impulses according to the character of the material undergoing the consolidating treatment.
The effect of the current of high amperage and low voltage is to heat the particles of the powder to a condition of plasticity at their points of contact. In the initial condition of the briquette, the particles of powder are in contact with one another at a comparatively few points of relatively narrow area. Resistance to flow of current from particle to particle is therefore very great, and is greatest at the points of contact which have the least area. These points are quickly brought to the plastic condition in which they join together cohesively and are sufliciently ductile to be readily deformed by the pressure. Such deformation enlarges the contact areas and causes the interparticles resistance to be diminished. With repeated impulses of current and continued pressure application, or repeated hammer blows, a progressive and irregular deformation of the particles occurs as the narrow contact areas become wider and the particles approach mutual conformity .of shape.
The method of applying current in brief impulses, analogous to mechanical jolts or hammer blows, is of advantage over continuously passing current through the material, in a number of respects. It enables the heating effects to be accurately controlled. It avoids any serious heating of the die member even though the latter be continuously conductive and thus capable of furnishing shunt paths for the current. Due to the short duration of current flow during each impulse, the powder particles are heated to welding temperature at their contact points while the die is not heated obiectionably. It enables the optimum treatment for any particular material or mixture of materials to be determined and accurately duplicated in treating successive powder masses of like composition.
By thus briefly applying current, and varying the strength and duration of different current impulses, the heat input and temperature may be easily and exactly controlled and adjusted to the characteristics of the metal operated on. At temperatures approaching their melting points, metals become plastic. The plastic range varies with diflerent metals, but with most metals its lower limit is at a temperature considerably below the melting point. However, in some cases the plastic range is very narrow and close to the melting point. It is necessary to maintain the metal in the plastic range While pressing for, if the metal melts, due to too great an input of heat or to the die being too highly heated, it acquires the undesirable properties of cast metal upon cooling. There would also be a tendency for the metal to adhere to the die walls or the rams.
Metals that are not heated to the plastic stage have low strength, both in tension and compression, low density, and poor structure. They are liable to change their dimensions in unpredictable methods referred to is shown diagrammatically in Fig. 10. Here P represents the primary, and S the secondary, windings of the high current transformer I. The primary winding is tapped at various points and such tapping points are connected electrically with removable contact buttons I99 on a tap selector I94. A contact arm I9! is connected in the circuit and is arranged to pass from one contact button to the next in succession in time with the rotation of the crank disk I22.
It may be carried by the crank shaft I29, or may be driven therefrom by intermediate gearing so as to turn through a larger or smaller arc than that through which the crank disk tums, if desired. The several contact buttons may be connected to any desired ones of the tapping points, so as to put different fractions of the primary winding in the circuit in any desired order. There may be more or fewer contacts I99 than the number shown here, with equal or unequal spacing as desired, and different ones may have a wider or narrower extent of contact area than others, whereby to vary the duration of the respective current impulses. Any of these contacts may be removed and wholly omitted, or others may be substituted for them.- The capacity for adjustmentand variation in these respects makes it possible to apply any desired number of current impulses during the cycle, to make such impulses longer or shorter, to make them of equal or unequal strength, and to apply relatively stronger or weaker current impulses in any desired sequence. For instance, thecurrent may be progressively incremd or decreased as the interparticle resistance diminishes with widened areas of contact, or an impulse of low strength may be administered between strong impulses, and vice versa.
A device for interrupting the transformer circuit in time with the movement of the selector arm is associated with the selector. This device comprises a cam I96 rotated in synchronism with the arm I and having projections I9'I arranged to open a face plate interlock I98 in circuit with a line contact switch I99. The projections I9'I are adjustable and removable for substitution of others subtending larger or smaller angles, to correspond with the spacing and extent of the selector contacts I93. They are located so as to open the switch I99 just before the selector arm leaves any one of the contacts I93 so as to avoid arcing and to prevent the transformer circuit from being closed whenever the selector arm bridges across two contacts. This device is timed also to insure that there will be no current in the electrodeswhen the rams are being retracted from the die.
The diagram further shows a starting switch 299 for the motor 96 of the measuring and precompresslon means, (called for convenience the loading motor), and a switch or interlock 29I for controlling the hammer motor I55. This interlock is shown as operated by a cam 292 on the crank shaft I23, which may be suitably designed to start and stop the hammer motor once or a number or times during the persistence of the continuous pressure loading. The diagram further shows main reversing switches 293 and 294 for the main motor I25; main switches 295, 296 and 29'! for the loading motor, indexing motor and hammer motor, respectively; auxiliary starting devices for these several motors; and a time relay 298 in connection with the main motor switch 293 and the interlock I99. The function of this time relay is to delay reversal of the main motor after the rams have been pressed together, for such length of time as may be prescribed for hammering or persistence of the squeezing pressure and heating effect. Holding circuits are also provided in order to insure continual supply of current to the main motor. But as the details of the electrical circuits and connections are not of the essence of the. invention, but are within the field of electrical engineering design and may be widely varied, it is unnecessary to describe them here.
The intermittent impact loading applied by blows of the hammer supplements the progressive pressure loading and brings the particles more rapidly into conformity with one another. It overcomes the tendency of the particles to form bridges or arches which, in some circumstances, prevent consolidation of powder masses in their central portions. Preferably the current is interrupted when the hammer blows are struck, so that lines of magnetic force, which cause bridging efiect, then disappear. The hammer action may be continued after the end of the pressing operation, or may be applied only at the end of that operation, or not at all.
Various modifications from the construction and combination here shown may be made within the scope of this invention. Thus the precompression step performed by the plungers 22 and 23 may be omitted and the powder may be loaded in a loose condition into the dies when in. the final compressing location. Preliminary compression, however, is desirable, as it brings the particles into a relation to one another which promotes and hastens the heating efiect under the electric current.
Any powders which have suflicient conductivity to permit current flow, and suflicient resistance to be heated to ductility when in contact at a limited number of points of small area, may be treated by the procedure here described. It is particularly effective, however, with the harder and more resistant metals, such as iron, iron alloys, and still harder metals and alloys. Powder mixtures of metals and non-metallic substances may likewise be converted into finished products of considerable strength, provided enough metal is present to afford conductive paths for the current.
The phase of the invention which comprises heating simultaneously with pressure application is not limited exclusively to the production of a heating efiect by electrical resistance, or even to heating the powder while in the die itself. For some classes of material the heating efiect may be obtained by induction, i. e., concentration of lines of magnetic force by high frequency current passed through coils surrounding the dies. Or powder briquettes previously heated to high temperature, (for instance, approaching white heat), may be placed in the dies while in loading position, and then compressed and forged by the rams in the forging position.
Products of many different forms and dimensions may be made according to the procedure here described by the selection of dies and complemental plungers and rams of appropriate forms and dimensions. Gears, other machine elements, armor piercing projectiles for artillery and small arms, and many other articles may be thus made. The resulting pieces are substantially without voids, have a density closely approximating the density of the constituent particles, and a perlection of dimensions and surface finish exceeding that obtainable by any method of casting. Products too hard to be finished economically by metal cutting tools may be thus made with an accuracy closely approximating that obtainable by the most accurate machining or grinding operations.
What I claim and desire to secure by Letters ratent is 1. An apparatus for hot pressing metal powder. comprising a die, rams arranged to confine a mass of powder in said die, a source of electric current in circuit connection with said rams for producing a flow of current from one ram to the other through the metal powder between them, means for exerting pressure loading on one of said rams and advancing the same toward the other, and means for varying the intensity of the current during the advance of one ram toward the other.
2. An apparatus for hot pressing metal powder, comprising a die, rams arranged to confine a mass of powder in said die, a source of electric current in circuit connection with said rams for producing a flow of current from one ram to the other through the metal powder between them. l .7
means for exerting pressure loading on one of said rams and advancing the same toward the other, means for applying impact loading to one of said rams during the persistence of such pressure loading, and means for interrupting and varying the intensity of the electric current in the course of such pressure and impact loadings.
'3. An apparatus for hot pressing metal powder, comprising a die, rams arranged to confine a mass of powder in said die, a source of electric current in circuit connection with said rams for producing a flow of current from one ram to the other through the metal powder between them, means for exerting pressure loading on one of said rams and advancing the same toward the other, means for repeatedly applying impact loading to one of said rams simultaneously with the exertion of such pressure loading, and means for interrupting the current while the impact loadings are applied and causing current flow between the repetitions of the impact loading.
4-. A powder compressing apparatus comprising a molding die, rams disposed to enter said die from opposite ends thereof, plungers carrying said rams, toggle linkages mounted for operation to exert pressure on said plungers, each in the direction toward the other, and common operating means coupled to both said linkages for bringing them toward the maximum pressureexerting condition simultaneously, one of said plungers being connected with its toggle linkage with capability for movement independently thereof in the direction of the pressure application exerted by said linkage, and means for applying impact loading to said plunger during persistence of the pressure exerted by the linkage.
5. A powder compressing apparatus comprising a molding die, rams disposed to enter said die from opposite ends thereof, toggle linkages mounted for operation to exert pressure on said rams, each in the direction toward the other, common operating means coupled to both said linkages for bringing them toward the maximum pressure-exerting condition simultaneously, one of said rams being movable independently of its toggle linkage in the direction of the pressure application exerted by said linkage, a hammer disposed for operation to apply impact loading to the last named ram in the same direction, and means correlated with said operating means to actuate said hammer for the purpose set forth while the associated toggle linkage is in pressure exerting condition.
6. A powder compressing apparatus comprising a molding die, rams disposed to enter said die from opposite ends thereof, toggle linkages mounted for operation to exert pressure on said rams, each toward the other, correlated cranks cooperatively related with the respective toggle linkages to cause approach of the toggles toward straightened condition while the cranks approach their dead center locations, one of said cranks being in advance of the other whereby to approach dead center sooner than the other.
7. The method of transforming metal powder into solid articles, which consists in placing a charge of metal powder in a die, advancing a ram into the die, applying pressure of progressively increasing intensity to the ram, passing a current of electricity through the mass of powder under compression in suflicient quantity to cause heating and softening of the particles of powder at their points of mutual contact, and altering the amount of current so passing while the powder is under compression.
8. The method of bonding discrete metal particles into a solid body, which consists in confining a quantity of such particles in a closed space, passing electric current in intermittent impulses oi brief duration, and of strength suflicient to make the particles plastic at their points of mutual contact, through such mass, and exerting pressure on the mass while the particles are in plastic condition at their contact points.
9. The method of bonding discrete metal particles into a solid body, which consists in confining a quantity of such particles in a closed space, passing electric current in intermittent impulses of brief duration, and of strength suificient to make the particles plastic at their points of mutual contact, through such mass, exerting pressure on the mass while the particles are in plastic condition at their contact points. and varying the current strength of different current impulses.
10. The method of converting vdiscrete metal Particles into cohesive solid bodies, which consists in placing a mass of such particles in a closed space, passing an electric current through the mass of particles in sufiicient strength to make the particles plastic at their points of mutual contact, applying pressure to said mass in a succession of impacts, and interrupting the current flow while such impacts are applied.
11. The method of bonding discrete metal particles into a cohesive body, which consists in placing a mass of such particles in a closed space, exerting progressively increasing pressure on the particles so confined, passing an electric current, of intensity suiiicient to make the particles plastic at their points of mutual contact, through such mass, in a series of intermittent impulses during the progress of the pressing action, and superimposing on the continuous pressure loading a succession of impact loadings.
12. The method of bonding discrete metal particles into a cohesive body, which consists in placing a mass of such particles in a closed space, exerting progressively increasing pressure on the particles so confined, passing an electric current of intensity suflicient to make the particles plastic at their points of mutual contact, through the mass, in a series of intermittent impulses during the progress of the pressing action, superimposing on the continuous pressure loading a succession of impact loadings, and timing the impact loading with the intermittent current application to cause occurrence of the impacts when there is no current passing through the mass.
WALTER F. ROSS.
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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2449365A (en) * 1945-12-14 1948-09-14 Hydraulic Dev Corp Inc Apparatus for forging
US2556921A (en) * 1947-08-28 1951-06-12 Hirsch Harold Gold beryllium alloy and method of making same
US2637671A (en) * 1948-03-13 1953-05-05 Simonds Saw & Steel Co Powder metallurgy method of making steel cutting tools
US2686822A (en) * 1950-09-12 1954-08-17 Rem Cru Titanium Inc Consumable electrode furnace and method for producing titanium
US2714556A (en) * 1950-11-25 1955-08-02 Sintercast Corp America Powder metallurgical method of shaping articles from high melting metals
US2767462A (en) * 1953-12-28 1956-10-23 Airetool Mfg Company Method of retractively expanding tubes into tube seats
US2907705A (en) * 1948-11-30 1959-10-06 Blainey Alan Thermal fission reactor compositions and method of fabricating same
US3008824A (en) * 1950-04-29 1961-11-14 Andrew C Dunn Method of forging powdered materials
DE976386C (en) * 1953-05-23 1963-08-01 Adolf Conrad Device for producing metal, in particular hard metal alloys
US4102679A (en) * 1975-12-23 1978-07-25 L.A. Levanto Oy Powder metallurgic manufacturing process
EP0013747A1 (en) * 1979-01-30 1980-08-06 Glacier Gmbh - Deva Werke Apparatus for the continuous extrusion of electrically conductive granular materials, preferably metal powder
US4372903A (en) * 1980-09-02 1983-02-08 Cts Corporation Process for controlling the movement of press components
US20060015187A1 (en) * 2004-07-19 2006-01-19 Smith & Nephew Inc. Pulsed current sintering for surfaces of medical implants

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2449365A (en) * 1945-12-14 1948-09-14 Hydraulic Dev Corp Inc Apparatus for forging
US2556921A (en) * 1947-08-28 1951-06-12 Hirsch Harold Gold beryllium alloy and method of making same
US2637671A (en) * 1948-03-13 1953-05-05 Simonds Saw & Steel Co Powder metallurgy method of making steel cutting tools
US2907705A (en) * 1948-11-30 1959-10-06 Blainey Alan Thermal fission reactor compositions and method of fabricating same
US3008824A (en) * 1950-04-29 1961-11-14 Andrew C Dunn Method of forging powdered materials
US2686822A (en) * 1950-09-12 1954-08-17 Rem Cru Titanium Inc Consumable electrode furnace and method for producing titanium
US2714556A (en) * 1950-11-25 1955-08-02 Sintercast Corp America Powder metallurgical method of shaping articles from high melting metals
DE976386C (en) * 1953-05-23 1963-08-01 Adolf Conrad Device for producing metal, in particular hard metal alloys
US2767462A (en) * 1953-12-28 1956-10-23 Airetool Mfg Company Method of retractively expanding tubes into tube seats
US4102679A (en) * 1975-12-23 1978-07-25 L.A. Levanto Oy Powder metallurgic manufacturing process
EP0013747A1 (en) * 1979-01-30 1980-08-06 Glacier Gmbh - Deva Werke Apparatus for the continuous extrusion of electrically conductive granular materials, preferably metal powder
US4372903A (en) * 1980-09-02 1983-02-08 Cts Corporation Process for controlling the movement of press components
US20060015187A1 (en) * 2004-07-19 2006-01-19 Smith & Nephew Inc. Pulsed current sintering for surfaces of medical implants

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