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US2132854A - Emulsifier - Google Patents

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Publication number
US2132854A
US2132854A US153928A US15392837A US2132854A US 2132854 A US2132854 A US 2132854A US 153928 A US153928 A US 153928A US 15392837 A US15392837 A US 15392837A US 2132854 A US2132854 A US 2132854A
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plates
plate
apertures
liquid
series
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US153928A
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Frank W Knott
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US case filed in Court of Appeals for the Federal Circuit litigation Critical https://portal.unifiedpatents.com/litigation/Court%20of%20Appeals%20for%20the%20Federal%20Circuit/case/2022-2165 Source: Court of Appeals for the Federal Circuit Jurisdiction: Court of Appeals for the Federal Circuit "Unified Patents Litigation Data" by Unified Patents is licensed under a Creative Commons Attribution 4.0 International License.
US case filed in Nevada District Court litigation https://portal.unifiedpatents.com/litigation/Nevada%20District%20Court/case/3%3A20-cv-00040 Source: District Court Jurisdiction: Nevada District Court "Unified Patents Litigation Data" by Unified Patents is licensed under a Creative Commons Attribution 4.0 International License.
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Priority to US153928A priority Critical patent/US2132854A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01JMANUFACTURE OF DAIRY PRODUCTS
    • A01J11/00Apparatus for treating milk
    • A01J11/16Homogenising milk
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/45Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B01F25/452Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
    • B01F25/4521Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through orifices in elements, e.g. flat plates or cylinders, which obstruct the whole diameter of the tube
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2215/00Auxiliary or complementary information in relation with mixing
    • B01F2215/04Technical information in relation with mixing
    • B01F2215/0413Numerical information
    • B01F2215/0418Geometrical information
    • B01F2215/0431Numerical size values, e.g. diameter of a hole or conduit, area, volume, length, width, or ratios thereof

Definitions

  • This invention relates to emulsifying heads, and the purpose of the invention is to provide a means for emulsifying various liquids and is par- I ticularly adapted for the emulsiflcation of milk to provide a product that is stable in that the butter fat does not separate from the body of the liquid in the form of a coagulated mass.
  • the object of this invention is to provide a device in which the liquid that is to be emulsified is forced under pressure in very fine streams, which streams in their progress through successive sections of the device discharge against flat surfaces and change in the direction of flow to again pass in fine streams to discharge against another flat surface and again change in direction of flow to thereby secure what may be termed a bombardment of the liquid constituents to cause a practically complete disruption of fat globules.
  • a feature of this invention resides in the provision of a series of finely apertured plates through which the liquid is passed in succession and this liquid assembles in a thin film between the plates, as is provided for by the construction of the succeeding plates, and is there changed in its direction of flow to again pass through a second and succeeding series of films and streams to finally discharge in emulsified condition from the device.
  • Fig. 1 is a cross sectional view of an emulsifymg device embodying my invention.
  • - Fig. 2 is an enlarged section of a. series of plates showing the relationship of the apertures in and recesses between the successive plates forming the flow path of the liquid.
  • Fig. 3 is a plan view of one of the recessed plates.
  • duit like portion 3 providing an inlet to the body through which fluid may be introduced.
  • the body also has a cap member 4 at the discharge end having an outlet conduit 6 for the emulsified liquid.
  • the cap 2 is threaded into the upper end of the body to engagement with the end plate 6 of a series of plates 6, 1, 6 and 9' but the number of plates may be even more or lessthan what is here shown, more being required for such liquids as are more diflicult to emulsify.
  • the plate 9 at the outlet end of the body rests on a 1 ledge ID of the casing and the cap member 2 has a threaded flange H engaging the plate 6 at the inlet end by means of which portions of the surfaces of the plates are held in pressure contact for which purpose these plates are provided with 15 finished contacting surfaces to prevent a flow of fluid between the same.
  • the end plates 6 and 9 are respectively spaced from the inlet and outlet openings of the body providing an inlet and an outlet chamber.
  • the 2 end plate 6 of the series has a series of flne apertures l2 preferably regularly arranged in concentric circles and opening through the upper surface of the plate 6 and these apertures below the upper surface open through the bottom sur- 25 face of the plate by a larger diameter portion as is shown in the sectional view Fig. 2.
  • the second plate I and the succeeding plates have a ring like recess B in the upper face thereof and thus liquid which is forced under .pressure from the 30 inlet conduit 3 into the device passes through the apertures l2 and then into a recess in the face of the next plate when the streams unite in a thin film.
  • the plate 1 and the succeeding plates having the similar recesses l3 in the upper 35 faces also have fine concentrically arranged apertures l4 extending through each of the plates and the succeeding plates are so located in respect one to the other as to offset or misalign the aperturesthat is, the apertures I2 of the 40 plate 6 discharge streams of liquid against the second plate between apertures l4 thereof.
  • the fluid cannot pass in continuous streams through the device but in passing through the plate 6 into the recess l3 of the plate 45 1 are required to flow at a right angle to the direction in which the fluid is flowing in the apertures of the plate 6 and then again change and flow at a right angle to the direction of flow in the recess l3 of the plate I to a similar recess 50 in a succeeding plate and this right angled change in direction of flow is rapid in the passage of liquid through the series of plates.
  • the device is of simple and nexpensive character and may be varied in size to correspond with the amount of liquid to be discharged to the device per unit of time and that the various features and objects of the invention are attained by the structure described.
  • An emulsifying head comprising a chambered member having an inlet and an outlet, a series of plates secured in surface contact therein with the end plates thereof in spaced relation respectively with the inlet and outlet, each of the said plates having a series of small diameter apertures therethrough and so arranged that the apertures of one plate are out of alignment with those of a succeeding plate, each of the plates, except the first, having a shallow recess in its surface toward the inlet side of the chamber providing a construction in which the liquid passes in a series of minute streams to each of the recesses in succession wherein the streams unite in a thinfilm and discharge therefrom through the apertures of the plate.
  • An emulsifying head comprising a chambered member having an inlet and outlet, a series of metal plates therein arranged in succession in surface contact, all of the plates having apertures extending therethrough at a right angle to the contacting surfaces with the apertures of successive plates respectively out of alignment, means for supporting the plates in pressure contact, the two end plates of the series being spaced respectively from the inlet and from the outlet providing chambers on the respective inlet and outlet sides, the face ef each plate in contact with the other having recesses of ring like form providing a central and a peripheral portion for contact with the preceding plate, said apertures and the recesses of the plate functioning to cause an abrupt change in the direction of flow of liquid through the device to thereby emulsify the liquid passing to the outlet.

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Animal Husbandry (AREA)
  • Environmental Sciences (AREA)

Description

F. W. KNOTT EMULSIFIER Oct. 11, 193$.
Filed July 16, 1937 1 NV ENT OR. 51 1/71 14 fih'of-r" BY W Z/aq ATTORNEY.
Patented Oct. 11, 1938 PATENT OFFICE EMULSIFIER Frank W. Knott, Detroit, Mich, assignor to John Duval Dodge, Grosse PointqMlch.
Application July 16, 1937, Serial No. 153,928 3 Claims. (01. 99-265) This invention relates to emulsifying heads, and the purpose of the invention is to provide a means for emulsifying various liquids and is par- I ticularly adapted for the emulsiflcation of milk to provide a product that is stable in that the butter fat does not separate from the body of the liquid in the form of a coagulated mass.
Various means have heretofore been devised for this general purpose and usually are of a form in which the liquid is forced between closely opposed surfaces to cause the liquid to flow in thin film and are somewhat ineffective due to the fact that fat globules are merely flattened and not disrupted.
The object of this invention is to provide a device in which the liquid that is to be emulsified is forced under pressure in very fine streams, which streams in their progress through successive sections of the device discharge against flat surfaces and change in the direction of flow to again pass in fine streams to discharge against another flat surface and again change in direction of flow to thereby secure what may be termed a bombardment of the liquid constituents to cause a practically complete disruption of fat globules.
A feature of this invention resides in the provision of a series of finely apertured plates through which the liquid is passed in succession and this liquid assembles in a thin film between the plates, as is provided for by the construction of the succeeding plates, and is there changed in its direction of flow to again pass through a second and succeeding series of films and streams to finally discharge in emulsified condition from the device.
It is also a feature and object of the invention to provide a comparatively inexpensive mechanical structure for producing the above described results.
The preferred form of the device embodying my invention is shown 'in the accompanying drawing in which- Fig. 1 is a cross sectional view of an emulsifymg device embodying my invention.
- Fig. 2 is an enlarged section of a. series of plates showing the relationship of the apertures in and recesses between the successive plates forming the flow path of the liquid.
Fig. 3 is a plan view of one of the recessed plates.
In Fig. 1 is shown an emulsifying head embodying my invention which comprises a hollow body I, a cap 2 at the upper end having a con-,
duit like portion 3 providing an inlet to the body through which fluid may be introduced. The body also has a cap member 4 at the discharge end having an outlet conduit 6 for the emulsified liquid. The cap 2 is threaded into the upper end of the body to engagement with the end plate 6 of a series of plates 6, 1, 6 and 9' but the number of plates may be even more or lessthan what is here shown, more being required for such liquids as are more diflicult to emulsify. The plate 9 at the outlet end of the body rests on a 1 ledge ID of the casing and the cap member 2 has a threaded flange H engaging the plate 6 at the inlet end by means of which portions of the surfaces of the plates are held in pressure contact for which purpose these plates are provided with 15 finished contacting surfaces to prevent a flow of fluid between the same.
The end plates 6 and 9 are respectively spaced from the inlet and outlet openings of the body providing an inlet and an outlet chamber. The 2 end plate 6 of the series has a series of flne apertures l2 preferably regularly arranged in concentric circles and opening through the upper surface of the plate 6 and these apertures below the upper surface open through the bottom sur- 25 face of the plate by a larger diameter portion as is shown in the sectional view Fig. 2. The second plate I and the succeeding plates have a ring like recess B in the upper face thereof and thus liquid which is forced under .pressure from the 30 inlet conduit 3 into the device passes through the apertures l2 and then into a recess in the face of the next plate when the streams unite in a thin film. The plate 1 and the succeeding plates having the similar recesses l3 in the upper 35 faces also have fine concentrically arranged apertures l4 extending through each of the plates and the succeeding plates are so located in respect one to the other as to offset or misalign the aperturesthat is, the apertures I2 of the 40 plate 6 discharge streams of liquid against the second plate between apertures l4 thereof. By this arrangement, the fluid cannot pass in continuous streams through the device but in passing through the plate 6 into the recess l3 of the plate 45 1 are required to flow at a right angle to the direction in which the fluid is flowing in the apertures of the plate 6 and then again change and flow at a right angle to the direction of flow in the recess l3 of the plate I to a similar recess 50 in a succeeding plate and this right angled change in direction of flow is rapid in the passage of liquid through the series of plates.
It is to be noted that, as the fluid passes through the apertures I! of the plate 6, they 5 strike against the flat face of the succeeding plate 8 and this provides what I have termed a "bombardment of the liquid in discharging through the successive plates. The succeeding plates and the form and relationship thereof therefore first force the fluid into very fine streams .in which the fat globules are to some degree disrupted and to some degree elongated and then they pass under pressure into the recess l3 which ehanges their direction of flow abruptly and tends to cause disruption of fat globules. This is repeated a number of times to complete the breaking up of the fat globules and consequent emulsiflcation of the liquid.
In the preferred construction of the device, the apertures I! in the plate 6 at the entrance end are about .020 of an inch in diameter and the apertures through the remaining plates of the series are approximately of the same diameter and while here shown as being of uniform diameter through the plates 1, 8 and Q, they may be enlarged at the discharge end if desired after the manner shown in plate 6. The plates 1, 8 and 9 are recessed in their upper surfaces to a depth of five to seven thousandths of an inch and provide for quite minute streams of fluid Passing through the plates and a very thin film of fluid between successive plates wherein bombardment takes place as well as a change in direction of flow. The recesses are preferably ring like in form having a central portion [5 in the same plane as the peripheral portion of the plate. The recessed plates thus support the contacting plate peripherally and centrally.
From the foregoing description, it is believed evident that the device is of simple and nexpensive character and may be varied in size to correspond with the amount of liquid to be discharged to the device per unit of time and that the various features and objects of the invention are attained by the structure described.
Having thus briefly described my invention, its
utility and mode of operation, ,what I claim and Y surface contact in the chambered member, all the plates having apertures extending therethrough at a right angle to their contacting surfaces and with the apertures of one plate out of alignment with apertures of the succeeding plate, each of the plates, except the first, having the face thereof in contact with a preceding plate recessed slightly whereby the streams discharging through a preceding plate strike against an impervious surface and then change indirection of travel in a thin fllni under pressure to pass through the apertures of the recessed plate.
2. An emulsifying head comprising a chambered member having an inlet and an outlet, a series of plates secured in surface contact therein with the end plates thereof in spaced relation respectively with the inlet and outlet, each of the said plates having a series of small diameter apertures therethrough and so arranged that the apertures of one plate are out of alignment with those of a succeeding plate, each of the plates, except the first, having a shallow recess in its surface toward the inlet side of the chamber providing a construction in which the liquid passes in a series of minute streams to each of the recesses in succession wherein the streams unite in a thinfilm and discharge therefrom through the apertures of the plate.
3. An emulsifying head comprising a chambered member having an inlet and outlet, a series of metal plates therein arranged in succession in surface contact, all of the plates having apertures extending therethrough at a right angle to the contacting surfaces with the apertures of successive plates respectively out of alignment, means for supporting the plates in pressure contact, the two end plates of the series being spaced respectively from the inlet and from the outlet providing chambers on the respective inlet and outlet sides, the face ef each plate in contact with the other having recesses of ring like form providing a central and a peripheral portion for contact with the preceding plate, said apertures and the recesses of the plate functioning to cause an abrupt change in the direction of flow of liquid through the device to thereby emulsify the liquid passing to the outlet.
FRANK W. KNO'II.
US153928A 1937-07-16 1937-07-16 Emulsifier Expired - Lifetime US2132854A (en)

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Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2435884A (en) * 1945-12-18 1948-02-10 Kermit B Niles Homogenizing unit
US2455235A (en) * 1939-12-23 1948-11-30 Crespi Silvio Benigno Process and apparatus for treating milk, blood, and other globular liquids
US2483429A (en) * 1945-08-06 1949-10-04 Raymond C Pierce Shock absorber
US2483430A (en) * 1945-10-29 1949-10-04 Raymond C Pierce Shock absorber
US2570155A (en) * 1948-02-25 1951-10-02 Westinghouse Electric Corp Flow apparatus
US2611707A (en) * 1948-04-01 1952-09-23 Lever Brothers Ltd Method and apparatus for manufacturing margarine
US2620172A (en) * 1949-03-18 1952-12-02 Selectronic Corp Dispersion method and apparatus
US2690329A (en) * 1950-10-25 1954-09-28 Alpura Ag Device for homogenizing liquids
US2769621A (en) * 1951-10-30 1956-11-06 Theodore H Nakken Device for charging lubricants
US2868516A (en) * 1956-03-05 1959-01-13 W M Sprinkman Corp Homogenizer
US4108210A (en) * 1973-10-09 1978-08-22 Fisher Controls Company Control valve trim assembly
US4109680A (en) * 1977-01-03 1978-08-29 Lavender Ardis R Plate type fluid distributing device
US4739795A (en) * 1986-07-18 1988-04-26 Sundstrand Corporation Flow control valve
US4762146A (en) * 1986-09-22 1988-08-09 Sundstrand Corporation Flow control valve
EP0285725A2 (en) * 1987-04-10 1988-10-12 Chugoku Kayaku Kabushiki Kaisha Mixing apparatus
DE19700810A1 (en) * 1997-01-13 1998-07-16 Bayer Ag Method and device for homogenizing milk
US5971601A (en) * 1998-02-06 1999-10-26 Kozyuk; Oleg Vyacheslavovich Method and apparatus of producing liquid disperse systems
EP1008380A2 (en) * 1998-12-07 2000-06-14 F. Hoffmann-La Roche Ag Process and apparatus for mixing or dispersing liquids
WO2003086601A1 (en) * 2002-04-17 2003-10-23 Ehrfeld Mikrotechnik Ag Method and device for homogenizing emulsions
US20050150155A1 (en) * 2004-01-09 2005-07-14 Clean Fuels Technology, Inc., A Nevada Corporation. Mixing apparatus and method for manufacturing an emulsified fuel
WO2007098853A1 (en) * 2006-02-24 2007-09-07 Bayer Technology Services Gmbh Jet disperser, filter fastening system, nozzle fastening system
US20090073801A1 (en) * 2004-11-17 2009-03-19 Basf Aktiengesellschaft Process and device for producing finely divided liquid-liquid formulations, and the uses of the liquid-liquid formulations
US20100186288A1 (en) * 2006-09-01 2010-07-29 Nanomizer Inc. Method for production of emulsion fuel and apparatus for production of the fuel
US20110068065A1 (en) * 2009-09-18 2011-03-24 Caterpillar Inc. Filter assembly
US20160184782A1 (en) * 2014-12-31 2016-06-30 ADT (China) Ltd. Self-pressurization gas-liquid mixing device used for making beverage
US20210008509A1 (en) * 2019-07-09 2021-01-14 Imagine Tf, Llc Parallel production of emulsification
US11666874B2 (en) * 2017-12-14 2023-06-06 Glaxosmithkline Intellectual Property Deveelopment Limited Methods and apparatus for variable emulsification

Cited By (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2455235A (en) * 1939-12-23 1948-11-30 Crespi Silvio Benigno Process and apparatus for treating milk, blood, and other globular liquids
US2483429A (en) * 1945-08-06 1949-10-04 Raymond C Pierce Shock absorber
US2483430A (en) * 1945-10-29 1949-10-04 Raymond C Pierce Shock absorber
US2435884A (en) * 1945-12-18 1948-02-10 Kermit B Niles Homogenizing unit
US2570155A (en) * 1948-02-25 1951-10-02 Westinghouse Electric Corp Flow apparatus
US2611707A (en) * 1948-04-01 1952-09-23 Lever Brothers Ltd Method and apparatus for manufacturing margarine
US2620172A (en) * 1949-03-18 1952-12-02 Selectronic Corp Dispersion method and apparatus
US2690329A (en) * 1950-10-25 1954-09-28 Alpura Ag Device for homogenizing liquids
US2769621A (en) * 1951-10-30 1956-11-06 Theodore H Nakken Device for charging lubricants
US2868516A (en) * 1956-03-05 1959-01-13 W M Sprinkman Corp Homogenizer
US4108210A (en) * 1973-10-09 1978-08-22 Fisher Controls Company Control valve trim assembly
US4109680A (en) * 1977-01-03 1978-08-29 Lavender Ardis R Plate type fluid distributing device
US4739795A (en) * 1986-07-18 1988-04-26 Sundstrand Corporation Flow control valve
US4762146A (en) * 1986-09-22 1988-08-09 Sundstrand Corporation Flow control valve
EP0285725A2 (en) * 1987-04-10 1988-10-12 Chugoku Kayaku Kabushiki Kaisha Mixing apparatus
EP0285725A3 (en) * 1987-04-10 1989-11-08 Chugoku Kayaku Kabushiki Kaisha Mixing apparatus
DE19700810A1 (en) * 1997-01-13 1998-07-16 Bayer Ag Method and device for homogenizing milk
US5971601A (en) * 1998-02-06 1999-10-26 Kozyuk; Oleg Vyacheslavovich Method and apparatus of producing liquid disperse systems
US6530684B1 (en) 1998-12-07 2003-03-11 Roche Vitamins Inc. Preparation of liquid dispersions
KR100685540B1 (en) * 1998-12-07 2007-02-22 디에스엠 아이피 어셋츠 비.브이. Process for mixing or dispersing liquids
EP1008380A2 (en) * 1998-12-07 2000-06-14 F. Hoffmann-La Roche Ag Process and apparatus for mixing or dispersing liquids
US6536940B1 (en) 1998-12-07 2003-03-25 Roche Vitamins Inc. Preparation of liquid dispersions
EP1008380A3 (en) * 1998-12-07 2000-12-13 F. Hoffmann-La Roche Ag Process and apparatus for mixing or dispersing liquids
US6722780B2 (en) 1998-12-07 2004-04-20 Roche Vitamins Inc. Preparation of liquid dispersions
WO2003086601A1 (en) * 2002-04-17 2003-10-23 Ehrfeld Mikrotechnik Ag Method and device for homogenizing emulsions
US20050233040A1 (en) * 2002-04-17 2005-10-20 Wolfgang Ehrfeld Method and device for homogenizing emulsions
WO2005070046A2 (en) * 2004-01-09 2005-08-04 Clean Fuels Technology, Inc. Mixing apparatus and method for manufacturing an emulsified fuel
WO2005070046A3 (en) * 2004-01-09 2006-03-02 Clean Fuels Technology Inc Mixing apparatus and method for manufacturing an emulsified fuel
US20050150155A1 (en) * 2004-01-09 2005-07-14 Clean Fuels Technology, Inc., A Nevada Corporation. Mixing apparatus and method for manufacturing an emulsified fuel
US8568019B2 (en) * 2004-01-09 2013-10-29 Talisman Capital Talon Fund, Ltd. Mixing apparatus for manufacturing an emulsified fuel
US20070294935A1 (en) * 2004-01-09 2007-12-27 Waldron Jack L Mixing apparatus and method for manufacturing an emulsified fuel
US8192073B1 (en) * 2004-01-09 2012-06-05 Waldron Jack L Mixing apparatus and method for manufacturing an emulsified fuel
US20120281496A1 (en) * 2004-01-09 2012-11-08 Waldron Jack L Mixing apparatus and method for manufacturing an emulsified fuel
US20090073801A1 (en) * 2004-11-17 2009-03-19 Basf Aktiengesellschaft Process and device for producing finely divided liquid-liquid formulations, and the uses of the liquid-liquid formulations
US20090272683A1 (en) * 2006-02-24 2009-11-05 Bayer Technology Services Gmbh Jet Dispenser, Filter Fastening System, Nozzle Fastening System
CN101389390B (en) * 2006-02-24 2012-11-14 拜尔技术服务有限责任公司 Device for processing transported mixtures in the high pressure
WO2007098853A1 (en) * 2006-02-24 2007-09-07 Bayer Technology Services Gmbh Jet disperser, filter fastening system, nozzle fastening system
US20100186288A1 (en) * 2006-09-01 2010-07-29 Nanomizer Inc. Method for production of emulsion fuel and apparatus for production of the fuel
US20110068065A1 (en) * 2009-09-18 2011-03-24 Caterpillar Inc. Filter assembly
US20160184782A1 (en) * 2014-12-31 2016-06-30 ADT (China) Ltd. Self-pressurization gas-liquid mixing device used for making beverage
US9566555B2 (en) * 2014-12-31 2017-02-14 ADT (China) Ltd. Self-pressurization gas-liquid mixing device used for making beverage
US11666874B2 (en) * 2017-12-14 2023-06-06 Glaxosmithkline Intellectual Property Deveelopment Limited Methods and apparatus for variable emulsification
US20210008509A1 (en) * 2019-07-09 2021-01-14 Imagine Tf, Llc Parallel production of emulsification

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