SU461492A3 - Способ получени -анилинокарбонитрилов - Google Patents
Способ получени -анилинокарбонитриловInfo
- Publication number
- SU461492A3 SU461492A3 SU1778332A SU1778332A SU461492A3 SU 461492 A3 SU461492 A3 SU 461492A3 SU 1778332 A SU1778332 A SU 1778332A SU 1778332 A SU1778332 A SU 1778332A SU 461492 A3 SU461492 A3 SU 461492A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- mol
- propionitrile
- ethanol
- mixture
- yield
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 23
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 18
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 12
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N N-phenyl amine Natural products NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 11
- 239000000203 mixture Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- SDYWXFYBZPNOFX-UHFFFAOYSA-N 3,4-dichloroaniline Chemical compound NC1=CC=C(Cl)C(Cl)=C1 SDYWXFYBZPNOFX-UHFFFAOYSA-N 0.000 description 6
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 6
- -1 aniline compound Chemical class 0.000 description 6
- 150000001448 anilines Chemical class 0.000 description 5
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 5
- WSGYTJNNHPZFKR-UHFFFAOYSA-N 3-hydroxypropanenitrile Chemical compound OCCC#N WSGYTJNNHPZFKR-UHFFFAOYSA-N 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- QSNSCYSYFYORTR-UHFFFAOYSA-N 4-chloroaniline Chemical compound NC1=CC=C(Cl)C=C1 QSNSCYSYFYORTR-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- ACMJJQYSPUPMPN-UHFFFAOYSA-N 4-chloro-3-fluoroaniline Chemical compound NC1=CC=C(Cl)C(F)=C1 ACMJJQYSPUPMPN-UHFFFAOYSA-N 0.000 description 1
- KRZCOLNOCZKSDF-UHFFFAOYSA-N 4-fluoroaniline Chemical compound NC1=CC=C(F)C=C1 KRZCOLNOCZKSDF-UHFFFAOYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 125000004093 cyano group Chemical class *C#N 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- FVSKHRXBFJPNKK-UHFFFAOYSA-N propionitrile Chemical compound CCC#N FVSKHRXBFJPNKK-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000012258 stirred mixture Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1241071 | 1971-04-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU461492A3 true SU461492A3 (ru) | 1975-02-25 |
Family
ID=10004092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1778332A SU461492A3 (ru) | 1971-04-30 | 1972-04-28 | Способ получени -анилинокарбонитрилов |
Country Status (18)
| Country | Link |
|---|---|
| JP (2) | JPS5749537B1 (hu) |
| BE (1) | BE782595A (hu) |
| CA (1) | CA982141A (hu) |
| CH (1) | CH589049A5 (hu) |
| CS (1) | CS195255B2 (hu) |
| DD (1) | DD101889A5 (hu) |
| DE (1) | DE2221109C2 (hu) |
| DK (1) | DK153472C (hu) |
| ES (1) | ES402224A1 (hu) |
| FR (1) | FR2139847B1 (hu) |
| GB (1) | GB1327294A (hu) |
| HU (1) | HU164835B (hu) |
| IT (1) | IT953845B (hu) |
| NL (1) | NL175173C (hu) |
| PL (1) | PL83652B1 (hu) |
| RO (1) | RO62750A (hu) |
| SU (1) | SU461492A3 (hu) |
| YU (1) | YU39269B (hu) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1547758A (en) * | 1975-07-29 | 1979-06-27 | Shell Int Research | Herbicidal composition |
| GB1577662A (en) * | 1976-05-08 | 1980-10-29 | Basf Ag | Manufacture of glycinonitriles |
| US4318920A (en) * | 1979-02-08 | 1982-03-09 | Abbott Laboratories | Ovicides |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE151538C (hu) * | ||||
| NL136594C (hu) * | 1965-10-22 | |||
| US3463805A (en) * | 1967-05-08 | 1969-08-26 | Grace W R & Co | Production of aminonitriles under adiabatic conditions |
| GB1307978A (en) * | 1969-02-28 | 1973-02-21 | Wellcome Found | Amidines processes for their preparation and pharmaceutical compo sitions incorporating the same |
-
1971
- 1971-04-30 GB GB1327294D patent/GB1327294A/en not_active Expired
-
1972
- 1972-04-25 BE BE782595A patent/BE782595A/nl not_active IP Right Cessation
- 1972-04-27 NL NL7205688A patent/NL175173C/xx not_active IP Right Cessation
- 1972-04-27 DK DK212772A patent/DK153472C/da not_active IP Right Cessation
- 1972-04-28 DE DE19722221109 patent/DE2221109C2/de not_active Expired
- 1972-04-28 SU SU1778332A patent/SU461492A3/ru active
- 1972-04-28 CH CH639572A patent/CH589049A5/xx not_active IP Right Cessation
- 1972-04-28 DD DD16264872A patent/DD101889A5/xx unknown
- 1972-04-28 FR FR7215325A patent/FR2139847B1/fr not_active Expired
- 1972-04-28 HU HUSE001623 patent/HU164835B/hu not_active IP Right Cessation
- 1972-04-28 RO RO7073672A patent/RO62750A/ro unknown
- 1972-04-28 ES ES402224A patent/ES402224A1/es not_active Expired
- 1972-04-28 CS CS289572A patent/CS195255B2/cs unknown
- 1972-04-28 IT IT2369672A patent/IT953845B/it active
- 1972-04-28 JP JP47042319A patent/JPS5749537B1/ja active Pending
- 1972-04-28 CA CA140,875A patent/CA982141A/en not_active Expired
- 1972-04-28 PL PL15504972A patent/PL83652B1/pl unknown
- 1972-05-03 YU YU115772A patent/YU39269B/xx unknown
-
1980
- 1980-07-30 JP JP10378180A patent/JPS5639057A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DD101889A5 (hu) | 1973-11-20 |
| JPS5736274B2 (hu) | 1982-08-03 |
| RO62750A (fr) | 1977-10-15 |
| DK153472B (da) | 1988-07-18 |
| IT953845B (it) | 1973-08-10 |
| AU4168072A (en) | 1973-11-01 |
| PL83652B1 (hu) | 1975-12-31 |
| CH589049A5 (hu) | 1977-06-30 |
| DK153472C (da) | 1988-11-21 |
| DE2221109C2 (de) | 1983-10-06 |
| FR2139847B1 (hu) | 1973-12-07 |
| DE2221109A1 (de) | 1972-11-16 |
| NL7205688A (hu) | 1972-11-01 |
| JPS5639057A (en) | 1981-04-14 |
| JPS5749537B1 (hu) | 1982-10-22 |
| CA982141A (en) | 1976-01-20 |
| YU39269B (en) | 1984-10-31 |
| FR2139847A1 (hu) | 1973-01-12 |
| CS195255B2 (en) | 1980-01-31 |
| GB1327294A (en) | 1973-08-22 |
| HU164835B (hu) | 1974-04-11 |
| NL175173C (nl) | 1984-10-01 |
| ES402224A1 (es) | 1976-01-01 |
| NL175173B (nl) | 1984-05-01 |
| BE782595A (nl) | 1972-10-25 |
| YU115772A (en) | 1982-05-31 |
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