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Organic Low-Molecular-Weight Compounds And Preparation Thereof
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Abstract
2-(3,5-dimethoxyphenyl) 3-methyl octane(I) was prepd. I is valuable for the prepn. of tetrahydrocarnnabinol. The process comprises two steps. 2-[1-(3,5-dimethoxyphenyl)ethyl heptanol was reacted with low mol.wt. alkanesulfonylchloride in liq. reaction solvents, e.g., methylenechloride. 2-[1-3,5-dimethoxyphenyl)ethyl low mol. wt. alkanesulfonic acid. Salt was reduced by lithium aluminium-hydride in an hydrous ether or THF reaction time was 1-5hr.
KR7402151A1974-04-111974-04-11Process for preparing 2-(3.5-dimethoxyphenyl)-3-methyloctane
KR790000215B1
(en)