KR20160084845A - 폴리우레탄 발포체 및 그의 제조 방법 - Google Patents
폴리우레탄 발포체 및 그의 제조 방법 Download PDFInfo
- Publication number
- KR20160084845A KR20160084845A KR1020167014768A KR20167014768A KR20160084845A KR 20160084845 A KR20160084845 A KR 20160084845A KR 1020167014768 A KR1020167014768 A KR 1020167014768A KR 20167014768 A KR20167014768 A KR 20167014768A KR 20160084845 A KR20160084845 A KR 20160084845A
- Authority
- KR
- South Korea
- Prior art keywords
- polyurethane
- polyisocyanurate
- isocyanate
- optionally
- weight
- Prior art date
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- 238000000034 method Methods 0.000 title claims description 14
- 229920005830 Polyurethane Foam Polymers 0.000 title abstract description 16
- 239000011496 polyurethane foam Substances 0.000 title abstract description 16
- 239000012948 isocyanate Substances 0.000 claims abstract description 53
- 150000002513 isocyanates Chemical class 0.000 claims abstract description 53
- 239000004604 Blowing Agent Substances 0.000 claims abstract description 35
- 239000006260 foam Substances 0.000 claims abstract description 31
- 150000001875 compounds Chemical class 0.000 claims abstract description 30
- 239000005056 polyisocyanate Substances 0.000 claims abstract description 30
- 229920001228 polyisocyanate Polymers 0.000 claims abstract description 30
- 229920000582 polyisocyanurate Polymers 0.000 claims abstract description 18
- 239000011495 polyisocyanurate Substances 0.000 claims abstract description 18
- 229920002396 Polyurea Polymers 0.000 claims abstract description 17
- 239000004094 surface-active agent Substances 0.000 claims abstract description 17
- 125000004122 cyclic group Chemical group 0.000 claims abstract description 11
- 238000004519 manufacturing process Methods 0.000 claims abstract description 9
- 239000000654 additive Substances 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 50
- 125000004432 carbon atom Chemical group C* 0.000 claims description 22
- 239000004814 polyurethane Substances 0.000 claims description 22
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 19
- 229920002635 polyurethane Polymers 0.000 claims description 17
- 230000002209 hydrophobic effect Effects 0.000 claims description 14
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 claims description 13
- 229920006395 saturated elastomer Polymers 0.000 claims description 13
- 150000002430 hydrocarbons Chemical group 0.000 claims description 12
- 229930195734 saturated hydrocarbon Natural products 0.000 claims description 12
- 229930195735 unsaturated hydrocarbon Natural products 0.000 claims description 12
- 150000002148 esters Chemical group 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 125000002947 alkylene group Chemical group 0.000 claims description 6
- 150000005846 sugar alcohols Polymers 0.000 claims description 6
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 claims description 5
- 239000000178 monomer Substances 0.000 claims description 5
- 239000004215 Carbon black (E152) Substances 0.000 claims description 4
- 229940126062 Compound A Drugs 0.000 claims description 4
- NLDMNSXOCDLTTB-UHFFFAOYSA-N Heterophylliin A Natural products O1C2COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC2C(OC(=O)C=2C=C(O)C(O)=C(O)C=2)C(O)C1OC(=O)C1=CC(O)=C(O)C(O)=C1 NLDMNSXOCDLTTB-UHFFFAOYSA-N 0.000 claims description 4
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 claims description 4
- 229920000233 poly(alkylene oxides) Polymers 0.000 claims description 3
- -1 C 6 hydrocarbons Chemical class 0.000 abstract description 18
- 229930195733 hydrocarbon Natural products 0.000 abstract description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 2
- 229910052786 argon Inorganic materials 0.000 abstract 1
- 230000001804 emulsifying effect Effects 0.000 abstract 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 34
- 229920005862 polyol Polymers 0.000 description 34
- 150000003077 polyols Chemical class 0.000 description 31
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 24
- 150000002009 diols Chemical class 0.000 description 15
- SFHYNDMGZXWXBU-LIMNOBDPSA-N 6-amino-2-[[(e)-(3-formylphenyl)methylideneamino]carbamoylamino]-1,3-dioxobenzo[de]isoquinoline-5,8-disulfonic acid Chemical compound O=C1C(C2=3)=CC(S(O)(=O)=O)=CC=3C(N)=C(S(O)(=O)=O)C=C2C(=O)N1NC(=O)N\N=C\C1=CC=CC(C=O)=C1 SFHYNDMGZXWXBU-LIMNOBDPSA-N 0.000 description 14
- 238000006243 chemical reaction Methods 0.000 description 14
- 235000014113 dietary fatty acids Nutrition 0.000 description 13
- 239000000194 fatty acid Substances 0.000 description 13
- 229930195729 fatty acid Natural products 0.000 description 13
- 239000011541 reaction mixture Substances 0.000 description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 12
- 239000012530 fluid Substances 0.000 description 12
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 12
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 12
- 150000004665 fatty acids Chemical class 0.000 description 11
- 229920000570 polyether Polymers 0.000 description 11
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 10
- 239000004721 Polyphenylene oxide Substances 0.000 description 10
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- 239000004530 micro-emulsion Substances 0.000 description 9
- 239000002253 acid Substances 0.000 description 8
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 8
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 7
- 239000007789 gas Substances 0.000 description 7
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 6
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 6
- 150000001412 amines Chemical class 0.000 description 6
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 6
- BTFJIXJJCSYFAL-UHFFFAOYSA-N icosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 description 6
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 5
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 5
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 5
- FDQSRULYDNDXQB-UHFFFAOYSA-N benzene-1,3-dicarbonyl chloride Chemical compound ClC(=O)C1=CC=CC(C(Cl)=O)=C1 FDQSRULYDNDXQB-UHFFFAOYSA-N 0.000 description 5
- 239000001569 carbon dioxide Substances 0.000 description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 description 5
- 239000004088 foaming agent Substances 0.000 description 5
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 5
- 230000006911 nucleation Effects 0.000 description 5
- 238000010899 nucleation Methods 0.000 description 5
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 5
- 239000004417 polycarbonate Substances 0.000 description 5
- 229920000515 polycarbonate Polymers 0.000 description 5
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 5
- ARXKVVRQIIOZGF-UHFFFAOYSA-N 1,2,4-butanetriol Chemical compound OCCC(O)CO ARXKVVRQIIOZGF-UHFFFAOYSA-N 0.000 description 4
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 4
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 4
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 4
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 4
- 150000001298 alcohols Chemical class 0.000 description 4
- 150000001414 amino alcohols Chemical class 0.000 description 4
- 125000005442 diisocyanate group Chemical group 0.000 description 4
- 230000032050 esterification Effects 0.000 description 4
- 238000005886 esterification reaction Methods 0.000 description 4
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 4
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 4
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 4
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 description 4
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 4
- OEIJHBUUFURJLI-UHFFFAOYSA-N octane-1,8-diol Chemical compound OCCCCCCCCO OEIJHBUUFURJLI-UHFFFAOYSA-N 0.000 description 4
- 229940059574 pentaerithrityl Drugs 0.000 description 4
- KIDHWZJUCRJVML-UHFFFAOYSA-N putrescine Chemical compound NCCCCN KIDHWZJUCRJVML-UHFFFAOYSA-N 0.000 description 4
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 4
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 description 3
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 3
- NMRPBPVERJPACX-UHFFFAOYSA-N (3S)-octan-3-ol Natural products CCCCCC(O)CC NMRPBPVERJPACX-UHFFFAOYSA-N 0.000 description 3
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 3
- QWGRWMMWNDWRQN-UHFFFAOYSA-N 2-methylpropane-1,3-diol Chemical compound OCC(C)CO QWGRWMMWNDWRQN-UHFFFAOYSA-N 0.000 description 3
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 3
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 3
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 3
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 3
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- 239000001361 adipic acid Substances 0.000 description 3
- 235000011037 adipic acid Nutrition 0.000 description 3
- 150000008064 anhydrides Chemical class 0.000 description 3
- 230000001588 bifunctional effect Effects 0.000 description 3
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 150000004985 diamines Chemical class 0.000 description 3
- 239000000539 dimer Substances 0.000 description 3
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 3
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229920000768 polyamine Polymers 0.000 description 3
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- 229920000642 polymer Polymers 0.000 description 3
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 3
- 235000013772 propylene glycol Nutrition 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N urea group Chemical group NC(=O)N XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 2
- ORTVZLZNOYNASJ-UPHRSURJSA-N (z)-but-2-ene-1,4-diol Chemical compound OC\C=C/CO ORTVZLZNOYNASJ-UPHRSURJSA-N 0.000 description 2
- ZWVMLYRJXORSEP-UHFFFAOYSA-N 1,2,6-Hexanetriol Chemical compound OCCCCC(O)CO ZWVMLYRJXORSEP-UHFFFAOYSA-N 0.000 description 2
- RTTZISZSHSCFRH-UHFFFAOYSA-N 1,3-bis(isocyanatomethyl)benzene Chemical compound O=C=NCC1=CC=CC(CN=C=O)=C1 RTTZISZSHSCFRH-UHFFFAOYSA-N 0.000 description 2
- PCHXZXKMYCGVFA-UHFFFAOYSA-N 1,3-diazetidine-2,4-dione Chemical compound O=C1NC(=O)N1 PCHXZXKMYCGVFA-UHFFFAOYSA-N 0.000 description 2
- HNSDLXPSAYFUHK-UHFFFAOYSA-N 1,4-bis(2-ethylhexyl) sulfosuccinate Chemical compound CCCCC(CC)COC(=O)CC(S(O)(=O)=O)C(=O)OCC(CC)CCCC HNSDLXPSAYFUHK-UHFFFAOYSA-N 0.000 description 2
- ALQLPWJFHRMHIU-UHFFFAOYSA-N 1,4-diisocyanatobenzene Chemical compound O=C=NC1=CC=C(N=C=O)C=C1 ALQLPWJFHRMHIU-UHFFFAOYSA-N 0.000 description 2
- OVBFMUAFNIIQAL-UHFFFAOYSA-N 1,4-diisocyanatobutane Chemical compound O=C=NCCCCN=C=O OVBFMUAFNIIQAL-UHFFFAOYSA-N 0.000 description 2
- SBJCUZQNHOLYMD-UHFFFAOYSA-N 1,5-Naphthalene diisocyanate Chemical compound C1=CC=C2C(N=C=O)=CC=CC2=C1N=C=O SBJCUZQNHOLYMD-UHFFFAOYSA-N 0.000 description 2
- DFPJRUKWEPYFJT-UHFFFAOYSA-N 1,5-diisocyanatopentane Chemical compound O=C=NCCCCCN=C=O DFPJRUKWEPYFJT-UHFFFAOYSA-N 0.000 description 2
- 229940008841 1,6-hexamethylene diisocyanate Drugs 0.000 description 2
- BMVXCPBXGZKUPN-UHFFFAOYSA-N 1-hexanamine Chemical compound CCCCCCN BMVXCPBXGZKUPN-UHFFFAOYSA-N 0.000 description 2
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- ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 2,3-dimethylbutane Chemical compound CC(C)C(C)C ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 0.000 description 2
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 2
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- DSKYSDCYIODJPC-UHFFFAOYSA-N 2-butyl-2-ethylpropane-1,3-diol Chemical compound CCCCC(CC)(CO)CO DSKYSDCYIODJPC-UHFFFAOYSA-N 0.000 description 2
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- 239000005700 Putrescine Substances 0.000 description 2
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- ISKQADXMHQSTHK-UHFFFAOYSA-N [4-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=C(CN)C=C1 ISKQADXMHQSTHK-UHFFFAOYSA-N 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 150000008051 alkyl sulfates Chemical class 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 2
- 238000000149 argon plasma sintering Methods 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- HIFVAOIJYDXIJG-UHFFFAOYSA-N benzylbenzene;isocyanic acid Chemical class N=C=O.N=C=O.C=1C=CC=CC=1CC1=CC=CC=C1 HIFVAOIJYDXIJG-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
- OHJMTUPIZMNBFR-UHFFFAOYSA-N biuret Chemical compound NC(=O)NC(N)=O OHJMTUPIZMNBFR-UHFFFAOYSA-N 0.000 description 2
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
- C08J2375/02—Polyureas
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
- C08J2375/04—Polyurethanes
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- Chemical & Material Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Dispersion Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Abstract
Description
Claims (15)
- A) 임의로는 이소시아네이트-반응성 화합물 ("NCO-반응성 화합물");
B) 선형, 분지형 또는 시클릭 C1- 내지 C6-탄화수소, 선형, 분지형 또는 시클릭 C1- 내지 C6-(히드로)플루오로카본, N2, O2, 아르곤 및/또는 CO2를 포함하는 군으로부터 선택되고, 초임계 또는 근임계 상태로 존재하는 발포제;
C) 임의로는 폴리이소시아네이트;
D) 친양쪽성 이소시아네이트; 및
E) 임의로는 계면활성제 및
F) 임의로는 추가 보조제/첨가 물질
을 포함하는 혼합물의 반응으로부터 수득가능한 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체. - 제1항 또는 제2항에 있어서, 친양쪽성 이소시아네이트가 1 내지 18의 HLB 값을 갖는 것인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 또는 제2항에 있어서, 친양쪽성 이소시아네이트가 2 내지 17의 HLB 값을 갖는 것인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 또는 제2항에 있어서, 친양쪽성 이소시아네이트가 3 내지 16의 HLB 값을 갖는 것인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 내지 제4항 중 어느 한 항에 있어서, 친양쪽성 이소시아네이트의 비율이 전체 조성물의 중량을 기준으로 5 내지 70 중량%인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 내지 제5항 중 어느 한 항에 있어서, 친양쪽성 이소시아네이트의 소수성 부분이 적어도 4개의 탄소 원자를 갖는 포화 또는 불포화 탄화수소 쇄를 갖는 1가 또는 다가 알콜을 포함하는 군으로부터 선택된 알콜의 라디칼인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 내지 제5항 중 어느 한 항에 있어서, 친양쪽성 이소시아네이트의 친수성 부분이 일관능성 또는 다관능성 폴리알킬렌 옥시드를 포함하는 군으로부터 선택된 알콜의 라디칼인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 내지 제7항 중 어느 한 항에 있어서, 성분 A) 내지 F)가 하기 중량 백분율 (중량%):
A) 0 내지 60 중량%, 바람직하게는 10 내지 60 중량%,
B) 2 내지 40 중량%,
C + D) 20 내지 70 중량% (여기서, C) : D)의 중량 백분율 비는 0:100 내지 75:25, 바람직하게는 1:99 내지 75:25임),
E) 0 내지 20 중량%,
F) 0 내지 10 중량%
로 전체 조성물 중에 존재하며, 여기서 모든 비율의 합은 100 중량% 양인, 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체. - 제1항 내지 제8항 중 어느 한 항에 있어서, 성분 A) 중 일부 또는 전부가, 소수성 부분 및 친수성 부분을 포함하고 1 초과의 평균 히드록실 관능가를 갖는 성분 A2)이며,
여기서 소수성 부분은 적어도 6개의 탄소 원자를 갖는 포화 또는 불포화 탄화수소 쇄를 포함하고,
여기서 친수성 부분은 알킬렌 옥시드 단위 및/또는 에스테르 단위를 포함하는 것인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체. - 제1항 내지 제9항 중 어느 한 항에 있어서, 폴리이소시아네이트 성분 C)가 단량체 및/또는 중합체 디페닐메탄 4,4'-디이소시아네이트를 포함하는 것인 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 내지 제10항 중 어느 한 항에 있어서, ≥ 20 kg/m3 내지 ≤ 160 kg/m3의 겉보기 밀도를 갖는 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체.
- 제1항 내지 제11항 중 어느 한 항에 청구된 바와 같은 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체를 제조하는 방법이며,
- 성분 A), B), C), D), 및 임의로는 E) 및 임의로는 F)를 포함하는 혼합물을 폐쇄된 몰드에 도입하며, 여기서 폐쇄된 몰드는 그의 내부 부피 및/또는 그의 내부에서 지배적인 압력이 혼합물이 도입된 후 외부 영향에 의해 변화될 수 있도록 설정되는 것인 단계;
- 성분 A), B), C), D), 및 임의로는 E) 및 임의로는 F)를 포함하는 혼합물을 폐쇄된 몰드에서 ≥ 0초의 미리 결정된 기간 동안 정치시키는 단계; 및
- 외부 영향에 의해 폐쇄된 몰드의 내부 부피를 증가시키고/거나 폐쇄된 몰드의 내부에서 지배적인 압력을 감소시키는 단계
를 포함하는, 제1항 내지 제11항 중 어느 한 항에 청구된 바와 같은 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체를 제조하는 방법. - 제1항 내지 제11항 중 어느 한 항에 청구된 바와 같은 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체를 제조하는 방법이며,
- 제1항 내지 제10항 중 어느 한 항에 기술된 바와 같은 화합물 A), B), C), D), 및 임의로는 E) 및 임의로는 F)의 혼합물을 승압 하에 제공하는 단계; 및
- 혼합물을 방출하며, 여기서 방출 동안 혼합물에서 지배적인 압력이 대기압으로 감소되는 것인 단계
를 포함하는, 제1항 내지 제11항 중 어느 한 항에 청구된 바와 같은 폴리우레탄, 폴리이소시아누레이트 또는 폴리우레아 발포체를 제조하는 방법. - 제12항 또는 제13항에 있어서, 성분 B) 중 일부 또는 전부가 친양쪽성 이소시아네이트 D) 또는 이소시아네이트 성분 C)와 D)의 혼합물 중에 제공되는 것인 방법.
- 제14항에 있어서, 성분 B) 중 일부가 성분 A2)를 포함하는 NCO-반응성 화합물 A) 중에 제공되는 것인 방법.
Applications Claiming Priority (3)
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EP13192109.0 | 2013-11-08 | ||
EP13192109 | 2013-11-08 | ||
PCT/EP2014/074038 WO2015067751A1 (de) | 2013-11-08 | 2014-11-07 | Polyurethanschaum und verfahren zu seiner herstellung |
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KR20160084845A true KR20160084845A (ko) | 2016-07-14 |
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US (1) | US10131759B2 (ko) |
EP (1) | EP3066144B1 (ko) |
JP (1) | JP2016537466A (ko) |
KR (1) | KR20160084845A (ko) |
CN (1) | CN105829385B (ko) |
CA (1) | CA2928632A1 (ko) |
MX (1) | MX2016005916A (ko) |
TR (1) | TR201903415T4 (ko) |
WO (1) | WO2015067751A1 (ko) |
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KR20190033058A (ko) * | 2016-07-22 | 2019-03-28 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 다당류를 포함하는 폴리우레탄 중합체 |
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WO2018018571A1 (en) * | 2016-07-29 | 2018-02-01 | Dow Global Technologies Llc | Insulative apparatus |
EP3864062A1 (en) | 2018-10-08 | 2021-08-18 | Dow Global Technologies LLC | Formulated polyol compositions |
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US3672955A (en) | 1970-05-20 | 1972-06-27 | Us Agriculture | Preparation of an insoluble active enzyme |
US5670601A (en) * | 1995-06-15 | 1997-09-23 | Arco Chemical Technology, L.P. | Polyurethane elastomers having improved green strength and demold time and polyoxyalkylene polyols suitable for their preparation |
US6051622A (en) * | 1998-09-17 | 2000-04-18 | Arco Chemical Technology, L.P. | Low resilience, low frequency molded polyurethane foam |
DE10030384A1 (de) | 2000-06-21 | 2002-01-03 | Hennecke Gmbh | Verfahren zur Herstellung von Blockschaum |
BR0214511B1 (pt) * | 2001-11-29 | 2012-09-04 | sistema de reação para a preparação de um material termocurável de poliuretano viscoelástico, material de poliuretano viscoelástico, sistema de reação para a preparação de materiais termocuráveis de poliuretano viscoelástico celular, e, material termocurável celular de poliuretano viscoelástico. | |
JP4154654B2 (ja) * | 2002-09-13 | 2008-09-24 | アキレス株式会社 | 硬質ポリウレタンフォームの製造方法 |
DE10260815B4 (de) | 2002-12-23 | 2008-07-03 | Universität Zu Köln | Aufgeschäumtes Material und Herstellverfahren für das aufgeschäumte Material |
WO2007094780A1 (en) * | 2006-02-15 | 2007-08-23 | Stepan Company | Compatibilizing surfactants for polyurethane polyols and resins |
JP5368716B2 (ja) * | 2007-03-01 | 2013-12-18 | 花王株式会社 | ポリウレタン成形品の製造方法 |
US20090325445A1 (en) * | 2008-06-27 | 2009-12-31 | Bogdan Mary C | Method of insulating temporary polymeric structures with polyurethane or polyisocyanurate foam |
DE102009053218A1 (de) * | 2009-11-06 | 2011-07-14 | Bayer MaterialScience AG, 51373 | Verfahren zur Herstellung eines Polyurethanschaums mittels über- oder nahekritischen Treibmittels |
DE102009053224A1 (de) | 2009-11-06 | 2011-07-14 | Bayer MaterialScience AG, 51373 | Verfahren zur Herstellung eines Polyurethanschaums und hieraus erhältlicher Polyurethanschaum |
JP5377368B2 (ja) * | 2010-03-10 | 2013-12-25 | 東洋ゴム工業株式会社 | 発泡ポリウレタンおよびその製造方法、ならびに発泡ポリウレタンで構成された自動車用防振部材 |
DE102011050013A1 (de) | 2011-04-29 | 2012-10-31 | Bayer Materialscience Aktiengesellschaft | Polyurethanschaum und Verfahren zu seiner Herstellung |
DE102011050014A1 (de) | 2011-04-29 | 2012-10-31 | Bayer Materialscience Aktiengesellschaft | Polyurethanschaum und Verfahren zu seiner Herstellung |
CN104619736B (zh) * | 2012-07-31 | 2017-08-18 | 科思创德国股份有限公司 | 使用乳化发泡剂制备聚氨酯泡沫的方法 |
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- 2014-11-07 JP JP2016528209A patent/JP2016537466A/ja active Pending
- 2014-11-07 TR TR2019/03415T patent/TR201903415T4/tr unknown
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KR20190033058A (ko) * | 2016-07-22 | 2019-03-28 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 다당류를 포함하는 폴리우레탄 중합체 |
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EP3066144A1 (de) | 2016-09-14 |
WO2015067751A1 (de) | 2015-05-14 |
TR201903415T4 (tr) | 2019-04-22 |
MX2016005916A (es) | 2016-07-13 |
JP2016537466A (ja) | 2016-12-01 |
CA2928632A1 (en) | 2015-05-14 |
US10131759B2 (en) | 2018-11-20 |
US20160264749A1 (en) | 2016-09-15 |
CN105829385B (zh) | 2020-03-31 |
CN105829385A (zh) | 2016-08-03 |
EP3066144B1 (de) | 2018-12-26 |
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