KR20020011587A - Process for preparation germanium water concentration powder and the apparatus - Google Patents

Abstract

PURPOSE: A preparation method of Ge powder by condensing Ge water through low temperature distillation by fan-drying unlike a conventional high temperature distillation is provided to enable mass production at low temperature and reduce production time. CONSTITUTION: The preparation method is as follows: supplying Ge water to a water evaporating part(120) which consists of square boxes(20) piled up to 6-10 floors, wherein fine holes are on the bottom of the box at 15-20cm of intervals and distillation hair boards are between the boxes; ventilation-drying by fans(60, 60-1) set on the upper and lower side; supplying Ge water passing through the boxes to the water evaporating part repeatedly until the amount of Ge water is 1/4 of the initial amount; centrifuging the distilled Ge water to remove heavy metals(Pb, Zn, etc,) and impurities; supplying Ge water to the water evaporating part by pump(80-1); drying at 65-75deg.C with stirring to evaporate water and prevent agglomeration; and grinding.

Description

Process for preparation germanium water concentration powder and the apparatus

The present invention relates to a method for producing germanium water concentrate powder and apparatus thereof. More specifically, the present invention relates to a method and apparatus for distilling germanium water to concentrate it in powdered germanium.

In the past, many people have confirmed that germanium water is effective in improving the health of the human body, and has been widely used by applying it to the hands, feet, baths, saunas, and the like.

However, since germanium water contains a large amount of heavy metals harmful to the human body, such as iron, aluminum, lead, and zinc, in addition to germanium, it is not only possible to take it as an edible drink but also has been reluctant to apply it to the body.

In view of the above, the present inventors distilled and concentrated the germanium water collected from Hambaeksan, Jeongseon-gun, Gangwon-do in a manner other than high temperature heating distillation, and centrifuged to reduce the concentration of heavy metals and foreign substances contained in the germanium water. The present invention was completed by preparing a large amount of germanium powder in a short time.

Accordingly, an object of the present invention is to provide a method for producing a large amount of germanium powder in a short time by distilling and concentrating water containing germanium.

Another object of the present invention is to provide a powder manufacturing apparatus which can mass-produce germanium water-enriched powder, which is low in manufacturing cost and shortened in production time.

The object of the present invention is to pass through the germanium water not heated to a high temperature or the germanium water heated to a low temperature through a rectangular box in which a through-hole is formed and a distillation cap is formed in turn through the air-dried distillation and the germanium water remaining without distillation again The germanium distillate obtained by repeating the above process was centrifuged to reduce the concentration of the heavy metal and the substance contained in the precipitate and the germanium water, and was slowly dried at low temperature to produce a powdered germanium.

Hereinafter, the configuration of the present invention will be described.

1 is a state diagram showing the use of the apparatus according to the germanium water concentrate powder production method of a preferred embodiment of the present invention,

Figure 2 is a perspective view showing the receiving portion and the positive distillation bed portion of the germanium water concentrate powder production apparatus of the present invention,

Figure 3 is a state diagram showing the tank portion of the germanium water concentrated powder production apparatus of the present invention.

* Explanation of symbols for the main parts of the drawings *

10: hole 20: receiving plate

30: long distilled hair 40: short distilled hair

50: positive distillation bed 60: blowing fan

100: partition 120: water vaporization

130: centrifuge 170: drying means

180: crushing unit

The present invention supplies germanium water that is not heated to the present evaporator, in which a rectangular box formed with fine pores having a diameter of 2-3 mm at intervals of 15 to 20 cm is stacked about 6 to 10 layers, and distilled hair is formed between the rectangular box layers and layers. At the same time, ventilate dry using a fan at the top and bottom, and the germanium water dropped under the receiving part is fed back to the evaporator, and the distillation is repeated to 1/4 level of the initial germanium water, and the germanium distillate obtained is centrifuged to separate germanium according to the weight. Preparing a germanium water concentrated powder of the present invention that is not lumped by supplying germanium distillate having reduced concentration of the heavy metal and the substance contained in the water to the water evaporation unit and evaporating the water and then putting it in a low temperature drying stand and stirring; Performing the same method as described above, but supplying germanium water having a water temperature of 35 to 45 ° C. to an evaporator to produce the germanium water concentrated powder of the present invention; It is carried out in the same manner as above but heated to supply a germanium water having a water temperature of 75 ~ 85 ℃ evaporator is composed of a process for producing a germanium water concentrated powder of the present invention.

Hereinafter, the specific method of the present invention will be described in detail with reference to the accompanying drawings and examples, but the scope of the present invention is not limited to these embodiments.

1 is a state diagram showing the apparatus according to the germanium water concentrate powder manufacturing method of the preferred embodiment of the present invention, Figure 2 is a perspective view showing the receiving portion and the positive distillation bed portion of the germanium water concentrate powder manufacturing apparatus of the present invention, Figure 3 is a state diagram showing the tank portion of the germanium water concentrated powder production apparatus of the present invention.

First, a method for producing germanium water concentrated powder of a preferred embodiment of the present invention will be described.

Example 1 Preparation of Germanium Water Concentrate Powder of the Invention Using Unheated Germanium Water

The germanium water used in this example is taken from Hambaeksan, Jeongseon-gun, Gangwon-do, and is in a natural state without heat treatment. Distillation was repeated until 18 L of germanium water was fed to the present invention evaporator and 4.5 L of germanium water eluted under the evaporator. At this time, the drying was ventilated dry using a fan up and down the evaporator. The distilled germanium distillate was transferred to a centrifuge to reduce the heavy metals such as lead and zinc, and other impurities, which were then dried on a drying rack. At the time of drying, the germanium must be continuously stirred to prevent it from sticking or agglomerating on the drying plate and the temperature should not exceed 70 ° C. The dried germanium was crushed into fine powder and commercialized, and the final germanium powder was 20 g.

Example 2 Preparation of Germanium Water Concentrate Powder of the Present Invention Using Germanium Water Heated at Low Temperature

The germanium water concentrate powder was prepared in the same manner as in Example 1, but 18 g of the used germanium water was heated at 35 to 45 ° C. at a low temperature in a heating tank and then applied to the evaporator of the present invention to obtain 22 g of the final germanium powder.

Example 3 Preparation of Germanium Water Concentrate Powder of the Present Invention Using Germanium Water Heated at High Temperature

The germanium water concentrate powder was prepared in the same manner as in Example 1, but 18 g of the used germanium water was heated at 70 ° C. at a low temperature in a heating tank, and then applied to the evaporator of the present invention to obtain 23 g of the final germanium powder.

In Examples 1, 2, and 3, the temperature of the germanium water and the drying temperature play an important role in showing the health promotion effect of the germanium powder, and the germanium temperature may be any of 10 to 90 ° C., but preferably 30 to 30 ° C. The temperature is 40 ℃ and the temperature of drying is 40 ~ 50 ℃, but if the temperature is low, it takes a long time. If the temperature is 80 ~ 90 ℃, it is dried for a short time, but the health promotion effect of germanium is reduced, so it is 65 ~ 75 ℃. Is preferred.

Hereinafter, the present invention will be described in detail with reference to the evaporation apparatus for germanium concentration.

First, the apparatus according to the germanium water concentrate powder manufacturing method of the present invention shown in Figs. 1 to 3 by laminating the positive distillation bed portion 50 and the receiving plate formed with pores in multiple stages by dropping the germanium water on the top Water evaporation unit 120 to evaporate moisture by blowing, centrifuge 130 to reduce the concentration of heavy metals and foreign substances contained in the germanium water evaporated a certain amount of water, and dry to completely remove the moisture And a means unit 170 and a pulverizing unit 180 for pulverizing and drying the dried germanium.

Next, the water vaporization unit 120 is a germanium water receiving plate 20 formed with a porous 10, the upper part of the long distilled hair 30 and the lower part of the short distilled hair 40 by inserting the germanium water by dry wind A multi-stage blower fan 50 is formed so as to be stacked in a multi-stage structure by placing the positive distillation bed plate 50 formed on the upper end of the receiving plate as a set, and a plurality of blower fans are supplied to the positive distillation bed plate 50 above. (80, 60-1), the pump 80 and the pipe 90 to supply the germanium water moved to the tank portion 70 at the bottom through the stacked support plate 20 of the multi-stage to the upper support plate. It is composed of In addition, a multi-stage partition 100 is formed in the tank, and a discharge pipe is mounted at the end to heat the water supplied to the upper support plate, and a heating unit 110 is configured at the lower end thereof to heat at a constant temperature.

The centrifuge 130 is mounted to reduce the concentration of heavy metals and foreign matter contained in the germanium water evaporated a certain amount of water in the water evaporation unit 120. The centrifuge uses machinery using rotational force.

The centrifugal separator 130 is configured to supply germanium water to the water evaporation unit 120 to the pump 80-1 to evaporate the second moisture.

On the other hand, the drying means unit 170 is the pump 80-2 and the heating unit 140, which is mounted to transfer to completely dry the germanium water in the water evaporation unit, and the germanium water by the heating unit to prevent the solidification and drying It consists of a crossbar 150 and the actuator 160 is mounted so that the crossbar reciprocates so that the actuator 160 reciprocates and mounted to prevent water from evaporating and solidifying.

The drying means unit 170 was equipped with a pulverization unit 180 for pulverizing and drying the germanium lumps to be pulverized to obtain germanium powder.

For example, the present invention is not limited to the above-described embodiment, and various modifications can be made by those skilled in the art without departing from the gist of the present invention as claimed in the claims. Such changes are intended to be within the scope of the present invention.

As described above, the present invention has the effect of distilling and concentrating germanium-containing water to obtain germanium powder, and also can produce large quantities quickly at low temperature, and thus, the manufacturing cost is low. Since it is an excellent effect, it is a very useful invention in the germanium powder manufacturing industry.

Claims (4)

After supplying germanium water to the evaporator (water evaporation unit) and ventilating with a fan at the side, the germanium water dropped under the receiving part is supplied to the water evaporator again and distilled to 1/4 level of the initial germanium water. After the germanium distillate obtained by centrifugation to reduce the concentration of heavy metals and the substance contained in the germanium water and evaporated again in the water evaporation zone, the germanium water concentrated powder production, characterized in that dried in a low temperature drying table and dried while reciprocating Way. The method of claim 1, wherein the temperature of the drying zone is 40 to 60 ° C. A water evaporation part for laminating the positive distillation bed plate part and the receiving plate formed with pores in multiple stages, dropping the germanium water on the upper part thereof, and evaporating water by forced air; A centrifugal separator, a drying part for completely removing water, and a pulverizing part for pulverizing and drying the dried germanium to reduce the concentration of heavy metals and foreign substances contained in the evaporated germanium water in a predetermined amount of water. Germanium water concentrate powder manufacturing apparatus. Germanium water receiver plate with perforations, and a distillation mother plate part formed on the upper part of the receiving plate by forming a long distillation cap on the upper part and a short distillation cap on the lower part so that the germanium water is dried by dry wind in one step. And a plurality of blowing fans to supply dry air to the positive distillation bed plate, and to supply germanium water moved to the tank part at the bottom of the multi-layered base plate to the top plate. A water vaporization part including a pipe; A centrifugal separator mounted to reduce the concentration of heavy metals and the substance contained in the germanium water evaporated a predetermined amount of water in the water evaporation unit; The second centrifugal separator is configured to supply germanium water to the water evaporation unit as a pump to evaporate the second moisture, Drying consisting of a pump and a heating unit mounted to transfer the germanium water in the water evaporation unit to completely dry, and a crossbar and an actuator mounted to reciprocate so that the germanium water is prevented from solidification and dried by the heating unit. A means section; Germanium water concentrate powder manufacturing apparatus, characterized in that consisting of a pulverizing unit for pulverizing the powdered germanium lump dried in the drying means.