KR101866581B1 - 폴리카보네이트 수지 조성물 및 폴리카보네이트 수지 성형체 - Google Patents
폴리카보네이트 수지 조성물 및 폴리카보네이트 수지 성형체 Download PDFInfo
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- KR101866581B1 KR101866581B1 KR1020127030448A KR20127030448A KR101866581B1 KR 101866581 B1 KR101866581 B1 KR 101866581B1 KR 1020127030448 A KR1020127030448 A KR 1020127030448A KR 20127030448 A KR20127030448 A KR 20127030448A KR 101866581 B1 KR101866581 B1 KR 101866581B1
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- polycarbonate resin
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- 229920005668 polycarbonate resin Polymers 0.000 title claims abstract description 81
- 239000004431 polycarbonate resin Substances 0.000 title claims abstract description 81
- 239000000203 mixture Substances 0.000 title claims abstract description 66
- 229920000515 polycarbonate Polymers 0.000 claims abstract description 69
- 239000004417 polycarbonate Substances 0.000 claims abstract description 69
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 63
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000003063 flame retardant Substances 0.000 claims abstract description 38
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 30
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 30
- 238000000465 moulding Methods 0.000 claims abstract description 18
- 125000003118 aryl group Chemical group 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims description 29
- BRPSWMCDEYMRPE-UHFFFAOYSA-N 4-[1,1-bis(4-hydroxyphenyl)ethyl]phenol Chemical compound C=1C=C(O)C=CC=1C(C=1C=CC(O)=CC=1)(C)C1=CC=C(O)C=C1 BRPSWMCDEYMRPE-UHFFFAOYSA-N 0.000 claims description 15
- 239000006085 branching agent Substances 0.000 claims description 15
- 125000004432 carbon atom Chemical group C* 0.000 claims description 13
- 239000003795 chemical substances by application Substances 0.000 claims description 13
- 229910052783 alkali metal Inorganic materials 0.000 claims description 11
- 238000009792 diffusion process Methods 0.000 claims description 11
- 125000000217 alkyl group Chemical group 0.000 claims description 10
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 9
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 8
- 239000003963 antioxidant agent Substances 0.000 claims description 7
- 230000003078 antioxidant effect Effects 0.000 claims description 7
- 229910052739 hydrogen Inorganic materials 0.000 claims description 6
- 239000001257 hydrogen Substances 0.000 claims description 6
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims description 5
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 239000011342 resin composition Substances 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 4
- 239000004973 liquid crystal related substance Substances 0.000 claims description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 4
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 238000002834 transmittance Methods 0.000 abstract description 14
- 238000004383 yellowing Methods 0.000 abstract description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 114
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 75
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 70
- 239000000243 solution Substances 0.000 description 34
- 239000007864 aqueous solution Substances 0.000 description 21
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 15
- 238000004519 manufacturing process Methods 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 238000012360 testing method Methods 0.000 description 10
- 238000005406 washing Methods 0.000 description 9
- QHPQWRBYOIRBIT-UHFFFAOYSA-N 4-tert-butylphenol Chemical compound CC(C)(C)C1=CC=C(O)C=C1 QHPQWRBYOIRBIT-UHFFFAOYSA-N 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 150000003839 salts Chemical class 0.000 description 7
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 6
- 239000012295 chemical reaction liquid Substances 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000012074 organic phase Substances 0.000 description 6
- 239000012071 phase Substances 0.000 description 6
- 239000011574 phosphorus Substances 0.000 description 6
- 229910052698 phosphorus Inorganic materials 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 5
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 5
- 238000004898 kneading Methods 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 239000008188 pellet Substances 0.000 description 5
- 238000006116 polymerization reaction Methods 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 238000003786 synthesis reaction Methods 0.000 description 5
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000001746 injection moulding Methods 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 150000002989 phenols Chemical class 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 229920002050 silicone resin Polymers 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 239000007983 Tris buffer Substances 0.000 description 3
- AOGYCOYQMAVAFD-UHFFFAOYSA-N chlorocarbonic acid Chemical group OC(Cl)=O AOGYCOYQMAVAFD-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
- 238000001125 extrusion Methods 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 150000007524 organic acids Chemical class 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- SUCTVKDVODFXFX-UHFFFAOYSA-N 4-(4-hydroxy-3,5-dimethylphenyl)sulfonyl-2,6-dimethylphenol Chemical compound CC1=C(O)C(C)=CC(S(=O)(=O)C=2C=C(C)C(O)=C(C)C=2)=C1 SUCTVKDVODFXFX-UHFFFAOYSA-N 0.000 description 2
- HXDOZKJGKXYMEW-UHFFFAOYSA-N 4-ethylphenol Chemical compound CCC1=CC=C(O)C=C1 HXDOZKJGKXYMEW-UHFFFAOYSA-N 0.000 description 2
- HTVITOHKHWFJKO-UHFFFAOYSA-N Bisphenol B Chemical compound C=1C=C(O)C=CC=1C(C)(CC)C1=CC=C(O)C=C1 HTVITOHKHWFJKO-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 229920006358 Fluon Polymers 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 150000001342 alkaline earth metals Chemical class 0.000 description 2
- 229910052788 barium Inorganic materials 0.000 description 2
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 2
- VCCBEIPGXKNHFW-UHFFFAOYSA-N biphenyl-4,4'-diol Chemical group C1=CC(O)=CC=C1C1=CC=C(O)C=C1 VCCBEIPGXKNHFW-UHFFFAOYSA-N 0.000 description 2
- 229910052792 caesium Inorganic materials 0.000 description 2
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 238000000748 compression moulding Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical group C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 2
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 238000007602 hot air drying Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- IWDCLRJOBJJRNH-UHFFFAOYSA-N p-cresol Chemical compound CC1=CC=C(O)C=C1 IWDCLRJOBJJRNH-UHFFFAOYSA-N 0.000 description 2
- YFSUTJLHUFNCNZ-UHFFFAOYSA-N perfluorooctane-1-sulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YFSUTJLHUFNCNZ-UHFFFAOYSA-N 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 159000000001 potassium salts Chemical class 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 229910052712 strontium Inorganic materials 0.000 description 2
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 2
- 229920005992 thermoplastic resin Polymers 0.000 description 2
- CNHDIAIOKMXOLK-UHFFFAOYSA-N toluquinol Chemical compound CC1=CC(O)=CC=C1O CNHDIAIOKMXOLK-UHFFFAOYSA-N 0.000 description 2
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical group OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 2
- 239000013585 weight reducing agent Substances 0.000 description 2
- JDWGPDRDUUNFIB-UHFFFAOYSA-N 1,1,1,2,3,3,4,4,5,5,5-undecafluoropentane-2-sulfonic acid Chemical compound OS(=O)(=O)C(F)(C(F)(F)F)C(F)(F)C(F)(F)C(F)(F)F JDWGPDRDUUNFIB-UHFFFAOYSA-N 0.000 description 1
- GKNWQHIXXANPTN-UHFFFAOYSA-N 1,1,2,2,2-pentafluoroethanesulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)F GKNWQHIXXANPTN-UHFFFAOYSA-N 0.000 description 1
- XBWQFDNGNOOMDZ-UHFFFAOYSA-N 1,1,2,2,3,3,3-heptafluoropropane-1-sulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)F XBWQFDNGNOOMDZ-UHFFFAOYSA-N 0.000 description 1
- OYGQVDSRYXATEL-UHFFFAOYSA-N 1,1,2,2,3,3,4,4,5,5,6,6,7,7,7-pentadecafluoroheptane-1-sulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F OYGQVDSRYXATEL-UHFFFAOYSA-N 0.000 description 1
- HCNHNBLSNVSJTJ-UHFFFAOYSA-N 1,1-Bis(4-hydroxyphenyl)ethane Chemical compound C=1C=C(O)C=CC=1C(C)C1=CC=C(O)C=C1 HCNHNBLSNVSJTJ-UHFFFAOYSA-N 0.000 description 1
- URFNSYWAGGETFK-UHFFFAOYSA-N 1,2-bis(4-hydroxyphenyl)ethane Natural products C1=CC(O)=CC=C1CCC1=CC=C(O)C=C1 URFNSYWAGGETFK-UHFFFAOYSA-N 0.000 description 1
- FRASJONUBLZVQX-UHFFFAOYSA-N 1,4-dioxonaphthalene Natural products C1=CC=C2C(=O)C=CC(=O)C2=C1 FRASJONUBLZVQX-UHFFFAOYSA-N 0.000 description 1
- BOKGTLAJQHTOKE-UHFFFAOYSA-N 1,5-dihydroxynaphthalene Chemical compound C1=CC=C2C(O)=CC=CC2=C1O BOKGTLAJQHTOKE-UHFFFAOYSA-N 0.000 description 1
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 1
- KDYHQAWOWCCBAJ-UHFFFAOYSA-N 1h-indole-2,3-dione;2-methylphenol Chemical group CC1=CC=CC=C1O.CC1=CC=CC=C1O.C1=CC=C2C(=O)C(=O)NC2=C1 KDYHQAWOWCCBAJ-UHFFFAOYSA-N 0.000 description 1
- LEDKKDPOPIKMSZ-UHFFFAOYSA-N 2,4,5-trichlorobenzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC(Cl)=C(Cl)C=C1Cl LEDKKDPOPIKMSZ-UHFFFAOYSA-N 0.000 description 1
- LFXZSGVZSSMCMB-UHFFFAOYSA-N 2,5-dichlorobenzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC(Cl)=CC=C1Cl LFXZSGVZSSMCMB-UHFFFAOYSA-N 0.000 description 1
- RKSBPFMNOJWYSB-UHFFFAOYSA-N 3,3-Bis(4-hydroxyphenyl)pentane Chemical compound C=1C=C(O)C=CC=1C(CC)(CC)C1=CC=C(O)C=C1 RKSBPFMNOJWYSB-UHFFFAOYSA-N 0.000 description 1
- SSADPHQCUURWSW-UHFFFAOYSA-N 3,9-bis(2,6-ditert-butyl-4-methylphenoxy)-2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane Chemical compound CC(C)(C)C1=CC(C)=CC(C(C)(C)C)=C1OP1OCC2(COP(OC=3C(=CC(C)=CC=3C(C)(C)C)C(C)(C)C)OC2)CO1 SSADPHQCUURWSW-UHFFFAOYSA-N 0.000 description 1
- YLZOPXRUQYQQID-UHFFFAOYSA-N 3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]propan-1-one Chemical compound N1N=NC=2CN(CCC=21)CCC(=O)N1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F YLZOPXRUQYQQID-UHFFFAOYSA-N 0.000 description 1
- ZGZVGZCIFZBNCN-UHFFFAOYSA-N 4,4'-(2-Methylpropylidene)bisphenol Chemical compound C=1C=C(O)C=CC=1C(C(C)C)C1=CC=C(O)C=C1 ZGZVGZCIFZBNCN-UHFFFAOYSA-N 0.000 description 1
- RXNYJUSEXLAVNQ-UHFFFAOYSA-N 4,4'-Dihydroxybenzophenone Chemical compound C1=CC(O)=CC=C1C(=O)C1=CC=C(O)C=C1 RXNYJUSEXLAVNQ-UHFFFAOYSA-N 0.000 description 1
- VWGKEVWFBOUAND-UHFFFAOYSA-N 4,4'-thiodiphenol Chemical compound C1=CC(O)=CC=C1SC1=CC=C(O)C=C1 VWGKEVWFBOUAND-UHFFFAOYSA-N 0.000 description 1
- PQOGFLAGJZXUAK-UHFFFAOYSA-N 4-(2-phenylpropyl)phenol Chemical compound C=1C=CC=CC=1C(C)CC1=CC=C(O)C=C1 PQOGFLAGJZXUAK-UHFFFAOYSA-N 0.000 description 1
- JPSMTGONABILTP-UHFFFAOYSA-N 4-(4-hydroxy-3,5-dimethylphenyl)sulfanyl-2,6-dimethylphenol Chemical compound CC1=C(O)C(C)=CC(SC=2C=C(C)C(O)=C(C)C=2)=C1 JPSMTGONABILTP-UHFFFAOYSA-N 0.000 description 1
- RSSGMIIGVQRGDS-UHFFFAOYSA-N 4-[(4-hydroxyphenyl)-phenylmethyl]phenol Chemical compound C1=CC(O)=CC=C1C(C=1C=CC(O)=CC=1)C1=CC=CC=C1 RSSGMIIGVQRGDS-UHFFFAOYSA-N 0.000 description 1
- FITMQUNIHVIGRV-UHFFFAOYSA-N 4-[1,2,2-tris(4-hydroxyphenyl)-3,3,5-trimethylcyclohexyl]phenol Chemical compound OC1=CC=C(C=C1)C1(C(CC(CC1(C)C)C)(C1=CC=C(C=C1)O)C1=CC=C(C=C1)O)C1=CC=C(C=C1)O FITMQUNIHVIGRV-UHFFFAOYSA-N 0.000 description 1
- UCZMNMPFXUIPAC-UHFFFAOYSA-N 4-[1-(4-hydroxyphenyl)cyclodecyl]phenol Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)CCCCCCCCC1 UCZMNMPFXUIPAC-UHFFFAOYSA-N 0.000 description 1
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- KJMVGAOYRRKQPY-UHFFFAOYSA-N 4-[2,4,6-tri(propan-2-yl)phenyl]phenol Chemical compound CC(C)C1=CC(C(C)C)=CC(C(C)C)=C1C1=CC=C(O)C=C1 KJMVGAOYRRKQPY-UHFFFAOYSA-N 0.000 description 1
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Abstract
점도 평균 분자량이 17,000 이상이고, (A-1) 분기형 폴리카보네이트 10∼100 질량부 및 (A-2) 방향족 폴리카보네이트 90∼0 질량부로 이루어지는 (A) 폴리카보네이트 100 질량부에 대해, (B) 광확산제 0.1∼5 질량부, (C) 난연제 0.01∼1.0 질량부, (D) 폴리테트라플루오로에틸렌 0∼0.5 질량부, (E) 폴리오르가노실록산 0∼2 질량부를 함유하는 것을 특징으로 하는 난연 광확산 폴리카보네이트 수지 조성물, 그리고, 그 폴리카보네이트 수지 조성물을 성형 가공하여 얻어지는 폴리카보네이트 수지 성형체이다.
Description
b : 광원
c : 확산광 각도
Claims (19)
- 점도 평균 분자량이 17,000 이상이고, (A-1) 분기형 폴리카보네이트 10∼100 질량부 및 (A-2) 방향족 폴리카보네이트 90∼0 질량부로 이루어지는 (A) 폴리카보네이트 100 질량부에 대해, (B) 광확산제 0.1∼5 질량부, (C) 난연제 0.01∼1.0 질량부, (D) 폴리테트라플루오로에틸렌 0∼0.5 질량부, (E) 폴리오르가노실록산 0∼1 질량부를 포함하고, 상기 (A-1) 성분이 하기 일반식 (I) 로 나타내는 분기제로부터 유도된 분기 핵 구조를 갖는 분기형 폴리카보네이트인 것을 특징으로 하는 난연 광확산 폴리카보네이트 수지 조성물.
[화학식 1]
[일반식 (I) 에 있어서, R 은 수소 또는 탄소수 1∼5 의 알킬기이고, R1∼R6 은 각각 독립적으로, 수소, 탄소수 1∼5 의 알킬기 혹은 할로겐 원자이다] - 제 1 항에 있어서,
(A) 성분 100 질량부에 대해, (F) 산화 방지제를 0.01∼1.0 질량부 함유하는 것을 특징으로 하는 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항 또는 제 2 항에 있어서,
(C) 성분이 유기 알칼리 금속염 및/또는 유기 알칼리 토금속염인 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항 또는 제 2 항에 있어서,
(D) 성분이 수성 분산형의 폴리테트라플루오로에틸렌인 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항 또는 제 2 항에 있어서,
(D) 성분이 아크릴 피복된 폴리테트라플루오로에틸렌인 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항 또는 제 2 항에 있어서,
(E) 성분이 페닐기, 메톡시기 및 비닐기를 갖는 폴리오르가노실록산인 난연 광확산 폴리카보네이트 수지 조성물. - 삭제
- 제 1 항에 있어서,
(A-1) 성분에 있어서, 상기 일반식 (I) 로 나타내는 분기제의 사용량이 (A-1) 성분의 원료인 2 가 페놀 화합물에 대해 0.01∼3.0 몰% 의 범위인 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항에 있어서,
상기 일반식 (I) 로 나타내는 분기제가 1,1,1-트리스(4-하이드록시페닐)에탄인 난연 광확산 폴리카보네이트 수지 조성물. - 제 9 항에 있어서,
1,1,1-트리스(4-하이드록시페닐)에탄의 사용량이 (A-1) 성분의 원료인 2 가 페놀 화합물에 대해 0.2∼2.0 몰% 의 범위인 난연 광확산 폴리카보네이트 수지 조성물. - 제 10 항에 있어서,
점도 평균 분자량이 17,000 이상 22,000 미만인 난연 광확산 폴리카보네이트 수지 조성물로서, (A-1) 성분에 있어서, 1,1,1-트리스(4-하이드록시페닐)에탄의 사용량이 (A-1) 성분의 원료인 2 가 페놀 화합물에 대해 0.2 몰% 이상 1.0 몰% 미만의 범위이고, (D) 성분의 함유량이 (A) 성분 100 질량부에 대해 0.03∼0.5 질량부인 난연 광확산 폴리카보네이트 수지 조성물. - 제 10 항에 있어서,
점도 평균 분자량이 17,000 이상 22,000 미만인 난연 광확산 폴리카보네이트 수지 조성물로서, (A-1) 성분에 있어서, 1,1,1-트리스(4-하이드록시페닐)에탄의 사용량이 (A-1) 성분의 원료인 2 가 페놀 화합물에 대해 1.0 몰% 이상 1.5 몰% 미만의 범위이고, (D) 성분의 함유량이 (A) 성분 100 질량부에 대해 0.01∼0.5 질량부인 난연 광확산 폴리카보네이트 수지 조성물. - 제 9 항에 있어서,
(A-1) 성분에 있어서, 1,1,1-트리스(4-하이드록시페닐)에탄의 사용량이 (A-1) 성분의 원료인 2 가 페놀 화합물에 대해 1.5 몰% 이상이고, (D) 성분의 함유량이 0 질량부인 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항 또는 제 2 항에 있어서,
점도 평균 분자량이 22,000 이상인 난연 광확산 폴리카보네이트 수지 조성물. - 제 14 항에 있어서,
(B) 성분이 Si 계 광확산제인 난연 광확산 폴리카보네이트 수지 조성물. - 제 1 항 또는 제 2 항에 기재된 난연 광확산 폴리카보네이트 수지 조성물을 성형 가공하여 얻어지는 폴리카보네이트 수지 성형체.
- 제 16 항에 있어서,
성형체가 조명 기구용 커버인 폴리카보네이트 수지 성형체. - 제 16 항에 있어서,
성형체가 표시 기구용 확산 커버인 폴리카보네이트 수지 성형체. - 제 16 항에 있어서,
성형체가 액정 디스플레이용 확산판인 폴리카보네이트 수지 성형체.
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JP2009108281A (ja) | 2007-11-01 | 2009-05-21 | Teijin Chem Ltd | 難燃光拡散性ポリカーボネート樹脂組成物 |
JP2009143995A (ja) | 2007-12-12 | 2009-07-02 | Idemitsu Kosan Co Ltd | ポリカーボネート樹脂組成物、ポリカーボネート樹脂成形品及びその製造方法 |
JP2010065164A (ja) * | 2008-09-11 | 2010-03-25 | Mitsubishi Engineering Plastics Corp | 芳香族ポリカーボネート樹脂組成物並びにそれらからなる成形体及び照明用部材 |
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JP6072841B2 (ja) | 2017-02-01 |
US10059840B2 (en) | 2018-08-28 |
CN105623231B (zh) | 2018-09-14 |
EP3336145B1 (en) | 2023-11-01 |
EP2578636B1 (en) | 2018-02-28 |
JPWO2011149030A1 (ja) | 2013-07-25 |
CN102906195A (zh) | 2013-01-30 |
CN105623231A (zh) | 2016-06-01 |
JP2017088892A (ja) | 2017-05-25 |
JP6259065B2 (ja) | 2018-01-10 |
CN102906195B (zh) | 2016-01-27 |
TWI592444B (zh) | 2017-07-21 |
JP2015108157A (ja) | 2015-06-11 |
WO2011149030A1 (ja) | 2011-12-01 |
TW201207038A (en) | 2012-02-16 |
JP5714576B2 (ja) | 2015-05-07 |
EP3336145A1 (en) | 2018-06-20 |
US9664818B2 (en) | 2017-05-30 |
US20190185663A1 (en) | 2019-06-20 |
TW201612238A (en) | 2016-04-01 |
EP2578636A4 (en) | 2014-11-12 |
US20130066002A1 (en) | 2013-03-14 |
KR20130081656A (ko) | 2013-07-17 |
US20170233570A1 (en) | 2017-08-17 |
US10995213B2 (en) | 2021-05-04 |
EP2578636A1 (en) | 2013-04-10 |
EP2578636B2 (en) | 2022-06-22 |
TWI521015B (zh) | 2016-02-11 |
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