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KR101732718B1 - Agents for Asphalt mixture and thereof manufacturing method and Asphalt mixture using the Agents and thereof manufacturing method - Google Patents

Agents for Asphalt mixture and thereof manufacturing method and Asphalt mixture using the Agents and thereof manufacturing method Download PDF

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Publication number
KR101732718B1
KR101732718B1 KR1020160001763A KR20160001763A KR101732718B1 KR 101732718 B1 KR101732718 B1 KR 101732718B1 KR 1020160001763 A KR1020160001763 A KR 1020160001763A KR 20160001763 A KR20160001763 A KR 20160001763A KR 101732718 B1 KR101732718 B1 KR 101732718B1
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weight
parts
asphalt
additive
rosin
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KR1020160001763A
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Korean (ko)
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황익현
황주철
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황익현
황주철
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/24Macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/08Fats; Fatty oils; Ester type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/24Macromolecular compounds
    • C04B24/26Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L95/00Compositions of bituminous materials, e.g. asphalt, tar, pitch

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  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Civil Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Road Paving Structures (AREA)

Abstract

Introduced are an asphalt additive, a method for producing the asphalt additive, an asphalt mixture using the same, and a method for producing the asphalt mixture. The method for producing the asphalt additive of the present invention comprises the steps of: producing a basic additive by heating, mixing, and dissolving 50-150 parts by weight of any one material selected from blown asphalt and gilsonite at 220-300C with 100 parts by weight of any one material selected from PET or PBT, by reducing a temperature to 200C or less, and by mixing 10-100 parts by weight of process oil and 10-100 parts by weight of rosin; heating 300-1000 parts by weight of rubber powder pulverized to 0.074-2 mm at 120-180C with respect to 100 parts by weight of any one material selected from the PET or the PBT; feeding and coating the heated rubber powder into the dissolved-state basic additive; mixing 10-100 parts by weight of any one or more warm mix materials selected from PE wax, Sasobit wax, and rosin; further adding 100-1000 parts by weight of process oil which is a softening agent; and further adding 20-200 parts by weight of any one selected from PE wax, Sasobit wax, and rosin.

Description

TECHNICAL FIELD The present invention relates to an asphalt additive, an asphalt mixture, and an asphalt mixture using the asphalt mixture,

The present invention relates to an asphalt additive added to an asphalt mixture for the purpose of improving the quality of the asphalt mixture, a method for producing the asphalt additive, and an asphalt mixture using the asphalt mixture and a method for producing the same. More particularly, Asphalt admixture which can be used at a temperature of 120 to 180 DEG C as a mixture of medium temperature, high temperature, new material and regenerated asphalt, a method for producing the same, as well as a method for producing the same.

In general, the asphalt modifying additive is divided into rubber series, plastic series, synthetic series, artificial series, Oxident series, hydrocarbon series, peeling reduction series, and middle temperature additive series.

As the rubber series, natural rubber, styrene butadiene rubber (SBR), styrene-butadiene-styrene (SBS) and crumb rubber modifier (CRM) are used. In the plastic series, polyethylene (PE), polypropylene Ethylene-Vinyl Acetate), and PVC (Poly-Vinyl-Chloride).

As synthetic products, rubber-based and plastic synthetic products exist. As natural fibers, asbestos exists as natural products. Polypropylene fiber, polyethylene fiber, glass fiber and PET fiber exist as artificial products. Oxident series Cam crete and Manganese slats are used for

As hydrocarbon series, ginsonite is used as natural asphalt. Amimen and limestone (Lime) are available as a peeling-reduction series. As a warming additive, PE WAX, SASOBIT WAX, rosin, and process oil and palm oil are mixed with each other. In order to improve the quality, SBS and PE are generally used.

On the other hand, the chemical foaming agent is used to improve the flexibility by generating fine bubbles. It contains the crystallized Hatrium Aluminum Silicate component which causes the hydration reaction. It penetrates about 20% of water and decomposes at 85 ~ 180 ℃ As a result, it is possible to improve the workability of the asphalt mixture and the aggregate coverage of the asphalt mixture even at a low temperature by inducing the foaming action on the asphalt by expanding the asphalt area.

That is, the asphalt modifying additive is used for the purpose of improving the quality of the asphalt and improving the workability. Especially, the moderate temperature additive improves the workability of the asphalt and improves the coverage of the aggregate at the middle temperature of 120 to 140 ° C.

On the other hand, PET (Polyethylene Phthalate) and PBT (Poly-Butylene-Terephthanate) have an advantage of excellent rigidity and heat resistance. Further, it has an advantage that it has a high melting point, a low water absorption rate and a low coefficient of linear expansion, and therefore is excellent in stability, excellent in impact resistance, and excellent in electrical properties and weather resistance.

However, there is a disadvantage that PET and PBT have a melting point of 220 ° C or higher and are difficult to use for an asphalt mixture below 180 ° C.

Therefore, in order to use PET for asphalt, PET has been used as a fiber additive or is melted, mixed, pulverized or extruded with an additive having a low melting point. Nevertheless, when melted and mixed with an asphalt mixture, As a result, the improvement of the quality of the asphalt mixture was not helped, and there was a limitation in using PET as an additive.

The inventor of the present invention came to the present invention after study for using PET and PBT having the above limitations as an additive for asphalt despite the excellent properties.

KR 10-1029912 (2011.04.11)

The present invention relates to an asphalt additive which can be used at a middle temperature by adding a material such as bronze asphalt or natural asphalt which is not ignited at 300 ° C or higher to PET and PBT so that it can be used in a high temperature asphalt mixture, A method of manufacturing the same, and an asphalt mixture using the same and a method of manufacturing the same.

In order to attain the above object, the present invention provides a method for manufacturing an asphalt additive, wherein 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is added to 100 parts by weight of PET or PBT at a temperature of 220 to 300 캜 Heating, mixing, melting, lowering the temperature to 200 ° C or less, mixing 10-100 parts by weight of the process oil and 10-100 parts by weight of rosin to prepare a base additive; Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C; Applying the heated rubber powder to the base additive in a molten state to coat the same; PE WAX, SASOBIT WAX, and rosin in an amount of 10 to 100 parts by weight; Adding 100 to 1000 parts by weight of a process oil as a softening agent; And PE WAX, SASOBIT WAX, and rosin, and further adding 20 to 200 parts by weight of the rosin.

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In order to attain the above object, the present invention provides a method for manufacturing an asphalt additive, wherein 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is added to 100 parts by weight of PET or PBT at a temperature of 220 to 300 캜 Heating, mixing and melting the mixture, lowering the temperature to 200 ° C or lower, mixing 10-100 parts by weight of the process oil and 10-100 parts by weight of the rosin to prepare a base additive; PE WAX, SASOBIT WAX, and rosin; Adding 30 to 200 parts by weight of a process oil; And further adding at least one material selected from SBS, LDPE and HDPE.

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The asphalt additive of the present invention is characterized by being produced by the above-mentioned production method.

In order to attain the above object, the present invention provides a method for producing an asphalt mixture using asphalt additive, wherein 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is added to 100 parts by weight of PET or PBT, To 300 ° C, melting the mixture, lowering the temperature to 200 ° C or lower, mixing 10-100 parts by weight of the process oil and 10-100 parts by weight of the rosin to prepare a base additive; Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C; And applying the heated rubber powder to the base additive in a molten state to coat the base additive; And mixing the base additive coated with the rubber powder into a mixture of aggregate, asphalt and filler.

In order to attain the above object, the present invention provides a method for producing an asphalt mixture using asphalt additive, wherein 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is added to 100 parts by weight of PET or PBT, To 300 ° C, melting the mixture, lowering the temperature to 200 ° C or lower, mixing 10-100 parts by weight of the process oil and 10-100 parts by weight of the rosin to prepare a base additive; Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C; Applying the heated rubber powder to the base additive in a molten state to coat the same; PE WAX, SASOBIT WAX, and rosin in an amount of 50 to 300 parts by weight; And mixing the mixture of the aggregate, the asphalt and the filler with the base additive coated with the rubber powder and the warming agent.

In order to attain the above object, the present invention provides a method for producing an asphalt mixture using asphalt additive, wherein 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is added to 100 parts by weight of PET or PBT, To 300 ° C, melting the mixture, lowering the temperature to 200 ° C or lower, mixing 10-100 parts by weight of the process oil and 10-100 parts by weight of the rosin to prepare a base additive; Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180; And applying the heated rubber powder to the base additive in a molten state to coat the base additive; Adding 100 to 1000 parts by weight of a process oil as a softening agent; PE WAX, SASOBIT WAX, and rosin, and further adding 20 to 200 parts by weight; And mixing the mixture of the aggregate, the asphalt and the filler with the base additive coated with the rubber powder and the warming agent.

In order to attain the above object, the present invention provides a method for producing an asphalt mixture using asphalt additive, wherein 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is added to 100 parts by weight of PET or PBT, To 300 ° C, melting the mixture, lowering the temperature to 200 ° C or lower, mixing 10-100 parts by weight of the process oil, and 10-100 parts by weight of the rosin to prepare a base additive; PE WAX, SASOBIT WAX, and rosin; And 30 to 200 parts by weight of a process oil; And mixing the mixture of the base additive, the warming agent and the process oil with a mixture of the aggregate and the asphalt and the filler.

The asphalt mixture using the asphalt additive of the present invention for achieving this object is characterized in that it is manufactured by the above-mentioned production method.

The features and advantages of the present invention will become more apparent from the following detailed description based on the accompanying drawings.

Prior to this, terms and words used in the present specification and claims should not be construed in a conventional and dictionary sense, and the inventor may appropriately define the concept of a term in order to best describe its invention The present invention should be construed in accordance with the spirit and scope of the present invention.

According to the present invention, the following various effects are realized.

First, since PET and PBT are used for the asphalt mixture, the stiffness and heat resistance of the asphalt mixture are improved.

Second, as the melting point increases, the plastic deformation resistance is excellent, and as the linear expansion coefficient decreases, the impact resistance and weather resistance are improved.

Third, PET and PBT can be used for various applications such as high temperature, medium temperature, new material, and recycled asphalt mixture.

Fourth, since recycled PET and PBT are used, there is an advantage that waste materials can be recycled.

BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a schematic view of a method for producing an asphalt additive and an asphalt additive according to the present invention,
Fig. 2 is a view showing an application range of the asphalt additive.

The objects, particular advantages and novel features of the present invention will become more apparent from the following detailed description and examples taken in conjunction with the accompanying drawings. It should be noted that, in the present specification, the reference numerals are added to the constituent elements of the drawings, and the same constituent elements are assigned the same number as much as possible even if they are displayed on different drawings. Also, the terms first, second, etc. may be used to describe various components, but the components should not be limited by the terms. The terms are used only for the purpose of distinguishing one component from another. In the following description, well-known functions or constructions are not described in detail since they would obscure the invention in unnecessary detail.

Hereinafter, the asphalt additive of the present invention, the method for producing the same, and the asphalt mixture and the method for producing the same will be described with reference to the accompanying drawings.

As shown in FIGS. 1 and 2, the mesophilic asphalt additive of the present invention is applied to a medium temperature asphalt mixture of 120 to 140, and can be applied to mesophilic, mesophilic modified, mesophilic, low-noise asphalt mixture and regenerated asphalt mixture.

The mesophilic asphalt additive of the present invention is produced by heating and mixing 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilnonite to 220 to 300 ° C in 100 parts by weight of any one material selected from PET or PBT to prepare a base additive .

Asphalt additives for medium temperature are mainly composed of PET and PBT. They are melted at 100 ℃ and can not be ignited even at 300 ℃ so that they can be melted and used. Bron asphalt or natural asphalt ginsonite do.

PET and PBT are excellent in rigidity, heat resistance, and high melting temperature, and are excellent in resistance to plastic deformation after asphalt pavement and low in absorption coefficient and linear expansion coefficient, thereby improving the stability of the mixture.

In addition, the above-mentioned characteristics improve the weather resistance and impact resistance of the mixture, thereby enabling production of a mixture of excellent quality.

PET and PBT are melted at a high temperature. Therefore, in order to use the PET and PBT stably, bronze asphalt having high asphalt content or ginsonite as natural asphalt is used among asphalt having high ignition point.

When oil is mixed, there is a risk of fire due to a low ignition point, so there is a limit to use.

Therefore, it is very important to first melt any one of the materials of PET and PBT and the material of bronze asphalt and gilsonite, and then mix it with other additives.

As described above, the content of bronze asphalt and gilsonite is controlled within the range of 50 to 150 parts by weight. When the content is less than 50 parts by weight, the flowability is decreased. When the content is more than 150 parts by weight, It is difficult to maintain the target quality because the use amount of PET and PBT decreases.

As described above, although the melting temperature is lowered by mixing at the above mixing ratio, it is preferable to add process oil and rosin (rosin) because the viscosity is high and it is difficult to handle. .

The process oil serves to increase the viscosity. When the addition amount is less than 10 parts by weight, the viscosity change is not affected. When the amount is more than 100 parts by weight, the quality of the asphalt mixture can not be stabilized .

When rosin is used in an amount of less than 10 parts by weight, it is difficult to expect an effect of use. When the amount of rosin is more than 100 parts by weight, it becomes brittle due to high stiffness. Therefore, Should be used.

Hereinafter, the plant type and the melting type in the new asphalt mixture will be described first, and the plant type and the melting type in the reclaimed asphalt mixture will be described later.

For the plant input type, the high-temperature additive used in the new asphalt mixture is applied only to the modified asphalt mixture having a PG grade of 70-22, 76-22, 82-22, since the PG grade of the asphalt itself is 64-22 .

The high temperature additive used in this new asphalt mixture is prepared by mixing crushed waste tire (CRM), which can act as a modifier, with 100 parts by weight of the base additive.

Since the crushed waste tire has a critical temperature of 250 DEG C or higher, there is an advantage that it can be stably coated by heating. The pulverized waste tire is used within a particle size range of 0.074 to 2 mm, and is used by heating within a range of about 120 to 180 ° C.

The amount of the ground additive to be coated is 100 parts by weight of the base additive, and 300 to 1000 parts by weight of the pulverized waste tire powder is heated.

When the amount of the heated pulverized waste tire powder is less than 300 parts by weight, the amount of the base additive to be used is excessively large, so that the pulverized waste tire powder particles adhere to each other, resulting in a decrease in productivity. If the heated pulverized waste tire powder exceeds 1000 parts by weight, The use amount of the base additive is low, which makes the use inconvenient.

In the plant type, the moderate temperature additives used in the new asphalt mixture are applied to PG grades 64-22, 70-22, 76-22, 82-22. In the high temperature additive used for the new asphalt mixture described above, .

The warming agent may be selected from PE WAX, SASOBIT WAX and rosin, and the amount thereof is adjusted within the range of 10 to 100 parts by weight.

When the thermosetting agent is added in an amount of less than 10 parts by weight, the effect of thermosetting is deteriorated. When the thermosetting agent is added in an amount exceeding 100 parts by weight, the amount of the base additive is decreased.

If the melt type is used (the melt type is applied only to the PG grade 64-22), one or more of PE WAX, SASOBIT WAX, and rosin, which are the thickening agents, may be selected without using pulverized waste tire as a base additive 10 to 100 parts by weight, and 30 to 200 parts by weight of process oil are added to the mixture.

When the process oil is added in an amount of less than 30 parts by weight, workability is deteriorated. When it exceeds 200 parts by weight, PG grade 64-22 can not be satisfied.

The additive used in regenerated asphalt can be used for 120 to 180 ° C asphalt mixture for both high temperature and medium temperature, and can be used in both plant type and melting type. PG grades 64-22, 70-22, 76-22 .

The additives used for the regenerated asphalt (high temperature and medium temperature) are prepared by adding 100 to 1000 parts by weight of process oil, which is a softener, to the additive used in the above-mentioned new asphalt mixture.

When the process oil is used in an amount of less than 100 parts by weight, the recycled aggregate can not be softened. When the process oil is used in an amount exceeding 1000 parts by weight, the PG grade 64 is not satisfied, thereby causing plastic deformation during asphalt pavement.

As the adhesive, any one of PE WAX, SASOBIT WAX and rosin is selected and used while controlling the amount of the adhesive in the range of 10 to 100 parts by weight. If the amount of the pressure-sensitive adhesive is less than 10 parts by weight, the effect of using the pressure-sensitive adhesive is hardly expected. If the amount is more than 100 parts by weight, the rigidity is excessively increased and the effect of the process oil is deteriorated.

On the other hand, SBS, LDPE, HDPE, etc. can be added for the workability and the PG grade control, without discriminating between the new asphalt, regenerated asphalt, high temperature and low temperature.

The asphalt mixture using the asphalt additive of the present invention and the method for producing the same are manufactured by mixing predetermined aggregate, filler and asphalt on the basis of the above-described asphalt additive and the production method thereof. The description of Examples 1 to 4 will be omitted.

Modified asphalt admixture of PG grade 76-22 and asphalt mixture of 140 ~ 180 ℃ is prepared as the KS standard grade WC-6 for the new asphalt mixture and the plant type.

1. Manufacture of asphalt reforming additive

(1) 100 kg of recycled PET and 120 kg of bronze asphalt are melted by heating at 250 캜, cooled to 190 캜, and then 30 kg of paraffin oil having a flash point of 230 캜 as a process oil and 30 kg of rosin are mixed as a base additive.

② Heat 1000 kg of pulverized tires 0.074 ~ 1.5mm to 150 ℃, mix 300kg of base additive, and transfer to a cooling mixer to prevent the particles from sticking together by lowering the temperature.

③ Newton asphalt modifier is 5.5kg per 1ton of ascon, so when packing, pack it at 5.5kg.

※ PG rating test

division
Modified asphalt Test result
Asphalt (AP-5) Base additive system PG rating Formulation (kg) 55
(AP content 5.5%)
5.5 60.5 76-22

The rubber powder is medium and the additive is 5.5 kg per 1 ton of the asconone. Therefore, excluding the crushed rubber, (140/300) * 100 = 47% becomes 5.5 kg * 47% = 2.59. The AP content of 1 ton of ascorbic acid is 55 kg. If it is reduced to 1/10, the amount of additive becomes 0.26, and the amount of the AP is determined.

2. Plant mixture

① Particle size of aggregate

Size of sieve
Type of mixture
WC-6




Percent of Pass Weight (%)
25mm
20mm
13mm
10mm
5mm
2.5 mm
0.6mm
0.3mm
0.15mm
0.08mm
-
100
90-100
73-90
40-60
25-40
11-22
7-16
4-12
3-9

② Filler: CaCO 3

③ Asphalt: AP-5

④ Modification additive: PET + Bron asphalt + rubber powder

⑤Barning table

Name of material aggregate Filler AP-5
Reforming additive
system
Size: WC-6 CaCO 3 Material weight (kg) 899.5 40.0 55.0 5.5 1000

3. Test results

Exam name Compaction temperature (℃) Stability
(N)
Flow value
(1/100 cm)
Porosity
(%)
Saturation
(%)
Indirect tensile strength
(N / mm < 2 &
Seal
Intensity ratio
(TSR)
dynamic
Intensity ratio
(Times / mm)
Test result 150 12750 28 3.3 82 0.8 0.91 8920 standard 145-160 5000 or more 20-40 3-5 70-85 0.75 or more 0.75 or more 3000 or more

The new asphalt concrete is a melting type KS-based grade WC-1, which produces an intermediate additive for asphalt of medium grade PG grade 64-22 and a medium temperature asphalt mixture of 120 ~ 140 ℃.

1. Manufacture of asphalt additives

 (1) 100 kg of recycled PET and 130 kg of Gilsonite are heated and melted at 250 캜 to lower the temperature to 180 캜. 30 kg of napatta type process oil and 30 kg of rosin are mixed to prepare a base additive.

② Add 20kg of process oil and 70kg of rosin to 100kg of base additive and melt.

※ PG rating test

division
Middle temperature asphalt additive Test result
Asphalt (AP-5) Melting type system PG rating Formulation (kg) 55
(AP content 5.5%)
1.2 56.2 64-22

2. Asphalt mixture

① Particle size of aggregate

Size of sieve
Type of mixture
WC-1



Percent of Pass Weight (%)
25mm
20mm
13mm
10mm
5mm
2.5 mm
0.6mm
0.3mm
0.15mm
0.08mm
-
100
90-100
76-90
44-74
28-58
11-32
5-21
3-15
2 to 10

② Filler: CaCO 3

③ Asphalt: AP-5

④ Modification Additive: PET + Gilsonite + Process Oil + Rosin

⑤Barning table

Name of material
aggregate Filler AP-5
Reforming additive
system
Size: WC-1 CaCO 3 Material weight (kg) 903.8 40.0 55.0 1.2 1000

 Mixing temperature: 130 캜, compaction temperature: 115 캜

3. Test results

Exam name promise
Temperature
(° C)
Stability
(N)
Flow value
(1/100 cm)
Porosity
(%)
Saturation
(%)
Indirect tensile strength
(N / mm < 2 &
Seal
Intensity ratio
(TSR)
dynamic
Intensity ratio
(Times / mm)
Test result 120 1072 36 4.5 72 0.8 0.8 2012 standard 120-140 500 or more 20-40 3-6 65-80 0.75 or more 0.75 or more 1000 or more

The recycled asphalt is a high temperature mixture of 140-180 ° C., and the PG grade of the asphalt binder mixed with the AP and the new AP additive material extracted from the recycled aggregate of 50% of the high temperature recycled mixture is 64-22 , And plant input method.

1. Preparation of asphalt regeneration additive

(1) 100 kg of recycled PET and 130 kg of bronze asphalt are mixed at 250 캜, melted and lowered to 200 캜, 50 kg of process oil and 50 kg of rosin are mixed to be used as a base additive.

(2) 100 kg of pulverized waste tire rubber of 0.6 to 1.2 mm is heated to 150 캜, 20 kg of the base additive is melted and mixed while cooling, and the temperature is brought to room temperature. In this process, 100 kg of process oil and 20 kg of pine .

③ Package 2.5kg of above materials to use 2.5kg per 1ton asphalt mixture.

※ PG rating test

division
Middle temperature asphalt additive Test result
Regenerated asphalt 50% + new asphalt (AP-5) 50% additive system PG rating Binder Formulation 55
(AP content 5.5%)
2.5 57.5 64-22

2. Asphalt mixture

① Particle size of aggregate

Size of sieve
Type of mixture
WC-1




Percent of Pass Weight (%)
25mm
20mm
13mm
10mm
5mm
2.5 mm
0.6mm
0.3mm
0.15mm
0.08mm
-
100
90-100
76-90
44-74
28-58
11-32
5-21
3-15
2 to 10

② Filler: CaCO 3

③ Asphalt: AP-5

④ Regeneration additive: (PET + Bron asphalt + process oil + rosin: melted) + rubber powder + process oil + rosin

⑤Barning table

Name of material
The new asphalt mixture (WC-1) Recycled aggregate
Regenerated Additives
system
New aggregate AP-5 CaCO 3 system Material amount
(kg)
441.5 36.0 20.0 497.5 500.0 2.5 1000

Mixing temperature: 130 캜, compaction temperature: 115 캜

3. Test results

Exam name
Stability
(N)
Flow value
(1/100 cm)
Porosity
(%)
Saturation
(%)
Indirect tensile strength
(N / mm < 2 &
Tensile strength ratio
(TSR)
dynamic
Stability
(Times / mm)
Test result 11000 32 4.0 76 0.79 0.80 2125 times standard 5000 or more 20-40 3-6 65-80 0.75 or more 0.75 or more 1000 or more

The medium temperature mixture of regenerated asphalt 120 ~ 140 is set to WC-1 according to KS standard, 50% of recycled aggregate is used, and the additive is melted type and applied to PG grade 64-22.

1. Asphalt Middle temperature  Preparation of recycling additive

(1) 100 kg of recycled PET and 100 kg of bronze asphalt are mixed and melted at 250 캜, lowered to 200 캜, and 50 kg of aromatic type process oil and 50 kg of rosin are mixed to prepare a base additive.

② Add 300kg of process oil (aroma type) and 10kg of SBS to the base additive and melt and heat mix.

※ PG rating test

division
Medium temperature asphalt Test result
AP-5 Regenerated asphalt Warm additive system PG rating Binder Formulation
(kg)
2.75 2.75 0.26 5.76 64-22

2. Asphalt mixture

① Particle size of aggregate

Size of sieve
Type of mixture
WC-1



Percent of Pass Weight (%)
25mm
20mm
13mm
10mm
5mm
2.5 mm
0.6mm
0.3mm
0.15mm
0.08mm
-
100
90-100
76-90
44-74
28-58
11-32
5-21
3-15
2 to 10

② Filler: CaCO 3

③ Asphalt: AP-5

④ Regeneration additive: (PET + Bron asphalt: melted) + process oil + rosin

⑤Barning table

Name of material
The new asphalt mixture (WC-1) Recycled aggregate
Regenerated Additives
system
New aggregate AP-5 CaCO 3 system Material amount 441.4 36.0 20.0 497.4 500.0 2.6 1000

Mixing temperature: 130 캜, compaction temperature: 115 캜

3. Test results

Exam name Stability
(N)
Flow value
(1/100 cm)
Porosity
(%)
Saturation
(%)
Indirect tensile strength
(N / mm < 2 &
Tensile strength ratio
(TSR)
Dynamic stability
(Times / mm)
Test result 13240 25.5 3.7 70.4 1.20 0.91 3012 standard 5000 or more 20-40 3-6 65-88 0.75 or more 0.75 or more 1000 or more

Although the present invention has been described in detail with reference to specific examples thereof, it is to be understood that the present invention is not limited to the asphalt additive, the method for producing the same, and the asphalt mixture and the method for producing the same, It will be apparent to those skilled in the art that variations and modifications may be made without departing from the scope of the present invention.

It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.

Claims (11)

50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is heated to 220 to 300 占 폚 and mixed with 100 parts by weight of any one material selected from PET and PBT, 10 to 100 parts by weight of process oil and 10 to 100 parts by weight of rosin to prepare a base additive;
Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C;
Applying the heated rubber powder to the base additive in a molten state to coat the same;
PE WAX, SASOBIT WAX, and rosin in an amount of 10 to 100 parts by weight;
Adding 100 to 1000 parts by weight of a process oil as a softening agent; And
PE WAX, SASOBIT WAX, and rosin, and further adding 20 to 200 parts by weight of the rosin.
delete delete 50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is heated to 220 to 300 占 폚 and mixed with 100 parts by weight of any one material selected from PET and PBT, 10 to 100 parts by weight of process oil and 10 to 100 parts by weight of rosin to prepare a base additive;
PE WAX, SASOBIT WAX, and rosin;
Adding 30 to 200 parts by weight of a process oil; And
SBS, LDPE, and HDPE is further added to the asphalt additive.
delete An asphalt additive prepared by the method of claim 1 or claim 4.
50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is heated to 220 to 300 占 폚 and mixed with 100 parts by weight of any one material selected from PET and PBT, 10 to 100 parts by weight of process oil and 10 to 100 parts by weight of rosin to prepare a base additive;
Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C; And
Applying the heated rubber powder to the base additive in a molten state to coat the same;
And mixing the base additive coated with the rubber powder into a mixture of an aggregate and an asphalt and a filler.
50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is heated to 220 to 300 占 폚 and mixed with 100 parts by weight of any one material selected from PET and PBT, 10 to 100 parts by weight of process oil and 10 to 100 parts by weight of rosin to prepare a base additive;
Heating the rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C;
Applying the heated rubber powder to the base additive in a molten state to coat the same;
PE WAX, SASOBIT WAX, and rosin in an amount of 50 to 300 parts by weight; And
A method for manufacturing an asphalt mixture using an asphalt additive, which comprises mixing a mixture of an aggregate, an asphalt and a filler with the base additive coated with a rubber powder and the medium temperature fire.
50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is heated to 220 to 300 占 폚 and mixed with 100 parts by weight of any one material selected from PET and PBT, 10 to 100 parts by weight of process oil and 10 to 100 parts by weight of rosin to prepare a base additive;
Heating rubber powder pulverized to 0.074 to 2 mm in an amount of 300 to 1000 parts by weight based on 100 parts by weight of any one material selected from the group consisting of PET and PBT to 120 to 180 ° C; And
Applying the heated rubber powder to the base additive in a molten state to coat the same;
Adding 100 to 1000 parts by weight of a process oil as a softening agent;
PE WAX, SASOBIT WAX, and rosin, and further adding 20 to 200 parts by weight; And
A method for manufacturing an asphalt mixture using an asphalt additive, which comprises mixing a mixture of an aggregate, an asphalt and a filler with the base additive coated with a rubber powder and the medium temperature fire.
50 to 150 parts by weight of any one material selected from among bronze asphalt and gilsonite is heated to 220 to 300 占 폚 and mixed with 100 parts by weight of any one material selected from PET and PBT, 10 to 100 parts by weight of process oil and 10 to 100 parts by weight of rosin to prepare a base additive;
PE WAX, SASOBIT WAX, and rosin; And
Adding 30 to 200 parts by weight of a process oil; And
And mixing the base additive, the warming agent, and the process oil with a mixture of an aggregate and an asphalt and a filler to prepare an asphalt mixture.
An asphalt mixture produced by the method of any one of claims 7 to 10.
KR1020160001763A 2016-01-06 2016-01-06 Agents for Asphalt mixture and thereof manufacturing method and Asphalt mixture using the Agents and thereof manufacturing method KR101732718B1 (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109665760A (en) * 2018-12-28 2019-04-23 陈永刚 A kind of maintenance of highway pavement material and maintenance of highway pavement method
KR20200095620A (en) * 2019-01-31 2020-08-11 황익현 Base for asphalt agent and thereof manufacturing method and, asphalt agent for low and high temperature asphalt mixture and thereof manufacturing method and, asphalt mixture and thereof manufacturing method using the same
CN114057427A (en) * 2021-11-27 2022-02-18 宁夏泰达路业工程有限公司 High-modulus asphalt concrete and asphalt concrete mold-increasing agent
KR102659645B1 (en) 2023-09-11 2024-04-23 (주)윤성산업개발 Carbon reduced low temperature asphalt additives composition and asphalt mixture using low temperature asphalt additives

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100974858B1 (en) 2009-07-03 2010-08-10 황익현 Additive to be applied in hot liquid phase for reforming asphalt concrete and asphalt concrete using the additive
KR101029912B1 (en) * 2010-03-16 2011-04-18 황익현 Modifier for manufacturing low or mid temperatured asphalt concrete and asphalt concrete with low carbon dioxide emission using the modifier

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100974858B1 (en) 2009-07-03 2010-08-10 황익현 Additive to be applied in hot liquid phase for reforming asphalt concrete and asphalt concrete using the additive
KR101029912B1 (en) * 2010-03-16 2011-04-18 황익현 Modifier for manufacturing low or mid temperatured asphalt concrete and asphalt concrete with low carbon dioxide emission using the modifier

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109665760A (en) * 2018-12-28 2019-04-23 陈永刚 A kind of maintenance of highway pavement material and maintenance of highway pavement method
KR20200095620A (en) * 2019-01-31 2020-08-11 황익현 Base for asphalt agent and thereof manufacturing method and, asphalt agent for low and high temperature asphalt mixture and thereof manufacturing method and, asphalt mixture and thereof manufacturing method using the same
KR102222350B1 (en) 2019-01-31 2021-03-03 황익현 Base for asphalt agent and thereof manufacturing method and, asphalt agent for low and high temperature asphalt mixture and thereof manufacturing method and, asphalt mixture and thereof manufacturing method using the same
CN114057427A (en) * 2021-11-27 2022-02-18 宁夏泰达路业工程有限公司 High-modulus asphalt concrete and asphalt concrete mold-increasing agent
KR102659645B1 (en) 2023-09-11 2024-04-23 (주)윤성산업개발 Carbon reduced low temperature asphalt additives composition and asphalt mixture using low temperature asphalt additives

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