JPS5770845A - Preparation of methacrylic acid dimenthylaminomethyl ester - Google Patents
Preparation of methacrylic acid dimenthylaminomethyl esterInfo
- Publication number
- JPS5770845A JPS5770845A JP55145720A JP14572080A JPS5770845A JP S5770845 A JPS5770845 A JP S5770845A JP 55145720 A JP55145720 A JP 55145720A JP 14572080 A JP14572080 A JP 14572080A JP S5770845 A JPS5770845 A JP S5770845A
- Authority
- JP
- Japan
- Prior art keywords
- carbonate
- ester
- compound shown
- catalyst
- raw material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PURPOSE: To obtain the titled compound useful as a raw material for a flocculating agent in high purity in high yield inexpensively, by subjecting methyl methacrylate to ester exchange with dimethylaminoethanol using a carbonate of a specific alkali metal as a catalyst.
CONSTITUTION: In the presence of a catalyst for ester exchange selected from the group consisting of potassium carbonate, cesium carbonate, and rubidium carbonate, a compound shown by the formulaIis reacted with a compound shown by the formula II, to give the desired compound shown by the formula III. The reactions is preferably carried out under reduced pressure in a range from 200W760Torr at 80W130°C. Methanol prepared as a by-product is removed out of the reaction system. Having sufficiently higher catalytic activity than other catalysts, and low reduction in yield caused by side reactions. The prepared ester is useful as a raw material for a cationic polymer to be used as a flocculating agent, electricallyconductive treatment, and agent for paper making.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55145720A JPS6023101B2 (en) | 1980-10-20 | 1980-10-20 | Method for producing methacrylic acid dimethylaminoethyl ester |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55145720A JPS6023101B2 (en) | 1980-10-20 | 1980-10-20 | Method for producing methacrylic acid dimethylaminoethyl ester |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5770845A true JPS5770845A (en) | 1982-05-01 |
JPS6023101B2 JPS6023101B2 (en) | 1985-06-05 |
Family
ID=15391563
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55145720A Expired JPS6023101B2 (en) | 1980-10-20 | 1980-10-20 | Method for producing methacrylic acid dimethylaminoethyl ester |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6023101B2 (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62175448A (en) * | 1986-01-28 | 1987-08-01 | Mitsui Toatsu Chem Inc | Production of alkylaminoalkyl acrylate or methacrylate |
JPS62242652A (en) * | 1986-04-16 | 1987-10-23 | Mitsui Toatsu Chem Inc | Production of acrylic acid or methacrylic acid alkylaminoalkyl ester |
JP2010529948A (en) * | 2007-02-15 | 2010-09-02 | ビーエーエスエフ ソシエタス・ヨーロピア | Method for producing (meth) acrylic acid ester of N-hydroxyalkylated imidazole |
-
1980
- 1980-10-20 JP JP55145720A patent/JPS6023101B2/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62175448A (en) * | 1986-01-28 | 1987-08-01 | Mitsui Toatsu Chem Inc | Production of alkylaminoalkyl acrylate or methacrylate |
JPS62242652A (en) * | 1986-04-16 | 1987-10-23 | Mitsui Toatsu Chem Inc | Production of acrylic acid or methacrylic acid alkylaminoalkyl ester |
JP2010529948A (en) * | 2007-02-15 | 2010-09-02 | ビーエーエスエフ ソシエタス・ヨーロピア | Method for producing (meth) acrylic acid ester of N-hydroxyalkylated imidazole |
Also Published As
Publication number | Publication date |
---|---|
JPS6023101B2 (en) | 1985-06-05 |
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