JPS5659751A - Preparation of 1-aryl-4-carboxytriethylammonium-5-(3'-methoxy-4'-oxyphenyl)-2-pyrrolidinone - Google Patents
Preparation of 1-aryl-4-carboxytriethylammonium-5-(3'-methoxy-4'-oxyphenyl)-2-pyrrolidinoneInfo
- Publication number
- JPS5659751A JPS5659751A JP13568779A JP13568779A JPS5659751A JP S5659751 A JPS5659751 A JP S5659751A JP 13568779 A JP13568779 A JP 13568779A JP 13568779 A JP13568779 A JP 13568779A JP S5659751 A JPS5659751 A JP S5659751A
- Authority
- JP
- Japan
- Prior art keywords
- triethylamine
- compound shown
- formula
- give
- succinic anhydride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Pyrrole Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
PURPOSE: To obtain the titled substance having improved antibacterial action, stable pharmaceutical effect and prolonged effectiveness, by subjecting triethylamine to addition reaction with the reaction product of 4-oxy-3-methoxybenzylidene-4'- substituted aniline and succinic anhydride.
CONSTITUTION: A compound shown by the formula I (X is H, CH3, or Cl) is reacted with succinic anhydride in dried xylene under reflux at elevated temperature for 40hr to give a compound shown by the formula II. This compound is dissolved in dried THF, and triethylamine is added dropwise little by little for 4hr to the prepared solution under cooling with ice with stirring. After adding dropwise, the solution is allowed to stand for 24hr, and the solvent and the remaining triethylamine are distilled away under reduced pressure at low temperature, to give a compound shown by the formula III.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13568779A JPS6033384B2 (en) | 1979-10-20 | 1979-10-20 | Method for producing 1-aryl-4-carboxytriethylammonium-5-(3'-methoxy-4'-oxyphenyl)-2-pyrrolidinone |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13568779A JPS6033384B2 (en) | 1979-10-20 | 1979-10-20 | Method for producing 1-aryl-4-carboxytriethylammonium-5-(3'-methoxy-4'-oxyphenyl)-2-pyrrolidinone |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5659751A true JPS5659751A (en) | 1981-05-23 |
JPS6033384B2 JPS6033384B2 (en) | 1985-08-02 |
Family
ID=15157559
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP13568779A Expired JPS6033384B2 (en) | 1979-10-20 | 1979-10-20 | Method for producing 1-aryl-4-carboxytriethylammonium-5-(3'-methoxy-4'-oxyphenyl)-2-pyrrolidinone |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6033384B2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4639529A (en) * | 1982-02-19 | 1987-01-27 | The Purdue Frederick Company | Analgesic and anti-inflammatory compounds |
JPS63264458A (en) * | 1986-12-03 | 1988-11-01 | Tanabe Seiyaku Co Ltd | Lactam derivative |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01169291U (en) * | 1988-05-20 | 1989-11-29 |
-
1979
- 1979-10-20 JP JP13568779A patent/JPS6033384B2/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4639529A (en) * | 1982-02-19 | 1987-01-27 | The Purdue Frederick Company | Analgesic and anti-inflammatory compounds |
JPS63264458A (en) * | 1986-12-03 | 1988-11-01 | Tanabe Seiyaku Co Ltd | Lactam derivative |
Also Published As
Publication number | Publication date |
---|---|
JPS6033384B2 (en) | 1985-08-02 |
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