JPH03285654A - Capsule material containing functional substance in high concentration and production thereof - Google Patents
Capsule material containing functional substance in high concentration and production thereofInfo
- Publication number
- JPH03285654A JPH03285654A JP2083769A JP8376990A JPH03285654A JP H03285654 A JPH03285654 A JP H03285654A JP 2083769 A JP2083769 A JP 2083769A JP 8376990 A JP8376990 A JP 8376990A JP H03285654 A JPH03285654 A JP H03285654A
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- aqueous solution
- capsule body
- high concentration
- functional substance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002775 capsule Substances 0.000 title claims abstract description 30
- 239000000126 substance Substances 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 239000000463 material Substances 0.000 title abstract 3
- 239000007788 liquid Substances 0.000 claims abstract description 35
- 239000007864 aqueous solution Substances 0.000 claims abstract description 19
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 18
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 10
- PYMYPHUHKUWMLA-UHFFFAOYSA-N 2,3,4,5-tetrahydroxypentanal Chemical compound OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 10
- 239000000661 sodium alginate Substances 0.000 claims abstract description 10
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 10
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 9
- 239000011575 calcium Substances 0.000 claims abstract description 9
- 239000008157 edible vegetable oil Substances 0.000 claims abstract description 9
- 229910052742 iron Inorganic materials 0.000 claims abstract description 9
- 229960005069 calcium Drugs 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims abstract description 7
- 229940088594 vitamin Drugs 0.000 claims abstract description 6
- 239000011782 vitamin Substances 0.000 claims abstract description 6
- 229930003231 vitamin Natural products 0.000 claims abstract description 6
- 235000013343 vitamin Nutrition 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims abstract description 5
- 229920001542 oligosaccharide Polymers 0.000 claims abstract description 5
- 150000002482 oligosaccharides Chemical class 0.000 claims abstract description 5
- 235000001465 calcium Nutrition 0.000 claims abstract description 3
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 3
- 229960003284 iron Drugs 0.000 claims abstract description 3
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 claims abstract 6
- 229960005135 eicosapentaenoic acid Drugs 0.000 claims abstract 6
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 claims abstract 6
- 235000020673 eicosapentaenoic acid Nutrition 0.000 claims abstract 6
- 150000007524 organic acids Chemical class 0.000 claims abstract 2
- 235000013325 dietary fiber Nutrition 0.000 claims description 10
- 229910021645 metal ion Inorganic materials 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 5
- 239000003349 gelling agent Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 102000011632 Caseins Human genes 0.000 claims 3
- 108010076119 Caseins Proteins 0.000 claims 3
- 108010001441 Phosphopeptides Proteins 0.000 claims 3
- 239000005018 casein Substances 0.000 claims 2
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims 2
- 235000021240 caseins Nutrition 0.000 claims 2
- 239000004615 ingredient Substances 0.000 claims 1
- 239000011162 core material Substances 0.000 abstract description 11
- 239000011248 coating agent Substances 0.000 abstract description 6
- 238000000576 coating method Methods 0.000 abstract description 6
- 239000003921 oil Substances 0.000 abstract description 5
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 abstract description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 abstract description 4
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 239000000174 gluconic acid Substances 0.000 abstract description 2
- 235000012208 gluconic acid Nutrition 0.000 abstract description 2
- 239000004310 lactic acid Substances 0.000 abstract description 2
- 235000014655 lactic acid Nutrition 0.000 abstract description 2
- 150000001455 metallic ions Chemical class 0.000 abstract 2
- 235000008429 bread Nutrition 0.000 abstract 1
- 239000000835 fiber Substances 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 235000013305 food Nutrition 0.000 description 5
- 235000015110 jellies Nutrition 0.000 description 5
- 239000008274 jelly Substances 0.000 description 5
- 108010010803 Gelatin Proteins 0.000 description 4
- 235000013361 beverage Nutrition 0.000 description 4
- 239000008273 gelatin Substances 0.000 description 4
- 229920000159 gelatin Polymers 0.000 description 4
- 235000019322 gelatine Nutrition 0.000 description 4
- 235000011852 gelatine desserts Nutrition 0.000 description 4
- 240000008415 Lactuca sativa Species 0.000 description 2
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 239000004227 calcium gluconate Substances 0.000 description 2
- 229960004494 calcium gluconate Drugs 0.000 description 2
- 235000013927 calcium gluconate Nutrition 0.000 description 2
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 description 2
- 239000001527 calcium lactate Substances 0.000 description 2
- 229960002401 calcium lactate Drugs 0.000 description 2
- 235000011086 calcium lactate Nutrition 0.000 description 2
- NEEHYRZPVYRGPP-UHFFFAOYSA-L calcium;2,3,4,5,6-pentahydroxyhexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(O)C([O-])=O.OCC(O)C(O)C(O)C(O)C([O-])=O NEEHYRZPVYRGPP-UHFFFAOYSA-L 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 235000012045 salad Nutrition 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- 229920002488 Hemicellulose Polymers 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 229920001100 Polydextrose Polymers 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 235000014171 carbonated beverage Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000013256 coordination polymer Substances 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 229940099112 cornstarch Drugs 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- -1 organic acid salts Chemical class 0.000 description 1
- 239000001259 polydextrose Substances 0.000 description 1
- 235000013856 polydextrose Nutrition 0.000 description 1
- 229940035035 polydextrose Drugs 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000009495 sugar coating Methods 0.000 description 1
- 235000010491 tara gum Nutrition 0.000 description 1
- 239000000213 tara gum Substances 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- General Preparation And Processing Of Foods (AREA)
- Jellies, Jams, And Syrups (AREA)
- Formation And Processing Of Food Products (AREA)
Abstract
Description
【発明の詳細な説明】
産呈上Ω刑月脅互
本発明は、機能性物質を高濃度に内包したカプセル体及
びその製造法に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a capsule containing a functional substance at a high concentration and a method for manufacturing the same.
従−米一芸」仔
近年、食物繊維、鉄、カルシうム等の生理上の活性成分
を含む、いわゆる機能性物質の摂取が、特に成人病予防
上重要視されてきており、数種類の機能性を有する物質
を含んだ食品が市販されている。In recent years, the intake of so-called functional substances, including physiologically active ingredients such as dietary fiber, iron, and calcium, has become particularly important for the prevention of adult diseases. There are foods on the market that contain substances with .
このような機能性物質を含有する食品として飲料やゼリ
ー、クツキーなどが提案されている。飲料では水溶性食
物繊維、カルシウム、ビタミン、鉄分を添加した清涼飲
料や炭酸飲料があり、ゼリー状のものとしては１０ザイ
ズのグミキャンデー状のものが販売されている。Beverages, jelly, kutsky, and the like have been proposed as foods containing such functional substances. Beverages include soft drinks and carbonated drinks with added water-soluble dietary fiber, calcium, vitamins, and iron, and jelly-like products are sold in the form of 10-size gummy candies.
しかし、食品や飲料に機能性を有する物質を添加するう
えで次のような問題点がみられる。However, the following problems are encountered when adding functional substances to foods and beverages.
■ 飲料水に機能性物質の含有濃度を高めると味、臭い
、色の面で問題がある。また粘度が上昇し添加しすらい
ため、粘度上昇の少ないポリデキストロースの使用が主
流である。■ Increasing the concentration of functional substances in drinking water causes problems in terms of taste, odor, and color. Furthermore, since the viscosity increases and it is difficult to add it, polydextrose, which has a small increase in viscosity, is mainly used.
■ ゼリー、クツキーにおいても■と同様に味の問題が
あり、高濃度利用は食品として好ましくない。■ Similar to ■, jelly and kutsky also have taste problems, and their use in high concentrations is not desirable as food.
しよ゛と る
本発明は、生理上の活性成分であるとされる食物繊維、
鉄、カルシウム、ＥＰＡ 、ビタミン類、オリゴ糖、ｃ
ｃｐ等を高濃度で芯材として包含し、かつ風味が良好な
カプセル体及びそれを得るための製造法を提供すること
を課題とする。The present invention is based on dietary fiber, which is said to be a physiologically active ingredient.
Iron, calcium, EPA, vitamins, oligosaccharides, c
It is an object of the present invention to provide a capsule body containing CP etc. as a core material at a high concentration and having a good flavor, and a manufacturing method for obtaining the same.
課業し」数粒（り１４９１段
本発明に係るカプセル体は、アルギン酸ナトリウム又は
低メトキシルペクチンの水溶液と２価の金属イオン水溶
液とを接触させて反応させることに形成されるものであ
って、この反応を行うに際し、アルギン酸ナトリウム又
は低メトキシルペクチンの水溶液もしくは２価の金属イ
オン水溶液のいずれかと、食物繊維、鉄、カルシウム等
の成分を含む機能性物質を、食用油中に分散させた油性
液との混合液を芯液として用いてゲル状のカプセルを形
成し、次いで該カプセルを乾燥してハードゼリ一体にし
たことを特徴とする。The capsule body according to the present invention is formed by contacting and reacting an aqueous solution of sodium alginate or low methoxyl pectin with an aqueous solution of divalent metal ions. When carrying out the reaction, either an aqueous solution of sodium alginate or low methoxyl pectin or an aqueous divalent metal ion solution, and a functional substance containing components such as dietary fiber, iron, and calcium are mixed with an oily liquid in which a functional substance containing components such as dietary fiber, iron, and calcium is dispersed in edible oil. A gel-like capsule is formed using the mixed liquid as a core liquid, and then the capsule is dried to form a hard jelly.
上述のように、機能性物質を食用油中に分散させた油性
液を芯液に用いると、該機能性物質を高濃度に分散させ
ても粘度の上昇がみられず、また、この物質特有の味、
臭いがマスキングされるので、従来の食品、飲料におけ
る前述したような問題点がみられなくなる。As mentioned above, when an oily liquid in which a functional substance is dispersed in edible oil is used as the core liquid, no increase in viscosity is observed even when the functional substance is dispersed at a high concentration, and Taste of,
Since odors are masked, the aforementioned problems with conventional foods and beverages are no longer observed.
また、本発明では、形成されたカプセル体をバンコーテ
ィーング装置や流動層乾燥装置などを用いて乾燥させて
その水分含量を低下させるため芯液中の機能性物質を高
濃度でカプセル体に包含させることができる。本発明で
得られる低水分カプセル体の食感もハードゼリータイプ
状であるのでその摂取も手軽にできる。In addition, in the present invention, the formed capsule body is dried using a van coating device, a fluidized bed drying device, etc. to reduce its moisture content, so that the functional substance in the core liquid is included in the capsule body at a high concentration. can be done. The texture of the low-moisture capsule obtained by the present invention is also like that of a hard jelly, so it can be easily ingested.
本発明において芯液として用いるアルギン酸ナトリウム
又は低メトキシルペクチンの水溶液と、機能性物質を食
用油中に分散させた油性液との混合液の混合割合は３：
１〜１９：１位が適当であり、また、２価の金属イオン
水溶液と上記油性液との混合液の混合割合も３：１〜１
９：１が適当である。In the present invention, the mixing ratio of the aqueous solution of sodium alginate or low methoxyl pectin used as the core liquid and the oily liquid in which functional substances are dispersed in edible oil is 3:
A ratio of 1 to 19:1 is appropriate, and a mixing ratio of the divalent metal ion aqueous solution and the above oily liquid is also 3:1 to 1.
9:1 is appropriate.
上記混合液を芯液とするカプセル化に当っての該混合液
を２価の金属イオン水溶液中もしくはアルギン酸ナトリ
ウム又は低メトキシルペクチンの水溶液中への滴下によ
る反応は、公知の手法に従って行うとよく、この場合ゼ
ラチンのようなゲル他剤を用いてもよい。なお、本発明
に用いるゲル化剤は熱可逆的なゼラチン、寒天のほかに
キサンクンガムやタラガムの混合ゲルを用いることがで
きる。特に、ゼラチンを高濃度に添加すると、グミ状の
ハードゼリ一体が得られる。In encapsulation using the above mixed liquid as a core liquid, the reaction by dropping the mixed liquid into an aqueous divalent metal ion solution or an aqueous solution of sodium alginate or low methoxyl pectin may be carried out according to a known method, In this case, a gel or other agent such as gelatin may be used. As the gelling agent used in the present invention, in addition to thermoreversible gelatin and agar, a mixed gel of xanthus gum and tara gum can be used. In particular, when gelatin is added at a high concentration, a gummy hard jelly is obtained.
２価の金属イオン水溶液としてはカルシウム塩、特に乳
酸やグルコン酸のような有機酸塩が好ましい。これは２
〜３％程度の濃度の水溶液で用いるとよい。As the divalent metal ion aqueous solution, calcium salts, particularly organic acid salts such as lactic acid and gluconic acid, are preferred. This is 2
It is preferable to use an aqueous solution with a concentration of about 3%.
一方、アルギン酸ナトリウム並びに低メトキシルペクチ
ンの水溶液は１〜２％程度の濃度で用いるとよく、両者
は混合して用いてもよい。On the other hand, an aqueous solution of sodium alginate and low methoxyl pectin may be used at a concentration of about 1 to 2%, and the two may be used in combination.
機能性物質、例えば食物繊維では、５重量％を食用油と
してのサラダ油中に分散させて用いるとよい。For functional substances such as dietary fiber, 5% by weight is preferably dispersed in salad oil as edible oil.
以下に実施例を示して本発明を具体的に説明する。EXAMPLES The present invention will be specifically described below with reference to Examples.
実施例
カプセル体の芯液の調製ニ
アルギン酸ナトリウム １重量％
ゼラチン ５重量％
低メ）・キシルベクヂン １重量％水
８３重量％上記配合のものを加
熱して溶解し、Ａ液とした。Example: Preparation of core liquid for capsule body Sodium nialginate 1% by weight Gelatin 5% by weight Xylbequidine 1% by weight Water
83% by weight of the above-mentioned mixture was heated and dissolved to obtain liquid A.
食物繊維として ５重量％ 米糖中のヘミセルロース サラダ油 ５重量％ 上記配合のものを混合し、Ｂ液とした。As dietary fiber 5% by weight Hemicellulose in rice sugar Salad oil 5% by weight The above formulations were mixed to obtain liquid B.
次に、」二記Ａ液とＢ液を９０：１．Ｏの割合に混合し
芯液とした。Next, mix liquid A and liquid B at a ratio of 90:1. The mixture was mixed with O in a proportion of 0 and used as a core liquid.
カプセル体の作成：
上述のようにして得た芯液を、乳酸カルシウム１重量％
とグルコン酸カルシウム２重量％を含有する水溶液中に
３ｍｍ径のノズルを介して滴下し、３分間反応させた。Creation of capsule body: The core liquid obtained as described above was mixed with 1% by weight of calcium lactate.
It was dropped into an aqueous solution containing 2% by weight of calcium gluconate through a nozzle with a diameter of 3 mm, and reacted for 3 minutes.
反応により径４〜６ｍｍのカプセル体が得られた。A capsule body with a diameter of 4 to 6 mm was obtained by the reaction.
このカプセル体の９重量部を上記の乳酸カルシウムと、
グルコン酸カルシウムとの混合水溶液１重量部に入れ、
約３０分聞耳度反応させて、中心部までゲル状とした。9 parts by weight of this capsule body with the above calcium lactate,
Add it to 1 part by weight of a mixed aqueous solution with calcium gluconate,
The mixture was left to react for about 30 minutes to form a gel-like mixture in the center.
得られたカプセル体を回収し、水切りした後、パンコー
ティング装置（糖衣装置）により乾燥した。乾燥は、パ
ンコーテイング装置角度３０’回転数１１．５〜２８ｒ
ｐｍ、風速２，５ｍノＳの条件下に１時間予備乾燥した
後、コーンスターチをカプセル重量の１％添加し、更に
１時間乾燥した。 次に、カプセル体に色素、糖液、ク
エン酸の混合水溶液を噴霧コーティングした。コーテイ
ング液はブドウ＃Ｎ４０％、蔗Ｉ！２０％、クエン酸２
％、色素０．８％及び水３７．８％から成るものを加熱
溶解して用いた。The obtained capsule bodies were collected, drained, and then dried using a pan coating device (sugar coating device). For drying, pan coating device angle 30' rotation speed 11.5~28r
After pre-drying for 1 hour under conditions of pm and wind speed of 2.5 mS, cornstarch was added in an amount of 1% of the weight of the capsule, and the capsule was further dried for 1 hour. Next, the capsule body was spray-coated with a mixed aqueous solution of the dye, sugar solution, and citric acid. Coating liquid is Grape #N40%, Potato I! 20%, citric acid 2
%, 0.8% of the dye, and 37.8% of water was used by heating and dissolving it.
なお、噴霧コーティング条件は、パンコーティング角度
３０°、風速２．５ｍ／ｓ、温度４０〜５０”Ｃで約２
〜４時間行った。The spray coating conditions were a pan coating angle of 30 degrees, a wind speed of 2.5 m/s, and a temperature of 40 to 50"C.
I went for ~4 hours.
その結果、径３．１〜４．２ｎｎｎを有するハードゼリ
ー状（グミ状）の食感を有するカプセル体が得られた。As a result, capsule bodies having a diameter of 3.1 to 4.2 nnn and a hard jelly-like (gummy-like) texture were obtained.
Claims (6)
を含有する水性液と、食物繊維、鉄、カルシウム、エイ
コサペンタエン酸（ＥＰＡ）、ビタミン類、オリゴ糖、
カゼインフォスフォペプチド（ＣＰＰ）等から成る群か
ら選択される成分を含む機能性物質の１種もしくは２種
以上を食用油中に高濃度に分散させた油性液との混合液
を、２価の金属イオン溶液中に滴下反応させて、上記混
合液を芯液とするゲル状のカプセル体を形成し、得られ
たカプセル体を乾燥することを特徴とする、機能性物質
を高濃度に内包したカプセル体の製造法。(1) An aqueous liquid containing sodium alginate or low methoxyl pectin, dietary fiber, iron, calcium, eicosapentaenoic acid (EPA), vitamins, oligosaccharides,
A mixture of one or more functional substances containing ingredients selected from the group consisting of casein phosphopeptides (CPP) and an oily liquid in which edible oil is dispersed at a high concentration is mixed with a divalent A highly concentrated functional substance encapsulated by dropwise reaction in a metal ion solution to form a gel-like capsule body using the above-mentioned mixed liquid as a core liquid, and drying the obtained capsule body. Method for manufacturing capsule bodies.
溶液である請求項（１）に記載の製造法。(2) The production method according to claim (1), wherein the divalent metal ion solution is an aqueous solution of a calcium salt of an organic acid.
を含有する水溶液は食用ゲル化剤を含むものである請求
項（１）に記載の製造法。(3) The production method according to claim (1), wherein the aqueous solution containing sodium alginate or low methoxyl pectin contains an edible gelling agent.
、鉄、カルシウム、エイコサペンタエン酸（ＥＰＡ）、
ビタミン類、オリゴ糖、カゼインフォスフォペプチド（
ＣＰＰ）等から成る群から選択される成分を含む機能性
物質の１種もしくは２種以上を食用油中に高濃度に分散
させた油性液との混合液を、アルギン酸ナトリウム又は
低メトキシルペクチンの水溶液中に滴下反応させて、上
記混合液を芯液とするカプセル体を形成し、次いでこの
カプセル体を放置又は冷却して芯液をゲル化させた後、
得られたカプセル体を乾燥することを特徴とする機能性
物質を高濃度に内包したカプセル体の製造法。(4) an aqueous liquid containing divalent metal ions, dietary fiber, iron, calcium, eicosapentaenoic acid (EPA),
Vitamins, oligosaccharides, casein phosphopeptides (
A mixture of one or more functional substances containing components selected from the group consisting of CPP, etc., dispersed in edible oil at a high concentration is mixed with an aqueous solution of sodium alginate or low methoxyl pectin. to form a capsule body using the above-mentioned mixed liquid as a core liquid, and then leave or cool the capsule body to gel the core liquid.
A method for producing a capsule body containing a functional substance at a high concentration, the method comprising drying the obtained capsule body.
むものである請求項（４）に記載の製造法。(5) The production method according to claim (4), wherein the aqueous liquid containing divalent metal ions contains a gelling agent.
と２価の金属イオンとの反応により形成される、芯液を
内包したカプセル体において、食物繊維、鉄、カルシウ
ム、エイコサペンタエン酸、ビタミン類、オリゴ糖、カ
ゼインフォスフォペプチド等から成る群から選択される
成分を含む機能性物質の少なくとも１種を食用油中に高
濃度に分散させた油性液を上記芯液中に混在させて成る
機能性物質を高濃度に内包したカプセル体。(6) In a capsule containing core liquid formed by the reaction of sodium alginate or low methoxyl pectin with divalent metal ions, dietary fiber, iron, calcium, eicosapentaenoic acid, vitamins, oligosaccharides, casein A highly concentrated functional substance is prepared by mixing in the core liquid an oily liquid in which at least one functional substance containing a component selected from the group consisting of phosphopeptides and the like is dispersed in edible oil at a high concentration. A capsule body enclosed in.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2083769A JPH03285654A (en) | 1990-03-30 | 1990-03-30 | Capsule material containing functional substance in high concentration and production thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2083769A JPH03285654A (en) | 1990-03-30 | 1990-03-30 | Capsule material containing functional substance in high concentration and production thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH03285654A true JPH03285654A (en) | 1991-12-16 |
Family
ID=13811806
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2083769A Pending JPH03285654A (en) | 1990-03-30 | 1990-03-30 | Capsule material containing functional substance in high concentration and production thereof |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH03285654A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000083601A (en) * | 1998-09-11 | 2000-03-28 | Sankyo:Kk | Soft capsule |
| US6607775B2 (en) * | 1998-08-06 | 2003-08-19 | Good Humor-Breyers Ice Cream, Division Of Conopco, Inc. | Frozen low-fat food emulsions |
| JP2005512552A (en) * | 2001-12-20 | 2005-05-12 | ソシエテ デ プロデユイ ネツスル ソシエテ アノニム | Food containing gel capsules or tablets |
| JP2008516623A (en) * | 2004-10-22 | 2008-05-22 | コンパニ・ジェルベ・ダノン | Protection of bioactive food ingredients by encapsulation |
| KR100860531B1 (en) * | 2008-03-03 | 2008-09-26 | 주식회사 에스앤텍 | Alginate-calcium-capsule on the various material and the method therof |
| JP2012504947A (en) * | 2008-10-08 | 2012-03-01 | エービー−バイオティクス，エセ．ア． | Iron-enriched food |
| EP1587375B1 (en) * | 2003-01-31 | 2019-03-27 | DSM IP Assets B.V. | Novel compositions comprising carotenoids |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5978654A (en) * | 1982-10-27 | 1984-05-07 | Q P Corp | Preparation of granular food |
| JPS59227240A (en) * | 1983-06-07 | 1984-12-20 | Q P Corp | Preparation of granular food |
| JPS60160840A (en) * | 1983-12-28 | 1985-08-22 | Miyoshi Oil & Fat Co Ltd | Health food |
| JPS6178351A (en) * | 1984-09-22 | 1986-04-21 | Toagosei Chem Ind Co Ltd | Microcapsules including lecithin |
-
1990
- 1990-03-30 JP JP2083769A patent/JPH03285654A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5978654A (en) * | 1982-10-27 | 1984-05-07 | Q P Corp | Preparation of granular food |
| JPS59227240A (en) * | 1983-06-07 | 1984-12-20 | Q P Corp | Preparation of granular food |
| JPS60160840A (en) * | 1983-12-28 | 1985-08-22 | Miyoshi Oil & Fat Co Ltd | Health food |
| JPS6178351A (en) * | 1984-09-22 | 1986-04-21 | Toagosei Chem Ind Co Ltd | Microcapsules including lecithin |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6607775B2 (en) * | 1998-08-06 | 2003-08-19 | Good Humor-Breyers Ice Cream, Division Of Conopco, Inc. | Frozen low-fat food emulsions |
| JP2000083601A (en) * | 1998-09-11 | 2000-03-28 | Sankyo:Kk | Soft capsule |
| JP2005512552A (en) * | 2001-12-20 | 2005-05-12 | ソシエテ デ プロデユイ ネツスル ソシエテ アノニム | Food containing gel capsules or tablets |
| EP1587375B1 (en) * | 2003-01-31 | 2019-03-27 | DSM IP Assets B.V. | Novel compositions comprising carotenoids |
| JP2008516623A (en) * | 2004-10-22 | 2008-05-22 | コンパニ・ジェルベ・ダノン | Protection of bioactive food ingredients by encapsulation |
| KR100860531B1 (en) * | 2008-03-03 | 2008-09-26 | 주식회사 에스앤텍 | Alginate-calcium-capsule on the various material and the method therof |
| JP2012504947A (en) * | 2008-10-08 | 2012-03-01 | エービー−バイオティクス，エセ．ア． | Iron-enriched food |
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