Nothing Special   »   [go: up one dir, main page]

JPH06331570A - High-speed neutron radiography and image recording body for high-speed neutron radiography - Google Patents

High-speed neutron radiography and image recording body for high-speed neutron radiography

Info

Publication number
JPH06331570A
JPH06331570A JP14257193A JP14257193A JPH06331570A JP H06331570 A JPH06331570 A JP H06331570A JP 14257193 A JP14257193 A JP 14257193A JP 14257193 A JP14257193 A JP 14257193A JP H06331570 A JPH06331570 A JP H06331570A
Authority
JP
Japan
Prior art keywords
image recording
film
subject
converter
recording body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP14257193A
Other languages
Japanese (ja)
Inventor
Yojiro Toda
陽二郎 戸田
Kazuhiro Okada
一宏 岡田
Yasushi Yoshii
康司 吉井
Hiroteru Hasegawa
弘照 長谷川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fukuvi Chemical Industry Co Ltd
Japan Steel Works Ltd
Original Assignee
Fukuvi Chemical Industry Co Ltd
Japan Steel Works Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fukuvi Chemical Industry Co Ltd, Japan Steel Works Ltd filed Critical Fukuvi Chemical Industry Co Ltd
Priority to JP14257193A priority Critical patent/JPH06331570A/en
Publication of JPH06331570A publication Critical patent/JPH06331570A/en
Pending legal-status Critical Current

Links

Landscapes

  • Measurement Of Radiation (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Conversion Of X-Rays Into Visible Images (AREA)
  • Particle Accelerators (AREA)

Abstract

PURPOSE:To obtain a clear image with a high resolution using a high-speed neutron. CONSTITUTION:An image recording body 5 where a film-shaped light emitting converter 3 and a sensitized film 4 are adhered is laid out at the rear of a subject 1, proton rays are applied from the front of the subject 1 toward a Be target 7 by a cyclotron 2, and high-speed neutrons discharged from the target 7 are applied, thus enabling the light emitting converter to emit light and sensitizing the sensitized film 4 and hence enabling the sensitized body to be sensitized with a high resolution and achieving an improved working efficiency.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】この発明は、高速中性子を利用し
て被写体の透過像を得る高速中性子ラジオグラフィ法お
よびこれに利用する画像記録体に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a fast neutron radiography method for obtaining a transmission image of an object using fast neutrons and an image recording body used for the method.

【0002】[0002]

【従来の技術】従来、低速の中性子(eV単位)を利用
して、被写体の欠陥、内部性状、構造などを画像化して
非破壊検査を行なうラジオグラフィ法が知られている
が、最近では、より高速の中性子(MeV単位)を利用
して透過性を向上させた高速中性子ラジオグラフィ法が
提案されており、実際に利用されつつある。この高速中
性子ラジオグラフィ法では、高速の中性子(0.1〜1
0MeV程度)を被写体に照射し、被写体を透過した中
性子を後方の高分子材料に照射させることにより、高分
子材料に反跳陽子の飛跡を生じさせる。この飛跡は非常
に小さくてそのままでは観察が困難であるので、その
後、上記高分子材料を強アルカリ溶液に浸漬するエッチ
ング処理を施すことにより飛跡を大きくし、この飛跡を
写真フィルムに転写するという手順を踏んでいる。
2. Description of the Related Art Conventionally, a radiography method has been known in which low-speed neutrons (eV units) are used to image defects, internal properties, structures, etc. of a subject for nondestructive inspection. A fast neutron radiography method, in which the transparency is improved by utilizing faster neutrons (MeV unit), has been proposed and is being practically used. In this fast neutron radiography method, fast neutrons (0.1-1
By irradiating the subject with about 0 MeV) and irradiating the polymer material in the rear with neutrons that have passed through the subject, recoil proton tracks are generated in the polymer material. Since this track is very small and difficult to observe as it is, the procedure of enlarging the track by subjecting the polymer material to an etching treatment by immersing it in a strong alkaline solution, and transferring this track to a photographic film Is stepping on.

【0003】[0003]

【発明が解決しようとする課題】しかし、上記した方法
では、高分子材料に確実に飛跡を生じさせるために、中
性子を長く照射する必要がある。また、飛跡を生じさせ
た後、さらに、エッチング、写真フィルムへの転写の作
業が必要であり、作業が面倒で能率が悪いという問題が
ある。このため、被写体の後方に発光体層を裏面に形成
した0.5mm〜数mm厚程度の薄板またフィルム状の
発光コンバータを配置し、発光コンバータの発光状態を
テレビカメラに記録したり、感光フィルムを感光させる
方法が行われている。
However, in the above method, it is necessary to irradiate neutrons for a long time in order to surely generate a track on the polymer material. Further, after the tracks are formed, the work of etching and transfer to the photographic film is further required, which is a troublesome work and inefficient. Therefore, a thin plate or a film-like light emitting converter having a thickness of about 0.5 mm to several mm with a light emitting layer formed on the back surface is arranged behind the subject, and the light emitting state of the light emitting converter is recorded in a television camera or a light sensitive film. The method of exposing to light is performed.

【0004】しかし、上記した発光コンバータを用いる
方法は、解像度が低く、被写体の小さな欠陥や構造の解
析には適していないという問題があり、高い解像度を必
要とする場合には、作業能率が悪いものの解像度は良好
である上記エッチング法を利用せざるを得ないという制
約がある。この発明は上記課題を解決することを基本的
な目的とし、高解像度を有し、しかも作業能率の優れた
高速中性子ラジオグラフィ法及び該ラジオグラフィ用画
像記録体を提供することを目的とする。
However, the above-mentioned method using the luminescence converter has a problem that it has a low resolution and is not suitable for analysis of small defects and structures of an object. When high resolution is required, work efficiency is poor. However, there is a constraint that the above etching method, which has a good resolution, must be used. The present invention has as its basic object to solve the above problems, and an object thereof is to provide a fast neutron radiography method having a high resolution and excellent work efficiency, and an image recording body for the radiography.

【0005】[0005]

【課題を解決するための手段】上記課題を解決するた
め、本願発明の高速中性子ラジオグラフィ法は、被写体
の後方に膜状の高速中性子用発光コンバータと感光フィ
ルムとを密着させた画像記録体を配置し、被写体の前方
から高速中性子を照射し、被写体を透過した高速中性子
で前記発光コンバータを発光させて感光フィルムを感光
させることを特徴とする。
In order to solve the above problems, the fast neutron radiography method of the present invention provides an image recording body in which a film-like fast neutron emission converter and a photosensitive film are adhered to the back of a subject. The luminescent converter is arranged so that fast neutrons are irradiated from the front of the subject, and the luminescence converter is caused to emit light by the fast neutrons that have passed through the subject to expose the photosensitive film.

【0006】また、本願発明の高速中性子ラジオグラフ
ィ用画像記録体は、膜状の高速中性子用発光コンバータ
の中性子照射裏面側に感光フィルムを密着させたことを
特徴とする。なお、上記発光コンバータは、中性子の照
射により反跳陽子が生じる中性子検出体と発光体とから
なる。例えば、中性子検出体となる高分子材料と、発光
体材料とを混練し、これを硬化させることで膜状の発光
コンバータを得ることができる。この発光コンバータの
膜厚は、10〜200μmであるのが望ましい。
The image recording body for fast neutron radiography of the present invention is characterized in that a photosensitive film is brought into close contact with the neutron irradiation back side of the film-form fast neutron emission converter. The luminescence converter includes a neutron detector that produces recoil protons upon irradiation with neutrons, and a light emitter. For example, a film-shaped luminescence converter can be obtained by kneading a polymer material serving as a neutron detector and a light emitter material and curing the mixture. The film thickness of this light emitting converter is preferably 10 to 200 μm.

【0007】[0007]

【作用】すなわち、この発明によれば、被写体に照射さ
れた高速中性子は、被写体を透過し、発光コンバータに
照射される。発光コンバータでは、反跳陽子が生じ、こ
の反跳陽子によって発光体が発光し、裏面側に密着させ
た感光フィルムを感光させる。発光コンバータは、膜状
とすることにより、発光量は減少するものの解像度は飛
躍的に向上する。発光量の減少は、発光コンバータに感
光フィルムが密着されているために、感光フィルムを十
分に感光させることが可能となる。
In other words, according to the present invention, the fast neutrons applied to the subject are transmitted through the subject and applied to the luminescence converter. In the luminescence converter, recoil protons are generated, and the recoil protons cause the light-emitting body to emit light, which exposes the photosensitive film adhered to the back surface side. By forming the light emitting converter into a film, the light emission amount is reduced, but the resolution is dramatically improved. The reduction in the amount of light emission enables the photosensitive film to be sufficiently exposed to light because the photosensitive film is in close contact with the emission converter.

【0008】この発光コンバータの膜厚は、200μm
を越えると、解像度が低下し、寸法の小さい欠陥などの
測定が困難になる。また、10μm未満では発光量が不
十分であり、感光フィルムを十分に感光させることがで
きないので、発光コンバータの膜厚を10〜200μm
の範囲とするのが望ましい。なお、同様の理由でさら
に、30〜100μmの範囲とするのが望ましい。
The thickness of this light emitting converter is 200 μm.
If it exceeds, the resolution is lowered and it becomes difficult to measure defects such as small dimensions. If the thickness is less than 10 μm, the amount of emitted light is insufficient and the photosensitive film cannot be sufficiently exposed.
It is desirable to set the range to. In addition, for the same reason, it is more preferable that the thickness is in the range of 30 to 100 μm.

【0009】[0009]

【実施例】以下に、この発明の一実施例を添付図面に基
づいて説明する。先ず、ラジオグラフィ装置を説明する
と、中性子を照射して非破壊検査を行なう被写体1の前
方に、高速中性子を放出するサイクロトロン2が配置さ
れており、被写体1の後方には、膜厚40μmの発光コ
ンバータ3と、この裏面に密着させた感光フィルム4と
からなる画像記録体5が配置されている。画像記録体5
は、保型用フレーム6に取り付けられている。なお画像
記録体5の保型はフレームで行なうものに限定されな
い。要は、画像記録体を保型できるものであればよく、
構造などを問わない。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS An embodiment of the present invention will be described below with reference to the accompanying drawings. First, the radiography apparatus will be described. A cyclotron 2 that emits fast neutrons is arranged in front of a subject 1 that irradiates neutrons for non-destructive inspection, and behind the subject 1, a light emission with a film thickness of 40 μm. An image recording body 5 including a converter 3 and a photosensitive film 4 adhered to the back surface of the converter 3 is arranged. Image recording body 5
Are attached to the frame 6 for shape retention. The shape retention of the image recording body 5 is not limited to the one performed in a frame. The point is that it can hold the image recording material,
The structure does not matter.

【0010】上記した発光コンバータ3は、中性子検出
体としてMMAポリマーを有機溶媒に溶解させ、この液
体に発光体としてZnSを混合し、これを乾燥して有機
溶剤を除去することにより製造した。なお、ZnSの含
有量は、60wt%に調製した。また、比較のため、反
跳陽子の飛跡を生じさせる高分子樹脂板を画像記録体と
して被写体の後方に配置した比較用装置を用意した。さ
らに、他の比較例として、上記MMAポリマーで2mm
厚の薄板を形成し、この裏面にZnSを塗布して発光体
層を形成した画像記録体を製造し、これを上記と同様に
被写体の後方に配置した装置を用意した。
The above-mentioned luminescence converter 3 was manufactured by dissolving MMA polymer as a neutron detector in an organic solvent, mixing ZnS as a luminescent material in this liquid, and drying the mixture to remove the organic solvent. The ZnS content was adjusted to 60 wt%. Also, for comparison, a comparative device was prepared in which a polymer resin plate that causes a recoiled proton track was disposed behind the subject as an image recording body. Further, as another comparative example, the above MMA polymer is 2 mm
An image recording body was prepared in which a thin thin plate was formed, and ZnS was applied to the back surface of the thin plate to form a light emitting layer, and an apparatus was prepared in which the image recording body was placed behind the subject in the same manner as described above.

【0011】実施例の装置の動作を説明すると、サイク
ロトロン2により16MeVまで加速した陽子線をBe
ターゲット7に照射して、このターゲット7から放出さ
れる0〜2MeVのエネルギー分布を持つ高速中性子線
7aを被写体1に照射した。高速中性子は、被写体1を
透過して、画像記録体5を照射した。画像記録体5で
は、中性子の照射により、発光コンバータ3が発光し、
感光フィルム4が感光した。この感光フィルム4を現像
して、記録画像を観察したところ、被写体1における
0.5mm径の孔が画像として明瞭に識別された。
Explaining the operation of the apparatus of the embodiment, the proton beam accelerated to 16 MeV by the cyclotron 2 is Be.
The target 1 was irradiated, and the fast neutron beam 7a having an energy distribution of 0 to 2 MeV emitted from the target 7 was irradiated to the subject 1. The fast neutrons passed through the subject 1 and irradiated the image recording body 5. In the image recording body 5, the luminescence converter 3 emits light by the irradiation of neutrons,
Photosensitive film 4 was exposed. When this photosensitive film 4 was developed and the recorded image was observed, a hole having a diameter of 0.5 mm in the subject 1 was clearly identified as an image.

【0012】一方、エッチング法による比較例では、上
記実施例と同程度の解像度は得られたものの、画像記録
体に必要な飛跡を生じさせるまでに、上記実施例に比べ
て5倍の時間を要した。また、その後、エッチング処
理、写真フィルムへの転写作業を必要としたため、作業
能率が極めて悪かった。さらに、薄板の画像記録体を用
いた比較例では、被写体1における0.5mmの孔は画
像上識別することは殆ど困難であり、解像度が不十分で
あった。
On the other hand, in the comparative example by the etching method, although a resolution similar to that of the above-mentioned embodiment was obtained, it took five times as long as that in the above-mentioned embodiment until a necessary track was formed on the image recording material. Needed Further, since the etching process and the transfer work to the photographic film were required thereafter, the work efficiency was extremely poor. Further, in the comparative example using the thin plate image recording body, it was almost difficult to identify the 0.5 mm hole in the subject 1 on the image, and the resolution was insufficient.

【0013】[0013]

【発明の効果】以上説明したように本願発明の高速中性
子ラジオグラフィ法によれば、被写体の後方に膜状の高
速中性子用発光コンバータと感光フィルムとを密着させ
た画像記録体を配置し、被写体の前方から高速中性子を
照射し、被写体を透過した高速中性子で前記発光コンバ
ータを発光させて感光フィルムを感光させるので、膜状
の発光コンバータを十分に発光させて、高い解像度で、
感光体を感光させることができる。しかも、エッチング
などの特別な作業が必要とされないので、能率よくラジ
オグラフィを行なうことができる効果がある。また、本
願発明の高速中性子ラジオグラフィ用画像記録体によれ
ば、膜状の高速中性子用発光コンバータの中性子照射裏
面側に感光フィルムを密着させたので、上記方法に用い
ることにより、高解像度で鮮明な記録画像が簡易に得ら
れる効果がある。
As described above, according to the fast neutron radiography method of the present invention, an image recording body in which a film-like fast neutron emission converter and a photosensitive film are closely attached is arranged behind the subject, Irradiate fast neutrons from the front of the, to sensitize the photosensitive film by emitting light from the luminescence converter with the fast neutrons that have passed through the subject, so that the film-like luminescence converter is sufficiently lit, at a high resolution,
The photoconductor can be exposed to light. Moreover, since special work such as etching is not required, there is an effect that radiography can be performed efficiently. Further, according to the image recording body for fast neutron radiography of the present invention, since the photosensitive film was adhered to the neutron irradiation back surface side of the film-form fast neutron luminescence converter, by using in the above method, it is clear at high resolution. There is an effect that various recorded images can be easily obtained.

【図面の簡単な説明】[Brief description of drawings]

【図1】図1は、この発明の一実施例を示す概略図であ
る。
FIG. 1 is a schematic view showing an embodiment of the present invention.

【符号の説明】[Explanation of symbols]

1 被写体 2 サイクロトロン 3 発光コンバータ 4 感光体 5 画像記録体 7a 高速中性子線 1 Subject 2 Cyclotron 3 Emission Converter 4 Photoreceptor 5 Image Recorder 7a Fast Neutron Beam

───────────────────────────────────────────────────── フロントページの続き (51)Int.Cl.5 識別記号 庁内整理番号 FI 技術表示箇所 H05H 13/00 9014−2G (72)発明者 吉井 康司 茨城県那珂郡東海村白方白根2−22 東京 大学工学部附属原子力工学研究施設内 (72)発明者 長谷川 弘照 福井県坂井郡坂井町定旨1−1 フクビ化 学工業株式会社坂井工場内─────────────────────────────────────────────────── ─── Continuation of the front page (51) Int.Cl. 5 Identification number Reference number within the agency FI Technical display location H05H 13/00 9014-2G (72) Inventor Koji Yoshii 2-Shirahone Shirane, Tokai-mura, Naka-gun, Ibaraki Prefecture 22 Inside the Nuclear Engineering Research Facility, Faculty of Engineering, University of Tokyo (72) Inventor Hiroteru Hasegawa 1-1 Sadamu Sakai-cho, Sakai-gun, Fukui Prefecture Fukubi Kagaku Kogyo Co., Ltd. Sakai Plant

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 被写体の後方に膜状の高速中性子用発光
コンバータと感光フィルムとを密着させた画像記録体を
配置し、被写体の前方から高速中性子を照射し、被写体
を透過した高速中性子で前記発光コンバータを発光させ
て感光フィルムを感光させることを特徴とする高速中性
子ラジオグラフィ法
1. An image recording body in which a film-form luminescence converter for fast neutrons and a photosensitive film are closely attached to the back of a subject, fast neutrons are irradiated from the front of the subject, and fast neutrons passing through the subject Fast neutron radiography method characterized by exposing a photosensitive film by causing an emission converter to emit light
【請求項2】 膜状の高速中性子用発光コンバータの中
性子照射裏面側に感光フィルムを密着させたことを特徴
とする高速中性子ラジオグラフィ用画像記録体
2. An image recording body for fast neutron radiography, characterized in that a photosensitive film is adhered to the neutron irradiation back surface side of a film-form luminescence converter for fast neutrons.
【請求項3】 高速中性子用発光コンバータの膜厚が1
0〜200μmであることを特徴とする請求項2記載の
高速中性子ラジオグラフィ用画像記録体
3. The film thickness of the luminescence converter for fast neutrons is 1
The image recording medium for fast neutron radiography according to claim 2, wherein the image recording medium has a thickness of 0 to 200 μm.
JP14257193A 1993-05-24 1993-05-24 High-speed neutron radiography and image recording body for high-speed neutron radiography Pending JPH06331570A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP14257193A JPH06331570A (en) 1993-05-24 1993-05-24 High-speed neutron radiography and image recording body for high-speed neutron radiography

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP14257193A JPH06331570A (en) 1993-05-24 1993-05-24 High-speed neutron radiography and image recording body for high-speed neutron radiography

Publications (1)

Publication Number Publication Date
JPH06331570A true JPH06331570A (en) 1994-12-02

Family

ID=15318426

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14257193A Pending JPH06331570A (en) 1993-05-24 1993-05-24 High-speed neutron radiography and image recording body for high-speed neutron radiography

Country Status (1)

Country Link
JP (1) JPH06331570A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006057178A1 (en) * 2004-11-25 2006-06-01 High Energy Accelerator Research Organization Neutron generating method and neutron generating device
KR100706416B1 (en) * 2004-12-14 2007-04-10 현대자동차주식회사 Void Fraction Measurement Method using Neutron Radiography
JP2007303983A (en) * 2006-05-12 2007-11-22 Tokyo Nuclear Services Co Ltd Method for manufacturing target of boron neutron capture therapy

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006057178A1 (en) * 2004-11-25 2006-06-01 High Energy Accelerator Research Organization Neutron generating method and neutron generating device
KR100706416B1 (en) * 2004-12-14 2007-04-10 현대자동차주식회사 Void Fraction Measurement Method using Neutron Radiography
JP2007303983A (en) * 2006-05-12 2007-11-22 Tokyo Nuclear Services Co Ltd Method for manufacturing target of boron neutron capture therapy

Similar Documents

Publication Publication Date Title
US4439682A (en) Noise erasing method in a radiation image recording and reproducing method
DE2363995A1 (en) METHOD FOR GENERATING A RADIOGRAPHIC IMAGE AND DEVICE FOR CARRYING OUT THE METHOD
US3493751A (en) Track registration alpha autoradiography
US4438333A (en) Noise erasing apparatus for stimulable phosphor sheet
EP0079691A1 (en) Noise erasing apparatus for stimulable phosphor sheet
JPH06331570A (en) High-speed neutron radiography and image recording body for high-speed neutron radiography
US3457408A (en) Track-etch neutron radiography
EP0986072A2 (en) Process for treatment of a resist
Farnell et al. The response of photographic materials to electrons with particular reference to electron micrography
US4002906A (en) Apparatus and method for the recording and reproduction of X-ray pictures
US2245787A (en) Examining bodies by means of neutrons and electron emitting material
Matsumoto et al. Track-etch neutron radiography with a new boron carbide converter
US3467951A (en) Electron beam recording and readout process for information storage and retrieval
US4085331A (en) Sources of nuclear radiation
Yamanaka et al. A URA coded aperture camera for the inertial confinement fusion experiments
JPH05297597A (en) Formation of resist pattern
US4085324A (en) Imaging by point absorption of radiation
US20060165216A1 (en) Method for detection of micrometric and sub-micrometric images by means of irradiation of a mask or of a biological specimen with ionizing radiation
JP2002067527A (en) Screen printing plate and its manufacturing method
US3505654A (en) Method for retrieving prerecorded information from a recording medium with an unmodulated electron beam
JPS6083941A (en) Inspection of mask pattern of mask for x-ray exposing
US6441389B1 (en) Process for reproducing radiation image using stimulable phosphor sheet having one-dimensionally extended partitions
JP2952629B2 (en) Method for evaluating uniformity of dose in ion beam irradiation modification, method for measuring ion implantation depth, and test material used for the method
JPH04296613A (en) Fast neutron radiography and its device
JPH03273199A (en) Fine x-ray generating device