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JP5819123B2 - Method of cleaning the base - Google Patents

Method of cleaning the base Download PDF

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Publication number
JP5819123B2
JP5819123B2 JP2011153903A JP2011153903A JP5819123B2 JP 5819123 B2 JP5819123 B2 JP 5819123B2 JP 2011153903 A JP2011153903 A JP 2011153903A JP 2011153903 A JP2011153903 A JP 2011153903A JP 5819123 B2 JP5819123 B2 JP 5819123B2
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Prior art keywords
cleaning
cleaning liquid
base
slit
tank
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JP2011153903A
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JP2013017961A (en
Inventor
健児 林田
健児 林田
洋 川竹
洋 川竹
展雄 堀内
展雄 堀内
禎彦 伊藤
禎彦 伊藤
学 釜谷
学 釜谷
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Toray Industries Inc
Toray Engineering Co Ltd
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Toray Industries Inc
Toray Engineering Co Ltd
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Priority to JP2011153903A priority Critical patent/JP5819123B2/en
Priority to KR1020110109865A priority patent/KR101175508B1/en
Priority to TW101124833A priority patent/TWI565526B/en
Priority to CN201210241658.2A priority patent/CN102873052B/en
Publication of JP2013017961A publication Critical patent/JP2013017961A/en
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Publication of JP5819123B2 publication Critical patent/JP5819123B2/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B15/00Details of spraying plant or spraying apparatus not otherwise provided for; Accessories
    • B05B15/50Arrangements for cleaning; Arrangements for preventing deposits, drying-out or blockage; Arrangements for detecting improper discharge caused by the presence of foreign matter
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05CAPPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C11/00Component parts, details or accessories not specifically provided for in groups B05C1/00 - B05C9/00
    • B05C11/10Storage, supply or control of liquid or other fluent material; Recovery of excess liquid or other fluent material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05CAPPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C3/00Apparatus in which the work is brought into contact with a bulk quantity of liquid or other fluent material
    • B05C3/02Apparatus in which the work is brought into contact with a bulk quantity of liquid or other fluent material the work being immersed in the liquid or other fluent material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05CAPPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C5/00Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work
    • B05C5/02Apparatus in which liquid or other fluent material is projected, poured or allowed to flow on to the surface of the work the liquid or other fluent material being discharged through an outlet orifice by pressure, e.g. from an outlet device in contact or almost in contact, with the work
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00Processes for applying liquids or other fluent materials
    • B05D1/18Processes for applying liquids or other fluent materials performed by dipping
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00Processes for applying liquids or other fluent materials
    • B05D1/26Processes for applying liquids or other fluent materials performed by applying the liquid or other fluent material from an outlet device in contact with, or almost in contact with, the surface
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/10Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
    • B08B3/12Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations

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  • Cleaning By Liquid Or Steam (AREA)
  • Coating Apparatus (AREA)
  • Details Or Accessories Of Spraying Plant Or Apparatus (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Description

本発明は、基板に対して塗布液を吐出する口金を洗浄する口金洗浄方法に関する。 The present invention relates to a spinneret cleaning how to clean the mouthpiece for discharging the coating liquid to the substrate.

液晶ディスプレイ等のフラットパネルディスプレイ、太陽電池パネル等には、画素、回路パターン等が形成された基板が用いられており、このような基板は、例えばレジスト液(塗布液)を塗布して行うフォトリソグラフィ技術が用いられることにより、製作されている。
そして、基板に対して塗布液を塗布する装置として、幅方向に長いスリットが内部に形成されている口金を有した塗布装置が知られている。この塗布装置によれば、基板に対して口金を水平移動させながら、スリットから塗布液を吐出することで、基板表面に塗布液の膜を形成することができる。
A flat panel display such as a liquid crystal display, a solar battery panel, and the like use a substrate on which pixels, circuit patterns, and the like are formed. Such a substrate is, for example, a photo that is performed by applying a resist solution (coating solution). It is manufactured by using a lithography technique.
As a device for applying a coating liquid to a substrate, a coating device having a base in which a slit long in the width direction is formed is known. According to this coating apparatus, a film of the coating liquid can be formed on the substrate surface by discharging the coating liquid from the slit while horizontally moving the base with respect to the substrate.

この塗布装置による塗布作業が長時間継続して行われていると、スリット、スリットが開口している口金先端、及び、口金先端の外側面などに、塗布液の固化物や塗布液に混入した異物といった固着物が固着することがあり、これら固着物は塗布液の吐出に影響を与え、塗布欠陥が発生するおそれがある。
そこで、例えば特許文献1に開示されているような、口金を洗浄する洗浄装置が提案されている。
When the coating operation by this coating apparatus is continued for a long time, it is mixed with the solidified product of the coating liquid or the coating liquid on the slit, the tip of the mouth opening the slit, and the outer surface of the tip of the mouth. There are cases where a fixed object such as a foreign substance is fixed, and the fixed object affects the discharge of the coating liquid and may cause a coating defect.
In view of this, for example, a cleaning device for cleaning the die as disclosed in Patent Document 1 has been proposed.

この洗浄装置は、洗浄液が貯留されこの洗浄液に口金先端を浸漬する洗浄槽と、洗浄液を口金(スリット)に流すための流路とを備えている。さらに、この流路の途中で洗浄液に超音波振動を付与する超音波発振器が設けられており、この超音波振動により口金内部に付着している固着物を浮かび上がらせ、洗浄効果を高めようとしている。   This cleaning apparatus includes a cleaning tank in which a cleaning liquid is stored and the tip of the base is immersed in the cleaning liquid, and a flow path for flowing the cleaning liquid through the base (slit). Furthermore, an ultrasonic oscillator for applying ultrasonic vibration to the cleaning liquid is provided in the middle of this flow path, and this ultrasonic vibration raises the sticking matter adhering to the inside of the base, thereby increasing the cleaning effect. .

特開2007−253093号公報(図1、図2、図3参照)Japanese Patent Laying-Open No. 2007-253093 (see FIGS. 1, 2 and 3)

しかし、特許文献1に記載の洗浄装置の場合、洗浄液に超音波振動を付与する位置は、洗浄液を流す流路の途中であって口金(スリット)から離れているため、超音波の振動エネルギーが減衰し、口金の洗浄効果を高めることはあまり期待できない。
そこで、洗浄液に対して超音波振動を付与する位置が、口金先端の近くとなるように、例えば、洗浄液を貯留していると共にこの洗浄液に口金先端を浸漬させる洗浄槽の底部に振動子を設け、この振動子によって洗浄液に振動波(超音波振動)を付与し、口金の洗浄を行うことが考えられる。
However, in the case of the cleaning apparatus described in Patent Document 1, the position where ultrasonic vibration is applied to the cleaning liquid is in the middle of the flow path through which the cleaning liquid flows and away from the base (slit). It cannot be expected to attenuate and enhance the cleaning effect of the base.
Therefore, for example, a vibrator is provided at the bottom of the cleaning tank in which the cleaning liquid is stored and the tip of the base is immersed in the cleaning liquid so that the position where the ultrasonic vibration is applied to the cleaning liquid is near the tip of the base. It is conceivable to apply a vibration wave (ultrasonic vibration) to the cleaning liquid by this vibrator to clean the die.

しかし、このように、洗浄液に浸漬した口金先端の近くに設けた振動子によって、洗浄液に振動波(超音波振動)を付与するだけでは、スリットが開口している口金先端、及び、口金先端の外側面は洗浄できるが、開口幅が非常に狭いスリット(特に口金先端から離れるスリット奥部)には、洗浄液に付与した振動波(振動波に基づくキャビテーション)が到達せずに、スリットの固着物を洗浄することができない。
そこで、洗浄液に付与した振動波(振動波に基づくキャビテーション)を口金のスリット(スリット奥部)まで到達させるために、振動波(超音波振動)が付与された洗浄液を口金先端から吸引する方法が考えられる。
しかし、固着物が固着している領域は固着物の抵抗により洗浄液が流れにくいため、単にキャビテーションを含む洗浄液を口金から吸引するだけでは、洗浄液は固着物を回避して流れてしまい、キャビテーションが固着物に到達せず、固着物を効率良く洗浄できないという問題がある。
つまり、従来では、洗浄作用が弱く、幅方向に長いスリット(口金)の全体にわたってムラのない所望の洗浄結果を得ることが困難であり、また、所望の洗浄結果を得るためには、洗浄を繰り返し行う必要があり、洗浄時間が多くかかる。このため、塗布作業を再開するまでの時間を要し、生産効率の向上の妨げとなっている。
However, just by applying a vibration wave (ultrasonic vibration) to the cleaning liquid by the vibrator provided near the tip of the base immersed in the cleaning liquid, the base of the base having the slit and the tip of the base are opened. The outer surface can be cleaned, but the vibration wave (cavitation based on the vibration wave) applied to the cleaning liquid does not reach the slit with a very narrow opening width (particularly the back of the slit away from the tip of the base), and the fixed object of the slit Can not be washed.
Therefore, in order to make the vibration wave (cavitation based on the vibration wave) applied to the cleaning liquid reach the slit (the back of the slit) of the base, there is a method of sucking the cleaning liquid to which the vibration wave (ultrasonic vibration) is applied from the tip of the base. Conceivable.
However, since the cleaning liquid is difficult to flow in the area where the fixed object is fixed, due to the resistance of the fixed object, simply sucking the cleaning liquid including cavitation from the base will cause the cleaning liquid to flow around the fixed object, and the cavitation is fixed. There is a problem in that it cannot reach the kimono and the fixed matter cannot be washed efficiently.
In other words, conventionally, the cleaning action is weak, and it is difficult to obtain a desired cleaning result without unevenness over the entire slit (die) that is long in the width direction. It needs to be repeated and takes a lot of cleaning time. For this reason, it takes time to restart the coating operation, which hinders improvement in production efficiency.

そこで、本発明の目的は、従来では振動波(振動波に基づくキャビテーション)の伝播が充分にされず残っていた固着物を、浮かび上がらせることが可能となり、短時間でムラのない所望の洗浄結果を効率良く得ることができる口金の洗浄方法を提供する。 Accordingly, an object of the present invention is to make it possible to lift up the remaining fixed matter that has not been sufficiently propagated in vibration waves (cavitation based on vibration waves) in the prior art, and to achieve a desired cleaning result with no unevenness in a short time. the provide cleaning how the mouthpiece can be obtained efficiently.

本発明の口金の洗浄方法は、幅方向に長く先端で開口しているスリットが内部に形成されている口金の洗浄方法であって、洗浄槽内の振動波を与えた洗浄液に口金先端を浸漬させ、前記スリットを通じて当該洗浄液を口金内部へ流入させる第1流入工程と、前記第1流入工程において洗浄液を口金内部へ流入させている状態から、前記スリットを通じて前記口金内部に気体を、当該スリットの幅方向全長にわたって、流入させる気体流入工程と、前記気体流入工程の後、前記口金先端を前記洗浄槽内の振動波を与えた洗浄液に浸漬させ、前記スリットを通じて当該洗浄液を前記口金内部へ流入させる第2流入工程とを含むことを特徴とする口金の洗浄方法。   The base cleaning method of the present invention is a base cleaning method in which a slit which is long in the width direction and opened at the tip is formed inside, and the tip of the base is immersed in a cleaning liquid to which a vibration wave is applied in the cleaning tank. A first inflow step for allowing the cleaning liquid to flow into the base through the slit, and a state in which the cleaning liquid is allowed to flow into the base in the first inflow step, gas is introduced into the base through the slit. After the gas inflow step to flow in over the entire length in the width direction and the gas inflow step, the tip of the base is immersed in a cleaning liquid provided with a vibration wave in the cleaning tank, and the cleaning liquid flows into the base through the slit. And a second inflow step.

本発明によれば、第1流入工程において、振動波を与えた洗浄液を口金内部へ流入させることにより、口金内部に固着していた固着物を浮き上がらせることが可能である。そして、洗浄液を口金内部へ流入させている状態から、スリットを通じて口金内部に気体を、スリットの幅方向全長にわたって、流入させることにより、スリットの幅方向全長にわたって気体と洗浄液との気液界面を一斉に移動させることができる。この結果、口金内部において固着物を剥ぎ取る効果を与えると共に、第2流入工程で再び振動波を与えた洗浄液を口金内部へ流入させる際に、振動波(振動波に基づくキャビテーション)が伝播する態様(経路)が第1流入工程から改められ、従来では振動波の伝播が充分にされず残っていた固着物を、浮かび上がらせることが可能となる。この結果、短時間で所望の洗浄結果を得ることができる。   According to the present invention, in the first inflow process, it is possible to float the fixed matter fixed inside the base by flowing the cleaning liquid to which the vibration wave is applied into the base. Then, from the state in which the cleaning liquid is flowing into the base, the gas is introduced into the base through the slit over the entire length in the width direction of the slit, so that the gas-liquid interface between the gas and the cleaning liquid is spread all over the entire length in the width direction of the slit. Can be moved to. As a result, it is possible to provide an effect of peeling off the fixed matter inside the base, and a vibration wave (cavitation based on the vibration wave) propagates when the cleaning liquid given the vibration wave again in the second inflow process is allowed to flow into the base. The (path) is changed from the first inflow process, and it is possible to lift up the fixed matter that has remained due to insufficient propagation of vibration waves in the past. As a result, a desired cleaning result can be obtained in a short time.

また、前記気体流入工程では、前記口金先端と前記洗浄液の液面とを離すことにより、前記スリットを通じて前記口金内部に気体を、前記スリットの幅方向全長にわたって、流入させるのが好ましい。
この場合、洗浄槽内の洗浄液に口金先端を浸漬させていた状態から、この口金先端と洗浄液の液面とを離す操作を行えばよく、簡単に、スリットを通じて口金内部に気体を、スリットの幅方向全長にわたって、流入させることができる。
Further, in the gas inflow step, it is preferable that gas is caused to flow through the slit over the entire length in the width direction of the slit by separating the tip of the base and the liquid surface of the cleaning liquid.
In this case, from the state in which the tip of the die is immersed in the cleaning liquid in the cleaning tank, it is only necessary to separate the tip of the die from the surface of the cleaning solution. It can be made to flow in over the entire length.

第1流入工程から気体流入工程へと移行した際に口金内部側へと流れた洗浄液には、気体が多く含まれるため、洗浄液中に気体が溶存することから、この洗浄液をそのまま洗浄槽へ戻して、後に第1流入工程(又は第2流入工程)を行う場合、溶存気体量が増加した洗浄液に対して振動波が与えられることとなる。この場合、溶存気体によって洗浄液中の振動波によるキャビテーションの発生が阻害され、キャビテーションによって固着物を浮き上がらせる効果が弱まるおそれがある。
そこで、前記口金の洗浄方法は、前記第1流入工程及び前記第2流入工程において前記スリットから流入させた洗浄液で満たされる流路を通じて洗浄液を前記洗浄槽に戻すと共に、前記流路から、前記気体流入工程で流入した気体を、前記スリットとは別の排出流路を通じて排出する気体排出工程を、更に含むのが好ましい。なお、「洗浄槽に戻す洗浄液」は、第1流入工程及び第2流入工程においてスリットから流入させた洗浄液であってもよく、又は、新たな洗浄液であってもよい。スリットから流入させた洗浄液を戻す場合、当該洗浄液に含まれている気体を、排出流路を通じて排出する。新たな洗浄液の場合、スリットから流入させた洗浄液に含まれている気体を、当該洗浄液と共に、排出流路を通じて排出し、この洗浄液の代わりに新たな洗浄液を洗浄槽に戻す。
この場合、洗浄液を洗浄槽に戻しても、洗浄槽内の洗浄液の溶存気体量が増えるのを抑えることができ、後に第1流入工程(又は第2流入工程)を行っても、振動波によって固着物を浮き上がらせる効果が弱まるのを防ぐことができる。
Since the cleaning liquid that has flowed to the inside of the base when moving from the first inflow process to the gas inflow process contains a large amount of gas, the gas is dissolved in the cleaning liquid, so this cleaning liquid is returned to the cleaning tank as it is. When performing the first inflow process (or the second inflow process) later, a vibration wave is given to the cleaning liquid in which the amount of dissolved gas is increased. In this case, the generation of cavitation due to the vibration wave in the cleaning liquid is hindered by the dissolved gas, and there is a possibility that the effect of floating the fixed object by cavitation may be weakened.
Therefore, the method of cleaning the base includes returning the cleaning liquid to the cleaning tank through the flow path filled with the cleaning liquid flowed from the slit in the first inflow process and the second inflow process, and from the flow path to the gas. It is preferable that the method further includes a gas discharge step of discharging the gas flowing in the inflow step through a discharge channel different from the slit. The “cleaning liquid to be returned to the cleaning tank” may be the cleaning liquid that has been introduced from the slit in the first inflow process and the second inflow process, or may be a new cleaning liquid. When returning the cleaning liquid introduced from the slit, the gas contained in the cleaning liquid is discharged through the discharge channel. In the case of a new cleaning liquid, the gas contained in the cleaning liquid introduced from the slit is discharged together with the cleaning liquid through the discharge channel, and the new cleaning liquid is returned to the cleaning tank instead of the cleaning liquid.
In this case, even if the cleaning liquid is returned to the cleaning tank, an increase in the amount of dissolved gas in the cleaning liquid in the cleaning tank can be suppressed, and even if the first inflow process (or the second inflow process) is performed later, It is possible to prevent the effect of floating the fixed matter from weakening.

また、洗浄液に振動波を与えることにより洗浄槽内で異物が浮遊している場合、第1流入工程及び第2流入工程の一方又は双方によれば、その洗浄槽内の浮遊異物が洗浄液と共に口金内部側へ吸い込まれるおそれがある。
そこで、前記口金の洗浄方法は、前記口金先端を前記洗浄槽の洗浄液に浸漬させた状態で、前記第1流入工程及び前記第2流入工程の一方又は双方において前記口金内部側へ洗浄液を流入させた後、(スリットから流入させた又は新たな)洗浄液を前記スリットから当該洗浄槽へ吐出する仕上げ工程を、更に含み、この仕上げ工程では、前記洗浄槽の洗浄液に振動波を付与したまま、当該洗浄槽の洗浄液に浸漬させていた前記口金先端を、当該洗浄液の液面から離すのが好ましい。
この場合、洗浄槽内の浮遊異物が洗浄液と共に、口金内部側へ吸い込まれ、口金内部の接液面に付着していても、仕上げ工程によれば、(スリットから流入させた又は新たな)洗浄液を洗浄槽へ吐出することで、口金内部の接液面に付着した洗浄槽内の異物を、振動波により浮き上がらせて、口金内部から吐き出すことができる。しかも、洗浄槽の洗浄液に振動波を付与したまま、洗浄槽の洗浄液に浸漬させていた口金先端を、当該洗浄液の液面から離すので、前記洗浄槽内を浮遊している異物が口金内部と口金先端とに再付着するのを防ぐことができる。その結果、洗浄作業が完了後、人手を介すことなく、速やかに塗布作業へ移行することが可能となる。
In addition, when foreign matter is floating in the cleaning tank by applying a vibration wave to the cleaning liquid, according to one or both of the first inflow process and the second inflow process, the floating foreign substance in the cleaning tank is connected to the base together with the cleaning liquid. There is a risk of being sucked into the inside.
Therefore, in the method of cleaning the base, the cleaning liquid is caused to flow into the base inside the base in one or both of the first inflow process and the second inflow process in a state where the tip of the base is immersed in the cleaning liquid in the cleaning tank. And further including a finishing step of discharging the cleaning liquid (flowed from the slit or new) from the slit to the cleaning tank, and in this finishing process, the vibration liquid is applied to the cleaning liquid in the cleaning tank. It is preferable that the tip of the die immersed in the cleaning liquid in the cleaning tank is separated from the liquid surface of the cleaning liquid.
In this case, even if the floating foreign matter in the cleaning tank is sucked into the base together with the cleaning liquid and adheres to the wetted surface inside the base, the cleaning liquid (flowed from the slit or new) is applied according to the finishing process. By discharging to the cleaning tank, the foreign matter in the cleaning tank attached to the liquid contact surface inside the base can be lifted by the vibration wave and discharged from the inside of the base. In addition, the tip of the base immersed in the cleaning liquid in the cleaning tank is separated from the liquid surface of the cleaning liquid while applying a vibration wave to the cleaning liquid in the cleaning tank, so that the foreign matter floating in the cleaning tank is separated from the inside of the base. It is possible to prevent reattachment to the tip of the base. As a result, after the cleaning operation is completed, it is possible to promptly shift to the application operation without human intervention.

また、洗浄槽内で浮遊する異物が、振動波によってスリット内を浮遊して口金内部へ侵入しやすい形態(比重、大きさなど)を有している場合は特に、第1流入工程及び第2流入工程の一方又は双方によれば、その洗浄槽内の浮遊異物が洗浄液と共に口金内部側へ吸い込まれやすくなる。
この場合、前記口金の洗浄方法は、前記口金先端を前記洗浄槽の洗浄液に浸漬させた状態で、前記第1流入工程及び前記第2流入工程の一方又は双方において前記口金内部側へ洗浄液を流入させた後、(スリットから流入させた又は新たな)洗浄液を前記スリットから当該洗浄槽へ吐出する仕上げ工程を、更に含み、この仕上げ工程では、洗浄液を前記洗浄槽へ吐出している途中で、当該洗浄槽内の洗浄液への振動波の付与を停止するのが好ましい。
この場合、洗浄槽内の浮遊異物が洗浄液と共に、口金内部側へ吸い込まれていても、この仕上げ工程によれば、洗浄槽内の洗浄液に振動波を付与している間に、(スリットから流入させた又は新たな)洗浄液を洗浄槽へ吐出することで、口金内部へ吸い込まれた洗浄槽内の浮遊異物を簡単に口金内部から吐き出すことができる。さらに、この際、超音波付与により口金先端に異物が付着するのを回避することができる。しかも、洗浄液を洗浄槽へ吐出している途中で、洗浄槽内の洗浄液への振動波の付与を停止することで、洗浄槽内の異物が沈降し、振動波によって洗浄槽内を浮遊するのを防ぐことができ、口金先端へ異物が付着するのを回避することができる。その結果、洗浄作業が完了後、人手を介すことなく、速やかに塗布作業へ移行することが可能となる。
Further, particularly when the foreign matter floating in the cleaning tank has a form (specific gravity, size, etc.) that easily floats in the slit by the vibration wave and enters the base, the first inflow step and the second inflow. According to one or both of the inflow processes, the floating foreign substances in the cleaning tank are easily sucked into the base inside along with the cleaning liquid.
In this case, in the method of cleaning the die, the cleaning liquid flows into the inner side of the die in one or both of the first inflow step and the second inflow step with the tip of the die immersed in the cleaning solution of the cleaning tank. And further including a finishing step of discharging the cleaning liquid (flowed from the slit or new) from the slit to the cleaning tank. In the finishing process, while the cleaning liquid is being discharged to the cleaning tank, It is preferable to stop applying the vibration wave to the cleaning liquid in the cleaning tank.
In this case, even if floating foreign matter in the cleaning tank is sucked into the base together with the cleaning liquid, according to this finishing process, while the vibration wave is applied to the cleaning liquid in the cleaning tank (inflow from the slit) By discharging the cleaning liquid (which has been or new) into the cleaning tank, floating foreign substances in the cleaning tank sucked into the base can be easily discharged from the base. Further, at this time, it is possible to avoid foreign matter from adhering to the tip of the die by applying ultrasonic waves. In addition, during the discharge of the cleaning liquid to the cleaning tank, by stopping the application of vibration waves to the cleaning liquid in the cleaning tank, foreign matter in the cleaning tank settles and floats in the cleaning tank by the vibration waves. It is possible to prevent the foreign matter from adhering to the tip of the base. As a result, after the cleaning operation is completed, it is possible to promptly shift to the application operation without human intervention.

また、前記口金の洗浄方法は、超音波振動子を低振動数で振動させることによって前記振動波を発生させて行った前記第1流入工程及び前記第2流入工程の後であって、再び前記第1流入工程を行う場合において、当該第1流入工程を再び行う前に、前記洗浄槽の洗浄液を少なくとも一部入れ替える入れ替え工程を、更に含むのが好ましい。
この場合、超音波振動子を低振動数で振動させることによって振動波を発生させて第1流入工程及び第2流入工程を行うことにより、口金の洗浄効果をより一層高めることが可能となる。なお、低振動数としては、20kHz以上であり40kHz以下である。しかし、このような低振動数の場合、洗浄液の温度が上昇しやすく、再び第1流入工程を行うことにより、このような洗浄液を口金内部側に流入させると、口金の温度も上昇する。この場合、口金が熱膨張してスリットの寸法が変化し、この口金を用いて直ぐに塗布作業を行うと、塗布品質に影響を与えるおそれがある。このため、洗浄液の温度が所定の温度に低下するまで作業を休止する必要があり、時間のロスとなる。そこで、このような場合には、前記入れ替え工程によって、洗浄槽の洗浄液を少なくとも一部入れ替え、温度が上昇した洗浄液によって再び第1流入工程が行われるのを防ぐことができる。
Further, the method of cleaning the base is after the first inflow step and the second inflow step performed by generating the vibration wave by vibrating an ultrasonic vibrator at a low frequency, and again When performing a 1st inflow process, it is preferable to further include the exchange process which replaces at least one part of the washing | cleaning liquid of the said washing tank before performing the said 1st inflow process again.
In this case, it is possible to further enhance the cleaning effect of the die by performing the first inflow process and the second inflow process by generating vibration waves by vibrating the ultrasonic vibrator at a low frequency. The low frequency is 20 kHz or more and 40 kHz or less. However, in the case of such a low frequency, the temperature of the cleaning liquid easily rises, and when the cleaning liquid is caused to flow into the base inside by performing the first inflow process again, the temperature of the base also increases. In this case, the size of the slit changes due to thermal expansion of the base, and if the coating operation is performed immediately using this base, there is a risk of affecting the coating quality. For this reason, it is necessary to suspend the operation until the temperature of the cleaning liquid is lowered to a predetermined temperature, resulting in time loss. Therefore, in such a case, at least part of the cleaning liquid in the cleaning tank is replaced by the replacement process, and the first inflow process can be prevented from being performed again by the cleaning liquid whose temperature has increased.

また、前記口金の洗浄方法は、超音波振動子を低振動数で振動させることによって前記振動波を発生させている間、前記洗浄槽の洗浄液を少なくとも一部入れ替える連続的入れ替え工程を、更に含むのが好ましい。
この場合、超音波振動子を低振動数(20kHz以上であり40kHz以下)で振動させることによって振動波を発生させることにより、口金の洗浄効果をより一層高めることが可能となるが、このような低振動数の場合、洗浄液の温度が上昇しやすく、後に、このような洗浄液を口金内部側に流入させると、口金の温度も上昇する。この場合、口金が熱膨張してスリットの寸法が変化し、この口金を用いて直ぐに塗布作業を行うと、塗布品質に影響を与えるおそれがある。このため、洗浄液の温度が所定の温度に低下するまで作業を休止する必要があり、時間のロスとなる。そこで、このような場合には、前記連続的入れ替え工程によって、洗浄槽の洗浄液を少なくとも一部入れ替え、温度が上昇した洗浄液を使用しないようにすることができる。
The base cleaning method further includes a continuous replacement step of replacing at least part of the cleaning liquid in the cleaning tank while the vibration wave is generated by vibrating an ultrasonic vibrator at a low frequency. Is preferred.
In this case, by generating a vibration wave by vibrating the ultrasonic vibrator at a low frequency (20 kHz or more and 40 kHz or less), the cleaning effect of the base can be further enhanced. In the case of a low frequency, the temperature of the cleaning liquid tends to rise, and when such a cleaning liquid is introduced into the base later, the temperature of the base also increases. In this case, the size of the slit changes due to thermal expansion of the base, and if the coating operation is performed immediately using this base, there is a risk of affecting the coating quality. For this reason, it is necessary to suspend the operation until the temperature of the cleaning liquid is lowered to a predetermined temperature, resulting in time loss. Therefore, in such a case, at least a part of the cleaning liquid in the cleaning tank can be replaced by the continuous replacement step so that the cleaning liquid whose temperature has risen is not used.

本発明によれば、スリットの幅方向全長にわたって気体と洗浄液との気液界面を一斉に移動させることによって、口金内部において固着物を剥ぎ取る効果を与えると共に、再び振動波を与えた洗浄液を口金内部へ流入させる際に、振動波(振動波に基づくキャビテーション)が伝播する態様(経路)が改められ、従来では振動波の伝播が充分にされず残っていた固着物を、浮かび上がらせることが可能となり、短時間で所望の洗浄結果を得ることができる。   According to the present invention, the gas-liquid interface between the gas and the cleaning liquid is moved all at once over the entire length in the width direction of the slit, thereby giving the effect of peeling off the fixed matter inside the base, and the cleaning liquid to which the vibration wave has been applied is applied to the base again. The mode (path) of propagation of vibration waves (cavitation based on vibration waves) when inflowing into the interior has been revised, and it is possible to lift up the fixed objects that have remained due to insufficient propagation of vibration waves. Thus, a desired cleaning result can be obtained in a short time.

本発明の塗布装置の実施の一形態を示す概略図である。It is the schematic which shows one Embodiment of the coating device of this invention. 口金及び洗浄機構の説明図である。It is explanatory drawing of a nozzle | cap | die and a washing | cleaning mechanism. 洗浄方法を説明するフロー図である。It is a flowchart explaining the washing | cleaning method. 洗浄方法に含まれる工程の説明図である。It is explanatory drawing of the process included in the washing | cleaning method. 口金及び洗浄槽の説明図であり、(A)は第1流入工程、(B)は気体流入工程、(C)と(D)は第2流入工程を示している。It is explanatory drawing of a nozzle | cap | die and a washing tank, (A) is a 1st inflow process, (B) is a gas inflow process, (C) and (D) has shown the 2nd inflow process. 仕上げ工程を説明するための口金及び洗浄槽の説明図である。It is explanatory drawing of a nozzle | cap | die and a washing tank for demonstrating a finishing process. 気体流入手段の他の例を説明する説明図である。It is explanatory drawing explaining the other example of a gas inflow means.

以下、本発明の実施の形態を図面に基づいて説明する。
〔塗布装置の構成について〕
図1は、本発明の塗布装置1の実施の一形態を示す概略図である。この塗布装置1は、基板(矩形の枚葉部材)Wを載置可能なステージ2と、スリット7が内部に形成されている口金3と、この口金3を搭載しステージ2上の基板Wに対して当該口金3を水平移動(X方向移動)させる駆動装置4とを備えている。これらにより装置本体8が構成されており、この装置本体8によれば、駆動装置4が口金3を水平移動させながら、スリット7から基板Wに対して塗布液を吐出して塗布することにより、基板W上に塗布液による膜(塗膜)Mを形成することができる。このため、口金3の移動方向が塗布方向(X方向)となる。さらに、塗布装置1は、口金3を洗浄する洗浄機構6を備えている。また、この塗布装置1は、装置本体8及び洗浄機構6の動作を制御する制御装置5を備えており、制御装置5は、塗布液を基板Wに吐出する塗布動作の制御、及び、洗浄機構6による口金3の洗浄動作の制御を行う。
Hereinafter, embodiments of the present invention will be described with reference to the drawings.
[About the configuration of the coating device]
FIG. 1 is a schematic view showing an embodiment of a coating apparatus 1 of the present invention. The coating apparatus 1 includes a stage 2 on which a substrate (rectangular sheet member) W can be placed, a base 3 in which a slit 7 is formed, and a base 3 on which the base 3 is mounted. On the other hand, a drive device 4 for moving the base 3 horizontally (moving in the X direction) is provided. The apparatus main body 8 is constituted by these, and according to the apparatus main body 8, the driving device 4 discharges and applies the coating liquid onto the substrate W from the slit 7 while horizontally moving the base 3. A film (coating film) M made of a coating solution can be formed on the substrate W. For this reason, the moving direction of the nozzle | cap | die 3 turns into an application | coating direction (X direction). Furthermore, the coating apparatus 1 includes a cleaning mechanism 6 that cleans the base 3. In addition, the coating apparatus 1 includes a control device 5 that controls operations of the apparatus main body 8 and the cleaning mechanism 6. The control device 5 controls the coating operation for discharging the coating liquid onto the substrate W and the cleaning mechanism. The cleaning operation of the base 3 by 6 is controlled.

口金3の内部に形成されているスリット7は、口金3の幅方向に長く、口金先端(口金下端)9で開口している。口金3の幅方向は、塗布方向(X方向)と直交する水平方向(Y方向)である。スリット7は、塗布方向に薄く、また、口金3の内部に形成されているマニホールド10と繋がっており、マニホールド10及びスリット7を通じて塗布液が口金先端9から吐出される。なお、マニホールド10も、スリット7と同様に、幅方向に長く形成されている。スリット7が開口している口金先端9(スリット7の開口端)は、水平であり、幅方向全長にわたって直線的に形成されている。   The slit 7 formed inside the base 3 is long in the width direction of the base 3 and opens at the base end (bottom end) 9. The width direction of the base 3 is a horizontal direction (Y direction) orthogonal to the application direction (X direction). The slit 7 is thin in the coating direction and is connected to the manifold 10 formed inside the base 3, and the coating liquid is discharged from the base end 9 through the manifold 10 and the slit 7. The manifold 10 is also formed long in the width direction like the slit 7. The base end 9 (opening end of the slit 7) where the slit 7 is open is horizontal and is linearly formed over the entire length in the width direction.

洗浄機構6は、口金3を洗浄する洗浄液Lが貯留されている洗浄槽11を備えており、この洗浄槽11は、ステージ2の近傍に設置されている。塗布動作を終えた後、駆動装置4が口金3を水平移動させることにより、口金3を洗浄槽11の上方に位置させることができる。駆動装置4は口金3を上下移動させる機能も有しており、口金3を降下させることにより、口金先端9を洗浄槽11内の洗浄液に浸漬させることができる。   The cleaning mechanism 6 includes a cleaning tank 11 in which a cleaning liquid L for cleaning the base 3 is stored. This cleaning tank 11 is installed in the vicinity of the stage 2. After finishing the application operation, the base 4 can be positioned above the cleaning tank 11 by the drive device 4 moving the base 3 horizontally. The driving device 4 also has a function of moving the base 3 up and down. By lowering the base 3, the base end 9 can be immersed in the cleaning liquid in the cleaning tank 11.

図2は、口金3及び洗浄機構6の説明図である。洗浄機構6は、洗浄液Lを貯留している前記洗浄槽11の他に、洗浄槽11内の洗浄液Lに振動波を与える発振装置12と、口金3と配管P1を介して繋がっているポンプ13とを備えている。さらに、本実施形態の洗浄機構6は、口金3と配管P2を介して繋がっている廃液部(廃液ボトル)14と、洗浄槽11内の洗浄液Lを吸い出すポンプ15aを含み吸い出した洗浄液Lを洗浄槽11へ戻す流路を構成している循環流路15と、循環流路15の途中に設けられ洗浄液Lから脱気を行う脱気モジュール16と、循環流路15の途中に設けられ洗浄液を冷却する熱交換機17とを備えている。また、循環流路15には、タンク24、フィルター18a,18b及び三方向弁19a,19bが設けられている。また、洗浄機構6は洗浄槽11を昇降させる昇降装置20を備えている。   FIG. 2 is an explanatory diagram of the base 3 and the cleaning mechanism 6. In addition to the cleaning tank 11 that stores the cleaning liquid L, the cleaning mechanism 6 includes an oscillation device 12 that applies a vibration wave to the cleaning liquid L in the cleaning tank 11, and a pump 13 that is connected to the base 3 via the pipe P1. And. Furthermore, the cleaning mechanism 6 of this embodiment cleans the cleaning liquid L sucked out including a waste liquid part (waste liquid bottle) 14 connected to the base 3 via the pipe P2 and a pump 15a for sucking out the cleaning liquid L in the cleaning tank 11. A circulation channel 15 constituting a channel returning to the tank 11, a degassing module 16 provided in the middle of the circulation channel 15 for degassing the cleaning liquid L, and a cleaning solution provided in the middle of the circulation channel 15 And a heat exchanger 17 for cooling. The circulation channel 15 is provided with a tank 24, filters 18a and 18b, and three-way valves 19a and 19b. The cleaning mechanism 6 includes a lifting device 20 that lifts and lowers the cleaning tank 11.

ポンプ13は、洗浄槽11内の洗浄液Lに口金先端9を浸漬させた状態で、当該口金先端9で開口しているスリット7を通じて、洗浄槽11内の洗浄液Lを口金内部へ流入させることができ、吸引した洗浄液を一時的に貯留することができる。
また、洗浄機構6は、ポンプ13によって口金内部側へ流入させた洗浄液を逆流させて洗浄槽11に戻す洗浄液戻し部を有している。本実施形態では、ポンプ13がこの洗浄液戻し部の機能を兼ね備えている。つまり、ポンプ13は、洗浄液Lを正逆の両方向へ送ることができる送液手段であり、運転状態を切り替えることにより、自身によって口金内部側へ流入させた洗浄液を逆流させ洗浄槽11に戻すことができる。更に、ポンプ13を、塗布運転の動作の際に、塗布液を口金3に供給する供給ポンプとして兼用することも可能である。この場合、図示しない塗布液貯蔵タンクと、この塗布液貯蔵タンクからポンプ13を繋ぐ塗布液の供給路とが、別回路としてポンプ13に接続されている。
なお、本実施形態では送液手段としてポンプ13を使用する例について示しているが、送液手段としてタンク(図示せず)を接続し、このタンク内の圧力を制御するものであってもよい。すなわち、ポンプ13の代わりにタンクを接続し、このタンクと真空源と加圧源とを連結させる。そして、真空源を制御することにより口金内部に洗浄液を流入させ、加圧源を制御することにより口金内部の洗浄液を逆流させる。
The pump 13 can cause the cleaning liquid L in the cleaning tank 11 to flow into the base through the slit 7 opened at the base tip 9 in a state where the base tip 9 is immersed in the cleaning liquid L in the cleaning tank 11. The suctioned cleaning liquid can be temporarily stored.
Further, the cleaning mechanism 6 has a cleaning liquid return unit that reversely flows the cleaning liquid that has flowed into the base inside by the pump 13 and returns the cleaning liquid to the cleaning tank 11. In the present embodiment, the pump 13 also has the function of the cleaning liquid returning unit. That is, the pump 13 is a liquid feeding means that can send the cleaning liquid L in both forward and reverse directions. By switching the operation state, the pump 13 returns the cleaning liquid that has flowed into the base by itself to return to the cleaning tank 11. Can do. Furthermore, the pump 13 can also be used as a supply pump that supplies the coating liquid to the base 3 during the coating operation. In this case, a coating solution storage tank (not shown) and a coating solution supply path connecting the coating solution storage tank to the pump 13 are connected to the pump 13 as separate circuits.
In this embodiment, an example in which the pump 13 is used as the liquid feeding means is shown, but a tank (not shown) may be connected as the liquid feeding means to control the pressure in the tank. . That is, a tank is connected instead of the pump 13, and this tank, a vacuum source, and a pressurization source are connected. Then, the cleaning liquid is caused to flow into the base by controlling the vacuum source, and the cleaning liquid inside the base is caused to flow backward by controlling the pressure source.

また、洗浄機構6は、このポンプ(洗浄液戻し部)13の機能によって逆流する洗浄液が流れる流路から分岐していると共に、この逆流する洗浄液に含まれている気体を洗浄槽11以外の領域に排出する排出流路を更に備えている。
本実施形態では、上記の「逆流する洗浄液が流れる流路」とは、図4(C)に示しているように、ポンプ13から口金内部のマニホールド10及びスリット7を経て洗浄槽11の洗浄液Lに至るまでの流路21である。そして、上記の排出流路22は、マニホールド10から分岐して口金3の外部の廃液部(廃液ボトル)14へと通じる流路であり、この流路の途中にバルブ(エアベントバルブ)22aが設けられている。なお、図2によれば、前記配管P2が排出流路22の一部を構成している。
Further, the cleaning mechanism 6 branches from the flow path through which the cleaning liquid that flows backward by the function of the pump (cleaning liquid return unit) 13, and the gas contained in the cleaning liquid that flows backward flows into a region other than the cleaning tank 11. A discharge passage for discharging is further provided.
In the present embodiment, the above-described “flow path through which the cleaning liquid that flows backward” refers to the cleaning liquid L in the cleaning tank 11 from the pump 13 through the manifold 10 and the slit 7 inside the base as shown in FIG. It is the flow path 21 leading to. The discharge flow path 22 is a flow path that branches from the manifold 10 and leads to a waste liquid portion (waste liquid bottle) 14 outside the base 3. A valve (air vent valve) 22a is provided in the middle of the flow path. It has been. According to FIG. 2, the pipe P <b> 2 constitutes a part of the discharge flow path 22.

図2において、発振装置12は、振動子(超音波振動子)12aと、この振動子12aの振動数(発振周波数)を制御するコントローラ12bとを有している。このコントローラ12bは、制御装置5と連係して機能する。発振装置12は、振動子12aを振動させることにより洗浄槽11内の洗浄液Lに対して振動波を付与する。本実施形態では、振動波として超音波振動を付与する。特に、振動子を低振動数(20kHz〜40kHz)で振動させることによって、超音波を付与する。ここで、20kHzより低い振動数や40kHzより高い振動数では、とりわけ強固に固着している固着物を短時間で剥離させるのに必要なキャビテーション効果の発現が困難であるため、20kHz〜40kHzが好ましい。   In FIG. 2, the oscillation device 12 includes a vibrator (ultrasonic vibrator) 12a and a controller 12b that controls the frequency (oscillation frequency) of the vibrator 12a. The controller 12b functions in conjunction with the control device 5. The oscillation device 12 applies a vibration wave to the cleaning liquid L in the cleaning tank 11 by vibrating the vibrator 12a. In this embodiment, ultrasonic vibration is applied as the vibration wave. In particular, ultrasonic waves are applied by vibrating the vibrator at a low frequency (20 kHz to 40 kHz). Here, when the frequency is lower than 20 kHz or higher than 40 kHz, it is difficult to express the cavitation effect necessary to peel off the firmly fixed object in a short time, so 20 kHz to 40 kHz is preferable. .

本実施形態の洗浄槽11は、二層式であり、振動子12aの振動波を伝播させる溶媒Sが貯留されている溶媒槽11aと、この溶媒槽11a内に設置され洗浄液Lを貯留している本洗浄槽11bとを有している。振動子12aが振動すると、その超音波(振動波)は、溶媒Sに伝播され、本洗浄槽11bを介して洗浄液Lに伝播される。そして、この洗浄液Lに口金先端9を浸漬させた状態で、振動子12aが振動し、当該洗浄液Lに超音波振動が付与され、当該洗浄液Lを口金3の内部へ流入させることができる。超音波振動により激しく揺さぶられた洗浄液L中では、正負の圧力が交互に作用し、洗浄液L中において、負圧が作用した場所に真空の空洞(泡)が発生し、この空洞(泡)が正の圧力により消滅するという現象が起こる(キャビテーション)。この空洞(泡)が消滅する際に衝撃波が発生して発現するキャビテーション効果により、口金3の内部の表面及び口金先端9の外側面から、固着物(汚れ)を浮き上がらせることが可能となる。
なお、洗浄槽11は二層式であることから、前記循環流路15は、本洗浄槽11b内の洗浄液Lがポンプ15aによって吸い出され、吸い出された洗浄液Lが本洗浄槽11bへ戻る流路となる。また、洗浄液Lの冷却効果をより一層高めるために、溶媒槽11aの溶媒Sについても、溶媒槽11a内と溶媒槽11a外との間を循環させてもよく、この場合、本洗浄槽11b及び溶媒槽11aの双方において、洗浄液L及び溶媒Sを循環させることとなる。
洗浄槽11は一層式であってもよく、この場合、洗浄液Lが貯留されている洗浄槽11に振動子12aが設けられている。
The cleaning tank 11 of this embodiment is a two-layer type, and stores a solvent tank 11a in which a solvent S that propagates vibration waves of the vibrator 12a is stored, and a cleaning liquid L that is installed in the solvent tank 11a. And a main cleaning tank 11b. When the vibrator 12a vibrates, the ultrasonic wave (vibration wave) propagates to the solvent S and propagates to the cleaning liquid L through the main cleaning tank 11b. Then, the vibrator 12 a vibrates in a state where the die tip 9 is immersed in the cleaning liquid L, ultrasonic vibration is applied to the cleaning liquid L, and the cleaning liquid L can flow into the base 3. In the cleaning liquid L vigorously shaken by the ultrasonic vibration, positive and negative pressures act alternately, and in the cleaning liquid L, a vacuum cavity (bubble) is generated at the place where the negative pressure is applied, and this cavity (bubble) is generated. The phenomenon of disappearing due to positive pressure occurs (cavitation). Due to the cavitation effect generated by the generation of shock waves when the cavities (bubbles) disappear, it is possible to lift the fixed matter (dirt) from the inner surface of the base 3 and the outer surface of the base end 9.
Since the cleaning tank 11 is of a two-layer type, the circulating flow path 15 has the cleaning liquid L in the main cleaning tank 11b sucked out by the pump 15a, and the sucked cleaning liquid L returns to the main cleaning tank 11b. It becomes a flow path. In order to further enhance the cooling effect of the cleaning liquid L, the solvent S in the solvent tank 11a may be circulated between the solvent tank 11a and the outside of the solvent tank 11a. In this case, the main cleaning tank 11b and The cleaning liquid L and the solvent S are circulated in both the solvent tanks 11a.
The cleaning tank 11 may be of a single layer type. In this case, the vibrator 12a is provided in the cleaning tank 11 in which the cleaning liquid L is stored.

脱気モジュール16は、洗浄槽11へ供給する洗浄液を予め脱気する機能を有し、洗浄液L中に溶存する気体を減少させることができる。洗浄液L中に溶存する気体が多く含まれていると、溶存気体によって洗浄液L中におけるキャビテーションの発生が阻害されるため、洗浄槽11において洗浄効果が低減されてしまう。   The degassing module 16 has a function of previously degassing the cleaning liquid supplied to the cleaning tank 11 and can reduce the gas dissolved in the cleaning liquid L. If a large amount of dissolved gas is contained in the cleaning liquid L, the generation of cavitation in the cleaning liquid L is inhibited by the dissolved gas, so that the cleaning effect in the cleaning tank 11 is reduced.

〔口金の洗浄方法について〕
以上の構成を備えた塗布装置1によって実行される口金3の洗浄方法を説明する。図3は、洗浄方法を説明するフロー図であり、図4は、洗浄方法に含まれる工程の説明図である。
[How to clean the base]
A method for cleaning the die 3 executed by the coating apparatus 1 having the above configuration will be described. FIG. 3 is a flowchart illustrating the cleaning method, and FIG. 4 is an explanatory diagram of the steps included in the cleaning method.

〔洗浄準備工程及び洗浄動作工程〕
口金3による塗布動作を終え、この口金3の洗浄を行うために、制御装置5の指令信号に基づいて駆動装置4(図1参照)が口金3を洗浄槽11の上方へ移動させ、その後、口金3を降下させ、口金先端9を、その幅方向全長にわたって、洗浄槽11(本洗浄槽11b)の洗浄液Lに浸漬させる(図4(A)参照:図3の洗浄準備工程S1)。
ここで、塗布動作を終えた後の口金3は、口金内部が塗布液で満たされている状態であっても、塗布液を排出して空の状態であっても良い。口金内部が塗布液で満たされている場合は、洗浄槽11内の洗浄液Lが汚れやすくなることから、また、口金内部が空の状態の場合は、口金内部に残存している塗布液が乾燥して新たな固着物が発生してしまうことから、口金内部は、洗浄液を満たした状態であるのが好ましい。
そして、振動子12aによって洗浄液Lに超音波振動(振動波)を与え、ポンプ13が吸引動作を開始し、スリット7の長手方向全長にわたって、スリット7を通じて洗浄液Lを口金内部へ流入させる(図3の第1流入工程S2)。つまり、洗浄液Lに超音波振動を与えながら当該洗浄液Lを口金内部へ吸引させる。この第1流入工程S2は、所定時間継続して行われる。
[Cleaning preparation process and cleaning operation process]
In order to finish the coating operation by the base 3 and clean the base 3, the driving device 4 (see FIG. 1) moves the base 3 above the cleaning tank 11 based on the command signal of the control device 5, and then The base 3 is lowered and the base tip 9 is immersed in the cleaning liquid L in the cleaning tank 11 (main cleaning tank 11b) over the entire length in the width direction (see FIG. 4A: cleaning preparation step S1 in FIG. 3).
Here, the base 3 after finishing the coating operation may be in a state where the inside of the base is filled with the coating liquid, or in an empty state after discharging the coating liquid. When the inside of the base is filled with the coating liquid, the cleaning liquid L in the cleaning tank 11 is easily contaminated. When the inside of the base is empty, the coating liquid remaining inside the base is dried. Then, since a new fixed matter is generated, the inside of the die is preferably filled with the cleaning liquid.
Then, ultrasonic vibration (vibration wave) is applied to the cleaning liquid L by the vibrator 12a, and the pump 13 starts the suction operation, and the cleaning liquid L flows into the base through the slit 7 over the entire length in the longitudinal direction of the slit 7 (FIG. 3). First inflow step S2). That is, the cleaning liquid L is sucked into the base while applying ultrasonic vibration to the cleaning liquid L. The first inflow step S2 is continuously performed for a predetermined time.

この第1流入工程S2によれば、図5(A)に示しているように、超音波振動(振動波)を与えた洗浄液Lにより、口金内部(特にスリット7)に付着していた固着物Fを浮き上がらせることが可能である。そして、この浮き上がらせた固着物Fを、洗浄液Lと共にポンプ13側へ吸い込ませる。なお、この第1流入工程S2では、スリット7において、超音波振動による微細な泡(キャビテーション)が多く衝突した領域では、固着物Fを浮き上がらせ、ポンプ13側へ吸い込むことができるが、微細な泡(キャビテーション)の衝突が弱い領域では、固着物Fは残留している。
このように領域の差が生じるのは、洗浄液Lの流れの態様(経路)、及び、超音波振動(超音波に基づくキャビテーション)が伝播する態様に起因しており、ある領域に向かって超音波振動による微細な泡(キャビテーション)が発生すると、その微細な泡はその領域に向かって効率よく発生し続けるが、微細な泡の発生効率が悪い領域では、その状態が継続することに基づく。特に、非常に薄い形状であるスリット7に、大きな固着物Fが存在している場合、その固着物Fは超音波振動で完全に浮き上がることが出来ずに残留する。このようにスリット7に固着物Fが残留すると、残留した固着物Fの抵抗により洗浄液Lが流れにくくなるため、洗浄液Lは固着物Fを回避して流れてしまう。その結果、この洗浄液Lが回避する領域が、微細な泡の衝突(キャビテーション)が弱い領域(洗浄効果が低い領域)となり、固着物Fが残留し続ける。
According to the first inflow step S2, as shown in FIG. 5 (A), the adhering matter adhered to the inside of the base (particularly, the slit 7) by the cleaning liquid L given ultrasonic vibration (vibration wave). F can be lifted. Then, the fixed matter F that has been lifted is sucked into the pump 13 together with the cleaning liquid L. In the first inflow step S2, in the area where a lot of fine bubbles (cavitation) due to ultrasonic vibration collide in the slit 7, the fixed matter F can be lifted and sucked into the pump 13 side. In the region where the bubble (cavitation) collision is weak, the fixed matter F remains.
The difference in region is caused by the flow mode (path) of the cleaning liquid L and the mode in which ultrasonic vibration (cavitation based on ultrasonic waves) propagates. When fine bubbles (cavitation) due to vibration are generated, the fine bubbles continue to be generated efficiently toward the region, but the state continues in a region where the generation efficiency of the fine bubbles is poor. In particular, when a large fixed matter F exists in the slit 7 having a very thin shape, the fixed matter F cannot remain completely lifted by ultrasonic vibration and remains. When the fixed matter F remains in the slit 7 in this manner, the cleaning liquid L is difficult to flow due to the resistance of the remaining fixed matter F, and therefore the cleaning liquid L flows while avoiding the fixed matter F. As a result, the region that the cleaning liquid L avoids becomes a region where the collision (cavitation) of fine bubbles is weak (region where the cleaning effect is low), and the fixed matter F continues to remain.

そして、この第1流入工程S2において、ポンプ13により洗浄液Lを口金内部へ流入させている状態から、制御装置5の指令信号に基づいて駆動装置4が口金3を上昇させることにより、スリット7が開口している口金先端9と、洗浄液Lの液面とを離す。これにより、口金内部を大気開放状態とし、ポンプ13により洗浄液Lを口金内部へ流入させている状態から、スリット7を通じて口金内部に気体(大気)を流入させる(図4(B)参照:図3の気体流入工程S3)。つまり、本実施形態では、駆動装置4が、スリット7の幅方向全長にわたって気体を流入させる気体流入手段となる。
スリット7が開口している口金先端9(スリット7の開口端)は、水平であり、直線的に形成されていることから、洗浄液Lを口金内部へ流入させている状態から、口金3が上昇し口金先端9と洗浄液Lの液面とが離れると、気体は、口金先端9からスリット7を通じて口金内部に、スリット7の幅方向(長手方向)全長にわたって流入する。
なお、本実施形態では気体として大気を使用しているが、窒素等でもよく、気体であれば特に限定されない。
And in this 1st inflow process S2, the drive device 4 raises the nozzle | cap | die 3 based on the command signal of the control apparatus 5 from the state which is making the washing | cleaning liquid L flow in into the nozzle | cap | die inside with the pump 13, The slit 7 is made. The base 9 that is open is separated from the surface of the cleaning liquid L. As a result, the inside of the base is opened to the atmosphere, and the gas (atmosphere) flows into the base through the slit 7 from the state in which the cleaning liquid L is introduced into the base by the pump 13 (see FIG. 4B: FIG. 3). Gas inflow step S3). That is, in the present embodiment, the driving device 4 serves as a gas inflow unit that causes gas to flow in over the entire width of the slit 7 in the width direction.
The base 9 (opening end of the slit 7) where the slit 7 is open is horizontal and linearly formed, so that the base 3 rises from the state in which the cleaning liquid L is allowed to flow into the base. When the tip end 9 and the liquid surface of the cleaning liquid L are separated from each other, the gas flows from the tip end 9 through the slit 7 into the base over the entire length in the width direction (longitudinal direction) of the slit 7.
In the present embodiment, the atmosphere is used as a gas, but it may be nitrogen or the like, and is not particularly limited as long as it is a gas.

このように、洗浄液Lを口金内部へ流入させている状態から、スリット7を通じて口金内部に気体を、スリットの幅方向全長にわたって、流入させることにより、図5(B)に示しているように、スリット7の幅方向全長にわたって、気体aと洗浄液Lとの気液界面B1(洗浄液Lから気体aへと変わる界面)を一斉にかつ一様に、マニホールド10側へ移動させることができる。
なお、この気体流入工程S3は、前記気液界面B1が、スリット7の開口端から始まって、気体aによる幅方向に長い帯状の空間が形成されて、この帯状の気体a(空間)がスリット7を通過することができる時間、行われればよく、この時間は数秒(2〜3秒)程度で充分に足り、この時間について口金先端9を洗浄液Lの液面から離せばよい。
Thus, from the state in which the cleaning liquid L is allowed to flow into the base, the gas is allowed to flow into the base through the slit 7 over the entire length in the width direction of the slit, as shown in FIG. The gas-liquid interface B1 (interface that changes from the cleaning liquid L to the gas a) between the gas a and the cleaning liquid L can be moved all at once to the manifold 10 side over the entire length of the slit 7 in the width direction.
In this gas inflow step S3, the gas-liquid interface B1 starts from the opening end of the slit 7, a band-like space is formed in the width direction by the gas a, and the band-like gas a (space) is slit. 7 suffices to be carried out for a period of time that can pass through 7, and this time is sufficient for a few seconds (2 to 3 seconds), and the die tip 9 may be separated from the surface of the cleaning liquid L for this time.

そして、気体流入工程S3の後、制御装置5の指令信号に基づいて駆動装置4が口金3を降下させることにより、口金先端9を洗浄槽11内の超音波振動を与えた洗浄液Lに再び浸漬させ、スリット7の長手方向全長にわたって、当該スリット7を通じて洗浄液Lを口金内部へ流入させる(図4(A)参照:図3の第2流入工程S4)。この第2流入工程S4は所定時間、継続して行われる。この気体流入工程S3は、口金先端9を液面から一時的に離す工程である。
このように、再びスリット7を通じて洗浄液Lを口金内部へ流入させることで、図5(C)から図5(D)に示しているように、超音波振動を与えている洗浄液Lが吸引され始め、超音波(超音波に基づくキャビテーション)を伝播させている洗浄液Lの、スリット7を流れる態様が、第1流入工程S2の際と比べて変化する。つまり、気体aから洗浄液Lに変わる気液界面B2(図5(C)参照)の移動に伴う揺さぶり効果により、固着物Fが完全に浮かび上がる、もしくは固着物Fの一部が浮かび上がることで固着物Fが縮小することにより、洗浄液Lのスリット7を流れる様態が、第1流入工程の際と比べて変化する。このため、第1流入工程S2では微細な泡(キャビテーション)の衝突が弱かった領域が、第2流入工程S4では、微細な泡(キャビテーション)が多く衝突する領域へと変化することが期待される。
Then, after the gas inflow step S3, the driving device 4 lowers the die 3 based on the command signal of the control device 5, whereby the tip 9 of the die is immersed again in the cleaning liquid L given ultrasonic vibration in the cleaning tank 11. Then, the cleaning liquid L is caused to flow into the base through the slit 7 over the entire length in the longitudinal direction of the slit 7 (see FIG. 4A: second inflow step S4 in FIG. 3). The second inflow step S4 is continuously performed for a predetermined time. This gas inflow step S3 is a step of temporarily separating the die tip 9 from the liquid surface.
In this way, by allowing the cleaning liquid L to flow into the base again through the slit 7, the cleaning liquid L giving ultrasonic vibration starts to be sucked as shown in FIGS. 5C to 5D. The manner in which the cleaning liquid L propagating ultrasonic waves (ultrasonic cavitation) flows through the slits 7 changes as compared with the first inflow step S2. That is, due to the shaking effect associated with the movement of the gas-liquid interface B2 (see FIG. 5C) that changes from the gas a to the cleaning liquid L, the fixed matter F is completely lifted or a part of the fixed matter F is lifted. As the fixed matter F shrinks, the manner in which the cleaning liquid L flows through the slit 7 changes as compared with the first inflow step. For this reason, it is expected that the region where the collision of fine bubbles (cavitation) was weak in the first inflow step S2 will be changed to the region where many fine bubbles (cavitation) collide in the second inflow step S4. .

以上の第1流入工程S2、気体流入工程S3及び第2流入工程S4によれば、超音波振動を与えた洗浄液により、口金内部に付着していた固着物Fを素早く、効率的に浮き上がらせることが可能である。そして、第1流入工程S2において洗浄液Lを口金内部へ流入させている状態から、スリット7を通じて口金内部に気体a(図5(B)参照)を、スリット7の幅方向全長にわたって、流入させることにより(気体流入工程S3)、スリット7の幅方向全長にわたって、気体aと洗浄液Lとの気液界面B1を、一斉にかつ一様に移動させることができる。さらに、スリット7を通じて口金内部に洗浄液Lを、再び、スリット7の幅方向全長にわたって、流入させることにより(図5(C)と(D)参照:第2流入工程S4)、スリット7の幅方向全長にわたって、気体aと洗浄液Lとの気液界面B2を、一斉にかつ一様に移動させることができる。
この結果、口金内部において固着物Fを剥ぎ取る効果を与えると共に、第2流入工程S4で再び振動波を与えた洗浄液Lを口金内部へ流入させる際に、この洗浄液Lの流れの態様(経路)、及び、超音波(超音波に基づくキャビテーション)が伝播する態様(経路)が改められ、従来では振動波の伝播が充分にされず残っていた固着物を、浮かび上がらせることが可能となる。
According to the first inflow step S2, the gas inflow step S3, and the second inflow step S4 described above, the fixed matter F adhering to the inside of the base can be quickly and efficiently lifted by the cleaning liquid to which ultrasonic vibration is applied. Is possible. Then, the gas a (see FIG. 5B) is caused to flow into the base through the slit 7 over the entire length in the width direction from the state in which the cleaning liquid L is introduced into the base in the first inflow step S2. (Gas inflow step S3), the gas-liquid interface B1 between the gas a and the cleaning liquid L can be moved simultaneously and uniformly over the entire length of the slit 7 in the width direction. Further, the cleaning liquid L is again introduced into the base through the slit 7 over the entire length in the width direction of the slit 7 (see FIGS. 5C and 5D: second inflow step S4), whereby the width direction of the slit 7 is reached. The gas-liquid interface B2 between the gas a and the cleaning liquid L can be moved all at once over the entire length.
As a result, while giving the effect which peels off the fixed matter F inside a nozzle | cap | die, when making the washing | cleaning liquid L which gave the vibration wave again in 2nd inflow process S4 flow in into the nozzle | cap | die inside, the aspect (path | route) of this washing | cleaning liquid L And the aspect (path | route) which an ultrasonic wave (cavitation based on an ultrasonic wave) propagates is amended, and it becomes possible to make the fixed thing which the propagation of a vibration wave did not fully propagate and remain.

また、第1流入工程S2から気体流入工程S3へと移行した際に口金内部側へと流れた洗浄液には、気体が多く含まれることから、この洗浄液をそのまま洗浄槽11へ戻した場合、後に再び第1流入工程S2を行うと、溶存気体量が増加した洗浄液Lに対して振動波が与えられることとなる。この場合、溶存気体によって洗浄液L中におけるキャビテーションの発生が阻害され、超音波振動によって固着物Fを浮き上がらせる効果が弱まるおそれがある。
そこで、前記第2流入工程S4を終えると、制御装置5によってポンプ13の運転状態が切り替えられ、第1流入工程S2及び第2流入工程S4において口金内部側へ流入させた洗浄液を、逆流させる(図4(C)参照)。この際、前記バルブ(エアベントバルブ22a)を開状態に切り替え、逆流によって洗浄液を洗浄槽11に戻す流路21の途中から、当該洗浄液に含まれている気体を、スリット7とは別の排出流路22を通じて排出する(図3の気体排出工程S5)。なお、バルブ22aを開状態とするのはこの気体排出工程S5のみであり、他の工程では閉状態とする。
Further, since the cleaning liquid that has flowed to the inside of the base when moving from the first inflow process S2 to the gas inflow process S3 contains a large amount of gas, when this cleaning liquid is returned to the cleaning tank 11 as it is, If 1st inflow process S2 is performed again, a vibration wave will be given with respect to the washing | cleaning liquid L whose dissolved gas amount increased. In this case, the generation of cavitation in the cleaning liquid L is hindered by the dissolved gas, and there is a possibility that the effect of floating the fixed substance F by ultrasonic vibration may be weakened.
Therefore, when the second inflow step S4 is finished, the operation state of the pump 13 is switched by the control device 5, and the cleaning liquid that has flowed into the base inside in the first inflow step S2 and the second inflow step S4 is made to flow backward ( (See FIG. 4C). At this time, the valve (air vent valve 22 a) is switched to the open state, and the gas contained in the cleaning liquid is discharged from the flow path 21 that returns the cleaning liquid to the cleaning tank 11 by backflow. It discharges | emits through the path | route 22 (gas discharge process S5 of FIG. 3). The valve 22a is opened only in the gas discharge step S5, and is closed in other steps.

この気体排出工程S5は、ポンプ13が吸い込んだ洗浄液をすべて吐き出すまで実行される。ポンプ13から吐き出された洗浄液は、一部が排出流路22を経て、廃液部14へ流れる。
前記流路21に含まれるスリット7は非常に薄いのに対し、排出流路22の流路断面ははるかに大きく、スリット7を通じて洗浄槽11へ逆流する洗浄液の抵抗は、排出流路22を流れる洗浄液の抵抗よりも大きい。また、マニホールド10における排出流路22の分岐部は、当該マニホールド10の上部に位置している。このため、逆流する洗浄液中に含まれる気体は、マニホールド10で捕捉され、捕捉された気体が洗浄液の一部に連れられて排出流路22へと流れることができる。そして、この気体がバルブ22aを通じて外へ排出される。
この気体排出工程S5によれば、ポンプ13の吸引によって口金内部側へと流れた洗浄液を、逆流させて洗浄槽11に戻しても、洗浄槽11内の洗浄液Lの溶存気体量が増えるのを抑えることができ、後に第1流入工程S2を行っても、超音波振動によって固着物Fを浮き上がらせる効果が弱まるのを防ぐことができる。
This gas discharge step S5 is executed until all the cleaning liquid sucked by the pump 13 is discharged. A part of the cleaning liquid discharged from the pump 13 flows to the waste liquid part 14 through the discharge flow path 22.
The slit 7 included in the flow path 21 is very thin, whereas the cross section of the discharge flow path 22 is much larger, and the resistance of the cleaning liquid flowing back to the cleaning tank 11 through the slit 7 flows through the discharge flow path 22. Greater than the resistance of the cleaning solution. Further, the branch portion of the discharge flow path 22 in the manifold 10 is located at the top of the manifold 10. For this reason, the gas contained in the cleaning liquid that flows backward is captured by the manifold 10, and the captured gas can flow to the discharge flow path 22 along with a part of the cleaning liquid. And this gas is discharged | emitted through the valve | bulb 22a outside.
According to this gas discharge step S5, the amount of dissolved gas in the cleaning liquid L in the cleaning tank 11 increases even if the cleaning liquid that has flowed to the inside of the base by suction of the pump 13 is returned to the cleaning tank 11. Even if the first inflow step S <b> 2 is performed later, it is possible to prevent the effect of floating the fixed object F by ultrasonic vibration from being weakened.

以上、第1流入工程S2から気体排出工程S5までが、1サイクルの洗浄動作工程であり、この洗浄動作工程は、複数サイクル繰り返し実行されてもよい。つまり、制御装置5には、この洗浄動作工程を実行する回数が設定されており、この回数に到達するまで、洗浄動作工程を繰り返し実行する(図3の判定工程S6のNoの場合)。設定回数について実行を終えると(判定工程S6のYesの場合)、仕上げ工程S7へと進む。   As described above, the first inflow process S2 to the gas discharge process S5 is one cycle of the cleaning operation process, and this cleaning operation process may be repeatedly executed a plurality of cycles. That is, the number of times that the cleaning operation process is executed is set in the control device 5, and the cleaning operation process is repeatedly executed until this number is reached (in the case of No in the determination step S6 in FIG. 3). When execution is completed for the set number of times (Yes in determination step S6), the process proceeds to finishing step S7.

〔仕上げ工程(その1)〕
図1の塗布装置1は、クリーンルームに設置されているが、例えば駆動装置4などが駆動することにより微細な金属粉が発生し、これらがクリーンルーム中(大気中)に舞い、洗浄槽11(本洗浄槽11b)に落下することがある。すると、このような金属粉は洗浄槽11に異物Rとして洗浄液L中に存在する。このように、洗浄槽11に異物Rが存在している場合、第1流入工程及び第2流入工程によれば、振動波を与えることで洗浄槽11内を異物Rが浮遊するため、その異物Rが洗浄液Lと共に口金内部側へ吸い込まれる。そこで、このような異物Rを口金内部側から排出する仕上げ工程S7が行われる。
[Finishing process (1)]
The coating apparatus 1 in FIG. 1 is installed in a clean room. For example, when the driving device 4 or the like is driven, fine metal powder is generated. It may fall into the washing tank 11b). Then, such a metal powder exists in the cleaning liquid L as the foreign matter R in the cleaning tank 11. Thus, when the foreign substance R exists in the washing tank 11, according to the 1st inflow process and the 2nd inflow process, since the foreign substance R floats in the washing tank 11 by giving a vibration wave, the foreign substance R is sucked into the base together with the cleaning liquid L. Therefore, a finishing step S7 for discharging such foreign matter R from the inside of the base is performed.

図6(A)に示しているように、口金先端9を洗浄槽11の洗浄液Lに浸漬させた状態で、第1流入工程S2及び第2流入工程S4において口金内部側へ流入させた洗浄液を、ポンプ13によって、逆流させることにより洗浄槽11へ吐出する(図3の仕上げ工程S7)。この際、バルブ22aは閉状態である。
そして、この仕上げ工程S7では、発振装置12によって、洗浄槽11の洗浄液Lに超音波振動を付与したまま、工程の途中から、制御装置5の指令信号に基づいて駆動装置4が口金3を上昇させることにより、洗浄槽11の洗浄液Lに浸漬させていた口金先端9を、洗浄液Lの液面から離す(図6(B)参照)。なお、洗浄液Lの液面から口金先端9を離す動作の間、口金内部側の洗浄液を吐出させた状態としている。
この場合、洗浄槽11に存在していた異物Rが、第1流入工程及び第2流入工程によって、洗浄液Lと共に、口金内部側へ吸い込まれていても、その洗浄液Lを洗浄槽11へ吐出することで、異物Rを口金内部から吐き出すことができる。しかも、洗浄槽11の洗浄液Lに超音波振動を付与したまま、洗浄槽11の洗浄液に浸漬させていた口金先端9を、洗浄液Lの液面から離すので、一旦、吐き出した異物Rが口金先端9に再付着するのを防ぐことができる。
また、この工程S7は、洗浄液Lに超音波振動を与えた状態で行われるので、口金内部に詰まっている異物Rを超音波振動によって浮き上がらせてスリット7の内壁面との摩擦抵抗を下げ、この状態で、洗浄液を吐出することにより、前記異物Rが口金内部に付着することなく効果的に排出することができる。
As shown in FIG. 6 (A), the cleaning liquid that has flowed into the base in the first inflow process S2 and the second inflow process S4 with the base tip 9 immersed in the cleaning liquid L of the cleaning tank 11 is used. Then, the liquid is discharged back to the cleaning tank 11 by the pump 13 (finishing step S7 in FIG. 3). At this time, the valve 22a is in a closed state.
And in this finishing process S7, the drive device 4 raises the nozzle | cap | die 3 based on the command signal of the control apparatus 5 from the middle of a process, giving the ultrasonic vibration to the washing | cleaning liquid L of the washing tank 11 with the oscillation apparatus 12. By doing so, the die tip 9 immersed in the cleaning liquid L of the cleaning tank 11 is separated from the liquid surface of the cleaning liquid L (see FIG. 6B). During the operation of separating the base 9 from the surface of the cleaning liquid L, the cleaning liquid inside the base is discharged.
In this case, even if the foreign matter R present in the cleaning tank 11 is sucked into the base inside along with the cleaning liquid L by the first inflow process and the second inflow process, the cleaning liquid L is discharged to the cleaning tank 11. Thus, the foreign matter R can be discharged from the inside of the base. In addition, since the tip 9 of the base immersed in the cleaning liquid of the cleaning tank 11 is separated from the liquid surface of the cleaning liquid L while the ultrasonic vibration is applied to the cleaning liquid L of the cleaning tank 11, the discharged foreign matter R is temporarily discharged from the tip of the base. 9 can be prevented from reattaching.
In addition, since this step S7 is performed in a state where ultrasonic vibration is applied to the cleaning liquid L, the foreign matter R clogged inside the base is lifted by ultrasonic vibration to reduce the frictional resistance with the inner wall surface of the slit 7, By discharging the cleaning liquid in this state, the foreign matter R can be effectively discharged without adhering to the inside of the base.

〔仕上げ工程(その2)〕
仕上げ工程S7の他の例を説明する。洗浄槽11に存在している異物Rが、超音波振動によってスリット7内を浮遊して口金内部へ侵入しやすい形態(比重、大きさなど)を有している場合、第1流入工程及び第2流入工程によれば、その異物Rが洗浄液と共に口金内部側へ吸い込まれやすくなる。この場合、以下の仕上げ工程S7とするのが好ましい。
[Finishing process (2)]
Another example of the finishing step S7 will be described. When the foreign matter R existing in the cleaning tank 11 has a form (specific gravity, size, etc.) that floats inside the slit 7 by ultrasonic vibration and easily enters the inside of the base, the first inflow step and the first step According to the 2 inflow process, the foreign matter R is easily sucked into the base inside along with the cleaning liquid. In this case, the following finishing step S7 is preferable.

図6(A)に示しているように、口金先端9を洗浄槽11の洗浄液Lに浸漬させた状態で、第1流入工程S2及び第2流入工程S4において口金内部側へ流入させた洗浄液を、ポンプ13によって、逆流させることにより洗浄槽11へ吐出する(図3の仕上げ工程S7)。この際、バルブ22aは閉状態である。
そして、この仕上げ工程S7では、洗浄液を逆流させることにより洗浄槽11へ吐出している途中で、洗浄槽11内の洗浄液Lへの超音波振動の付与を停止する(図6(C)参照。)。
この場合、洗浄槽11に存在していた異物Rが、第1流入工程及び第2流入工程によって、洗浄液Lと共に、口金内部側へ吸い込まれても、その洗浄液Lを洗浄槽11へ吐出することで、異物Rを口金内部から吐き出すことができる。しかも、洗浄液Lを逆流させることにより洗浄槽11へ吐出している途中で、洗浄槽11内の洗浄液Lへの超音波振動(振動波)の付与を停止するので、異物Rが、超音波振動によって洗浄槽11内を浮遊して口金内部へ侵入するのを防ぐことができる。
As shown in FIG. 6 (A), the cleaning liquid that has flowed into the base in the first inflow process S2 and the second inflow process S4 with the base tip 9 immersed in the cleaning liquid L of the cleaning tank 11 is used. Then, the liquid is discharged back to the cleaning tank 11 by the pump 13 (finishing step S7 in FIG. 3). At this time, the valve 22a is in a closed state.
And in this finishing process S7, provision of the ultrasonic vibration to the washing | cleaning liquid L in the washing tank 11 is stopped in the middle of discharging to the washing tank 11 by making the washing | cleaning liquid flow backward (refer FIG.6 (C)). ).
In this case, even if the foreign matter R existing in the cleaning tank 11 is sucked into the inner side of the base together with the cleaning liquid L by the first inflow process and the second inflow process, the cleaning liquid L is discharged to the cleaning tank 11. Thus, the foreign matter R can be discharged from the inside of the base. Moreover, since the application of ultrasonic vibration (vibration wave) to the cleaning liquid L in the cleaning tank 11 is stopped while the cleaning liquid L is discharged back into the cleaning tank 11 by causing the cleaning liquid L to flow backward, the foreign matter R is subjected to ultrasonic vibration. Therefore, it is possible to prevent the inside of the washing tank 11 from floating and entering the inside of the base.

以上の仕上げ工程(その1又はその2)が終了されると、制御装置5の指令信号に基づいて駆動装置4(図1参照)が口金3を装置本体8側へ移動させ、ステージ2上に保持されている基板Wに対して塗布液を吐出して塗布する塗布動作を開始する準備を行う(塗布準備工程S8)。なお、前記仕上げ工程(その1又はその2)では、洗浄液を洗浄槽11へ吐出させているが、この洗浄液は、口金内部側へと吸い込んだ洗浄液だけでなく、口金3へ供給した新たな洗浄液であってもよい。   When the above finishing process (No. 1 or No. 2) is completed, the driving device 4 (see FIG. 1) moves the base 3 toward the device main body 8 based on the command signal of the control device 5, and on the stage 2 Preparation for starting an application operation for discharging and applying an application liquid to the substrate W held is performed (application preparation step S8). In the finishing step (No. 1 or No. 2), the cleaning liquid is discharged to the cleaning tank 11. This cleaning liquid is not only the cleaning liquid sucked into the inner side of the base, but also a new cleaning liquid supplied to the base 3. It may be.

また、上記の各工程において、発振装置12による振動子12aの振動数は、高い洗浄効果が得られるキャビテーションを発生させることができる低い帯域(20kHz〜40kHz)である。この低振動数に基づく超音波振動を発生させて第1流入工程S2及び第2流入工程S4を行うことにより、この帯域以外の振動数で行う場合に比べて、口金先端9の洗浄効果をより一層高めることが可能となる。
しかし、このような振動子12aを低振動数で振動させることによって超音波振動を発生させて第1流入工程S2及び第2流入工程S4を行った場合、洗浄液Lの温度が上昇しやすい。そして、図3の判定工程S6に基づいて(判定工程S6でNo)、再び、第1流入工程S2が行われ、温度が上昇した洗浄液Lを口金内部側に流入させると、口金3の温度も上昇する。この場合、口金3が熱膨張してスリット7の寸法が変化し、この口金3を用いて直ぐに塗布作業を行うと、塗布品質に影響を与えるおそれがある。このため、洗浄槽11の洗浄液Lの温度が所定の温度に低下するまで作業を休止する必要があり、時間のロスとなる。
In each of the above steps, the vibration frequency of the vibrator 12a by the oscillating device 12 is a low band (20 kHz to 40 kHz) in which cavitation with a high cleaning effect can be generated. By generating the ultrasonic vibration based on this low frequency and performing the first inflow step S2 and the second inflow step S4, the cleaning effect of the base tip 9 can be further improved as compared with the case where the frequency is outside this band. This can be further enhanced.
However, when the first inflow step S2 and the second inflow step S4 are performed by generating ultrasonic vibration by vibrating such a vibrator 12a at a low frequency, the temperature of the cleaning liquid L is likely to rise. Then, based on the determination step S6 of FIG. 3 (No in the determination step S6), the first inflow step S2 is performed again, and when the cleaning liquid L whose temperature has risen is caused to flow into the inner side of the base, the temperature of the base 3 is also increased. To rise. In this case, the size of the slit 7 changes due to the thermal expansion of the base 3, and if the coating operation is performed immediately using the base 3, the coating quality may be affected. For this reason, it is necessary to suspend the operation until the temperature of the cleaning liquid L in the cleaning tank 11 is lowered to a predetermined temperature, resulting in a time loss.

そこで、再び、第1流入工程S2を行う前に、洗浄槽11の洗浄液Lを少なくとも一部入れ替える入れ替え工程S9(図3参照)を行うのが好ましい。この工程S9によれば、温度が上昇した洗浄液Lによって再び第1流入工程S2が行われるのを防ぐことができる。入れ替え工程S9の具体例を説明する。第1の方法としては、図2において、ポンプ15aによって吸い出した洗浄液を、三方向弁19aによって、廃液としてタンク23に回収する。そして、廃液とする洗浄液に代わる新しい洗浄液を、三方向弁19bを通じて供給する。なお、本実施形態では新しい洗浄液は、脱気モジュール16を経てから洗浄槽11に供給される。以上より、洗浄槽11の使用済みの洗浄液Lの一部を、新しい洗浄液に入れ替えることができ、洗浄槽11の洗浄液Lの温度が高くなるのを防ぐことができる。   Therefore, it is preferable to perform a replacement step S9 (see FIG. 3) in which at least a part of the cleaning liquid L in the cleaning tank 11 is replaced before performing the first inflow step S2. According to this step S9, it is possible to prevent the first inflow step S2 from being performed again by the cleaning liquid L whose temperature has increased. A specific example of the replacement step S9 will be described. As a first method, in FIG. 2, the cleaning liquid sucked out by the pump 15a is recovered in the tank 23 as waste liquid by the three-way valve 19a. And the new washing | cleaning liquid replaced with the washing | cleaning liquid used as a waste liquid is supplied through the three-way valve 19b. In the present embodiment, the new cleaning liquid is supplied to the cleaning tank 11 after passing through the deaeration module 16. As described above, a part of the used cleaning liquid L in the cleaning tank 11 can be replaced with a new cleaning liquid, and the temperature of the cleaning liquid L in the cleaning tank 11 can be prevented from increasing.

第2の方法としては、ポンプ15aによって吸い出された洗浄液は、三方向弁19aを通じて、熱交換機17に送られ、冷却される。冷却された洗浄液は、循環流路15を通じて、洗浄槽11へ戻される。なお、本実施形態では循環する洗浄液は、脱気モジュール16を経てから洗浄槽11に戻される。以上より、洗浄槽11の使用済みの洗浄液Lの一部を循環させ、その途中で熱交換が行われ、洗浄槽11では冷えた洗浄液Lに入れ替えられる。   As a second method, the cleaning liquid sucked out by the pump 15a is sent to the heat exchanger 17 through the three-way valve 19a and cooled. The cooled cleaning liquid is returned to the cleaning tank 11 through the circulation channel 15. In the present embodiment, the circulating cleaning liquid is returned to the cleaning tank 11 after passing through the deaeration module 16. As described above, a part of the used cleaning liquid L in the cleaning tank 11 is circulated, heat exchange is performed in the middle thereof, and the cleaning liquid 11 is replaced with a cooled cleaning liquid L.

また、このような洗浄液Lの入れ替えを、第1流入工程S2、気体流入工程S3及び第2流入工程S4の、各工程中において、又は、各工程後において、実行してもよい。つまり、本実施形態における口金の洗浄方法には、超音波振動子12aを低振動数(20kHz〜40kHz)で振動させることによって超音波を発生させている間、洗浄槽11の洗浄液Lを少なくとも一部入れ替える工程(連続的入れ替え工程)が、更に含まれていてもよい。   Moreover, you may perform such replacement | exchange of the washing | cleaning liquid L in each process of 1st inflow process S2, gas inflow process S3, and 2nd inflow process S4, or after each process. In other words, in the method of cleaning the die in the present embodiment, at least one cleaning liquid L in the cleaning tank 11 is used while ultrasonic waves are generated by vibrating the ultrasonic vibrator 12a at a low frequency (20 kHz to 40 kHz). A step of replacing parts (continuous replacement step) may be further included.

以上、本実施形態に係る口金の洗浄方法によれば、図5(B)に示しているように、スリット7の幅方向全長にわたって気体aと洗浄液Lとの気液界面B1を一斉に上に移動させ、また、図5(C)に示しているように、スリット7の幅方向全長にわたって気体aと洗浄液Lとの気液界面B2を一斉に上に移動させることによって、口金内部において固着物Fを剥ぎ取る効果を与えると共に、超音波振動を与えた洗浄液Lを再び口金内部へ流入させる際に、洗浄液Lの流れの態様(経路)、及び、超音波(超音波に基づくキャビテーション)が伝播する態様(経路)が改められる。このため、従来では超音波振動の伝播が充分にされず残っていた固着物を、浮かび上がらせることが可能となり、超音波振動を与えた洗浄液Lを再び口金内部へ流入させることで、従来では残留していたであろう固着物を洗浄することができる。この結果、短時間で所望の洗浄結果を得ることができる。
そして、洗浄時間が短時間でよいことから、超音波振動を洗浄液Lに付与する時間も短くて済み、超音波振動による口金3の発熱を抑えることができ、迅速に塗布作業を開始することが可能となる。
As described above, according to the method for cleaning the die according to the present embodiment, as shown in FIG. 5B, the gas-liquid interface B1 between the gas a and the cleaning liquid L is increased all at once over the entire length in the width direction of the slit 7. As shown in FIG. 5 (C), by moving the gas-liquid interface B2 between the gas a and the cleaning liquid L all at once over the entire length in the width direction of the slit 7, When the cleaning liquid L given the ultrasonic vibration is allowed to flow into the base again, the flow mode (path) of the cleaning liquid L and ultrasonic waves (cavitation based on ultrasonic waves) propagate. The mode (route) to perform is amended. For this reason, it is possible to float up the fixed matter that has not been sufficiently propagated in the ultrasonic vibration in the past, and the cleaning liquid L that has been subjected to the ultrasonic vibration is allowed to flow into the base again. The fixed matter that would have been removed can be washed. As a result, a desired cleaning result can be obtained in a short time.
Since the cleaning time is short, the time for applying the ultrasonic vibration to the cleaning liquid L can be short, the heat generation of the base 3 due to the ultrasonic vibration can be suppressed, and the coating operation can be started quickly. It becomes possible.

また、振動子12aを中空の部材から構成し、内部に冷媒を通過させてもよい。中空の振動子12aに冷媒(例えば窒素ガス)を供給する接続口を設け、この接合口を通じて振動子12a内に冷媒を流し、振動子12a及び洗浄液Lに熱が蓄えられないようにするのが好ましい。   Further, the vibrator 12a may be constituted by a hollow member, and the refrigerant may be passed through the inside. A connection port for supplying a refrigerant (for example, nitrogen gas) to the hollow vibrator 12a is provided, and the refrigerant is caused to flow into the vibrator 12a through this joint port so that heat is not stored in the vibrator 12a and the cleaning liquid L. preferable.

また、本発明の塗布装置及び口金の洗浄方法は、図示する形態に限らず本発明の範囲内において他の形態のものであってもよい。
前記実施形態では、気体流入工程において、洗浄槽11の洗浄液Lの液面と口金先端9とを離すために、当該液面と当該口金先端9との高さ方向についての相対位置を変更する位置変更手段を、口金3を上下移動させる駆動装置4として説明したが、これ以外であってもよく、位置変更手段を、洗浄槽11を昇降させる昇降装置20(図2参照)としてもよい。または、口金先端9と洗浄槽11との高さ方向の相対位置は変化しないが、気体流入工程の際に、洗浄液Lの液面の高さを低下させ、その後、その液面を上昇させてもよい。これは、洗浄槽11に対する洗浄液Lの排出・供給を行えばよい。
Moreover, the washing | cleaning method of the coating device and nozzle | cap | die of this invention is not restricted to the form to show in figure, The thing of another form may be sufficient within the scope of the present invention.
In the embodiment, in the gas inflow step, in order to separate the liquid surface of the cleaning liquid L in the cleaning tank 11 and the base tip 9, the position of changing the relative position in the height direction between the liquid level and the base tip 9. Although the changing means has been described as the driving device 4 that moves the base 3 up and down, the changing means may be other than this, and the position changing means may be the lifting device 20 (see FIG. 2) that moves the cleaning tank 11 up and down. Alternatively, although the relative position in the height direction between the die tip 9 and the cleaning tank 11 does not change, the level of the cleaning liquid L is lowered during the gas inflow process, and then the liquid level is raised. Also good. This may be performed by discharging and supplying the cleaning liquid L to the cleaning tank 11.

また、気体流入工程において、ポンプ13によって洗浄槽11内の洗浄液Lを口金内部へと流入させている状態から、スリット7を通じて口金内部に気体を、スリット7の幅方向全長にわたって、流入させるために、上記実施形態では、洗浄液Lの液面に対する口金先端9の高さを変更することによって実現する場合を説明したが、これ以外であってもよい。例えば、図7(A)に示すように、本洗浄槽11b内に、口金先端9と接続可能となる接続ポート50aを有した気体供給部50が設けられており、この気体供給部50には、洗浄槽11外から気体が供給されている。駆動装置4(図1参照)によって、図7(B)に示すように、口金3を降下させることにより、口金先端9が接続ポート50aと接続され、気体供給部50からスリット7を通じて口金内部に気体を流入させる。図7(C)に示すように、接続ポート50aは、スリット7(口金先端9)の幅方向全長にわたって設けられており、スリット7の幅方向全長にわたって、気体を流入させることができる。
以上より、洗浄液Lを口金内部へ流入させている状態(図7(A))から、スリット7を通じて口金内部に気体を、スリット7の幅方向全長にわたって、流入させるために(図7(B))、駆動装置4によって口金3を降下させればよく、この降下は、制御装置5の制御によって実行される。つまり、この場合、駆動装置4及び気体供給部50が、口金内部に気体を、スリット7の幅方向全長にわたって流入させる気体流入手段となる。
In addition, in the gas inflow process, in order to cause the gas to flow into the base through the slit 7 over the entire length in the width direction of the slit 7 from the state in which the cleaning liquid L in the cleaning tank 11 is caused to flow into the base by the pump 13. In the above embodiment, the case has been described in which the height of the nozzle tip 9 with respect to the liquid surface of the cleaning liquid L is changed. For example, as shown in FIG. 7A, a gas supply unit 50 having a connection port 50a that can be connected to the base tip 9 is provided in the main cleaning tank 11b. Gas is supplied from the outside of the cleaning tank 11. As shown in FIG. 7 (B) by the drive device 4 (see FIG. 1), the base 3 is lowered to connect the connection port 50a to the inside of the base through the slit 7 from the gas supply part 50. Inject gas. As shown in FIG. 7C, the connection port 50 a is provided over the entire length in the width direction of the slit 7 (cap end 9), and gas can flow in over the entire length in the width direction of the slit 7.
As described above, in order to allow the gas to flow into the base through the slit 7 from the state in which the cleaning liquid L is flowed into the base (FIG. 7A) (FIG. 7B). ), The base 3 may be lowered by the driving device 4, and this lowering is executed by the control of the control device 5. That is, in this case, the driving device 4 and the gas supply unit 50 serve as gas inflow means for causing the gas to flow into the base over the entire length in the width direction of the slit 7.

また、上記実施形態では、気体排出工程、仕上げ工程において、口金内部に流入させた洗浄槽11の洗浄液Lを逆流させて洗浄槽11に戻す例について説明したが、口金内部に洗浄液Lを流入させた後、新たな洗浄液を洗浄槽11に戻してもよい。
例えば、図2に示すように、配管P1(口金3とポンプ13との間)にバルブ25を設け、ポンプ13と洗浄液供給タンク28との間に三方弁27を設け、この三方弁27の出力ポートの一つは廃液タンク23と接続されている。また、三方弁27とポンプ13との間にはバルブ26が設けられている。この構成によっても、洗浄液Lに含まれる気体(気体流入工程でスリット7から吸い込んだ気体)が洗浄槽11に戻るのを抑えることができる。
Moreover, although the said embodiment demonstrated the example which reversely flows back the washing | cleaning liquid L of the washing tank 11 flowed into the inside of a nozzle | cap | die in the gas discharge process and a finishing process, and returns to the washing tank 11, the washing | cleaning liquid L was made to flow in into a nozzle | cap | die. After that, a new cleaning liquid may be returned to the cleaning tank 11.
For example, as shown in FIG. 2, a valve 25 is provided in the pipe P1 (between the base 3 and the pump 13), a three-way valve 27 is provided between the pump 13 and the cleaning liquid supply tank 28, and an output of the three-way valve 27 is provided. One of the ports is connected to the waste liquid tank 23. A valve 26 is provided between the three-way valve 27 and the pump 13. Also with this configuration, the gas contained in the cleaning liquid L (the gas sucked from the slit 7 in the gas inflow process) can be prevented from returning to the cleaning tank 11.

すなわち、バルブ25を開、バルブ26を閉状態にしてポンプ13を吸引動作させることにより、口金内部の気体を含む洗浄液が、配管P1を通ってポンプ13内に吸入される。そして、バルブ25を閉、バルブ26を開、三方弁27をポンプ13側からタンク23へ繋がるルート(図2ではC1ルート)にして、ポンプ13を吐出動作させることにより、ポンプ13の洗浄液がタンク23に排出される。つまり、スリット7からポンプ13へと流入させた洗浄液で満たされる流路(スリット7からポンプ13までの流路)から、気体流入工程で流入した気体を、当該洗浄液と共に、ポンプ13からタンク23までの流路(排出流路)を通じて、当該タンク23に排出することができる。
そして、バルブ25を閉、バルブ26を開、三方弁27を洗浄液供給タンク28からポンプ13側へと繋がるルート(図2ではC2ルート)に切り替え、ポンプ13を吸引動作させることにより、洗浄液供給タンク28内の新しい洗浄液がポンプ13に吸入される。そして、バルブ25を開、バルブ26を閉にしてポンプ13を吐出動作させることにより、ポンプ13に吸入されていた新しい洗浄液が配管P1を通じて口金内部に供給される。さらに、ポンプ13を作動させ続けることによりスリット7を通じて新しい洗浄液が洗浄槽11に戻される。これにより、気体流入工程により洗浄液に取り込まれた気体を、洗浄槽11に戻るのを抑えることができ、溶存気体によって洗浄槽11内の洗浄液中における振動波の伝播が阻害され、振動波によって固着物を浮き上がらせる効果が弱まるのを抑えることができる。この場合においても、洗浄液供給タンク28とポンプ13との間に脱気モジュール17を備えておくことが好ましい。
That is, by opening the valve 25 and closing the valve 26 and causing the pump 13 to perform the suction operation, the cleaning liquid containing the gas inside the base is sucked into the pump 13 through the pipe P1. Then, the valve 25 is closed, the valve 26 is opened, and the three-way valve 27 is routed to the tank 23 from the pump 13 side (C1 route in FIG. 2). 23 is discharged. That is, the gas flowing in the gas inflow process from the flow path (flow path from the slit 7 to the pump 13) filled with the cleaning liquid flowing from the slit 7 to the pump 13 together with the cleaning liquid from the pump 13 to the tank 23. It can be discharged to the tank 23 through the flow path (discharge flow path).
Then, the valve 25 is closed, the valve 26 is opened, and the three-way valve 27 is switched to a route (C2 route in FIG. 2) connected from the cleaning liquid supply tank 28 to the pump 13 side. The new cleaning liquid in 28 is sucked into the pump 13. Then, by opening the valve 25 and closing the valve 26 and causing the pump 13 to discharge, the new cleaning liquid sucked into the pump 13 is supplied into the base through the pipe P1. Further, by continuing to operate the pump 13, new cleaning liquid is returned to the cleaning tank 11 through the slit 7. As a result, the gas taken into the cleaning liquid by the gas inflow process can be prevented from returning to the cleaning tank 11, and the propagation of the vibration wave in the cleaning liquid in the cleaning tank 11 is hindered by the dissolved gas. It can suppress that the effect which makes kimono rise is weakened. Even in this case, it is preferable to provide the deaeration module 17 between the cleaning liquid supply tank 28 and the pump 13.

また、上記実施形態では、洗浄液の入れ替え工程は、第1流入工程及び第2流入工程の後であって、再び第1流入工程を行う場合において、この第1流入工程を再び行う前に、洗浄槽11の洗浄液Lを少なくとも一部入れ替える例について説明したが、いずれの工程においても入れ替え工程が、連続的に行われてもよい。具体的には、各工程において、超音波振動子12aを低振動で振動させて振動波を発生させている間、常時、入れ替え工程を行うことにより、洗浄液を常時循環させる。
すなわち、洗浄液の温度によっては、洗浄液に口金3を浸漬させているだけで口金3の温度が上昇する場合がある。この場合、口金3が熱膨張してスリット7の寸法が変化することにより塗布品質に影響を与えるおそれがある。そこで、超音波振動子12aを低振動数で作動させている際に、洗浄液を常時循環させることにより、洗浄液を常に冷却させる。これにより、洗浄液の温度上昇を抑えることができ、口金3の温度上昇を抑え、塗布品質への影響を抑えることが可能となる。
In the above embodiment, the cleaning liquid replacement step is performed after the first inflow step and the second inflow step, and when the first inflow step is performed again, before the first inflow step is performed again. Although the example which replaces at least one part of the washing | cleaning liquid L of the tank 11 was demonstrated, the replacement | exchange process may be performed continuously in any process. Specifically, in each process, while the ultrasonic transducer 12a is vibrated with low vibration to generate a vibration wave, the cleaning liquid is constantly circulated by performing the replacement process at all times.
That is, depending on the temperature of the cleaning liquid, the temperature of the base 3 may rise only by immersing the base 3 in the cleaning liquid. In this case, there is a possibility that the coating quality may be affected by the thermal expansion of the base 3 and the change of the size of the slit 7. Therefore, when the ultrasonic vibrator 12a is operated at a low frequency, the cleaning liquid is always circulated to constantly cool the cleaning liquid. Thereby, the temperature rise of the cleaning liquid can be suppressed, the temperature rise of the base 3 can be suppressed, and the influence on the coating quality can be suppressed.

口金の洗浄方法に関して、参考発明を説明する。
この参考発明の課題は、洗浄液に対して超音波振動を付与する位置が、口金先端の近くとなるように、例えば、洗浄液を貯留していると共にこの洗浄液に口金先端を浸漬させる洗浄槽の底部に振動子を設け、この振動子によって洗浄液に振動波(超音波振動)を付与し、口金の洗浄を行うことが考えられるが、洗浄槽内の洗浄液に対して振動波を与えることにより、この洗浄槽内で異物が浮遊して、口金の洗浄中に、その浮遊している異物が口金内部へ侵入するおそれがある、という点である。
そこで、参考発明は、幅方向に長く先端で開口しているスリットが内部に形成されている口金の洗浄方法であって、
洗浄槽内の振動波を与えた洗浄液に口金先端を浸漬させ、前記スリットを通じて洗浄液を流して口金内部の洗浄を行う洗浄工程と、
前記口金先端を前記洗浄槽の洗浄液に浸漬させた状態で、前記洗浄工程において前記口金内部の洗浄を行った後、洗浄液を前記スリットから当該洗浄槽へ吐出する仕上げ工程を、更に含み、
この仕上げ工程では、前記洗浄槽の洗浄液に振動波を付与したまま、当該洗浄槽の洗浄液に浸漬させていた前記口金先端を、当該洗浄液の液面から離す洗浄方法である。
この参考発明によれば、洗浄工程において、洗浄槽内で浮遊している異物が、口金内部へ侵入し、口金内部の接液面に付着していても、仕上げ工程によれば、洗浄液を洗浄槽へ吐出することで、口金内部の接液面に付着した異物を、振動波により浮き上がらせて、口金内部から吐き出すことができる。しかも、洗浄槽の洗浄液に振動波を付与したまま、洗浄槽の洗浄液に浸漬させていた口金先端を、当該洗浄液の液面から離すので、洗浄槽内を浮遊している異物が口金内部と口金先端とに再付着するのを防ぐことができる。これにより、洗浄工程から素早く塗布運転に移行することが可能となる。
The reference invention will be described with respect to the method for cleaning the die.
The problem of this reference invention is that, for example, the bottom portion of the cleaning tank that stores the cleaning liquid and immerses the front end of the base in the cleaning liquid so that the position where the ultrasonic vibration is applied to the cleaning liquid is close to the front end of the base. It is conceivable that the vibrator is provided with a vibration wave (ultrasonic vibration) applied to the cleaning liquid by this vibrator to clean the die, but by applying a vibration wave to the cleaning liquid in the cleaning tank, The foreign matter floats in the cleaning tank, and the floating foreign matter may enter the base during the cleaning of the base.
Therefore, the reference invention is a method for cleaning a die in which a slit that is long in the width direction and opened at the tip is formed inside,
A cleaning step of immersing the tip of the die in a cleaning solution provided with vibration waves in the cleaning tank, and cleaning the inside of the die by flowing the cleaning solution through the slit,
In the state where the tip of the die is immersed in the cleaning liquid of the cleaning tank, after the inside of the base is cleaned in the cleaning process, further including a finishing step of discharging the cleaning liquid from the slit to the cleaning tank,
This finishing step is a cleaning method in which the tip of the die that has been immersed in the cleaning liquid in the cleaning tank is separated from the liquid surface of the cleaning liquid while applying a vibration wave to the cleaning liquid in the cleaning tank.
According to this reference invention, in the cleaning process, even if foreign matter floating in the cleaning tank penetrates into the base and adheres to the liquid contact surface inside the base, the cleaning liquid is cleaned according to the finishing process. By discharging to the tank, the foreign matter adhering to the liquid contact surface inside the base can be lifted by the vibration wave and discharged from the inside of the base. In addition, the tip of the base immersed in the cleaning liquid in the cleaning tank is separated from the surface of the cleaning liquid while applying a vibration wave to the cleaning liquid in the cleaning tank, so that the foreign matter floating in the cleaning tank is separated from the inside of the base and the base. It is possible to prevent reattachment to the tip. Thereby, it becomes possible to transfer to a coating operation quickly from a washing process.

また、口金の洗浄方法に関して、他の参考発明を説明する。
この参考発明の課題は、
洗浄液に対して超音波振動を付与する位置が、口金先端の近くとなるように、例えば、洗浄液を貯留していると共にこの洗浄液に口金先端を浸漬させる洗浄槽の底部に振動子を設け、この振動子によって洗浄液に振動波(超音波振動)を付与し、口金の洗浄を行うことが考えられるが、洗浄槽内で浮遊する異物が、振動波によってスリット内を浮遊して口金内部へ侵入しやすい形態(比重、大きさなど)を有している場合は特に、その洗浄槽内で浮遊している異物が口金内部側へ侵入し付着するおそれがある、という点である。
そこで、参考発明は、幅方向に長く先端で開口しているスリットが内部に形成されている口金の洗浄方法であって、
洗浄槽内の振動波を与えた洗浄液に口金先端を浸漬させ、前記スリットを通じて洗浄液を流して口金内部の洗浄を行う洗浄工程と、
前記口金先端を前記洗浄槽の洗浄液に浸漬させた状態で、前記洗浄工程において前記口金内部の洗浄を行った後、洗浄液を前記スリットから当該洗浄槽へ吐出する仕上げ工程を、更に含み、
この仕上げ工程では、洗浄液を前記洗浄槽へ吐出している途中で、当該洗浄槽内の洗浄液への振動波の付与を停止する洗浄方法である。
この参考発明によれば、洗浄工程において、洗浄槽内で浮遊している異物が、口金内部側へ侵入していても、仕上げ工程によれば、洗浄液を洗浄槽へ吐出することで、前記異物を簡単に口金内部から吐き出すことができる。さらに、この際、超音波付与により口金先端に異物が付着するのを回避することができる。しかも、洗浄液を洗浄槽へ吐出している途中で、洗浄槽内の洗浄液への振動波の付与を停止するので、洗浄槽内の異物が、振動波によって洗浄槽内を浮遊するのを防ぐことができ、口金先端へ異物が付着するのを回避することができる。これにより、洗浄工程から素早く塗布運転に移行することが可能となる。
Further, another reference invention will be described regarding the method of cleaning the die.
The subject of this reference invention is
For example, the vibrator is provided at the bottom of the cleaning tank that stores the cleaning liquid and immerses the tip of the base in the cleaning liquid so that the position where the ultrasonic vibration is applied to the cleaning liquid is near the tip of the base. It is conceivable to apply a vibration wave (ultrasonic vibration) to the cleaning liquid using a vibrator to clean the die. However, foreign matter floating in the cleaning tank floats in the slit by the vibration wave and enters the die. Especially when it has an easy form (specific gravity, size, etc.), there is a possibility that foreign matters floating in the cleaning tank may enter and adhere to the inside of the base.
Therefore, the reference invention is a method for cleaning a die in which a slit that is long in the width direction and opened at the tip is formed inside,
A cleaning step of immersing the tip of the die in a cleaning solution provided with vibration waves in the cleaning tank, and cleaning the inside of the die by flowing the cleaning solution through the slit,
In the state where the tip of the die is immersed in the cleaning liquid of the cleaning tank, after the inside of the base is cleaned in the cleaning process, further including a finishing step of discharging the cleaning liquid from the slit to the cleaning tank,
This finishing step is a cleaning method in which application of vibration waves to the cleaning liquid in the cleaning tank is stopped while the cleaning liquid is being discharged to the cleaning tank.
According to this reference invention, in the cleaning process, even if foreign matter floating in the cleaning tank penetrates into the inside of the base, according to the finishing process, the cleaning liquid is discharged into the cleaning tank, thereby Can be easily discharged from the inside of the base. Further, at this time, it is possible to avoid foreign matter from adhering to the tip of the die by applying ultrasonic waves. In addition, since the application of vibration waves to the cleaning liquid in the cleaning tank is stopped while the cleaning liquid is being discharged into the cleaning tank, foreign substances in the cleaning tank are prevented from floating in the cleaning tank due to vibration waves. It is possible to prevent foreign matter from adhering to the tip of the base. Thereby, it becomes possible to transfer to a coating operation quickly from a washing process.

なお、これら参考発明それぞれにおける洗浄工程は、前記実施形態で説明した第1流入工程、気体流入工程及び前記第2流入工程を含む前記洗浄動作工程と同じであり、また、参考発明それぞれにおける洗浄工程及び仕上げ工程に対して、前記各実施形態の口金の洗浄方法で説明した洗浄動作工程及び仕上げ工程の各事項を、適用することができる。   The cleaning process in each of the reference inventions is the same as the cleaning operation process including the first inflow process, the gas inflow process, and the second inflow process described in the embodiment, and the cleaning process in each of the reference inventions. In addition, the items of the cleaning operation process and the finishing process described in the method of cleaning the die according to each of the embodiments can be applied to the finishing process.

1:塗布装置 3:口金 4:駆動装置(位置変更手段) 5:制御装置 6:洗浄機構 7:スリット 8:装置本体 9:口金先端 11:洗浄槽 12a:振動子 13:ポンプ(洗浄液戻し部) 21:流路 22:排出流路 a:気体 B1,B2:気液界面 F:固着物 L:洗浄液 R:異物 W:基板   1: coating device 3: base 4: drive device (position changing means) 5: control device 6: cleaning mechanism 7: slit 8: device main body 9: tip of the base 11: cleaning tank 12a: vibrator 13: pump (cleaning liquid returning section) ) 21: flow path 22: discharge flow path a: gas B1, B2: gas-liquid interface F: fixed matter L: cleaning liquid R: foreign matter W: substrate

Claims (7)

幅方向に長く先端で開口しているスリットが内部に形成されている口金の洗浄方法であって、
洗浄槽内の振動波を与えた洗浄液に口金先端を浸漬させ、前記スリットを通じて当該洗浄液を口金内部へ流入させる第1流入工程と、
前記第1流入工程において洗浄液を口金内部へ流入させている状態から、前記スリットを通じて前記口金内部に気体を、当該スリットの幅方向全長にわたって、流入させる気体流入工程と、
前記気体流入工程の後、前記口金先端を前記洗浄槽内の振動波を与えた洗浄液に浸漬させ、前記スリットを通じて当該洗浄液を前記口金内部へ流入させる第2流入工程と、
を含むことを特徴とする口金の洗浄方法。
A method of cleaning a base in which a slit that is long in the width direction and opened at the tip is formed inside,
A first inflow step of immersing the tip of the base in the cleaning liquid provided with the vibration wave in the cleaning tank, and allowing the cleaning liquid to flow into the base through the slit;
A gas inflow step for allowing a gas to flow into the base through the slit from the state in which the cleaning liquid is caused to flow into the base in the first inflow step;
After the gas inflow step, a second inflow step of immersing the tip of the base in a cleaning liquid provided with a vibration wave in the cleaning tank and flowing the cleaning liquid into the base through the slit;
A method for cleaning a base, comprising:
前記気体流入工程では、前記口金先端と前記洗浄液の液面とを離すことにより、前記スリットを通じて前記口金内部に気体を、前記スリットの幅方向全長にわたって、流入させる請求項1に記載の口金の洗浄方法。   The said metal inflow process WHEREIN: By separating | separating the said nozzle | tip front-end | tip and the liquid level of the said washing | cleaning liquid, gas is made to flow in into the said nozzle | cap | die through the said slit over the width direction full length of the said slit. Method. 前記第1流入工程及び前記第2流入工程において前記スリットから流入させた洗浄液で満たされる流路を通じて洗浄液を前記洗浄槽に戻すと共に、前記流路から、前記気体流入工程で流入した気体を、前記スリットとは別の排出流路を通じて排出する気体排出工程を、更に含む請求項1又は2に記載の口金の洗浄方法。   In the first inflow step and the second inflow step, the cleaning liquid is returned to the cleaning tank through the flow path filled with the cleaning liquid introduced from the slit, and the gas flowing in the gas inflow process from the flow path is The base cleaning method according to claim 1, further comprising a gas discharge step of discharging through a discharge flow path different from the slit. 前記口金先端を前記洗浄槽の洗浄液に浸漬させた状態で、前記第1流入工程及び前記第2流入工程の一方又は双方において前記口金内部側へ洗浄液を流入させた後、洗浄液を前記スリットから当該洗浄槽へ吐出する仕上げ工程を、更に含み、
この仕上げ工程では、前記洗浄槽の洗浄液に振動波を付与したまま、当該洗浄槽の洗浄液に浸漬させていた前記口金先端を、当該洗浄液の液面から離す請求項1〜3のいずれか一項に記載の口金の洗浄方法。
In a state where the tip of the base is immersed in the cleaning liquid in the cleaning tank, the cleaning liquid is allowed to flow into the base inside in one or both of the first inflow process and the second inflow process, and then the cleaning liquid is supplied from the slit. It further includes a finishing process for discharging to the washing tank,
In this finishing step, the tip of the die that has been immersed in the cleaning liquid of the cleaning tank is separated from the liquid surface of the cleaning liquid while applying a vibration wave to the cleaning liquid of the cleaning tank. The method of cleaning the base described in 1.
前記口金先端を前記洗浄槽の洗浄液に浸漬させた状態で、前記第1流入工程及び前記第2流入工程の一方又は双方において前記口金内部側へ洗浄液を流入させた後、洗浄液を前記スリットから当該洗浄槽へ吐出する仕上げ工程を、更に含み、
この仕上げ工程では、洗浄液を前記洗浄槽へ吐出している途中で、当該洗浄槽内の洗浄液への振動波の付与を停止する請求項1〜3のいずれか一項に記載の口金の洗浄方法。
In a state where the tip of the base is immersed in the cleaning liquid in the cleaning tank, the cleaning liquid is allowed to flow into the base inside in one or both of the first inflow process and the second inflow process, and then the cleaning liquid is supplied from the slit. It further includes a finishing process for discharging to the washing tank,
The method of cleaning a die according to any one of claims 1 to 3, wherein in the finishing step, the application of the vibration wave to the cleaning liquid in the cleaning tank is stopped while the cleaning liquid is being discharged to the cleaning tank. .
超音波振動子を低振動数で振動させることによって前記振動波を発生させて行った前記第1流入工程及び前記第2流入工程の後であって、再び前記第1流入工程を行う場合において、当該第1流入工程を再び行う前に、前記洗浄槽の洗浄液を少なくとも一部入れ替える入れ替え工程を、更に含む請求項1〜5のいずれか一項に記載の口金の洗浄方法。   In the case where the first inflow step is performed again after the first inflow step and the second inflow step performed by generating the vibration wave by vibrating the ultrasonic vibrator at a low frequency, The base cleaning method according to any one of claims 1 to 5, further including a replacement step of replacing at least a part of the cleaning liquid in the cleaning tank before performing the first inflow step again. 超音波振動子を低振動数で振動させることによって前記振動波を発生させている間、前記洗浄槽の洗浄液を少なくとも一部入れ替える連続的入れ替え工程を、更に含む請求項1〜6のいずれか一項に記載の口金の洗浄方法。   7. The continuous replacement step of further replacing at least part of the cleaning liquid in the cleaning tank while the vibration wave is generated by vibrating the ultrasonic vibrator at a low frequency. The method for cleaning the die according to the item.
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