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JP4818879B2 - Method for producing cold-rolled steel sheet with excellent ductility and room temperature aging resistance - Google Patents

Method for producing cold-rolled steel sheet with excellent ductility and room temperature aging resistance Download PDF

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JP4818879B2
JP4818879B2 JP2006296021A JP2006296021A JP4818879B2 JP 4818879 B2 JP4818879 B2 JP 4818879B2 JP 2006296021 A JP2006296021 A JP 2006296021A JP 2006296021 A JP2006296021 A JP 2006296021A JP 4818879 B2 JP4818879 B2 JP 4818879B2
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川田  裕之
夏子 杉浦
直紀 丸山
学 高橋
利幸 白石
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Nippon Steel Corp
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Description

本発明は、特に自動車及び家庭電気製品の材料、建材などに好適な、高い延性を有し、かつ耐常温時効性に優れた冷延鋼板の製造方法に関する。なお、本発明には、冷延鋼板の表面に更に、防錆のために、例えばZnめっきや合金化Znめっきなどの表面処理を施す製造方法も含まれる。   The present invention relates to a method for producing a cold-rolled steel sheet having high ductility and excellent room temperature aging resistance, particularly suitable for materials for automobiles and household electrical products, building materials, and the like. In addition, the present invention includes a manufacturing method in which the surface of the cold-rolled steel sheet is further subjected to surface treatment such as Zn plating or alloyed Zn plating for rust prevention.

従来、C、Nの添加量の制御、製鋼、熱延、焼鈍工程での最適化、Ti、Nbなどの炭窒化物形成元素の添加などによって軟質化し、成形性を向上させた冷延鋼板は、固溶C、固溶Nが残存していると、室温で歪時効が進行して降伏伸びが発生する。これにより、冷延鋼板にはプレス時にストレッチャーストレインと呼ばれるしわ模様が発生して表面品位を損なうという問題がある。   Conventionally, cold-rolled steel sheets that have been softened and improved in formability by control of addition amounts of C and N, steelmaking, hot rolling, optimization in annealing processes, addition of carbonitride-forming elements such as Ti and Nb, etc. When solid solution C and solid solution N remain, strain aging proceeds at room temperature and yield elongation occurs. As a result, the cold-rolled steel sheet has a problem that a wrinkle pattern called a stretcher strain is generated at the time of pressing and the surface quality is impaired.

そこで、耐常温時効性を確保するために、成分組成及び焼鈍までの製造工程を最適化して固溶C量及びN量を低減させ、更に、調質圧延によってバルク内に可動転移が導入されている。また、冷延鋼板への可動転位の導入を促進させるには、調質圧延による伸び率の増加が必要であり、これにより耐常温時効性を向上させることができる。   Therefore, in order to ensure normal temperature aging resistance, the component composition and the manufacturing process up to annealing are optimized to reduce the amount of solid solution C and N, and furthermore, a movable transition is introduced into the bulk by temper rolling. Yes. Further, in order to promote the introduction of movable dislocations in the cold-rolled steel sheet, it is necessary to increase the elongation by temper rolling, thereby improving the normal temperature aging resistance.

しかしながら、調質圧延の伸び率を増加させると、冷延鋼板の延性が劣化し、製品の成形性を損なうことがある。一方、成形性の低下を回避するために、低い伸び率での調質圧延を従来の圧延機を用いて行うと、平坦度が低下するなど、冷延鋼板の形状を損なうことがある。また、調質圧延の伸び率を低下させると、冷延鋼板の板幅方向で伸び率が不均一になり、伸び率が不十分である部位では、充分な耐常温時効性が得られない。   However, when the elongation rate of temper rolling is increased, the ductility of the cold-rolled steel sheet deteriorates and the formability of the product may be impaired. On the other hand, when temper rolling at a low elongation rate is performed using a conventional rolling mill in order to avoid a decrease in formability, the shape of the cold-rolled steel sheet may be impaired, for example, the flatness is lowered. Moreover, when the elongation rate of temper rolling is lowered, the elongation rate becomes non-uniform in the sheet width direction of the cold-rolled steel sheet, and sufficient room temperature aging resistance cannot be obtained at sites where the elongation rate is insufficient.

このため、従来では、冷延鋼板の幅方向において局所的な伸び率が最も低くなる部位でも十分な伸び率を確保できるように、調質圧延の伸び率を高めており、このことが冷延鋼板の成形性を若干低下させる原因になっていた。   For this reason, conventionally, the elongation rate of temper rolling has been increased so that sufficient elongation can be ensured even in a region where the local elongation is lowest in the width direction of the cold-rolled steel sheet. This has caused a slight decrease in the formability of the steel sheet.

これまで、板幅方向の圧下率の均一性を高める方法としては、例えば分割バックアップロールを備える軽圧下圧延機を用いた方法が提案されている(例えば、特許文献1を参照)。しかしながら、この特許文献1に記載される圧延機は、板厚5mm以上の厚鋼板の製造方法に関するものであり、また、耐常温時効性や延性等の材質に関する記載はない。
特開2002−66603号公報
Until now, as a method for improving the uniformity of the rolling reduction in the sheet width direction, for example, a method using a light rolling mill provided with a divided backup roll has been proposed (for example, see Patent Document 1). However, the rolling mill described in Patent Document 1 relates to a method of manufacturing a thick steel plate having a thickness of 5 mm or more, and there is no description regarding materials such as normal temperature aging resistance and ductility.
JP 2002-66603 A

本発明は、このような従来の事情に鑑みて提案されたものであり、形状を損なうことなく、板幅方向の材質の均質性を確保することが可能な、延性及び耐常温時効性に優れた冷延鋼板の製造方法を提供することを目的とする。   The present invention has been proposed in view of such conventional circumstances, and is excellent in ductility and room temperature aging resistance, which can ensure the homogeneity of the material in the plate width direction without impairing the shape. An object of the present invention is to provide a method for producing a cold-rolled steel sheet.

従来、鋼板の全幅において十分な耐常温時効性を持たせるために、調質圧延の伸び率は、局所的な伸び率の低下を想定して、0.8%以上が必要とされており、そのため、成形性の劣化を避けることが困難であった。そこで、本発明は、固溶C、固溶Nの量を制限した軟質の冷延鋼板を、分割バックアップロールでワークロールを支持した圧延機により、伸び率を低下させた調質圧延を行うことによって、形状及び板幅方向の材質の均質性を損なうことなく、延性及び耐常温時効性に優れた冷延鋼板を製造することを可能した方法であり、その要旨は以下のとおりである。   Conventionally, in order to have sufficient room temperature aging resistance in the full width of the steel sheet, the elongation rate of temper rolling is required to be 0.8% or more, assuming a decrease in the local elongation rate, Therefore, it has been difficult to avoid deterioration of moldability. Therefore, the present invention performs temper rolling of a soft cold-rolled steel sheet in which the amount of solute C and solute N is limited by a rolling mill that supports a work roll with a divided backup roll, with a reduced elongation rate. Thus, it is possible to produce a cold-rolled steel sheet having excellent ductility and room temperature aging resistance without impairing the homogeneity of the shape and the material in the sheet width direction, and the gist thereof is as follows.

(1) 上下のロールアセンブリーの一方又は双方が、軸方向に3以上に分割された分割バックアップロールによってワークロールを支持する支持機構を有し、前記分割バックアップロールのそれぞれに負荷される荷重を検出する荷重検出装置と前記分割バックアップロールを独立して昇降させる圧下装置を設けた圧延機により、固溶C量と固溶N量の一方又は双方の合計が0.0010%未満であり、板厚が0.3〜2.0mm、板幅が600〜2000mmである冷延鋼鈑に対して、板幅方向での伸び率が均一となるように、所定の伸び率を得るために必要な圧延荷重を計算した後、板幅方向の部位毎の圧延荷重を検出し、この部位毎の圧延荷重をコントロールしながら、伸び率が0.1以上0.8%未満の調質圧延を施すことを特徴とする延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。 (1) One or both of the upper and lower roll assemblies have a support mechanism that supports a work roll by a divided backup roll divided into three or more in the axial direction, and a load applied to each of the divided backup rolls. A rolling mill provided with a load detection device to detect and a reduction device that raises and lowers the divided backup roll independently, the total of one or both of the solid solution C amount and the solid solution N amount is less than 0.0010%, thickness 0.3 to 2.0 mm, for the cold-rolled steel sheet strip width is 600~2000Mm, like elongation in the plate width direction becomes uniform, required to obtain a given elongation After calculating the rolling load, the rolling load for each part in the sheet width direction is detected, and the temper rolling with an elongation of 0.1 or more and less than 0.8% is performed while controlling the rolling load for each part. Features A method for producing cold-rolled steel sheets with excellent ductility and room temperature aging resistance.

(2) 冷延鋼板の成分組成が、質量%で、
C:0.0010%未満、
Si:1.00%以下、
Mn:3.00%以下、
P:0.100%以下、
S:0.100%以下、
Al:1.000%以下、
N:0.0010%未満を含有し、残部がFe及び不可避的不純物からなり、
前記CとNの含有量の合計が0.0010%未満であることを特徴とする前記(1)に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。
(2) The component composition of the cold rolled steel sheet is mass%,
C: less than 0.0010%,
Si: 1.00% or less,
Mn: 3.00% or less,
P: 0.100% or less,
S: 0.100% or less,
Al: 1.000% or less,
N: containing less than 0.0010%, the balance consisting of Fe and inevitable impurities,
The total content of C and N is less than 0.0010%, The method for producing a cold-rolled steel plate having excellent ductility and room temperature aging resistance as described in (1) above.

(3) 冷延鋼板の成分組成が、質量%で、
C:0.0500%以下、
Si:1.00%以下、
Mn:3.00%以下、
P:0.100%以下、
S:0.100%以下、
Al:1.000%以下、
N:0.0500%以下を含有し、残部がFe及び不可避的不純物からなり、
更に、質量%で、
Nb:0.001〜0.150%、
Ti:0.001〜0.150%
の一方又は双方を含有し、
前記C、N、Ti及びNbの含有量が、
1/4Ti+1/8Nb≧C+N−0.0010
の関係を満たすことを特徴とする前記(1)に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。
(3) The component composition of the cold-rolled steel sheet is mass%,
C: 0.0500% or less,
Si: 1.00% or less,
Mn: 3.00% or less,
P: 0.100% or less,
S: 0.100% or less,
Al: 1.000% or less,
N: 0.0500% or less, the balance is made of Fe and inevitable impurities,
Furthermore, in mass%,
Nb: 0.001 to 0.150%,
Ti: 0.001 to 0.150%
One or both of
The content of C, N, Ti and Nb is
1 / 4Ti + 1 / 8Nb ≧ C + N−0.0010
The manufacturing method of the cold-rolled steel plate excellent in ductility and normal temperature aging resistance as described in said (1) characterized by satisfy | filling the relationship of these.

(4) 前記ワークロールの表面粗さRaが0.2μm以上であることを特徴とする前記(1)〜(3)の何れか1項に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。 (4) The surface roughness Ra of the work roll is 0.2 μm or more, and cold rolling excellent in ductility and normal temperature aging resistance according to any one of (1) to (3) above Steel plate manufacturing method.

(5) 前記調質圧延前の冷延鋼板の表面にめっきを施すことを特徴とする前記(1)〜(4)の何れか1項に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。 (5) Cold rolling excellent in ductility and normal temperature aging resistance according to any one of (1) to (4), wherein the surface of the cold rolled steel sheet before temper rolling is plated. Steel plate manufacturing method.

以上のように、本発明によれば、平坦度等の形状を損なうことなく、局所的な表面品位の劣化も抑制した、延性及び耐常温時効性に優れた、軟質の冷延鋼板を製造することができる。また、鋼種によっては、生産性の低下の要因となっていた成分及び製造条件に対する規制を緩和できることができるなど、産業上の貢献が顕著である。   As described above, according to the present invention, a soft cold-rolled steel sheet excellent in ductility and room temperature aging resistance is produced, which suppresses local surface quality deterioration without impairing the shape such as flatness. be able to. Further, depending on the steel type, the industrial contribution is remarkable, such as the restriction on the components and production conditions that have been the cause of the decrease in productivity can be relaxed.

以下、本発明の実施の形態について、図面を参照しながら詳細に説明する。
本発明の圧延機は、上下の少なくとも何れか一方のロールアセンブリーが、軸方向に3以上に分割された分割バックアップロールによってワークロールを支持する支持機構を有し、各分割バックアップロールに負荷される荷重を検出する独立した荷重検出装置と、各分割バックアップロールを個別に昇降させる独立した圧下装置とが配置された構成となっている。
Hereinafter, embodiments of the present invention will be described in detail with reference to the drawings.
The rolling mill of the present invention has a support mechanism in which at least one of the upper and lower roll assemblies supports a work roll by a divided backup roll divided into three or more in the axial direction, and is loaded on each divided backup roll. An independent load detection device that detects the load to be detected and an independent reduction device that raises and lowers each divided backup roll individually are arranged.

この分割バックアップロールの採用により、低い伸び率で調質圧延を行っても板幅方向の伸び率が均一となる。なお、本発明の調質圧延では、板厚の変化が小さいため、圧延方向の長さの変化率、すなわち伸び率を規定する。   By employing this divided backup roll, the elongation in the sheet width direction becomes uniform even when temper rolling is performed at a low elongation. In the temper rolling of the present invention, since the change in the plate thickness is small, the rate of change in the length in the rolling direction, that is, the elongation rate is specified.

本発明の圧延機によって、固溶C量、固溶N量が制御された、焼鈍後の冷延鋼板に伸び率の低い調質圧延を施すと、形状を損なうことなく、延性及び常温での耐時効性に優れる冷延鋼板を製造方法することができる。   When the temper rolling with low elongation rate is performed on the cold-rolled steel sheet after annealing, in which the amount of solute C and the amount of solute N are controlled by the rolling mill of the present invention, the ductility and the room temperature are not impaired without damaging the shape A cold-rolled steel sheet having excellent aging resistance can be produced.

本発明の圧延機は、図1に示すように、電動モータによるパスライン調整機1及び油圧圧下を用いた主圧下装置2で上下する上下のインナーハウジング内に、分割バックアップロール3、4によって支持される上下のワークロール5を有するものである。なお、パスライン調整機1は、ロール交換した際のロール径の変化に対応してパスラインを調整する装置である。また、主圧下装置2は、油圧シリンダーの位置を検出する機構を有し、これにより圧下位置が測定される。   As shown in FIG. 1, the rolling mill of the present invention is supported by split backup rolls 3 and 4 in upper and lower inner housings that move up and down by a pass line adjuster 1 using an electric motor and a main reduction device 2 using hydraulic reduction. The upper and lower work rolls 5 are provided. The pass line adjuster 1 is a device that adjusts the pass line in response to a change in roll diameter when the roll is replaced. Further, the main reduction device 2 has a mechanism for detecting the position of the hydraulic cylinder, whereby the reduction position is measured.

更に、上下のワークロール5は、図2に示すように、軸方向に分割された分割バックアップロール3a〜3d、4a〜4eによって支持される。また、各々の分割バックアップロール3a〜3d、4a〜4eのそれぞれに独立に負荷される荷重を検出する荷重検出装置と、各々の分割バックアップロール3a〜3d、4a〜4eを独立に昇降させる圧下機構及び各分割バックアップロールの位置を検出する位置検出機構を備えている。なお、図示はしていないが、上下のワークロール5は、駆動モータによって回転され、圧延に必要なトルクが伝達されている。さらに、インナーハウジング内には、ワークロール5の交換に使用されるワークロールチョックが設けられている。   Furthermore, as shown in FIG. 2, the upper and lower work rolls 5 are supported by the divided backup rolls 3a to 3d and 4a to 4e divided in the axial direction. In addition, a load detection device that detects a load that is independently applied to each of the divided backup rolls 3a to 3d and 4a to 4e, and a reduction mechanism that moves the divided backup rolls 3a to 3d and 4a to 4e independently And a position detection mechanism for detecting the position of each divided backup roll. Although not shown, the upper and lower work rolls 5 are rotated by a drive motor to transmit torque necessary for rolling. Furthermore, a work roll chock used for replacing the work roll 5 is provided in the inner housing.

本発明者らは、図1及び2に示す圧延機により、焼付硬化性冷延鋼板の調質圧延を施し、調質圧延の伸び率と、延性及び耐時効硬化性との関係を調査した。
先ず、質量%で、固溶C量及び固溶N量との合計が0.0010%未満になるように、C:0.0005〜0.0500%、Si:1.00%以下、Mn:3.00%以下、P:0.100%以下、S:0.100%以下、Al:1.000%以下、N:0.1000%以下、必要に応じて、Nb:0.001〜0.150%、Ti:0.001〜0.150%の一方又は双方を、1/4Ti+1/8Nb≧C+N−0.0010の関係を満足するように含有し、残部がFe及び不可避的不純物からなる鋼を溶製して鋳造した。
The present inventors performed temper rolling of a bake-hardening cold-rolled steel sheet using the rolling mill shown in FIGS. 1 and 2, and investigated the relationship between the elongation rate of temper rolling, ductility and age-hardening resistance.
First, C: 0.0005 to 0.0500%, Si: 1.00% or less, Mn: so that the total of the solid solution C amount and the solid solution N amount is less than 0.0010% by mass%. 3.00% or less, P: 0.100% or less, S: 0.100% or less, Al: 1.000% or less, N: 0.1000% or less, Nb: 0.001 to 0 as necessary 150%, Ti: 0.001 to 0.150% or both are contained so as to satisfy the relationship of 1 / 4Ti + 1 / 8Nb ≧ C + N−0.0010, with the balance being Fe and inevitable impurities Steel was melted and cast.

得られた鋼片を熱間圧延、冷間圧延して、板厚0.8mmの冷延鋼板とした。冷延鋼板の焼鈍は、焼鈍温度を750〜850℃の範囲内、焼鈍時間を40〜100秒の範囲内とし、冷却速度を60〜120℃/秒の範囲内として行い、調整した。   The obtained steel slab was hot-rolled and cold-rolled to obtain a cold-rolled steel plate having a thickness of 0.8 mm. The cold-rolled steel sheet was annealed by adjusting the annealing temperature within the range of 750 to 850 ° C., the annealing time within the range of 40 to 100 seconds, and the cooling rate within the range of 60 to 120 ° C./second.

次に、これらの鋼板に図1及び図2に示した圧延機により、伸び率0.3%の調質圧延を施した。また、比較例として分割されていないバックアップロールからなる通常の軽圧下圧延機を用いて伸び率0.3%及び1.4%の調質圧延を施した。これらの冷延鋼板から、板幅100mm毎に圧延方向を長手方向としてJIS Z 2201の5号試験片を作製した。なお、調質圧延後、1週間以内に引張試験片を作製し、引張試験を実施するまで、引張試験片を−40℃で保管した。   Next, these steel sheets were subjected to temper rolling with an elongation of 0.3% by the rolling mill shown in FIGS. Further, as a comparative example, temper rolling with an elongation of 0.3% and 1.4% was performed using a normal light rolling mill composed of backup rolls that were not divided. From these cold-rolled steel plates, No. 5 test pieces of JIS Z 2201 were produced with the rolling direction as the longitudinal direction for every 100 mm of plate width. In addition, the tensile test piece was produced within one week after the temper rolling, and the tensile test piece was stored at −40 ° C. until the tensile test was performed.

これらの引張試験片を用いて、JIS Z 2241に準拠して引張試験を行い、降伏伸び及び全伸びを測定した。更に、降伏伸びの測定については、25℃の恒温室に30、60、90日保持した後にも行い、0.2%以上の顕著な降伏伸びが観察された最小の日数を耐常温時効性の指標とした。なお、90日保持後の試験においても降伏伸びが現れない場合に充分な耐室温時効性が得られたものとする。   Using these tensile test pieces, a tensile test was performed in accordance with JIS Z 2241, and the yield elongation and total elongation were measured. Furthermore, the measurement of the yield elongation is performed after holding in a constant temperature room at 25 ° C. for 30, 60, 90 days, and the minimum number of days in which a remarkable yield elongation of 0.2% or more is observed is determined at room temperature aging resistance. It was used as an index. In addition, it is assumed that sufficient room temperature aging resistance is obtained when yield elongation does not appear in the test after 90 days.

調質圧延後に25℃で保持することなく引張試験を行って測定した全伸びを図3に示す。また、耐常温時効性を評価した結果を図4に示す。
図3及び図4から、本発明に従って製造した鋼板は従来の調質圧延と比較してより高い延性を保ちつつ、優れた耐常温時効性を示すことが分かる。
FIG. 3 shows the total elongation measured by conducting a tensile test without holding at 25 ° C. after temper rolling. Moreover, the result of having evaluated normal temperature aging resistance is shown in FIG.
3 and 4, it can be seen that the steel sheet produced according to the present invention exhibits excellent normal temperature aging resistance while maintaining higher ductility than conventional temper rolling.

以下、本発明の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法について詳細に説明する。
まず、本発明において最も重要な工程である調質圧延に関する限定理由を述べる。
Hereinafter, the manufacturing method of the cold rolled steel plate excellent in ductility and room temperature aging resistance of the present invention will be described in detail.
First, the reason for limitation related to temper rolling, which is the most important process in the present invention, will be described.

(圧延機)
通常の調質圧延機では、伸び率を低下させて調質圧延を施すと、板幅方向で伸び率が不均一となる。特に、鋼板の端部では調質圧延の伸び率が不十分となり、耐常温時効性が確保できない。そのため、本発明では、板幅方向の部位によって鋼板の伸び率を適宜調整し得る機構を有する、上述した圧延機により、調質圧延を行う。
本発明の圧延機は、バックアップロールを板幅方向に分割させて、各分割バックアップロールを独立に制御するものである。すなわち、所定の伸び率を得るために必要な圧延荷重を計算した後、板幅方向の部位毎の圧延荷重を検出し、独立に設けられた圧下装置によって圧延荷重をコントロールする。これにより、調質圧延における伸び率が低い場合でも、板幅方向での伸び率を均一とすることができる。
(Rolling mill)
In an ordinary temper rolling mill, when temper rolling is performed with the elongation rate lowered, the elongation rate becomes non-uniform in the sheet width direction. In particular, the elongation of temper rolling becomes insufficient at the end of the steel sheet, and room temperature aging resistance cannot be ensured. Therefore, in the present invention, the temper rolling is performed by the above-described rolling mill having a mechanism capable of appropriately adjusting the elongation of the steel sheet depending on the portion in the sheet width direction.
The rolling mill of the present invention divides a backup roll in the plate width direction and controls each divided backup roll independently. That is, after calculating the rolling load necessary to obtain a predetermined elongation, the rolling load for each part in the sheet width direction is detected, and the rolling load is controlled by a separately provided reduction device. Thereby, even when the elongation rate in temper rolling is low, the elongation rate in the sheet width direction can be made uniform.

(伸び率:0.1%以上0.8%未満)
本発明の圧延機を用いても、伸び率が0.1%未満になると、形状矯正の目的が達成できなくなる。このため、伸び率の下限は0.1%以上とする。また、伸び率が0.8%以上となると、冷延鋼板の延性が低下し、また、耐力が原板と比べて大きくなるため加工性が低下することから、伸び率の上限は0.8%未満とする。好ましくは0.6%未満、さらに好ましくは0.5%未満とする。
(Elongation: 0.1% or more and less than 0.8%)
Even if the rolling mill of the present invention is used, if the elongation is less than 0.1%, the purpose of shape correction cannot be achieved. For this reason, the minimum of elongation is made into 0.1% or more. Further, when the elongation is 0.8% or more, the ductility of the cold-rolled steel sheet is lowered, and the workability is lowered because the proof stress is larger than that of the original sheet, so the upper limit of the elongation is 0.8%. Less than. Preferably it is less than 0.6%, more preferably less than 0.5%.

(ワークロールの直径:30〜1000mm)
調質圧延のワークロールの直径は特に規定しないが、30mm未満になると、圧延の制御が困難になり長手方向での均一な圧下率の確保が難しくなることがある。そのため、ワークロールの直径の下限は30mmとすることが好ましい。また、調質圧延のワークロールの直径が1000mmを超えると、例えば、軸方向の両端への荷重を大きくしても撓み量が小さくなり、部位による伸び率の制御が難しくなるため、上限は1000mm以下とすることが好ましい。また、板厚方向に対して変形が均一に進行させ、表層への歪みの集中による成形性の低下を防ぐには、ワークロールの直径は300mm超であることが好ましく、低い伸び率での形状の確保には、上限を800mm以下とすることが好ましい。一方、直径が30〜300mmの小径のワークロールを採用すると、冷延鋼板の表層に可動転位が導入されるため、耐時効性の確保が確実になる。
(Work roll diameter: 30-1000 mm)
The diameter of the work roll for temper rolling is not particularly defined, but if it is less than 30 mm, it may be difficult to control the rolling, and it may be difficult to ensure a uniform rolling reduction in the longitudinal direction. Therefore, the lower limit of the diameter of the work roll is preferably 30 mm. Further, when the diameter of the work roll for temper rolling exceeds 1000 mm, for example, even if the load on both ends in the axial direction is increased, the amount of bending becomes small, and it becomes difficult to control the elongation rate by the part, so the upper limit is 1000 mm. The following is preferable. Further, in order to cause the deformation to progress uniformly in the plate thickness direction and prevent deterioration of formability due to concentration of strain on the surface layer, the diameter of the work roll is preferably more than 300 mm, and the shape with a low elongation rate In order to ensure this, the upper limit is preferably set to 800 mm or less. On the other hand, when a small-diameter work roll having a diameter of 30 to 300 mm is adopted, movable dislocations are introduced into the surface layer of the cold-rolled steel sheet, so that aging resistance is ensured.

(ワークロールの表面粗さRa:0.2〜3.0μm)
調質圧延のワークロールの表面粗さRaを大きくすることで、ワークロールと冷延鋼板の表面との摩擦係数が大きくなり、負荷される荷重が局所的に低くなった部位においても、滑ることがなくなり、形状が良好になる。また、冷延鋼板の表層への可動転位の導入が促進されることから、表面粗さRaの大きなワークロールを用いて調質圧延を施すことが好ましい。この効果を得るためには、表面粗さRaを0.2μm以上とすることが好ましい。表面粗さRaの上限は特に設けないが、冷延鋼板の表面品位など、実用性の観点から、3.0μm以下とすることが好ましい。
(Work roll surface roughness Ra: 0.2 to 3.0 μm)
By increasing the surface roughness Ra of the temper rolled work roll, the coefficient of friction between the work roll and the surface of the cold-rolled steel sheet increases, and even in a region where the applied load is locally lowered, it slides. Disappears and the shape becomes good. Moreover, since introduction of movable dislocations into the surface layer of the cold-rolled steel sheet is promoted, it is preferable to perform temper rolling using a work roll having a large surface roughness Ra. In order to obtain this effect, the surface roughness Ra is preferably set to 0.2 μm or more. The upper limit of the surface roughness Ra is not particularly provided, but is preferably 3.0 μm or less from the viewpoint of practicality such as the surface quality of the cold-rolled steel sheet.

次に、化学成分の限定理由について説明する。
(固溶C及び固溶N:合計0.0010%未満)
耐常温時効性を得るには製品の状態での固溶C、固溶Nの残存量を制御することが重要である。固溶C量と固溶N量の一方又は双方の合計が0.0010%以上になると、本発明の調質圧延を施しても耐常温時効性を確保することができない。したがって、固溶Cと固溶Nの一方又は双方の合計の上限を0.0010%未満とする。また、延性を向上させるために調質圧延の伸び率を低くしても、優れた耐常温非時効性を得るためには、固溶C量と固溶N量の一方又は双方の合計を0.0008%未満とすることが好ましく、更に、直径の大きいワークロールを使用する場合には、0.0005%以下とすることが好ましい。
Next, the reason for limiting the chemical components will be described.
(Solution C and Solution N: Total less than 0.0010%)
In order to obtain normal temperature aging resistance, it is important to control the residual amount of solute C and solute N in the product state. When the total of one or both of the solid solution C amount and the solid solution N amount is 0.0010% or more, normal temperature aging resistance cannot be ensured even if the temper rolling of the present invention is performed. Therefore, the upper limit of the total of one or both of the solid solution C and the solid solution N is set to less than 0.0010%. Moreover, even if the elongation rate of temper rolling is lowered to improve ductility, in order to obtain excellent room temperature non-aging resistance, the total of one or both of the solid solution C amount and the solid solution N amount is reduced to 0. It is preferable that the content be less than .0008%, and when a work roll having a large diameter is used, the content is preferably 0.0005% or less.

固溶N量は、JIS A 5523の付属書に記載されている鋼−窒化物型窒素定量方法に準じて、ろ液を分析することにより求めることができる。固溶C量については電解抽出法により、析出物を採取後のろ液を直接分析するか、あるいは全C量と電解抽出法により採取した析出物中のC量を定量し、その差により評価しても構わない。不溶解残さをろ過するフィルターとしてはAgを使用するのが好適である。   The amount of solute N can be determined by analyzing the filtrate according to the steel-nitride type nitrogen determination method described in the appendix of JIS A 5523. For the amount of dissolved C, the filtrate after collecting the precipitate is directly analyzed by electrolytic extraction, or the amount of C in the precipitate collected by electrolytic extraction is quantified and evaluated by the difference. It doesn't matter. Ag is preferably used as a filter for filtering insoluble residue.

(C:0.0010%未満)
Cは、鋼中に不可避的に含有される元素であり、Ti、Nbを含有しない場合には、C量が0.0010%以上になると、固溶C量が増加して、耐常温時効性が劣化するため、0.0010%未満を上限とすることが好ましい。
(C: less than 0.0010%)
C is an element inevitably contained in the steel. When Ti and Nb are not contained, when the C content is 0.0010% or more, the amount of dissolved C increases and normal temperature aging resistance is increased. Therefore, the upper limit is preferably less than 0.0010%.

(N:0.0010%未満)
Nは、鋼中に不可避的に含有される元素であり、N量が0.0010%以上になると固溶N量が増加し、耐常温時効性が低下するため、0.0010%未満を上限とすることが好ましい。
(N: less than 0.0010%)
N is an element inevitably contained in the steel, and when the N amount is 0.0010% or more, the amount of dissolved N increases and the normal temperature aging resistance decreases, so the upper limit is less than 0.0010%. It is preferable that

(Si:1.00%以下)
(Mn:3.00%以下)
(P:0.100%以下)
Si、Mn、Pは、鋼中に不可避的に含有される元素であり、強度を向上させる効果を有するが、含有量が過剰であると加工性を損なうため、上限をそれぞれ、Si:1.00%以下、Mn:3.00%以下、P:0.100%以下とすることが好ましい。強度を低下させて延性を向上させるには、Si、Mn、Pの上限をそれぞれ、0.500%以下、1.000%以下、0.050%以下とすることが好ましい。
(Si: 1.00% or less)
(Mn: 3.00% or less)
(P: 0.100% or less)
Si, Mn, and P are elements inevitably contained in the steel and have the effect of improving the strength. However, if the content is excessive, the workability is impaired, so the upper limit is Si: 1. 00% or less, Mn: 3.00% or less, and P: 0.100% or less are preferable. In order to decrease the strength and improve the ductility, it is preferable that the upper limits of Si, Mn, and P are 0.500% or less, 1.000% or less, and 0.050% or less, respectively.

(Al:1.000%以下)
Alは、脱酸剤であり、強度の向上にも寄与するが、1.000%を超えて添加すると加工性が劣化するため、1.000%以下を上限とすることが好ましい。特に延性を向上させるには、Alの上限を0.100%以下とすることが好ましい。
(Al: 1.000% or less)
Al is a deoxidizer and contributes to the improvement of strength. However, if it exceeds 1.000%, the workability deteriorates, so it is preferable that the upper limit is 1.000% or less. In particular, in order to improve ductility, the upper limit of Al is preferably 0.100% or less.

(S:0.100%以下)
Sは、不純物であり、加工性を劣化させるので低減させることが好ましい。0.100%を超えて添加すると延性が大きく劣化するため、0.100%以下を上限とすることが好ましい。
(S: 0.100% or less)
Since S is an impurity and deteriorates workability, it is preferably reduced. If added over 0.100%, the ductility is greatly deteriorated, so the upper limit is preferably made 0.100% or less.

(Nb:0.001〜0.150%)
(Ti:0.001〜0.150%)
Nb及びTiは、炭化物及び窒化物を形成する元素である。そのため、C、Nの含有量を多くする場合には、固溶C量、固溶N量を制御するためにNb、Tiの一方又は双方を添加してもよい。ただし、Nb、Tiの添加量がそれぞれ、0.001%未満では添加による効果が顕著には認められず、0.150%を超えて添加すると再結晶温度が上昇し、材質が劣化することがある。そのため、Nb、Tiの添加量はそれぞれ、0.001〜0.150%とすることが好ましい。
(Nb: 0.001 to 0.150%)
(Ti: 0.001 to 0.150%)
Nb and Ti are elements that form carbides and nitrides. Therefore, when increasing the content of C and N, one or both of Nb and Ti may be added to control the amount of dissolved C and the amount of dissolved N. However, if the addition amount of Nb and Ti is less than 0.001%, the effect by addition is not recognized remarkably. If the addition amount exceeds 0.150%, the recrystallization temperature rises and the material deteriorates. is there. Therefore, the addition amount of Nb and Ti is preferably 0.001 to 0.150%, respectively.

Nb、Tiの一方又は双方を含有させる場合には、C量、N量を多くすることが可能である。しかし、C量、N量が、それぞれ、0.0500%を超えると、固溶C量、固溶N量が増加して、耐常温時効性が劣化することがある。したがって、C量の上限、N量の上限を、それぞれ、0.0500%とする。Cを0.0005%未満とするためには製造コストが大きくなることから、Cの下限は0.0005%とすることが好ましい。N量の上限は、調質圧延の伸び率を低下させても耐常温時効性を確保するには、0.0100%以下とすることが好ましい。   When one or both of Nb and Ti are contained, the amount of C and the amount of N can be increased. However, if the amount of C and the amount of N exceed 0.0500%, respectively, the amount of solute C and the amount of solute N may increase and the normal temperature aging resistance may deteriorate. Therefore, the upper limit of the C amount and the upper limit of the N amount are 0.0500%, respectively. In order to make C less than 0.0005%, the manufacturing cost increases, so the lower limit of C is preferably made 0.0005%. The upper limit of the N amount is preferably set to 0.0100% or less in order to ensure normal temperature aging resistance even if the elongation of temper rolling is reduced.

また、Nb、TiとC、Nとの関係は、固溶Cと固溶Nの制御の観点から、以下の関係式(1)を満たすことが好ましい。
1/4Ti+1/8Nb≧C+N−0.0010 …(1)
ここで、式(1)中、Ti、Nb、C及びNは、各元素の含有量[質量%]であり、Ti、Nbの含有量が0.001%未満である場合は、0として左辺を計算する。
The relationship between Nb and Ti and C and N preferably satisfies the following relational expression (1) from the viewpoint of controlling the solute C and the solute N.
1 / 4Ti + 1 / 8Nb ≧ C + N−0.0010 (1)
Here, in the formula (1), Ti, Nb, C, and N are the contents [% by mass] of each element. When the contents of Ti and Nb are less than 0.001%, the left side is set to 0. Calculate

更に、Ti、Nbの含有量が0.100%超になると、析出物の量が多くなり、延性を損なうことがあるため、それぞれ、上限を0.100%とすることが好ましい。また、この場合は、固溶Cと固溶Nの制御の観点から、C量の上限、N量の上限を、それぞれ、0.0135%とすることが好ましい。   Furthermore, when the content of Ti and Nb exceeds 0.100%, the amount of precipitates increases and the ductility may be impaired. Therefore, the upper limit is preferably set to 0.100%. Further, in this case, from the viewpoint of controlling the solid solution C and the solid solution N, it is preferable that the upper limit of the C amount and the upper limit of the N amount be 0.0135%, respectively.

また、炭窒化物を形成する元素である、B、Mo、Cr、V、Wをそれぞれ0.001〜0.100%含有してもよい。   Moreover, you may contain 0.001-0.100% of B, Mo, Cr, V, and W which are the elements which form a carbonitride, respectively.

上記成分を得るための原料は特に限定しないが、鉄鉱石を原料として、高炉、転炉により成分を調整する方法以外に、スクラップを原料としてもよいし、これを電炉で溶製してもよい。スクラップを原料の全部又は一部として使用する際には、Cu、Ni、Sn、Sb、Zn、Pb等の元素を含んでもよい。   The raw materials for obtaining the above components are not particularly limited, but in addition to the method of adjusting the components by iron ore as a raw material and using a blast furnace and a converter, scrap may be used as a raw material, or this may be melted in an electric furnace. . When scrap is used as all or part of the raw material, elements such as Cu, Ni, Sn, Sb, Zn, Pb may be included.

調質圧延より前の冷延鋼板の製造方法については常法でよく、鋼を溶製、鋳造し、熱間圧延、酸洗、冷間圧延、焼鈍を施して冷延鋼板とすればよい。更に、めっきなどの表面処理を施してもよい。熱間圧延に供する鋼片は特に限定せず、連続鋳造されたスラブ、薄スラブキャスターで製造したものでもよい。また、鋳造後に直ちに熱間圧延を行う、連続鋳造―直接圧延(CC−DR)のようなプロセスにも適合する。   The manufacturing method of the cold-rolled steel sheet before the temper rolling may be a conventional method, and the steel may be melted and cast, and hot-rolled, pickled, cold-rolled, and annealed to obtain a cold-rolled steel sheet. Furthermore, surface treatment such as plating may be performed. The steel slab used for hot rolling is not particularly limited, and it may be manufactured by a continuously cast slab or a thin slab caster. It is also suitable for processes such as continuous casting-direct rolling (CC-DR) in which hot rolling is performed immediately after casting.

熱間圧延の仕上温度は、鋼板の異方性を低減させるために、Ar3変態点より高いことが好ましい。また、熱間圧延については、粗圧延後の鋼片を接合し、仕上圧延を行う、連続熱延プロセスを採用してもよい。更に、連続熱延プロセスでは、仕上圧延をフェライト域で行ってもよい。
熱間圧延における巻取りは、炭化物及び窒化物の生成により固溶C及び固溶N量を低下させるため、600℃以上で行うことが好ましく、さらに好ましい温度は650℃以上である。
冷間圧延率は、生産性の観点から、50〜90%が好ましい。
焼鈍温度は、延性を確保するために再結晶温度以上で行うことが好ましく、製造設備による制約、生産性の観点から、950℃以下が好ましい。また、焼鈍時に炭化物及び析出物が溶解することにより固溶C及び固溶Nが増加することを避けるため、焼鈍温度は850℃以下とすることが好ましい。
In order to reduce the anisotropy of the steel sheet, the hot rolling finishing temperature is preferably higher than the Ar3 transformation point. Moreover, about hot rolling, you may employ | adopt the continuous hot rolling process which joins the steel piece after rough rolling, and performs finish rolling. Further, in the continuous hot rolling process, finish rolling may be performed in the ferrite region.
The winding in the hot rolling is preferably performed at 600 ° C. or higher, and more preferably 650 ° C. or higher, in order to reduce the amount of solid solution C and solid solution N due to the formation of carbides and nitrides.
The cold rolling rate is preferably 50 to 90% from the viewpoint of productivity.
The annealing temperature is preferably higher than the recrystallization temperature in order to ensure ductility, and is preferably 950 ° C. or lower from the viewpoints of restrictions due to manufacturing equipment and productivity. Moreover, in order to avoid that solid solution C and solid solution N increase by a carbide | carbonized_material and precipitate melt | dissolving at the time of annealing, it is preferable that an annealing temperature shall be 850 degrees C or less.

以下、実施例を挙げて本発明をより具体的に説明するが、本発明は、下記実施例に限定されるものではなく、本発明の趣旨に適合し得る範囲で適宜変更を加えて実施することも可能であり、それらは何れも本発明の技術的範囲に含まれる。   EXAMPLES Hereinafter, the present invention will be described more specifically with reference to examples. However, the present invention is not limited to the following examples, and is implemented with appropriate modifications within a scope that can meet the gist of the present invention. These are all included in the technical scope of the present invention.

(実施例1)
実施例1では、表1に示す化学成分を有する鋼を溶製して鋳造し、鋼片を熱間圧延、冷間圧延して、板厚0.8mmの冷延鋼板とした。表1のNb及びTiの空欄は、分析値が0.001%未満であったことを意味する。そのため、鋼No.A〜Gの(Ti/4+Nb/8)−(C+N−0.001)は、空欄である元素の数値を0として計算した。なお、鋼No.HはTi及びNbの双方の分析値が0.001%未満であるため、(Ti/4+Nb/8)−(C+N−0.001)は「−」を示した。
Example 1
In Example 1, steel having chemical components shown in Table 1 was melted and cast, and a steel piece was hot-rolled and cold-rolled to obtain a cold-rolled steel plate having a thickness of 0.8 mm. The blanks for Nb and Ti in Table 1 mean that the analytical value was less than 0.001%. Therefore, Steel No. In (Ti / 4 + Nb / 8) − (C + N−0.001) of A to G, the numerical value of the blank element was calculated as 0. Steel No. Since H has analytical values of both Ti and Nb of less than 0.001%, (Ti / 4 + Nb / 8) − (C + N−0.001) indicates “−”.

Figure 0004818879
Figure 0004818879

表1の鋼No.A〜Hの冷延鋼板の焼鈍は、焼鈍温度を750〜850℃の範囲内、焼鈍時間を40〜100秒の範囲内とし、冷却速度を60〜120℃/秒の範囲内として行い、固溶C量及び固溶N量を調整した。固溶C量は電解抽出法により、析出物を採取後のろ液を直接分析して評価した。固溶N量は、JIS A 5523の付属書に記載されている鋼−窒化物型窒素定量方法に準じて、ろ液を分析することにより求めた。   Steel No. 1 in Table 1 Annealing of the cold rolled steel sheets A to H is performed with the annealing temperature in the range of 750 to 850 ° C., the annealing time in the range of 40 to 100 seconds, and the cooling rate in the range of 60 to 120 ° C./second. The amount of dissolved C and the amount of dissolved N were adjusted. The amount of dissolved C was evaluated by directly analyzing the filtrate after collecting the precipitate by electrolytic extraction. The amount of solute N was determined by analyzing the filtrate according to the steel-nitride type nitrogen determination method described in the appendix of JIS A 5523.

表1の鋼No.Iの冷延鋼板の焼鈍は、鋼板温度が960℃に到達した後、60℃/秒で冷却したため、固溶C量及び固溶N量が本発明の範囲よりも多くなった例である。   Steel No. 1 in Table 1 Annealing of the cold-rolled steel sheet I is an example in which the amount of solute C and the amount of solute N are larger than the range of the present invention because the steel sheet temperature is 960 ° C. and then cooled at 60 ° C./second.

これらの鋼板に対して図1及び2に示した圧延機にて種々の伸び率の調質圧延を施した。なお、直径500mm、胴長2070mmのワークロールが、軸方向に9分割された直径550mm、胴長230mmの分割バックアップロールにより支持されている。   These steel sheets were subjected to temper rolling with various elongation rates using the rolling mill shown in FIGS. A work roll having a diameter of 500 mm and a cylinder length of 2070 mm is supported by a divided backup roll having a diameter of 550 mm and a cylinder length of 230 mm divided into nine in the axial direction.

Figure 0004818879
Figure 0004818879

調質圧延の条件及び機械的性質を表2に示す。JIS Z 2201の5号試験片は圧延方向を長手とし、板幅方向の採取位置は、端部、中央部及びその中間である1/4部とした。なお、引張試験片は、調質圧延後、1週間以内にし、引張試験を実施するまで−40℃で保管した。表2中の降伏応力、引張応力、全伸びは端部、中央部及び1/4部の3ヶ所での試験結果の平均を表し、全伸びについては、端部、中央部及び1/4部の3ヶ所での最大値と最小値の差を求め、ΔELとして示した。   Table 2 shows the conditions and mechanical properties of temper rolling. The No. 5 test piece of JIS Z 2201 had the rolling direction as the longitudinal direction, and the sampling position in the plate width direction was the end part, the central part, and a quarter part that was in the middle. In addition, the tensile test piece was stored within −1 week after temper rolling and stored at −40 ° C. until the tensile test was performed. The yield stress, tensile stress, and total elongation in Table 2 represent the average of the test results at the end, center, and 1/4 part. For the total elongation, the end, center, and 1/4 part. The difference between the maximum value and the minimum value at the three locations was determined and indicated as ΔEL.

また、耐常温時効性は、引張試験片を25℃の恒温室に0、30、60、90日保持した後に引張試験を行い、0.2%以上の顕著な降伏伸びが観察された最小の日数で評価した。
更に、鋼板の板幅方向で伸びに差異があると、鋼板の形状が悪化するため、形状の良否を目視で評価した。例えば、鋼板の板幅方向の端部での伸びが大きい場合には、端部が繰り返し波打つ耳伸びが見られ、中央部の伸びが大きいと中央部が繰り返し波打つ中伸びが見られる。また、板幅方向の特定の部位が波打つ局部伸びや、これらが複合して見られることもある。このような形状の悪化が目視で判断できないものを「○」、判断できるものを「×」で示した。
Moreover, the normal temperature aging resistance is the minimum in which a tensile test piece was held in a thermostatic chamber at 25 ° C. for 0, 30, 60, 90 days and a tensile test was performed, and a remarkable yield elongation of 0.2% or more was observed. The number of days was evaluated.
Furthermore, when there is a difference in elongation in the sheet width direction of the steel sheet, the shape of the steel sheet deteriorates, so the quality of the shape was evaluated visually. For example, when the elongation at the end in the plate width direction of the steel plate is large, the edge is repeatedly undulated, and when the center is large, the middle is repeatedly undulated. Moreover, the local expansion | swelling which the specific site | part of a board width direction undulates, and these may be seen combining. “◯” indicates that such deterioration of the shape cannot be visually determined, and “×” indicates that it can be determined.

表2に示したように、本発明の製造方法によって得られた冷延鋼板は板幅方向の全域において耐常温時効性に優れ、かつ延性も高い値を示し、形状にも優れることが分かる。
一方、従来の軽圧下圧延機を用いて伸び率を0.3%で行った製造No.2は、板幅の端部に向かうほど伸び率が不十分になったため、耐常温時効性は板幅方向の中央部では良好であるが、端部及び1/4部では低下し、形状も悪化している。また、製造No.3は、従来の圧延機で伸び率の大きい調質圧延を行った例であり、板幅方向の伸びのばらつきが大きい。製造No.10は、調質圧延の伸び率が大きいため、延性が低下している。
製造No.6は調質圧延を行わず、製造No.14は固溶C、N量の合計が多い冷延鋼板であるため、耐常温時効性が不十分である。
As shown in Table 2, it can be seen that the cold-rolled steel sheet obtained by the production method of the present invention is excellent in room temperature aging resistance, has a high ductility, and is excellent in shape in the entire region in the sheet width direction.
On the other hand, the production No. 1 was carried out at 0.3% elongation using a conventional light rolling mill. No. 2, because the elongation rate became insufficient toward the end of the plate width, room temperature aging resistance was good at the center in the plate width direction, but decreased at the end and ¼ part, and the shape was also It is getting worse. In addition, production No. No. 3 is an example in which temper rolling with a high elongation rate is performed with a conventional rolling mill, and the variation in elongation in the sheet width direction is large. Production No. No. 10 has a large elongation at temper rolling, and therefore has a reduced ductility.
Production No. No. 6 does not perform temper rolling, and production no. Since 14 is a cold-rolled steel sheet having a large total amount of solute C and N, room temperature aging resistance is insufficient.

(実施例2)
実施例2では、表1に示した鋼No.A及びDの冷延鋼板について、焼鈍温度を750〜850℃の範囲内、焼鈍時間を40〜100秒の範囲内とし、冷却速度を60〜120℃/秒の範囲内として行い、固溶C量及び固溶N量を調整した。その後、表面粗さRaの異なる直径500mmのワークロールを有する本発明の圧延機により調質圧延を施し、実施例1と同様に板幅の各点にける機械的性質を測定し、その測定結果を表3に示した。表3には、ワークロールの表面粗さRaが0.12であった表2の製造No.1及び7の結果も比較のために示した。
(Example 2)
In Example 2, the steel No. shown in Table 1 was used. About the cold-rolled steel sheets of A and D, the annealing temperature is set in the range of 750 to 850 ° C., the annealing time is set in the range of 40 to 100 seconds, and the cooling rate is set in the range of 60 to 120 ° C./second. The amount and the amount of solute N were adjusted. Thereafter, temper rolling was performed by the rolling mill of the present invention having work rolls having a diameter of 500 mm with different surface roughness Ra, and the mechanical properties at each point of the sheet width were measured in the same manner as in Example 1, and the measurement results Are shown in Table 3. Table 3 shows the production No. in Table 2 in which the surface roughness Ra of the work roll was 0.12. The results of 1 and 7 are also shown for comparison.

Figure 0004818879
Figure 0004818879

表3から明らかな通り、本発明の化学成分を有する鋼において、表面粗さRaの大きいワークロールを用いて調質圧延を施すことにより、伸び率を低下させても、形状を損なうことなく耐常温時効性を確保することが可能であり、より延性に優れた冷延鋼板が得られる。   As is apparent from Table 3, in the steel having the chemical component of the present invention, temper rolling is performed using a work roll having a large surface roughness Ra, and even if the elongation rate is reduced, the shape is not damaged. It is possible to ensure normal temperature aging, and a cold-rolled steel sheet having more excellent ductility can be obtained.

(実施例3)
実施例3では、表1に示した鋼No.C及びFの冷延鋼板について、最高到達温度を800℃とし、亜鉛めっき浴に浸漬後、500℃で20秒間の合金化処理を実施する連続溶融亜鉛めっきを施した。その後、本発明の圧延機を用いて、調質圧延を施し、実施例1と同様にして板幅の各点での機械的性質を測定した。その測定結果を表4に示す。
(Example 3)
In Example 3, the steel No. shown in Table 1 was used. The C and F cold-rolled steel sheets were subjected to continuous hot dip galvanization at a maximum temperature of 800 ° C. and immersion in a galvanizing bath followed by alloying treatment at 500 ° C. for 20 seconds. Thereafter, temper rolling was performed using the rolling mill of the present invention, and the mechanical properties at each point of the sheet width were measured in the same manner as in Example 1. The measurement results are shown in Table 4.

Figure 0004818879
Figure 0004818879

表4から明らかな通り、本発明の化学成分を有する鋼において、調質圧延前にめっきを施した冷延鋼板でも、本発明の条件の調質圧延を施すことで、形状を損なうことなく、耐常温時効性と延性に優れた冷延鋼板が得られる。   As is apparent from Table 4, in the steel having the chemical components of the present invention, even in the cold-rolled steel sheet plated before the temper rolling, by performing the temper rolling under the conditions of the present invention, without damaging the shape, A cold-rolled steel sheet having excellent room temperature aging resistance and ductility is obtained.

本発明の圧延機の模式図である。It is a schematic diagram of the rolling mill of this invention. 本発明の分割バックアップロールの模式図である。It is a schematic diagram of the division | segmentation backup roll of this invention. 本発明による板幅方向の全伸びの均一性を示す図である。It is a figure which shows the uniformity of the total elongation of the board width direction by this invention. 本発明による板幅方向の耐常温時効性の均一性を示す図である。It is a figure which shows the uniformity of the normal temperature aging resistance of the board width direction by this invention.

符号の説明Explanation of symbols

1 パスライン調整機
2 主圧下装置
3,4 バックアップロール
3a〜3g 分割バックアップロール
4a〜4h 分割バックアップロール
5 ワークロール
DESCRIPTION OF SYMBOLS 1 Passline adjustment machine 2 Main reduction device 3, 4 Backup roll 3a-3g Division backup roll 4a-4h Division backup roll 5 Work roll

Claims (5)

上下のロールアセンブリーの一方又は双方が、軸方向に3以上に分割された分割バックアップロールによってワークロールを支持する支持機構を有し、前記分割バックアップロールのそれぞれに負荷される荷重を検出する荷重検出装置と前記分割バックアップロールを独立して昇降させる圧下装置を設けた圧延機により、固溶C量と固溶N量の一方又は双方の合計が0.0010%未満であり、板厚が0.3〜2.0mm、板幅が600〜2000mmである冷延鋼鈑に対して、板幅方向での伸び率が均一となるように、所定の伸び率を得るために必要な圧延荷重を計算した後、板幅方向の部位毎の圧延荷重を検出し、この部位毎の圧延荷重をコントロールしながら、伸び率が0.1%以上0.8%未満の調質圧延を施すことを特徴とする延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。 One or both of the upper and lower roll assemblies have a support mechanism for supporting the work roll by a divided backup roll divided into three or more in the axial direction, and a load for detecting a load applied to each of the divided backup rolls By a rolling mill provided with a reduction device that raises and lowers the detection device and the divided backup roll independently, the total of one or both of the solid solution C amount and the solid solution N amount is less than 0.0010%, and the plate thickness is 0. .3~2.0Mm, for the cold-rolled steel sheet strip width is 600~2000Mm, like elongation in the plate width direction becomes uniform, the rolling load required to obtain a given elongation After the calculation, the rolling load for each part in the sheet width direction is detected, and temper rolling with an elongation of 0.1% or more and less than 0.8% is performed while controlling the rolling load for each part. To Excellent production method for cold rolled steel sheet in and anti-aging properties. 冷延鋼板の成分組成が、質量%で、
C:0.0010%未満、
Si:1.00%以下、
Mn:3.00%以下、
P:0.100%以下、
S:0.100%以下、
Al:1.000%以下、
N:0.0010%未満
を含有し、残部がFe及び不可避的不純物からなり、
前記CとNの含有量の合計が0.0010%未満であることを特徴とする請求項1に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。
The component composition of the cold-rolled steel sheet is mass%,
C: less than 0.0010%,
Si: 1.00% or less,
Mn: 3.00% or less,
P: 0.100% or less,
S: 0.100% or less,
Al: 1.000% or less,
N: containing less than 0.0010%, the balance consisting of Fe and inevitable impurities,
The total content of said C and N is less than 0.0010%, The manufacturing method of the cold-rolled steel plate excellent in ductility and normal temperature aging resistance of Claim 1 characterized by the above-mentioned.
冷延鋼板の成分組成が、質量%で、
C:0.0500%以下、
Si:1.00%以下、
Mn:3.00%以下、
P:0.100%以下、
S:0.100%以下、
Al:1.000%以下、
N:0.0500%以下
を含有し、残部がFe及び不可避的不純物からなり、
更に、質量%で、
Nb:0.001〜0.150%、
Ti:0.001〜0.150%
の一方又は双方を含有し、
前記C、N、Ti及びNbの含有量が、
1/4Ti+1/8Nb≧C+N−0.0010
の関係を満たすことを特徴とする請求項1に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。
The component composition of the cold-rolled steel sheet is mass%,
C: 0.0500% or less,
Si: 1.00% or less,
Mn: 3.00% or less,
P: 0.100% or less,
S: 0.100% or less,
Al: 1.000% or less,
N: 0.0500% or less, the balance is made of Fe and inevitable impurities,
Furthermore, in mass%,
Nb: 0.001 to 0.150%,
Ti: 0.001 to 0.150%
One or both of
The content of C, N, Ti and Nb is
1 / 4Ti + 1 / 8Nb ≧ C + N−0.0010
The manufacturing method of the cold-rolled steel plate excellent in ductility and normal temperature aging resistance of Claim 1 characterized by satisfy | filling the relationship of these.
前記ワークロールの表面粗さRaが0.2μm以上であることを特徴とする請求項1〜3の何れか1項に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。   The method for producing a cold-rolled steel sheet excellent in ductility and room temperature aging resistance according to any one of claims 1 to 3, wherein the work roll has a surface roughness Ra of 0.2 µm or more. 前記調質圧延前の冷延鋼板の表面にめっきを施すことを特徴とする請求項1〜4の何れか1項に記載の延性及び耐常温時効性に優れた冷延鋼鈑の製造方法。   The method for producing a cold-rolled steel sheet excellent in ductility and room temperature aging resistance according to any one of claims 1 to 4, wherein the surface of the cold-rolled steel sheet before the temper rolling is plated.
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