JP4535810B2 - Composition for enhancing coffee flavor - Google Patents
Composition for enhancing coffee flavor Download PDFInfo
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- JP4535810B2 JP4535810B2 JP2004256914A JP2004256914A JP4535810B2 JP 4535810 B2 JP4535810 B2 JP 4535810B2 JP 2004256914 A JP2004256914 A JP 2004256914A JP 2004256914 A JP2004256914 A JP 2004256914A JP 4535810 B2 JP4535810 B2 JP 4535810B2
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- 239000000203 mixture Substances 0.000 title claims description 19
- 230000002708 enhancing effect Effects 0.000 title claims description 7
- 239000002245 particle Substances 0.000 claims description 25
- 241000533293 Sesbania emerus Species 0.000 claims description 19
- 108090000790 Enzymes Proteins 0.000 claims description 8
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- OMDQUFIYNPYJFM-XKDAHURESA-N (2r,3r,4s,5r,6s)-2-(hydroxymethyl)-6-[[(2r,3s,4r,5s,6r)-4,5,6-trihydroxy-3-[(2s,3s,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H](O)[C@H](O)O1 OMDQUFIYNPYJFM-XKDAHURESA-N 0.000 claims description 4
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- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 description 3
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- MLXMMJOETFQFAL-UHFFFAOYSA-N C(CCCCCCC)(=O)O.C(CCC(=O)O)(=O)OCC(O)CO Chemical compound C(CCCCCCC)(=O)O.C(CCC(=O)O)(=O)OCC(O)CO MLXMMJOETFQFAL-UHFFFAOYSA-N 0.000 description 2
- 235000010469 Glycine max Nutrition 0.000 description 2
- SZYSLWCAWVWFLT-UTGHZIEOSA-N [(2s,3s,4s,5r)-3,4-dihydroxy-5-(hydroxymethyl)-2-[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxolan-2-yl]methyl octadecanoate Chemical compound O([C@@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@]1(COC(=O)CCCCCCCCCCCCCCCCC)O[C@H](CO)[C@@H](O)[C@@H]1O SZYSLWCAWVWFLT-UTGHZIEOSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
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- OKSFAFCZNADJOC-UHFFFAOYSA-N propane-1,2,3-triol tetradecanoic acid Chemical compound OCC(O)CO.OCC(O)CO.OCC(O)CO.OCC(O)CO.OCC(O)CO.CCCCCCCCCCCCCC(O)=O OKSFAFCZNADJOC-UHFFFAOYSA-N 0.000 description 2
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- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 1
- PZNPLUBHRSSFHT-RRHRGVEJSA-N 1-hexadecanoyl-2-octadecanoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCCCC(=O)O[C@@H](COP([O-])(=O)OCC[N+](C)(C)C)COC(=O)CCCCCCCCCCCCCCC PZNPLUBHRSSFHT-RRHRGVEJSA-N 0.000 description 1
- LRZBIPQJHILPJI-UHFFFAOYSA-N 2,3-dihydroxypropyl 2-(2,3-dihydroxypropyl)octadecanoate Chemical compound CCCCCCCCCCCCCCCCC(CC(O)CO)C(=O)OCC(O)CO LRZBIPQJHILPJI-UHFFFAOYSA-N 0.000 description 1
- 102100032487 Beta-mannosidase Human genes 0.000 description 1
- 108010059892 Cellulase Proteins 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
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- JHSNLCCMZMGXLK-UHFFFAOYSA-N [3-[3-(2,3-dihydroxypropoxy)-2-hydroxypropoxy]-2-hydroxypropyl] octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)COCC(O)COCC(O)CO JHSNLCCMZMGXLK-UHFFFAOYSA-N 0.000 description 1
- NPTLAYTZMHJJDP-KTKRTIGZSA-N [3-[3-[3-[3-[3-[3-[3-[3-[3-(2,3-dihydroxypropoxy)-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropyl] (z)-octadec-9-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)CO NPTLAYTZMHJJDP-KTKRTIGZSA-N 0.000 description 1
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- 239000003205 fragrance Substances 0.000 description 1
- 108010066429 galactomannanase Proteins 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229940059442 hemicellulase Drugs 0.000 description 1
- 108010002430 hemicellulase Proteins 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
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- 239000000463 material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
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- Tea And Coffee (AREA)
Description
本発明は、コーヒー豆の平均粒子径が10μm以下、20℃における粘度が300mPa・s以下であることを特徴とする風味強化用組成物及びそれを含有する飲食品に関するものである。 The present invention relates to a flavor enhancing composition characterized in that the average particle size of coffee beans is 10 μm or less and the viscosity at 20 ° C. is 300 mPa · s or less, and a food or drink containing the same.
従来、飲食品のコーヒー風味を付与する場合、香料やコーヒーの抽出液、濃縮液、スプレードライにより粉末化されたコーヒー粉末などを利用することが多い。また、風味の良いコーヒー粉末の製造方法に関して、焙煎コーヒーの粉砕時の香り成分の揮発を防止することによる香り成分の含有量の豊富な粉末レギュラーコーヒーの製造方法(例えば、特許文献1参照。)が開示されている。
一方、コーヒーを微粉末にする方法は、インスタントコーヒーの製造方法に関して、凍結させたコーヒー豆を粉砕して、抽出液に添加して乾燥させる方法(例えば特許文献2参照)、さらに、コーヒー豆を水と一緒に入れ、粉砕した後に懸濁液を噴霧乾燥機で乾燥する微粉末コーヒーの製造方法(例えば、特許文献3参照。)が開示されおり、コーヒー粉末の粒子径としては最も微粉砕されたもので平均粒子径30μmという粒子径となっている。
しかし、これらを飲食品に入れた場合、香料や濃縮エキスではボディ感のない風味となり、コーヒー本来の風味が出にくく、上記記載の微粉末コーヒーや風味の良いコーヒー粉末を使用した場合も、二次凝集や粒子自体のザラツキ及び沈殿等の問題があり、満足されるものが得られていないのが現状である。またコーヒー豆を平均粒子径30μm以下に湿式粉砕する製造方法も開発されているが、コーヒーの含有量が10重量%より多い場合には、該組成物の構造粘度が極度に高まり流動性を失ってしまう為に後の加工特性及び応用範囲を著しく狭めることとなっている。(例えば、特許文献4参照。)
Conventionally, when a coffee flavor of a food or drink is imparted, a fragrance, a coffee extract, a concentrated liquid, a coffee powder powdered by spray drying, or the like is often used. In addition, regarding a method for producing a coffee powder having a good flavor, a method for producing a regular coffee powder rich in scent components by preventing volatilization of the scent components during roasted coffee grinding (see, for example, Patent Document 1). ) Is disclosed.
On the other hand, the method of making coffee into fine powder is a method of pulverizing frozen coffee beans, adding them to the extract and drying them (for example, see Patent Document 2), and further producing coffee beans. There is disclosed a method for producing finely ground coffee (for example, see Patent Document 3) in which a suspension is dried with a spray dryer after pulverizing with water, and the particle size of the coffee powder is most finely ground. The average particle size is 30 μm.
However, when these are added to foods and drinks, flavors and concentrated extracts have a flavor that does not have a body feeling, and it is difficult to produce the original flavor of coffee. There are problems such as subsequent agglomeration, grain roughness and precipitation, and the present situation is that satisfactory products are not obtained. A production method has also been developed in which coffee beans are wet pulverized to an average particle size of 30 μm or less. However, when the coffee content is more than 10% by weight, the structural viscosity of the composition becomes extremely high and the fluidity is lost. Therefore, later processing characteristics and application range are remarkably narrowed. (For example, see Patent Document 4)
従って、本発明の目的は粒径が細かく、粘度が低い、コーヒー風味を強化する効果の高いコーヒー風味強化組成物を提供することにある。 Accordingly, an object of the present invention is to provide a coffee flavor enhancing composition having a fine particle size, a low viscosity, and a high effect of enhancing coffee flavor.
本発明者らは鋭意研究を重ねた結果、コーヒー豆を超微粒子に分散させることを特徴とするコーヒー風味強化剤を開発し、飲食品へ添加によって食感等に影響を及ぼすことなくコーヒー風味を強化できることを見出し、本発明を完成するに至った。本発明はコーヒー豆を超微粒子に分散させたことを特徴とするコーヒー風味強化剤の製造法、及びそれを含有する飲食品に関する。 As a result of intensive research, the present inventors have developed a coffee flavor enhancer characterized by dispersing coffee beans in ultrafine particles, and adding a coffee flavor without affecting the texture etc. The inventors have found that it can be strengthened, and have completed the present invention. The present invention relates to a method for producing a coffee flavor enhancer characterized in that coffee beans are dispersed in ultrafine particles, and a food or drink containing the same.
以下、本発明の実施形態について、詳細に説明する。 Hereinafter, embodiments of the present invention will be described in detail.
本発明におけるコーヒー豆の品種は、特に限定されるものではないが、アラビカ種、ロブスタ種、リベリカ種等があげられる。原料となるコーヒー豆の形状については特に限定されるものではないが、酵素反応効率および目的の粒子径を得る点によりコーヒーミル、ハンマーミル、グローミル、凍結粉砕機などで、予備粉砕されたものが好ましく、また風味の点により特に凍結粉砕したコーヒーを用いることが最も好ましい。その平均粒子径は100μm以下が好ましく、さらに50μm以下がより好ましい。
次いで、コーヒーの焙煎は、公知の方法で行ったもので、焙煎度合いについても特に限定されるものではない。
The variety of coffee beans in the present invention is not particularly limited, and examples thereof include Arabica, Robusta, and Riberica. The shape of the coffee beans used as a raw material is not particularly limited, but the coffee beans, hammer mills, glow mills, freeze grinders, etc. that have been pre-ground by the point of obtaining the enzyme reaction efficiency and the target particle size are not limited. It is preferred to use coffee that has been freeze-ground, particularly in terms of flavor. The average particle diameter is preferably 100 μm or less, and more preferably 50 μm or less.
Next, the roasting of the coffee is performed by a known method, and the degree of roasting is not particularly limited.
本発明のコーヒー豆の含有量は特に限定するものではないが、該組成物中10〜50重量%であることが好ましく、より好ましくは15〜30重量%である。コーヒーの含有量が10重量%より少ない場合にはコーヒー風味強化の効果が十分ではなく、50重量%より多い場合には、該組成物の構造粘度が極度に高まり流動性を失ってしまう為に後の加工特性及び応用範囲を著しく狭めることとなる。 Although content of the coffee bean of this invention is not specifically limited, It is preferable that it is 10 to 50 weight% in this composition, More preferably, it is 15 to 30 weight%. When the coffee content is less than 10% by weight, the effect of enhancing the coffee flavor is not sufficient, and when it is more than 50% by weight, the structural viscosity of the composition becomes extremely high and the fluidity is lost. Later processing characteristics and application range will be significantly narrowed.
本発明のコーヒー豆は、粘度低下の点より酵素処理されていることが好ましい。
本発明の酵素は特に限定されるものではないが、セルラーゼ、ヘミセルラーゼ、ペクチダーゼ、キシラーゼ、マンナナーゼ等があげられるが、粘度低下効率の点よりガラクトマンナナーゼを用いることが好ましい。
The coffee beans of the present invention are preferably treated with an enzyme from the viewpoint of viscosity reduction.
The enzyme of the present invention is not particularly limited, and examples thereof include cellulase, hemicellulase, pectinase, xylase, mannanase, etc., but galactomannanase is preferably used from the viewpoint of viscosity reduction efficiency.
前記ガラクトマンナン分解酵素の添加量は、ガラクトマンナンの分解を必要かつ十分に行うためにはコーヒー豆含量あたり0.01〜0.5重量%であることが好ましく、より好ましくは0.05〜0.2重量%である。反応温度は5〜90℃、また風味を保つ点により30〜50℃で10分から5時間、好ましくは2時間〜4時間の処理をする。 The addition amount of the galactomannan degrading enzyme is preferably 0.01 to 0.5% by weight, more preferably 0.05 to 0% per coffee bean content in order to perform the necessary and sufficient degradation of galactomannan. .2% by weight. The reaction temperature is 5 to 90 ° C., and the treatment is performed at 30 to 50 ° C. for 10 minutes to 5 hours, preferably 2 hours to 4 hours depending on the point of keeping the flavor.
本発明の粉砕方法は特に限定されるものではないが、一般的な粉砕方法には乾式粉砕、湿式粉砕、凍結粉砕、湿式摩砕等があげられる。本発明で用いる粉砕法で好ましいものは、湿式摩砕法である。 The pulverization method of the present invention is not particularly limited, and general pulverization methods include dry pulverization, wet pulverization, freeze pulverization, and wet grinding. A preferable grinding method used in the present invention is a wet grinding method.
湿式摩砕法とは、粉砕室(ベッセル容器)中でガラスビ−ズ、アルミナビ−ズ、ジルコニアビ−ズ、チタニアビ−ズ等のメディアをディスク又はロ−タ−を回転させることにより、メディア同士を衝突させて該粉砕室中に供給される被粉砕物スラリ−をせん断応力を生じさせ粉砕する方法である。本発明におけるメディアは、好ましくはアルミナビ−ズ、ジルコニアビ−ズ、チタニアビ−ズが使用される。さらに、メディアの粒径は特に限定されるものではないが、好ましくは1mm以下、より好ましくは0.8mm以下、更に好ましくは0.5mm以下が使用される。メディアの充填量は特に限定されるものではないが、通常摩砕室の有効容積に対して50%以上であるが、摩砕効率から好ましくは70%以上、更に好ましくは80%以上が望ましい。本発明に用いられる湿式摩砕機は、本発明によって得られるコーヒーの平均粒径が10μm以下にする性質を有するものであれば特に限定するものではないが、一般的にコボ−ルミル、ダイノ−ミル、サンドミル、レディミル等と呼称されているものであり、更に縦型、横型、バッチ式、連続式などいずれのタイプでも差し支えないが生産効率の面から、好ましくは連続式が望ましい。なお、摩砕室の材質は余分な異物が混入しないよう金属ではなく、セラミック等が望ましい。 The wet grinding method means that media such as glass beads, alumina beads, zirconia beads, and titania beads are rotated in a grinding chamber (vessel container) by rotating a disk or a rotor. In this method, the slurry to be crushed supplied to the pulverization chamber by being collided is crushed by generating shear stress. As the media in the present invention, alumina beads, zirconia beads, and titania beads are preferably used. Further, the particle size of the media is not particularly limited, but preferably 1 mm or less, more preferably 0.8 mm or less, and still more preferably 0.5 mm or less. The filling amount of the media is not particularly limited, but is usually 50% or more with respect to the effective volume of the grinding chamber, but is preferably 70% or more, more preferably 80% or more from the viewpoint of grinding efficiency. The wet mill used in the present invention is not particularly limited as long as it has the property that the average particle size of the coffee obtained by the present invention is 10 μm or less, but is generally limited to a cobal mill and a dyno mill. , Sand mill, ready mill and the like, and any type such as vertical type, horizontal type, batch type and continuous type may be used, but from the viewpoint of production efficiency, the continuous type is preferable. The material of the grinding chamber is preferably ceramic, not metal, so that extraneous foreign matter is not mixed.
本発明において、コーヒー風味強化用組成物の粘度上昇や離水を防止する点、および目的の粒子径のコーヒー豆を得ることができる点より、製造工程において乳化剤を使用することが好ましい。
使用する乳化剤については特に限定されるものではなく、飲食品に通常使用されるグリセリン脂肪酸エステル、ポリグリセリン脂肪酸エステル、有機酸モノグリセリド、レシチン、酵素分解レシチンなどを用いることができ、好ましくはポリグリセリン脂肪酸エステルであり、その中でもHLB6以上のものが好ましく、具体例として、モノステアリン酸ジグリセリン、モノステアリン酸ヘキサグリセリン、モノオレイン酸ヘキサグリセリン、モノミリスチン酸ヘキサグリセリン、モノラウリン酸ヘキサグリセリン、モノステアリン酸デカグリセリン、ジステアリン酸デカグリセリン、モノオレイン酸デカグリセリン、モノミリスチン酸デカグリセリン、モノラウリン酸デカグリセリン、モノラウリン酸トリグリセリン、モノミリスチン酸トリグリセリン、モノオレイン酸トリグリセリン、モノステアリン酸トリグリセリン、モノラウリン酸ペンタグリセリン、モノミリスチン酸ペンタグリセリン、トリミリスチン酸ペンタグリセリン、モノステアリン酸ペンタグリセリン等があげられるが、中でもモノミリスチン酸ペンタグリセリンが最も好ましい。
In this invention, it is preferable to use an emulsifier in a manufacturing process from the point which prevents the viscosity raise and water separation of the composition for coffee flavor reinforcement | strengthening, and the point which can obtain the coffee beans of the target particle diameter.
The emulsifier to be used is not particularly limited, and glycerin fatty acid ester, polyglycerin fatty acid ester, organic acid monoglyceride, lecithin, enzymatically decomposed lecithin and the like that are usually used for food and drink can be used, and preferably polyglycerin fatty acid. Among them, those having an HLB of 6 or more are preferred, and specific examples include diglyceryl monostearate, hexaglyceryl monostearate, hexaglyceryl monooleate, hexaglyceryl monomyristate, hexaglyceryl monolaurate, decamonostearate Glycerin, Decaglyceryl distearate, Decaglyceryl monooleate, Decaglyceryl monomyristate, Decaglyceryl monolaurate, Triglyceryl monolaurate, Monomyristate Examples include glycerin, triglyceryl monooleate, triglyceryl monostearate, pentaglyceryl monolaurate, pentaglyceryl monomyristate, pentaglyceryl trimyristate, pentaglyceryl monostearate, and most preferably pentaglyceryl monomyristate. preferable.
他の乳化剤としては、食品に供するものであれば特に限定するものではないが具体例として、クエン酸モノステアリン酸グリセリン、コハク酸モノカプリル酸グリセリン、ジアセチル酒石酸モノステアリン酸グリセリン、ショ糖ステアリン酸エステル、大豆レシチン、酵素分解大豆レシチンから選ばれる1種または2種以上の混合物が挙げられ、特に酵素分解大豆レシチンが好ましく、ポリグリセリン脂肪酸エステルと併用することによって相乗効果が期待できる。 Other emulsifiers are not particularly limited as long as they are used in foods. Specific examples include glyceryl monostearate glycerol, glyceryl succinate monocaprylate, glyceryl distearate monostearate, and sucrose stearate. In addition, one or a mixture of two or more selected from soybean lecithin and enzyme-decomposed soybean lecithin can be mentioned. Particularly, enzyme-decomposed soybean lecithin is preferable, and a synergistic effect can be expected by using it together with a polyglycerol fatty acid ester.
ここで、粒子径の測定については、特に限定するものではないが、レーザー回折型粒度分布測定装置(ベックマン コールター(R)LXS230)等を使用することができる。 Here, the measurement of the particle diameter is not particularly limited, but a laser diffraction type particle size distribution measuring device (Beckman Coulter (R) LXS230) or the like can be used.
本発明に用いる乳化剤はコーヒー風味強化剤に対して0.1〜10重量%配合することが好ましく、1〜2重量%がさらに好ましい。添加量が0.1重量%未満の場合はコーヒー固体微粒子を十分に分散させることが困難であり、10重量%より多い場合には該組成物のコーヒー風味の点より好ましくない。 The emulsifier used in the present invention is preferably blended in an amount of 0.1 to 10% by weight, more preferably 1 to 2% by weight, based on the coffee flavor enhancer. When the addition amount is less than 0.1% by weight, it is difficult to sufficiently disperse the coffee solid fine particles, and when it is more than 10% by weight, it is not preferable from the viewpoint of the coffee flavor of the composition.
他の乳化剤としては、食品に供するものであれば特に限定するものではないが具体例として、クエン酸モノステアリン酸グリセリン、コハク酸モノカプリル酸グリセリン、ジアセチル酒石酸モノステアリン酸グリセリン、ショ糖ステアリン酸エステル、大豆レシチン、酵素分解から選ばれる1種または2種以上の混合物が挙げられ、ポリグリセリン脂肪酸エステルと併用することによって相乗効果が期待できる。 Other emulsifiers are not particularly limited as long as they are used in foods. Specific examples include glyceryl monostearate glycerin, glyceryl succinate monocaprylate, glyceryl distearate monostearate, and sucrose stearate. , Soy lecithin, or one or a mixture of two or more selected from enzymatic degradation, and a synergistic effect can be expected when used in combination with a polyglycerol fatty acid ester.
本発明のコーヒー風味強化剤は、缶コーヒーなどの嗜好飲料、アイスクリーム等の冷菓、クッキ−、ビスケット等製菓・製パン類などのさまざまな食品への応用が可能である。 The coffee flavor enhancer of the present invention can be applied to various foods such as beverages such as canned coffee, frozen confectionery such as ice cream, confectionery and bread making such as cookie and biscuits.
以下に実施例及び試験例によって本発明を説明するが、その内容に制限されるものではない。 The present invention will be described below with reference to examples and test examples, but the present invention is not limited thereto.
《実施例1》
凍結粉砕コーヒー豆100g(リンレックスミルにて粉砕したもの平均粒子径約30μm、太陽化学株式会社製)、ガラクトマンナン分解酵素1g(セルロシンGM5 エイチビィアイ株式会社製)、モノミリスチン酸ペンタグリセリン10g(サンソフトA−141E、太陽化学株式会社製)、大豆酵素分解レシチン5g(サンレシチンA−1 太陽化学株式会社製)、還元水飴284g(アマミール 東和化成工業株式会社製)、水道水600gを混合し、37℃ 3時間攪拌した。これをレディミル(株式会社アイメックス製)に掛け、レーザー回折型粒度分布測定によりコーヒーの平均粒子径が9.2μmとなったコーヒー風味強化剤を700g得た。
Example 1
100 g of frozen ground coffee beans (averaged particle size of about 30 μm ground with Linlex Mill, manufactured by Taiyo Kagaku Co., Ltd.), 1 g of galactomannan degrading enzyme (manufactured by Cellulosin GM5 HBI Co., Ltd.), 10 g of pentaglycerin monomyristate (Sunsoft) A-141E, manufactured by Taiyo Kagaku Co., Ltd.), soy enzyme-degraded lecithin 5 g (San lecithin A-1 manufactured by Taiyo Kagaku Co., Ltd.), 284 g of reduced starch syrup (manufactured by Amami Towa Kasei Kogyo Co., Ltd.), and 600 g of tap water 37 The mixture was stirred for 3 hours. This was applied to Ready Mill (manufactured by Imex Co., Ltd.) to obtain 700 g of a coffee flavor enhancer having an average particle diameter of coffee of 9.2 μm by laser diffraction particle size distribution measurement.
《実施例2》
凍結粉砕コーヒー豆100g(リンレックスミルにて粉砕したもの平均粒子径約30μm、太陽化学株式会社製)、ガラクトマンナン分解酵素1g(セルロシンGM5 エイチビィアイ株式会社製)、還元水飴300g(アマミール 東和化成工業株式会社製)、水道水600gを混合し、37℃ 3時間攪拌した。これをレディミル(株式会社アイメックス製)に掛け、レーザー回折型粒度分布測定によりコーヒーの平均粒子径が9.8μmとなったコーヒー風味強化剤を520g得た。
Example 2
100 g of freeze-ground coffee beans (averaged particle size of about 30 μm, pulverized with Linlex Mill, manufactured by Taiyo Kagaku Co., Ltd.), 1 g of galactomannan-degrading enzyme (Cellulosin GM5, manufactured by HIBI Co., Ltd.), 300 g of reduced starch syrup And 600 g of tap water were mixed and stirred at 37 ° C. for 3 hours. This was applied to Ready Mill (manufactured by Imex Co., Ltd.) to obtain 520 g of a coffee flavor enhancer having an average particle diameter of coffee of 9.8 μm by laser diffraction type particle size distribution measurement.
《比較例1》
凍結粉砕コーヒー豆100g(リンレックスミルにて粉砕したもの平均粒子径約30μm、太陽化学株式会社製)、還元水あめ300g(アマミール 東和化成工業株式会社製)、水道水600gを混合し、これをホモミキサー(特殊機化株式会社)で分散させ、レーザー回折型粒度分布測定によりコーヒーの平均粒子径が約24.8μmとなったコーヒー風味強化剤を980gを得た。
<< Comparative Example 1 >>
100 g of freeze-ground coffee beans (average pulverized by Linlex Mill, average particle size of about 30 μm, manufactured by Taiyo Kagaku Co., Ltd.), 300 g of reduced water candy (Amamiru Towa Kasei Kogyo Co., Ltd.), and 600 g of tap water are mixed. 980 g of a coffee flavor enhancer in which the average particle size of the coffee was about 24.8 μm was measured by laser diffraction particle size distribution measurement by dispersing with a mixer (Special Machine Co., Ltd.).
《比較例2》
凍結粉砕コーヒー豆100g(リンレックスミルにて粉砕したもの平均粒子径約30μm、太陽化学株式会社製)、モノミリスチン酸ペンタグリセリン10g(サンソフトA−141E、太陽化学株式会社製)、大豆酵素分解レシチン5g(サンレシチンA−1 太陽化学株式会社製)、還元水飴285g(アマミール 東和化成工業株式会社製)、水道水600gを混合し、37℃ 3時間攪拌した。これをレディミル(株式会社アイメックス製)に掛け、レーザー回折型粒度分布測定によりコーヒーの平均粒子径が約18.2μmとなったコーヒー風味強化剤を480g得た。
<< Comparative Example 2 >>
100 g of freeze-ground coffee beans (averaged particle size of about 30 μm, pulverized by Linlex Mill, manufactured by Taiyo Chemical Co., Ltd.), 10 g of pentaglycerin monomyristic acid (Sunsoft A-141E, manufactured by Taiyo Chemical Co., Ltd.), soybean enzymatic degradation 5 g of lecithin (San lecithin A-1 manufactured by Taiyo Kagaku Co., Ltd.), 285 g of reduced starch syrup (manufactured by Amami Towa Kasei Kogyo Co., Ltd.) and 600 g of tap water were mixed and stirred at 37 ° C. for 3 hours. This was subjected to Ready Mill (manufactured by Imex Co., Ltd.) to obtain 480 g of a coffee flavor enhancer having an average particle diameter of coffee of about 18.2 μm by laser diffraction particle size distribution measurement.
《試験例1》
実施例1、2および比較例1、2で得られたコーヒー風味強化物を20℃、1時間静置させた製剤の状態、および粘度、粒子径、水への分散性について評価した。
<< Test Example 1 >>
The coffee flavor-enhanced products obtained in Examples 1 and 2 and Comparative Examples 1 and 2 were evaluated for the state of preparations allowed to stand at 20 ° C. for 1 hour, and the viscosity, particle size, and dispersibility in water.
実施例1、2および比較例1、2で得られたコーヒー風味強化物5g、コーヒーエキストラクト(Bx25)50g(太陽化学株式会社製)、砂糖50g、牛乳130g、乳化安定剤製剤1.3g、イオン交換水765gを混合後、100kg/cm2ホモジナイザー処理を行い、缶に充填し、レトルト殺菌機121℃、30分殺菌を行って冷却した。
対照品として、コーヒー風味強化剤無添加品を調製してそれぞれの喉ごし、旨み、香り、ザラツキについて比較した。官能評価については、それぞれの飲料をパネラー20人で、苦味、ボディ感、香り、ザラツキについて5段階評価(5が最も良い、1が最も悪い)を行いその平均値であらわした。
5 g of the coffee flavor enhancement product obtained in Examples 1 and 2 and Comparative Examples 1 and 2, 50 g of coffee extract (Bx25) (manufactured by Taiyo Chemical Co., Ltd.), 50 g of sugar, 130 g of milk, 1.3 g of an emulsion stabilizer formulation, After mixing 765 g of ion-exchanged water, 100 kg / cm 2 homogenizer treatment was performed, the can was filled, and retort sterilizer was sterilized at 121 ° C. for 30 minutes and cooled.
As a control product, a coffee flavor enhancer-free product was prepared and compared for each throat, umami, aroma, and roughness. For sensory evaluation, each drink was evaluated by 20 panelists, and the bitterness, body feeling, aroma, and roughness were evaluated on a five-point scale (5 being the best and 1 being the worst), and the average value was expressed.
本発明のコーヒー風味強化用組成物は様々な飲食品に利用可能である。またコーヒー豆まるごとを原料とし、コーヒー風味を付与することのできるコーヒー風味用組成物を、広く食品分野に提供するものである。
また、いままで廃棄物として処理されていたコーヒー抽出残渣を減らすことにもつながり、社会への利益にもつながるものである。
The composition for enhancing coffee flavor of the present invention can be used for various foods and drinks. Moreover, the composition for coffee flavors which can give the coffee flavor from the whole coffee beans as a raw material is provided widely to the food field.
It also leads to a reduction in coffee extraction residues that have been treated as waste until now, which also benefits society.
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