JP3057943B2 - Film thickness measuring device - Google Patents
Film thickness measuring deviceInfo
- Publication number
- JP3057943B2 JP3057943B2 JP5001169A JP116993A JP3057943B2 JP 3057943 B2 JP3057943 B2 JP 3057943B2 JP 5001169 A JP5001169 A JP 5001169A JP 116993 A JP116993 A JP 116993A JP 3057943 B2 JP3057943 B2 JP 3057943B2
- Authority
- JP
- Japan
- Prior art keywords
- film thickness
- sample
- fourier transform
- large peak
- light
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Length Measuring Devices By Optical Means (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Description
【0001】[0001]
【産業上の利用分野】本発明は、フィルム厚さ計など、
試料の吸光特性を用いて膜厚を測定する装置に関し、特
に膜の上下面によって生じる干渉縞を低減し、測定精度
を向上させるものである。BACKGROUND OF THE INVENTION 1. Field of the Invention
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an apparatus for measuring a film thickness using the light absorption characteristics of a sample, and in particular, to reduce interference fringes generated by upper and lower surfaces of a film and improve measurement accuracy.
【0002】[0002]
【従来の技術】図3はこのような膜厚測定装置の一種で
ある赤外線フィルム厚さ計の一例を示す構成図である。
この赤外線フィルム厚さ計ではCH基によって吸収を受
ける波長3.3μmの光(M光)とCH基によって吸収
を受けない波長2.8μmの光(R光)とをフィルムに
当て、フィルムを透過したM光の測定光出力VMとR光
の参照光出力VRとの比(VR/VM)をとって、フィル
ムの厚さに関する信号を得ている。2. Description of the Related Art FIG. 3 is a block diagram showing an example of an infrared film thickness gauge which is a kind of such a film thickness measuring device.
In this infrared film thickness meter, light having a wavelength of 3.3 μm (M light) absorbed by a CH group and light having a wavelength of 2.8 μm (R light) not absorbed by a CH group are applied to the film and transmitted through the film. taking the ratio of the measured light output V M and R light of the reference light output V R of the M light (V R / V M), to obtain a signal related to the thickness of the film.
【0003】図3において、1は光源、2は集光レン
ズ、3はフィルタ・ホイールで、このフィルタ・ホイー
ル3にはフィルムによる吸収係数が大きな第1波長域の
赤外線(例えば3.3μm)を透過するフィルタ31、
フィルムによる吸収係数が小さな第2波長域の赤外線
(例えば2.8μm)を透過するフィルタ32、フィル
ムによって吸収を受けない第3の波長域の赤外線(例え
ば5.0μm)を透過するフィルタ33が同心円上に形
成されている。4は測定対象であるフィルム、5は受光
素子である。In FIG. 3, reference numeral 1 denotes a light source, 2 denotes a condenser lens, and 3 denotes a filter wheel. The filter wheel 3 receives infrared rays (for example, 3.3 μm) in a first wavelength region having a large absorption coefficient by a film. Transmitting filter 31,
A filter 32 that transmits infrared light in a second wavelength range (for example, 2.8 μm) having a small absorption coefficient by the film and a filter 33 that transmits infrared light in a third wavelength range (for example, 5.0 μm) that is not absorbed by the film are concentric circles. Is formed on. Reference numeral 4 denotes a film to be measured, and reference numeral 5 denotes a light receiving element.
【0004】このような構成において、フィルタ・ホイ
ール3の回転によって、フィルタ31を透過した3.3
μmの赤外線、フィルタ32を透過した2.8μmの赤
外線、フィルタ33を透過した5.0μmの赤外線が順
次、フィルム4に照射される。これら3種の赤外線に基
づく透過光が受光素子5で検出され、それぞれの波長域
の赤外線に対する検出出力が得られる。In such a configuration, the 3.3 transmitted through the filter 31 by the rotation of the filter wheel 3.
The film 4 is irradiated with an infrared ray of μm, an infrared ray of 2.8 μm transmitted through the filter 32, and an infrared ray of 5.0 μm transmitted through the filter 33 sequentially. The transmitted light based on these three types of infrared rays is detected by the light receiving element 5, and a detection output for infrared rays in each wavelength range is obtained.
【0005】[0005]
【発明が解決しようとする課題】しかしながら、上記従
来技術に示す膜厚測定装置においては、試料が薄いと、
試料の上下面の表面反射により干渉縞が生じてしまう。
例えば、図4に示すように、試料が厚い場合(イ図)と
試料が薄い場合(ロ図)を比較すると明らかなように、
干渉縞が生じている。したがって、得られる膜厚には誤
差が生じることになる。However, in the film thickness measuring apparatus shown in the above prior art, if the sample is thin,
Interference fringes occur due to surface reflections on the upper and lower surfaces of the sample.
For example, as shown in FIG. 4, when the sample is thick (a) and the sample is thin (b),
Interference fringes have occurred. Therefore, an error occurs in the obtained film thickness.
【0006】本発明は、上記従来技術の課題を踏まえて
成されたものであり、薄い厚みの試料でも高精度に膜厚
を測定できる膜厚測定装置を提供することを目的とした
ものである。The present invention has been made in view of the above-mentioned problems of the prior art, and has as its object to provide a film thickness measuring apparatus capable of measuring a film thickness with high accuracy even for a sample having a small thickness. .
【0007】[0007]
【課題を解決するための手段】上記課題を解決するため
の本発明の構成は、試料の吸光特性を利用して膜厚を測
定する膜厚測定装置において、前記試料の吸光特性をス
ペクトルで測定する手段と、この測定されたスペクトル
をフーリエ変換する手段と、このフーリエ変換された値
から大きなピークを検出する手段と、この大きなピーク
のゲインのみを低減させる手段と、この低減されたフー
リエ変換値を逆フーリエ変換する手段と、この逆フーリ
エ変換された値から前記試料の膜厚を求める手段とを備
えた構成としたことを特徴とする。また、前記大きなピ
ークを検出する手段で検出した大きなピークの次数から
前記試料の膜厚を求めるようにしたことを特徴とする。According to a first aspect of the present invention, there is provided a film thickness measuring apparatus for measuring a film thickness using a light absorption characteristic of a sample, wherein the light absorption characteristic of the sample is measured by a spectrum. Means for performing a Fourier transform on the measured spectrum; means for detecting a large peak from the Fourier transformed value; means for reducing only the gain of the large peak; and a means for reducing the reduced Fourier transform value. And a means for calculating the film thickness of the sample from the value obtained by performing the inverse Fourier transform. Further, the film thickness of the sample is obtained from the order of the large peak detected by the large peak detecting means.
【0008】[0008]
【作用】本発明によれば、フーリエ変換により薄膜の干
渉縞を除去できるため、薄膜でも高精度の厚さ測定がで
きる。According to the present invention, since interference fringes of a thin film can be removed by Fourier transform, a highly accurate thickness measurement can be performed even for a thin film.
【0009】[0009]
【実施例】以下、本発明を図面に基づいて説明する。図
1は本発明の膜厚測定装置の一実施例を示す構成図およ
び動作説明のためのフローチャートである。なお、図1
において図3と同一要素には同一符号を付して重複する
説明は省略する。図1(イ)において、受光器5からの
受光信号をA/D変換器6にてA/D変換し、CPU7
に取り込む。このCPU7では、図1(ロ)に示すフロ
ーチャートの流れで演算が行われる。A/D変換された
試料4の吸光特性のスペクトル値をフーリエ変換する。 →フーリエ変換値から大きなピークを検出する。 →大きなピークのゲインだけを低減させる。 →大きなピークのゲインが低減されたフーリエ変換値を
逆フーリエ変換する。 →逆フーリエ変換値から試料4の厚さを計算する。DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will be described below with reference to the drawings. FIG. 1 is a block diagram showing one embodiment of a film thickness measuring apparatus according to the present invention and a flowchart for explaining the operation. FIG.
In FIG. 3, the same elements as those in FIG. 3 are denoted by the same reference numerals, and a duplicate description will be omitted. In FIG. 1A, the light receiving signal from the light receiving device 5 is A / D converted by the A / D converter 6, and the CPU 7
Take in. In the CPU 7, the calculation is performed according to the flow of the flowchart shown in FIG. Fourier transform is performed on the A / D converted spectrum value of the light absorption characteristic of the sample 4. → A large peak is detected from the Fourier transform value. → Reduce only the large peak gain. → Inverse Fourier transform is performed on the Fourier transform value in which the gain of the large peak is reduced. → Calculate the thickness of the sample 4 from the inverse Fourier transform value.
【0010】ここで、図2に測定結果を示す。なお、試
料は厚さ16μmのPET(ポリエチレンテレフタレー
ト)である。(イ)図は、測定されたPETの吸光スペ
クトルである。この測定データをフーリエ変換した結果
が(ロ)図である。(ロ)図に示すフーリエ変換値か
ら、大きなピークである※部(13±2次)部を検出
し、そのゲインだけを低減させるために、0.2倍した
結果が点線部である。この点線部を含めた結果を逆フー
リエ変換したものが、(ハ)図であり、干渉縞が低減さ
れていることがわかる。その後、この逆フーリエ変換結
果を基に、従来と同様の演算が行われ、試料の厚さが求
められる。FIG. 2 shows the measurement results. The sample is a 16 μm thick PET (polyethylene terephthalate). (A) The figure is the measured absorption spectrum of PET. The result of Fourier transform of this measurement data is (b). (B) From the Fourier transform values shown in the figure, the * part (13 ± second order) part which is a large peak is detected, and the result obtained by multiplying by 0.2 in order to reduce only the gain is the dotted line part. The result obtained by performing an inverse Fourier transform on the result including the dotted line is (c), and it can be seen that interference fringes are reduced. Thereafter, based on the result of the inverse Fourier transform, the same operation as in the related art is performed to obtain the thickness of the sample.
【0011】ここで、図2(ロ)のフーリエ変換データ
の大きなピークは、下記の動作により検出できる。 (1) 予め試料の概厚の上限と下限を入力しておき、走査
域を仮に決定しておく。 (2) その領域内でピークを捜す。 また、検出された大きなピークのゲインだけを低減する
ためには、フーリエ変換データの実部(Re)と虚部(I
m)に同一の比率(図2のデータでは、0.2)を乗算
すれば良い。なお、単に、パワー値√(Re2 +I
m2 )に或る比率を乗算し、平方根を求めると、位相も
ずれてしまうことになる。Here, a large peak of the Fourier transform data in FIG. 2B can be detected by the following operation. (1) The upper and lower limits of the approximate thickness of the sample are input in advance, and the scanning area is temporarily determined. (2) Search for a peak in the area. Also, in order to reduce only the gain of the detected large peak, the real part (Re) and the imaginary part (I
m) may be multiplied by the same ratio (0.2 in the data of FIG. 2). Note that simply the power value √ (Re 2 + I
If m 2 ) is multiplied by a certain ratio to obtain the square root, the phase will be shifted.
【0012】次に、或る仮の厚さを入力して、真のピー
クをデータから検出できるため、逆に、このピークの次
数からも厚さを推定することができる。ただし、この値
は、吸光ではなく、光路長であるため、屈折率は外部か
ら入力する必要がある。この場合の干渉縞は、等傾角干
渉のため、次式で表される。 k=m/2nd [cm-1] ただし、 n:屈折率 d:試料の厚さ [cm] k:縞のピッチ [cm-1] m:縞の次数(通常は1) である。Next, since a true peak can be detected from the data by inputting a certain temporary thickness, conversely, the thickness can be estimated from the order of this peak. However, since this value is not the light absorption but the optical path length, it is necessary to input the refractive index from the outside. The interference fringes in this case are expressed by the following equation because of the equi-tilt interference. k = m / 2nd [cm -1 ] where n: refractive index d: sample thickness [cm] k: stripe pitch [cm -1 ] m: order of stripe (usually 1).
【0013】なお、上記実施例において、フーリエ変換
は、FFT(高速フーリエ変換)だけでなく、離散フー
リエ変換などでも良い。また、ピークの検出や低減する
値は、予め干渉縞のない厚い試料によって得られたフー
リエ変換値との比較(パターンマッチなど)によっても
良い。In the above embodiment, the Fourier transform may be not only FFT (fast Fourier transform) but also discrete Fourier transform. Further, the value of peak detection or reduction may be determined by comparing (eg, pattern matching) with a Fourier transform value obtained in advance from a thick sample without interference fringes.
【0014】[0014]
【発明の効果】以上、実施例と共に具体的に説明したよ
うに、本発明によれば、薄い厚みの試料でも高精度に膜
厚を測定できる膜厚測定装置を実現できる。As described above in detail with the embodiments, according to the present invention, it is possible to realize a film thickness measuring apparatus capable of measuring a film thickness with high accuracy even for a sample having a small thickness.
【図面の簡単な説明】[Brief description of the drawings]
【図1】本発明の膜厚測定装置の一実施例を示す構成図
および動作説明のためのフローチャートである。FIG. 1 is a configuration diagram showing an embodiment of a film thickness measuring apparatus according to the present invention and a flowchart for explaining the operation.
【図2】図1装置による測定データ例である。FIG. 2 is an example of data measured by the apparatus of FIG. 1;
【図3】従来の膜圧測定装置の一例を示す構成図であ
る。FIG. 3 is a configuration diagram showing an example of a conventional membrane pressure measuring device.
【図4】図3装置の測定データ例である。FIG. 4 is an example of measurement data of the apparatus in FIG. 3;
5 受光器 6 A/D変換器 7 CPU 5 light receiver 6 A / D converter 7 CPU
Claims (2)
る膜厚測定装置において、 前記試料の吸光特性をスペクトルで測定する手段と、 この測定されたスペクトルをフーリエ変換する手段と、 このフーリエ変換された値から大きなピークを検出する
手段と、 この大きなピークのゲインのみを低減させる手段と、 この低減されたフーリエ変換値を逆フーリエ変換する手
段と、 この逆フーリエ変換された値から前記試料の膜厚を求め
る手段とを備えた構成としたことを特徴とする膜厚測定
装置。1. A film thickness measuring device for measuring a film thickness using the light absorption characteristics of a sample, a means for measuring the light absorption characteristics of the sample by a spectrum, a means for Fourier transforming the measured spectrum, Means for detecting a large peak from the Fourier-transformed value; means for reducing only the gain of the large peak; means for performing an inverse Fourier transform on the reduced Fourier-transformed value; A film thickness measuring device comprising: means for determining a film thickness of a sample.
した大きなピークの次数から前記試料の膜厚を求めるよ
うにしたことを特徴とする請求項1記載の膜厚測定装
置。2. The film thickness measuring apparatus according to claim 1, wherein the thickness of the sample is obtained from the order of the large peak detected by the means for detecting the large peak.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5001169A JP3057943B2 (en) | 1993-01-07 | 1993-01-07 | Film thickness measuring device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5001169A JP3057943B2 (en) | 1993-01-07 | 1993-01-07 | Film thickness measuring device |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH06201335A JPH06201335A (en) | 1994-07-19 |
JP3057943B2 true JP3057943B2 (en) | 2000-07-04 |
Family
ID=11493940
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP5001169A Expired - Fee Related JP3057943B2 (en) | 1993-01-07 | 1993-01-07 | Film thickness measuring device |
Country Status (1)
Country | Link |
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JP (1) | JP3057943B2 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110160450B (en) * | 2019-05-13 | 2020-12-25 | 天津大学 | Method for rapidly measuring height of large step based on white light interference spectrum |
-
1993
- 1993-01-07 JP JP5001169A patent/JP3057943B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
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JPH06201335A (en) | 1994-07-19 |
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