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GB2006201A - Production of nitroguanidine from guanidine nitrate and nitric acid - Google Patents

Production of nitroguanidine from guanidine nitrate and nitric acid

Info

Publication number
GB2006201A
GB2006201A GB7839830A GB7839830A GB2006201A GB 2006201 A GB2006201 A GB 2006201A GB 7839830 A GB7839830 A GB 7839830A GB 7839830 A GB7839830 A GB 7839830A GB 2006201 A GB2006201 A GB 2006201A
Authority
GB
United Kingdom
Prior art keywords
nitric acid
nitroguanidine
guanidine nitrate
production
nitrate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB7839830A
Other versions
GB2006201B (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nigu Chemie GmbH
Original Assignee
Nigu Chemie GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nigu Chemie GmbH filed Critical Nigu Chemie GmbH
Publication of GB2006201A publication Critical patent/GB2006201A/en
Application granted granted Critical
Publication of GB2006201B publication Critical patent/GB2006201B/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C277/00Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
    • C07C277/08Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines
    • CCHEMISTRY; METALLURGY
    • C06EXPLOSIVES; MATCHES
    • C06BEXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00Compositions containing a nitrated organic compound
    • C06B25/34Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Nitroguanidine is produced from guanidine nitrate by reacting guanidine nitrate with nitric acid to give a reaction mixture comprising nitroguanidine, said nitric acid being 92% to 100% w/w, said nitric acid being used in a mole ratio of 2.5 to 5.0 moles of nitric acid per mole of guanidine nitrate, said reaction being carried out at 80 DEG C or less.
GB7839830A 1977-10-12 1978-10-09 Process for the production of nitroguanidine Expired GB2006201B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19772745774 DE2745774A1 (en) 1977-10-12 1977-10-12 PROCESS FOR THE PRODUCTION OF NITROGUANIDINE

Publications (2)

Publication Number Publication Date
GB2006201A true GB2006201A (en) 1979-05-02
GB2006201B GB2006201B (en) 1982-02-24

Family

ID=6021210

Family Applications (1)

Application Number Title Priority Date Filing Date
GB7839830A Expired GB2006201B (en) 1977-10-12 1978-10-09 Process for the production of nitroguanidine

Country Status (5)

Country Link
DE (1) DE2745774A1 (en)
FR (1) FR2405930A1 (en)
GB (1) GB2006201B (en)
IT (1) IT1099364B (en)
ZA (1) ZA785678B (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001046129A2 (en) * 1999-12-20 2001-06-28 Dynamit Nobel Gmbh Explosivstoff- Und Systemtechnik Method for producing nitroguanidine
CN101497579B (en) * 2009-03-26 2012-05-23 里程 Process for producing nitroguanidine
CN102827038A (en) * 2012-08-28 2012-12-19 西安近代化学研究所 Preparation process for nitroguanidine
CN103787922A (en) * 2014-03-04 2014-05-14 章方军 Industrial catalysis method of synthetic nitro substitution compound
CN107721884A (en) * 2017-11-06 2018-02-23 西安近代化学研究所 A kind of nitroguanidine is engineered production technology
CN110204461A (en) * 2019-05-15 2019-09-06 西安万德能源化学股份有限公司 The microchannel crystallization processes and device of a kind of nitroguanidine crystal and nitroguanidine

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19947332A1 (en) * 1999-10-01 2001-04-05 Nigu Chemie Gmbh Multi-stage production of 3-Alkyl-N-nitro-4H-1,3,5-oxadiazine-4-imine compounds from alkylamine and nitric acid via alkylammonium nitrate, alkylguanidine nitrate and alkylnitroguanidine

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2878290A (en) * 1956-07-23 1959-03-17 American Cyanamid Co Nitroguanidine preparation

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001046129A2 (en) * 1999-12-20 2001-06-28 Dynamit Nobel Gmbh Explosivstoff- Und Systemtechnik Method for producing nitroguanidine
WO2001046129A3 (en) * 1999-12-20 2002-01-10 Dynamit Nobel Ag Method for producing nitroguanidine
CN101497579B (en) * 2009-03-26 2012-05-23 里程 Process for producing nitroguanidine
CN102827038A (en) * 2012-08-28 2012-12-19 西安近代化学研究所 Preparation process for nitroguanidine
CN102827038B (en) * 2012-08-28 2014-02-05 西安近代化学研究所 Preparation process for nitroguanidine
CN103787922A (en) * 2014-03-04 2014-05-14 章方军 Industrial catalysis method of synthetic nitro substitution compound
CN103787922B (en) * 2014-03-04 2016-06-01 新昌县鸿吉电子科技有限公司 A kind of Industrial Catalysis method of synthesizing nitryl substitution compound
CN107721884A (en) * 2017-11-06 2018-02-23 西安近代化学研究所 A kind of nitroguanidine is engineered production technology
CN107721884B (en) * 2017-11-06 2020-05-05 西安近代化学研究所 Nitroguanidine engineering production process
CN110204461A (en) * 2019-05-15 2019-09-06 西安万德能源化学股份有限公司 The microchannel crystallization processes and device of a kind of nitroguanidine crystal and nitroguanidine
CN110204461B (en) * 2019-05-15 2022-04-05 西安万德能源化学股份有限公司 Nitroguanidine crystal and microchannel crystallization process and device of nitroguanidine

Also Published As

Publication number Publication date
DE2745774A1 (en) 1979-04-19
IT1099364B (en) 1985-09-18
FR2405930A1 (en) 1979-05-11
GB2006201B (en) 1982-02-24
IT7828659A0 (en) 1978-10-11
FR2405930B1 (en) 1984-08-31
ZA785678B (en) 1979-10-31

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Legal Events

Date Code Title Description
PCNP Patent ceased through non-payment of renewal fee