EP1827142B1 - Defibration of tobacco material - Google Patents
Defibration of tobacco material Download PDFInfo
- Publication number
- EP1827142B1 EP1827142B1 EP05811333A EP05811333A EP1827142B1 EP 1827142 B1 EP1827142 B1 EP 1827142B1 EP 05811333 A EP05811333 A EP 05811333A EP 05811333 A EP05811333 A EP 05811333A EP 1827142 B1 EP1827142 B1 EP 1827142B1
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- EP
- European Patent Office
- Prior art keywords
- gap
- tobacco material
- tobacco
- pressure
- shearing
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000463 material Substances 0.000 title claims abstract description 141
- 241000208125 Nicotiana Species 0.000 title claims abstract description 125
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 125
- 238000010008 shearing Methods 0.000 claims abstract description 21
- 230000000391 smoking effect Effects 0.000 claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims description 75
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- 238000011144 upstream manufacturing Methods 0.000 claims description 5
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/18—Other treatment of leaves, e.g. puffing, crimpling, cleaning
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
Definitions
- the present invention relates to the defibering of tobacco material.
- it relates to the production of shredded tobacco material by defibration and, more particularly, the invention shreds a tobacco rib material to produce a product having particularly advantageous properties which can ultimately be used to make smoking articles.
- tobacco preparation i. in those processing operations that take place prior to actual cigarette making and packaging, the major tobacco materials, namely tobacco leaves (lamina) and tobacco stems, undergo several process steps before they can be used to make smoking articles.
- Smoking articles may e.g. Cigarettes, cigarillos, rolls and sticks products as well as fine cut or pipe tobacco. Tobacco ribs can also be used at least partially in all of these smoking articles.
- the said tobacco ribs may be whole tobacco ribs, which are also referred to below as tube ribs, or incompletely shredded tubular ribs, which are also referred to below as winnowings.
- Winnowings are coarse shredded rib particles that are usually sorted out by sight processes from already shredded tobacco because they are undesirable in smoking articles due to their size and shape and would degrade the smoking article quality.
- ZHV Winnowings Winnowings from cigarette manufacturing pack
- TV Winnowings Winnowings are usually recycled or disposed of as waste.
- the method of ribbed shredding has, in addition to the very high necessary processing humidity of e.g. about 40 to 45% the big disadvantage that the shredded material has too many small parts (fines), namely about 15 to 30%, depending on the process, which must be screened and either discarded or recycled to film recycled.
- This disadvantage also has some other methods, e.g. Use mills in ribbed mincing.
- rib processing processes process the ribs into tobacco sheet for mixing with a leaf tobacco mix. For this ribs are crushed into very small parts.
- tobacco sheet manufacturing processes are known for example from DE 40 05 656 C2 and the DE 43 25 497 A1 known.
- the tobacco foil processes work with additives such as binders (eg starch), humectants (eg glycerine) and other additives (eg flavor enhancers), and they produce a product depending on the process moderate to poor fillability and sensory deficits compared to leaf tobacco.
- a process for producing agglomerates is known.
- the finest tobacco dust particles are mixed with binders and liquid as in the aforementioned methods, and then ejected from a compression and heating chamber to form agglomerates, that is, the larger units.
- binders there are the above-mentioned disadvantages of using binders.
- Another disadvantage is that such a process is in principle not suitable for processing coarser tobacco material, since it is designed to produce larger agglomerates from small amounts of particles. A shredding of tobacco material is not possible in this process.
- WO 94/01007 From the WO 94/01007 is a method for processing consisting of dried or mechanically dehydrated beet pulp or dried or mechanically dehydrated beet pulp containing material to feed known, wherein the material is compressed by a conveying element against the discharge end of a container, so that there with simultaneous increase in temperature on the material acting elevated pressure, and there is expressed from the container through a discharge out, which is changeable and closable by a counter-pressure element in the passage cross-section.
- the object of the present invention to enable the production of shredded tobacco material without the above-mentioned disadvantages occurring.
- the invention should make it possible to produce by comminution a tobacco product which is suitable directly or with little post-processing as a smoking article material. Furthermore, the processing time and complexity should be reduced.
- the above-defined invention provides, inter alia, the following advantages:
- the rib materials used are upgraded, so that the product produced has only slight sensory deficits compared to leaf tobacco and are therefore used to a greater extent in the tobacco blend of a smoking article can.
- the product produced has a well-shredded and shredded structure, and is therefore optically scarcely discernible in cut-tobacco mixtures.
- the processes are simple and inexpensive, resulting in low investment and production costs.
- the space requirement for the devices to be used is very low due to the low complexity of the method.
- the defibration produces a product that can result in a reduced CO / condensate ratio in cigarette smoke compared to otherwise processed rib products.
- the invention enables continuous processing within a very short period of time; long storage times are avoided.
- the advantages of the method according to the invention are based in particular on the combination of relaxation of the pressurized and heated tobacco material and the shear in the gap, whereby a very good defibering takes place overall.
- the device according to the invention is concerned, its advantages are based in particular on the fact that the optimally shredded product can be produced by the mutually moving gap walls with high consistency and reliability.
- the product obtainable by the invention in addition to the above-mentioned advantages, still has a filling capacity which is in the range of leaf tobacco and enables a high material yield; There are a few small parts. Storage times for tobacco rib material are greatly reduced or unnecessary.
- the tobacco raw material may principally comprise a coarse tobacco material, in particular having a particle size of more than 2 mm. It can be a tobacco rib material or a winnowing material, in particular with a rib size of more than 2 mm. It should be noted that tobacco materials such as pipe fins, winnowings, short stems or stem fibers but also scraps (small leaf tobacco particles), other small tobacco pieces or a mixture of the components mentioned can be used.
- the process according to the invention offers the possibility of processing the tobacco materials used without the addition of structure-forming materials to a product which can be used in the smoking article.
- the tobacco starting material can be heated to a temperature of 60 ° to 180 ° C, in particular 100 ° to 140 ° C, preferably 110 ° to 130 ° C and to a pressure of 10 to 200 bar, in particular 40 to 150 bar, preferably 60 to 120 bar, wherein the residence time of the tobacco material in a continuous pass can be less than 3 minutes, in particular less than 2 minutes and preferably less than 1 minute.
- the tobacco starting material is mechanically pressurized, in particular mechanically pressed in a chamber against the shear gap.
- the material can be pressurized by means of a screw conveyor, which presses the material against the outlet side of the chamber of a heatable screw conveyor on which the shear gap is located.
- the material can also be coarsely pre-shredded in the chamber or in the screw conveyor during transport to the shearing gap or coarsely pre-shredded.
- the shear gap is biased closed according to one embodiment and is opened intermittently by the pressure of the tobacco material, wherein the material passes through the gap.
- the material can also advantageously be passed through a continuously opened shear gap.
- the shear gap walls perform a relative movement during the passage of the tobacco material, even at a constant gap distance, ie with a continuous gap opening.
- the relaxation of the tobacco material takes place when passing through the shear gap in one embodiment to atmospheric pressure.
- tobacco material conditioning may take place with or without casing and / or flavor feeding, with the increase in material moisture from about 9 to 12% to about 18 to 45%, more preferably 20 to 30%.
- the tobacco material After relaxation and passing through the shear gap, the tobacco material According to one embodiment, have a moisture content of about 14 to 42%, preferably 16 to 18%, and it is possible to cool the tobacco material behind the shear gap at room temperature and under atmospheric pressure and thereby to dry or let it dry until it Has moisture of about 12 to 16%.
- the shredded, pressure-shredded tobacco material from the method according to the invention can be supplied directly to further processing as a smoking article material if the tobacco raw material is a winnowing material or if sufficient pre-shredded material is used.
- the shredded, pressure-shredded tobacco material may be subjected to classification according to the method of the invention, e.g. if the starting material is a very coarse rib material.
- the materials which have been rejected during classification are subjected to the process again, and the residue which has not been separated out can be directly supplied for further use as a smoking article material.
- the gap walls of the device may be away from each other and movable towards each other; the gap walls may be biased toward the closed state of the gap.
- the gap walls with a fixed or fixed adjustable distance against each other be movable, in particular, the gap walls at a fixed distance of 0.01 mm to 2mm, in particular 0.1 mm to 0.5 mm.
- the gap walls on roughness or profiles in particular groove or Wienrillenprofil isten which are arranged longitudinally or transversely to the gap wall movement direction and have a depth of up to 2 to 3 mm.
- the distances of the shear gap are of course correspondingly larger than indicated above.
- the gap wall arranged on the pressure chamber is fixed, while the counter wall is arranged movably on a counter holder provided with a movement drive.
- the gap walls may be movable against each other continuously or intermittently, in one or two directions, or reciprocally.
- the gap may be an annular gap, preferably a cone gap.
- the pressure chamber has a plug screw as a conveyor for conveying the tobacco material from the inlet to the outlet.
- a pressure generation by mechanical means such as is produced for example by a plug screw, in the context of the invention can in principle also take place otherwise. It is not excluded that the pressure is generated mechanically in other ways, for example by a piston device or not mechanically or not only mechanically via a gas pressure.
- a Schneckenhunt pressure conditioning device is set in the same or in an upstream pressure chamber housing a Schneckenhunt pressure conditioning device.
- a pressure conditioning device is for example in the DE 103 04 629 A1 described, and it is very well suited for combination with the Druckzermaschineung invention.
- the pressure conditioning device may include all of the structural features disclosed in U.S. Pat FIG. 1 and the associated description of DE 103 04 629 A1 and these design features are hereby incorporated by reference.
- the smoking article comprises a shredded, shredded tobacco material product made by any of the foregoing methods or apparatuses. It may have the tobacco material product in a proportion of up to 50%, in particular from 0.5% to 35% and particularly preferably from 0.5% to 25%.
- the invention further includes the use of a one or two worm conveyor with a shear gap outlet for defibering tobacco material.
- a shearing gap is an opening in which material is sheared during passage.
- the process according to the invention can be carried out in all process variants and the device according to the invention can be used in all embodiments.
- FIG. 1 the schematic procedure of tobacco preparation is FIG. 1 represented by ribs from the tubular to use in the final product.
- Moisture values are given in terms of wetness and represent recommended and preferred values. Those skilled in the art can set optimum conditions if they follow the principles of the invention and thus adapt to optimal conditions of a particular device according to the invention (expansion plant).
- the pipe fins typically enter the conditioning at a moisture content of about 10%.
- the conditioning can be carried out under atmospheric conditions, advantageous is a conditioning at superatmospheric pressure, such as in the previously mentioned DE 103 04 629 A1 described.
- a conditioning at superatmospheric pressure such as in the previously mentioned DE 103 04 629 A1 described.
- the addition of casing and flavoring agents can also be carried out.
- the ribs leave the conditioning with a humidity of about 18% to 45% and are handed over to the defibration of the invention. Details of the defibration will be described below, also with reference to embodiments according to the FIGS. 3 to 5 ,
- the ribs When shredded, the ribs usually lose some moisture, so that now the shredded ribs with 16% to 42% moisture are classified. There too large rib parts are conveyed back again and go through the previously described sequence again. Typically, this proportion is low and is less than 10% of the total mass.
- the other portion of the shredded ribs can now be treated differently depending on the desired process parameters. At humidities of, for example, 14% to 15%, the ribs go directly into the tobacco mixture for the end product smoking article. At higher humidities, eg 15% Up to 40%, the ribs still undergo expansion and drying and can then be added at the same 14% to 15% moisture in the mixture for the final product.
- FIG. 2 shows the process, in particular with regard to the defibration according to the invention and the process steps taking place immediately thereafter, somewhat more detailed and with more limited or slightly different moisture values.
- these values can always be selected and set by experts depending on the desired end product and the overall process parameters.
- the FIG. 2 actually includes the first two process steps shown in boxes FIG. 1 (Conditioning, defibration, sifter).
- the tobacco material in particular rib materials such as pipe lips, Winnowings, Short Stems and Stem Fibers, but also Scraps (small Blatttabakteilchen), other tobacco small parts or even a mixture of the individual enumerated components are conditioned in the first process step and depending on the material to about 20 % to 30% moistened.
- the moistening and, if appropriate, the addition of flavor and casing can conventionally be carried out under atmospheric pressure with a short storage time or even without storage time or under pressure, such as in the DE 100 38 114 A1 and the DE 103 04 629 A1 is described.
- Short Stems or Stem Fibres pre-crushing of the material can be carried out on particle sizes between 2 and 15 mm, which is depending on the selected method and partially already frayed.
- the pre-shredding can be done by all common methods. However, dust and small parts should be avoided (smaller quantities of very small parts are tolerable). With the smaller starting materials, pre-shredding can be completely dispensed with.
- the material is heated (about 60 ° to 180 ° C) and pressurized (about 10 to 200 bar), on the one hand to achieve the desired taste improvement by chemically running processes (eg Maillard reaction or caramelization) and on the other hand Sufficient energy to store the defibration by shearing and relaxing over a shear gap.
- chemically running processes eg Maillard reaction or caramelization
- Sufficient energy to store the defibration by shearing and relaxing over a shear gap can be carried out with commercially available stuffing screws whose housing can also be heated in particular. Such systems will be described in more detail below.
- the tobacco material loses further moisture by evaporative cooling, so that it is possible to come without a dryer to a final product moisture, which allows a direct blending into the leaf tobacco mixture.
- Whether a classification of the shredded tobacco material and the associated return of too large particles in the process is necessary depends on the material to be crushed and the type of pre-crushing. For ZHV winnowings or similar sized material, classification is usually not necessary.
- the extruder instead of e.g. preferably pre-shredded with a mill or crusher and with a heated plug screw to produce pressure and temperature, it is also preferable to use a single- or twin-screw extruder, because here the material pre-shredded by shearing, heated by the friction during crushing simultaneously and by the compression of the screw, a corresponding pressure is built up. So you can summarize with a device equal to three necessary process steps. In this case, the extruder must be designed so that the material is not otherwise comminuted and plasticized as usual in extrusion processes and desired (high density), but the fiber structure of the tobacco material is maintained. So there should be no extrusion in the classical sense.
- a DruckzerfaserungsVoroplasty invention is shown, which is provided overall with the reference numeral 1. It has a chamber housing 2 and an auger 3 provided in this, which is rotated via the motor 4. Furthermore, in the drawing of FIG. 3 a tobacco material inlet 5 and optional inlets, for water, casing (and / or flavor) and steam are shown, bearing the reference numerals 6 and 7. At the outlet end (in the figure on the right), the chamber has a head 8, which forms an inner cone. The inner cone wall of the head 8 forms together with the outer cone wall of the outer cone 10, the gap 9 through which the subsidized by the screw 3 tobacco material can escape. At the gap tip of the inner cone 8 is an opening to the interior of the chamber 2 out. The leaked, shredded tobacco material is designated by the reference numeral 12.
- the outer cone 10 is positioned by a counter-holder 11, which can simultaneously provide a rotary drive for the cone body 10.
- the cone 10 By means of this rotary drive, the cone 10, as shown by the curved arrow, are rotated about the central axis.
- the connection between the counter-holder 11 and the cone 10 is represented by a double arrow, which means that the cone 10 can be moved up on the axis of the inner cone 8. There he can be held firmly in its axial position, but also be arranged axially movable.
- the width of the gap can be adjusted or adjusted, in addition, a back pressure to the left, ie generated in the direction of the closure of the gap 9 out, preferably by hydraulic means.
- the first part of the defibration of the tobacco ribs is carried out according to the invention under superatmospheric pressure.
- This overpressure is generated by the tobacco material, in the special case conditioned tobacco ribs are conveyed in the chamber 2 by the screw 3, after they were introduced via the inlet 5.
- a shear gap outlet At the end of the auger there is a shear gap outlet, which almost closes off the delivery chamber similar to an extruder.
- this stencil outlet is as in FIG. 3 shown, designed as an annular gap, namely as a cone gap 9, the gap width by the outer cone 10 (punch) is adjustable.
- the ribs are under an increased pressure (up to 200 bar) and an elevated temperature (in particular well above 100 ° C).
- conditioning and pressure fraying depends on the pressure conditions at which conditioning is performed.
- the tobacco material is simply conveyed via conveyors or a conveyor belt into the inlet 5, e.g. an inlet funnel fed.
- the conditioning can then take place, for example, at an intermediate point of the housing 2 by introducing water and casing, as indicated by the reference numeral 6.
- the crucial step of the defibration takes place during the passage and the exit from the gap 9.
- the tobacco ribs are subjected to shearing between the gap walls, and upon exiting the gap, the previously mentioned flash evaporation takes place.
- the interaction of these effects produces the very well-shredded process product, which can be used at least to a large extent already in the production of smoking articles.
- This rotation can be continuous or interrupted in one direction or change the direction of rotation.
- the rotation may be complete or may include only quarter / or third turns or smaller / larger units.
- the surface of at least one of the cones, the inner cone on the head 8 or the outer cone on the punch 10 is roughened or profiled, for example by the introduction of grooves or cross grooves up to 2 or 3 mm depth.
- the depth and the course (direction) of the grooves can be adjusted in any way.
- blockages can be greatly reduced. This gives more homogeneous pressure conditions, which also lead to a more homogeneous end product.
- the resulting defibrated process product exhibits similar appearance and usage characteristics as are known from shredded ribs.
- the pressure defibration according to the invention does not have the disadvantage of a high dust accumulation, as it is known in shredding ribs, also does not need to be pre-moistened as much as shredding, so that subsequent drying can be greatly reduced or eliminated.
- the pressure conditioning device 20 is generally such as shown in the DE 103 04 629 A1 especially in FIG. 1 and the associated description. Reference is additionally made to this. It has a tobacco material inlet 25 and a differential-pressure-resistant rotary valve 26, via which the tobacco material is introduced into the pressure chamber 21, where it is transported by means of a screw conveyor 22. The screw conveyor 22 is driven by the motor 24.
- an outlet 27 for the tobacco material is shown, which simultaneously forms the inlet for the pressure-fusing device 1.
- the tobacco material is transferred under the pressure of the chamber 21 into the inlet of the pressure-fusing device 1.
- FIG. 4 it is preferable to avoid a pressure drop when passing from the pressure conditioning into the pressure defibration in order to be able to provide a superatmospheric pressure over the entire process range from the beginning of the conditioning to the defibration, as in FIG. 4 is shown.
- the entire facility in FIG. 4 corresponds to the box "conditioning (and casing) / defibration" in FIG. 1 .
- the ribs are fed via the differential-pressure-tight rotary valve 26.
- the tightness of the lock 26 on one side and the narrow annular gap 9, which is always filled with shredded ribs in operation, allow to maintain a superatmospheric pressure throughout the combined device.
- the tightness of the rotary valve 26 can be optimized for this purpose by heating its housing.
- the ribs After the introduction of the tobacco ribs in the chamber 21, the ribs are under superatmospheric pressure, which is maintained by steam supply against the naturally leaking rates of the rotary valve 26 (column and Schöpfvolumen). The steam heats the ribs and increases the humidity. In principle, in such a chamber, a drying with supersaturated steam is possible, but it is usually already for the application to defibration advantageous if the registered ribs have significantly higher humidities.
- the screw conveyor 22 By means of the screw conveyor 22, the tobacco ribs are conveyed through the conditioning chamber 21. In this case, various settings can be made (pitch of the screw, speed and inclination of the chamber), with which the residence time of the tobacco ribs can be adjusted. It is usually between 2 and 10 minutes.
- the ribs are then transferred through the outlet 27 in the Druckzerfaserungsvorraum 1, and this entry can be easily achieved if the housing also funnel-shaped is trained.
- the typical residence time of the ribs in the area of defibration is less than 2 minutes, in particular less than 1 minute. The ribs then leave the pressure defibration in the desired, previously described condition.
- a conditioning screw under atmospheric pressures can also be used.
- FIG. 5 shows a further embodiment of a plant with combined pressure conditioning and pressure defibration.
- the pressure conditioning device 20 and the pressure fiberizer 1 are basically constructed as in FIGS Figures 3 and 4 illustrated, why the designation of the individual components is unnecessary.
- the difference to the embodiment according to FIG. 4 is that the auger of the conditioning device 20 and the fiberizing screw of the pressure fusing device 1 sit on an axle and can be driven by a single motor. If the same rotational speed is then used for both screws, the different residence times in both process steps can be achieved by other means, eg by different cross-sectional volumes, fallback possibilities in the area of conditioning, etc.
- the conditioning measures and the steam injection are made by the corresponding already existing introduction possibilities of the pressure conditioning device, so it must not be made appropriate entries on the Druckzerfaserungsvorraum.
- the introduction of flavor and / or casing can be carried out both in the pressure range, ie in one of the pressure chambers, or atmospherically, ie outside the chambers.
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Manufacturing Of Cigar And Cigarette Tobacco (AREA)
Abstract
Description
Die vorliegende Erfindung betrifft die Zerfaserung von Tabakmaterial. Insbesondere betrifft sie die Herstellung von zerkleinertem Tabakmaterial durch Zerfaserung, und speziell wird mit der Erfindung ein Tabakrippenmaterial so zerfasert, dass ein Produkt mit ganz besonders vorteilhaften Eigenschaften hergestellt wird, welches letztendlich zur Herstellung von Rauchartikeln verwendet werden kann.The present invention relates to the defibering of tobacco material. In particular, it relates to the production of shredded tobacco material by defibration and, more particularly, the invention shreds a tobacco rib material to produce a product having particularly advantageous properties which can ultimately be used to make smoking articles.
Bei der Tabakvorbereitung, d.h. bei denjenigen Verarbeitungsprozessen, die vor der eigentlichen Zigarettenherstellung und Verpackung stattfinden, werden die wichtigsten Tabakmaterialien, nämlich Tabakblätter (Lamina) und Tabakrippen (Stems) mehreren Prozessschritten unterzogen, bevor sie für die Herstellung von Rauchartikeln verwendet werden können. Rauchartikel können dabei z.B. Zigaretten, Zigarillos, Rolls- und Sticks-Produkte sowie auch Feinschnitt oder Pfeifentabak sein. In all diesen Rauchartikeln können auch Tabakrippen zumindest teilweise verwendet werden.In tobacco preparation, i. in those processing operations that take place prior to actual cigarette making and packaging, the major tobacco materials, namely tobacco leaves (lamina) and tobacco stems, undergo several process steps before they can be used to make smoking articles. Smoking articles may e.g. Cigarettes, cigarillos, rolls and sticks products as well as fine cut or pipe tobacco. Tobacco ribs can also be used at least partially in all of these smoking articles.
Die genannten Tabakrippen können ganze Tabakrippen sein, die im Folgenden auch Rohrippen genannt werden, oder unvollständig zerkleinerte Rohrippen, die im Folgenden auch Winnowings genannt werden. Winnowings sind grob zerkleinerte Rippenteilchen, die in der Regel durch Sichtprozesse aus bereits zerkleinertem Tabak aussortiert werden, da sie aufgrund ihrer Größe und Form in Rauchartikeln unerwünscht sind und die Rauchartikelqualität verschlechtern würden. Man unterscheidet noch Winnowings aus der Zigarettenherstellung (ZHV-Winnowings = Winnowings aus ZigarettenherstellungNerpackung) und solche aus der Tabakvorbereitung (TV-Winnowings). Winnowings werden üblicherweise recycelt oder als Abfallprodukt entsorgt.The said tobacco ribs may be whole tobacco ribs, which are also referred to below as tube ribs, or incompletely shredded tubular ribs, which are also referred to below as winnowings. Winnowings are coarse shredded rib particles that are usually sorted out by sight processes from already shredded tobacco because they are undesirable in smoking articles due to their size and shape and would degrade the smoking article quality. One differentiates still Winnowings from the cigarette production (ZHV Winnowings = Winnowings from cigarette manufacturing pack) and those from the tobacco preparation (TV Winnowings). Winnowings are usually recycled or disposed of as waste.
Herkömmliche Rippenzerkleinerungsverfahren wie z.B. das Schneiden oder Schreddern stellen für den Tabakvorbereitungsprozess eine große Herausforderung dar. Das Rippenmaterial muss für diese Prozesse auf relativ hohe Feuchten von 30 bis 50% gleichmäßig bis auf den Kern durchfeuchtet werden, um ein optimales Zerkleinerungsergebnis ohne zu hohe Materialverluste durch Tabakstaub zu gewährleisten. Auch nachgeschaltete Expansionsprozesse zur Füllfähigkeitssteigerung benötigen häufig möglichst hohe Eingangsfeuchten. Da sich das Rippenmaterial aufgrund seiner groben Beschaffenheit (holzig und mit Materialdicken von 1 bis ca. 15 mm) nur sehr schwer gleichmäßig konditionieren (erwärmen, kühlen, trocknen und auffeuchten) lässt, sind die meisten Konditionierungsprozesse an sehr lange Verweilzeiten gebunden. Dies trifft insbesondere für die Befeuchtung zu, die sogar eine Zwischenlagerung des befeuchteten Materials von meist 2 bis 6 Stunden notwendig macht, um das Eindringen der Feuchte bis ins Materialinnere sicher zu stellen. Sogar zweistufige Auffeuchtungsprozesse finden Anwendung. Die hohe notwendige Auffeuchtung für die beschriebenen herkömmlichen Standardverfahren ist mit einem weiteren großen Nachteil verbunden, nämlich der Notwendigkeit des Trocknens des zerkleinerten Tabakmaterials, wobei solche Trocknungsprozesse hohe Energie- und Anlagenkosten verursachen.Conventional ribbing operations such as cutting or shredding pose a major challenge to the tobacco preparation process The rib material must be moistened evenly to the core to relatively high moistures of 30 to 50% for these processes, in order to ensure an optimum crushing result without excessive material losses due to tobacco dust. Subsequent expansion processes to increase filling capacity often require the highest possible input moisture content. Since the fin material is very difficult to uniformly condition (heat, cool, dry and moisturize) due to its coarse nature (woody and with material thicknesses of 1 to approx. 15 mm), most conditioning processes are linked to very long residence times. This is especially true for the humidification, which makes even an intermediate storage of humidified material of usually 2 to 6 hours necessary to ensure the penetration of moisture into the material interior. Even two-stage moistening processes are used. The high level of humidification required for the conventional standard processes described involves another major drawback, namely the need to dry the shredded tobacco material, such drying processes causing high energy and equipment costs.
Das Verfahren des Rippenschredderns hat neben der sehr hohen notwendigen Verarbeitungsfeuchte von z.B. ca. 40 bis 45% den großen Nachteil, dass das geschredderte Material zu viele Kleinteile (Fines) besitzt, nämlich ca. 15 bis 30%, je nach Prozessausführung, welche abgesiebt werden müssen und entweder verworfen oder zur Folie verarbeitet wieder recycelt werden. Diesen Nachteil besitzen auch noch einige andere Verfahren, die z.B. Mühlen bei der Rippenzerkleinerung benutzen.The method of ribbed shredding has, in addition to the very high necessary processing humidity of e.g. about 40 to 45% the big disadvantage that the shredded material has too many small parts (fines), namely about 15 to 30%, depending on the process, which must be screened and either discarded or recycled to film recycled. This disadvantage also has some other methods, e.g. Use mills in ribbed mincing.
Andere Rippenverarbeitungsprozesse verarbeiten die Rippen zu Tabakfolie, um diese dann einer Blatttabakmischung beizumischen. Hierzu werden Rippen zu Kleinstteilen zerkleinert. Solche Tabakfolien-Herstellungsverfahren sind beispielsweise aus der
Aus der
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Es ist die Aufgabe der vorliegenden Erfindung, die Herstellung von zerkleinertem Tabakmaterial zu ermöglichen, ohne dass die oben genannten Nachteile auftreten. Insbesondere soll die Erfindung möglich machen, durch Zerkleinerung ein Tabakprodukt herzustellen, welches sich unmittelbar oder mit nur wenig Nachverarbeitung als Rauchartikelmaterial eignet. Ferner soll die Verarbeitungszeit und -Komplexität verringert werden.It is the object of the present invention to enable the production of shredded tobacco material without the above-mentioned disadvantages occurring. In particular, the invention should make it possible to produce by comminution a tobacco product which is suitable directly or with little post-processing as a smoking article material. Furthermore, the processing time and complexity should be reduced.
Diese Aufgabe wird gemäß der Erfindung durch ein Verfahren gemäß dem Anspruch 1 gelöst, sowie durch eine Vorrichtung gemäß dem Anspruch 18. Ferner umfasst die Erfindung noch eine Verwendung gemäß Anspruch 32. Die Unteransprüche beschreiben vorteilhafte Ausführungsformen der Erfindung.This object is achieved according to the invention by a method according to
Die oben definierte Erfindung bringt unter anderem die folgenden Vorteile mit sich: Die eingesetzten Rippenmaterialien erhalten eine Aufwertung, so dass das erzeugte Produkt nur geringe sensorische Defizite gegenüber Blatttabak hat und deshalb in erhöhtem Umfang in der Tabakmischung eines Rauchartikels Verwendung finden kann. Das erzeugte Produkt hat eine gut zerfaserte und zerkleinerte Struktur, und ist deshalb in Schnitttabakmischungen optisch kaum auszumachen. Die Verfahrensabläufe sind einfach und unaufwändig, was zu geringen Investitions- und Produktionskosten führt. Der Raumbedarf für die zu verwendenden Vorrichtungen ist aufgrund der niedrigen Komplexität des Verfahrens sehr gering. Die Zerfaserung erzeugt ein Produkt, das im Zigarettenrauch, verglichen mit anders prozessierten Rippenprodukten, zu einem reduzierten CO/Kondensat-Verhältnis führen kann. Die Erfindung ermöglicht eine kontinuierliche Verarbeitung innerhalb sehr kurzer Zeiträume; lange Lagerungszeiten werden vermieden.The above-defined invention provides, inter alia, the following advantages: The rib materials used are upgraded, so that the product produced has only slight sensory deficits compared to leaf tobacco and are therefore used to a greater extent in the tobacco blend of a smoking article can. The product produced has a well-shredded and shredded structure, and is therefore optically scarcely discernible in cut-tobacco mixtures. The processes are simple and inexpensive, resulting in low investment and production costs. The space requirement for the devices to be used is very low due to the low complexity of the method. The defibration produces a product that can result in a reduced CO / condensate ratio in cigarette smoke compared to otherwise processed rib products. The invention enables continuous processing within a very short period of time; long storage times are avoided.
Die Vorteile des erfindungsgemäßen Verfahrens beruhen insbesondere auf der Kombination von Entspannung des unter Druck gesetzten und erwärmten Tabakmaterials und der Scherung im Spalt, wodurch insgesamt eine sehr gute Zerfaserung erfolgt. Was die erfindungsgemäße Vorrichtung betrifft, so beruhen deren Vorteile insbesonders darauf, dass durch die sich gegeneinander bewegenden Spaltwände mit hoher Konstanz und Zuverlässigkeit das optimal zerfaserte Produkt hergestellt werden kann. Das durch die Erfindung herstellbare Produkt weist zusätzlich zu den oben genannten Vorteilen noch eine Füllfähigkeit auf, die im Bereich von Blatttabak liegt und ermöglicht eine hohe Materialausbeute; es entstehen wenige Kleinteile. Lagerzeiten für Tabakrippenmaterial werden stark verkürzt bzw. überflüssig.The advantages of the method according to the invention are based in particular on the combination of relaxation of the pressurized and heated tobacco material and the shear in the gap, whereby a very good defibering takes place overall. As far as the device according to the invention is concerned, its advantages are based in particular on the fact that the optimally shredded product can be produced by the mutually moving gap walls with high consistency and reliability. The product obtainable by the invention, in addition to the above-mentioned advantages, still has a filling capacity which is in the range of leaf tobacco and enables a high material yield; There are a few small parts. Storage times for tobacco rib material are greatly reduced or unnecessary.
Das erfindungsgemäße Verfahren kann in folgenden Ausführungsvarianten durchgeführt werden:The process according to the invention can be carried out in the following variants:
Das Tabak-Ausgangsmaterial kann vornehmlich ein grobes Tabakmaterial, insbesondere mit einer Teilchengröße von mehr als 2 mm aufweisen. Es kann ein Tabakrippenmaterial bzw. ein Winnowing-Material sein, insbesondere mit einer Rippengröße von mehr als 2 mm. Anzumerken ist hierzu, dass Tabakmaterialien wie Rohrippen, Winnowings, Short Stems oder Stem Fibres aber auch Scraps (kleine Blatttabakteilchen), sonstige Tabakkleinteile oder eine Mischung aus den genannten Komponenten zum Einsatz kommen kann.The tobacco raw material may principally comprise a coarse tobacco material, in particular having a particle size of more than 2 mm. It can be a tobacco rib material or a winnowing material, in particular with a rib size of more than 2 mm. It should be noted that tobacco materials such as pipe fins, winnowings, short stems or stem fibers but also scraps (small leaf tobacco particles), other small tobacco pieces or a mixture of the components mentioned can be used.
Im Gegensatz zur Folienherstellung bietet das erfindungsgemäße Verfahren die Möglichkeit die eingesetzten Tabakmaterialien ohne den Zusatz strukturbildender Materialien zu einem im Rauchartikel einsetzbaren Produkt zu verarbeiten.In contrast to film production, the process according to the invention offers the possibility of processing the tobacco materials used without the addition of structure-forming materials to a product which can be used in the smoking article.
Das Tabak-Ausgangsmaterial kann auf eine Temperatur von 60° bis 180° C, insbesondere 100° bis 140°C, vorzugsweise 110° bis 130°C erwärmt werden und auf einen Druck von 10 bis 200 bar, insbesondere 40 bis 150 bar, vorzugsweise 60 bis 120 bar gebracht werden, wobei die Verweilzeit des Tabakmaterials im kontinuierlichen Durchlauf bei weniger als 3 Minuten, insbesondere weniger als 2 Minuten und vorzugsweise weniger als 1 Minute liegen kann.The tobacco starting material can be heated to a temperature of 60 ° to 180 ° C, in particular 100 ° to 140 ° C, preferably 110 ° to 130 ° C and to a pressure of 10 to 200 bar, in particular 40 to 150 bar, preferably 60 to 120 bar, wherein the residence time of the tobacco material in a continuous pass can be less than 3 minutes, in particular less than 2 minutes and preferably less than 1 minute.
Bevorzugt wird das Tabak-Ausgangsmaterial mechanisch unter Druck gesetzt, insbesondere mechanisch in einer Kammer gegen den Scherspalt gepresst. Dabei kann das Material mittels einer Förderschnecke unter Druck gesetzt werden, die das Material gegen die Austrittsseite der Kammer eines beheizbaren Schneckenförderers presst, an der sich der Scherspalt befindet. Das Material kann ferner in der Kammer bzw. im Schneckenförderer während des Transports zum Scherspalt grob vorzerkleinert bzw. grob vorzerfasert werden.Preferably, the tobacco starting material is mechanically pressurized, in particular mechanically pressed in a chamber against the shear gap. In this case, the material can be pressurized by means of a screw conveyor, which presses the material against the outlet side of the chamber of a heatable screw conveyor on which the shear gap is located. The material can also be coarsely pre-shredded in the chamber or in the screw conveyor during transport to the shearing gap or coarsely pre-shredded.
Der Scherspalt ist gemäß einer Ausführungsform vorgespannt verschlossen und wird durch den Druck des Tabakmaterials intermittierend geöffnet, wobei das Material durch den Spalt hindurchgeht. Andererseits kann das Material auch vorteilhafterweise durch einen kontinuierlich geöffneten Scherspalt hindurchgeführt werden.The shear gap is biased closed according to one embodiment and is opened intermittently by the pressure of the tobacco material, wherein the material passes through the gap. On the other hand, the material can also advantageously be passed through a continuously opened shear gap.
Die Scherspaltwände führen beim Durchführen des Tabakmaterials eine Relativbewegung aus, und zwar auch bei einem gleich bleibenden Spaltabstand, d.h. bei kontinuierlicher Spaltöffnung. Die Entspannung des Tabakmaterials erfolgt beim Durchgang durch den Scherspalt bei einer Ausführungsform auf atmosphärischen Druck. Vor oder während der Erwärmung und Druckerzeugung kann eine Tabakmaterial-Konditionierung mit oder ohne Casing und/oder Flavourzuführung stattfinden, wobei die Erhöhung der Materialfeuchte von ungefähr 9 bis 12% auf etwa 18 bis 45% insbesondere 20 bis 30% erfolgt. Nach der Entspannung und hindurchführung durch den Scherspalt wird das Tabakmaterial gemäß einer Ausführungsvariante eine Feuchte von etwa 14 bis 42%, vorzugsweise 16 bis 18% aufweisen, und es besteht die Möglichkeit, das Tabakmaterial hinter dem Scherspalt bei Raumtemperatur und unter atmosphärischen Druck zu kühlen und dabei zu trocknen bzw. trocknen zu lassen bis es eine Feuchte von etwa 12 bis 16% aufweist.The shear gap walls perform a relative movement during the passage of the tobacco material, even at a constant gap distance, ie with a continuous gap opening. The relaxation of the tobacco material takes place when passing through the shear gap in one embodiment to atmospheric pressure. Prior to or during heating and pressurization, tobacco material conditioning may take place with or without casing and / or flavor feeding, with the increase in material moisture from about 9 to 12% to about 18 to 45%, more preferably 20 to 30%. After relaxation and passing through the shear gap, the tobacco material According to one embodiment, have a moisture content of about 14 to 42%, preferably 16 to 18%, and it is possible to cool the tobacco material behind the shear gap at room temperature and under atmospheric pressure and thereby to dry or let it dry until it Has moisture of about 12 to 16%.
Das zerkleinerte, druckzerfaserte Tabakmaterial aus dem erfindungsgemäßen Verfahren kann unmittelbar der Weiterverarbeitung als Rauchartikelmaterial zugeführt werden, wenn das Tabak-Ausgangsmaterial ein Winnowing-Material ist oder wenn ausreichend vorzerkleinertes Material verwendet wird. Andererseits kann das zerkleinerte, druckzerfaserte Tabakmaterial nach dem erfindungsgemäßen Verfahren einer Klassifizierung unterzogen werden, z.B. wenn das Ausgangsmaterial ein sehr grobes Rippenmaterial ist. Dabei werden gemäß einer bevorzugten Ausführungsform die bei der Klassifizierung ausgesonderten zu groben Materialien nochmals dem Verfahren unterzogen, und der nicht ausgesonderte Rest kann unmittelbar der Weiterverwendung als Rauchartikelmaterial zugeführt werden.The shredded, pressure-shredded tobacco material from the method according to the invention can be supplied directly to further processing as a smoking article material if the tobacco raw material is a winnowing material or if sufficient pre-shredded material is used. On the other hand, the shredded, pressure-shredded tobacco material may be subjected to classification according to the method of the invention, e.g. if the starting material is a very coarse rib material. In this case, according to a preferred embodiment, the materials which have been rejected during classification are subjected to the process again, and the residue which has not been separated out can be directly supplied for further use as a smoking article material.
Die erfindungsgemäße Vorrichtung kann in den folgenden Ausführungsformen bereitgestellt werden:The device according to the invention can be provided in the following embodiments:
Die Spaltwände der Vorrichtung können voneinander weg und aufeinander zu bewegbar sein; die Spaltwände können zum geschlossenen Zustand des Spalts hin vorgespannt sein. Andererseits können die Spaltwände mit festem oder fest einstellbarem Abstand gegeneinander beweglich sein, wobei insbesondere die Spaltwände in einem festen Abstand von 0,01 mm bis 2mm, insbesondere 0,1 mm bis 0,5mm liegen. Diese Angaben beziehen sich auf glatte Spaltwände.The gap walls of the device may be away from each other and movable towards each other; the gap walls may be biased toward the closed state of the gap. On the other hand, the gap walls with a fixed or fixed adjustable distance against each other be movable, in particular, the gap walls at a fixed distance of 0.01 mm to 2mm, in particular 0.1 mm to 0.5 mm. These figures refer to smooth split walls.
Gemäß einer bevorzugten Ausführungsform weisen die Spaltwände Rauheiten oder Profilierungen auf, insbesondere Rillen- oder Kreuzrillenprofilierungen, die längs oder quer zur Spaltwand-Bewegungsrichtung angeordnet sind und eine Tiefe von bis zu 2 bis 3 mm aufweisen. In den tiefen Bereichen der Profilierungen sind die Abstände des Scherspalts natürlich entsprechend größer als oben angegeben.According to a preferred embodiment, the gap walls on roughness or profiles, in particular groove or Kreuzrillenprofilierungen which are arranged longitudinally or transversely to the gap wall movement direction and have a depth of up to 2 to 3 mm. In the deep areas of the profiles, the distances of the shear gap are of course correspondingly larger than indicated above.
Bei einer Ausführungsvariante ist die an der Druckkammer angeordnete Spaltwand fest, während die Gegenwand beweglich an einer mit einem Bewegungsantrieb versehenen Gegenhalterung angeordnet ist. Die Spaltwände können gegeneinander kontinuierlich oder intermittierend, in eine oder zwei Richtungen oder hin und her bewegbar sein. Im Besonderen kann der Spalt ein Ringspalt sein, vorzugsweise ein Kegelspalt.In one embodiment variant, the gap wall arranged on the pressure chamber is fixed, while the counter wall is arranged movably on a counter holder provided with a movement drive. The gap walls may be movable against each other continuously or intermittently, in one or two directions, or reciprocally. In particular, the gap may be an annular gap, preferably a cone gap.
Gemäß einer Ausführungsform der Erfindung weist die Druckkammer eine Stopfschnecke als Fördereinrichtung zum Fördern des Tabakmaterials vom Einlass zum Auslass auf. Hierbei ist anzumerken, dass eine Druckerzeugung mit mechanischen Mitteln, wie sie beispielsweise durch eine Stopfschnecke erzeugt wird, im Rahmen der Erfindung grundsätzlich auch anders vonstatten gehen kann. Es ist nicht ausgeschlossen, dass der Druck in anderer Weise mechanisch erzeugt wird, beispielsweise durch eine Kolbenvorrichtung oder aber nicht mechanisch oder nicht lediglich mechanisch über einen Gasdruck.According to one embodiment of the invention, the pressure chamber has a plug screw as a conveyor for conveying the tobacco material from the inlet to the outlet. It should be noted that a pressure generation by mechanical means, such as is produced for example by a plug screw, in the context of the invention can in principle also take place otherwise. It is not excluded that the pressure is generated mechanically in other ways, for example by a piston device or not mechanically or not only mechanically via a gas pressure.
Wenn eine Stopfschnecke verwendet wird, so weist diese vorteilhafterweise zum Bereich des Auslasses hin Kammervolumen mindernde Maßnahmen, z.B. kleinere Schneckensteigungen, auf.If a plug screw is used, this advantageously means towards the area of the outlet chamber volume reducing measures, e.g. smaller slants, on.
In der Druckkammer sind mit Vorteil mechanische Vorzerkleinerungsmittel bzw. Vorzerfaserungsmittel angeordnet. Gemäß einer vorteilhaften Ausführungsform ist der erfindungsgemäßen Vorrichtung im gleichen oder in einem vorgeschalteten Druckkammergehäuse eine Schneckenkammer-Druckkonditionierungsvorrichtung vorangesetzt. Eine solche Druckkonditionierungsvorrichtung ist beispielsweise in der
Ferner besteht noch die Möglichkeit, die Druckkammer mit Einlässen für Konditionierungs- oder Casingmittel bzw. Flavour auszustatten.Furthermore, it is still possible to equip the pressure chamber with inlets for conditioning or casing agent or flavor.
Der Rauchartikel weist ein zerkleinertes, zerfasertes Tabakmaterial-Produkt auf, das mittels einem der vorgenannten Verfahren oder mit einer der oben beschriebenen Vorrichtungen hergestellt wurde. Er kann das Tabakmaterial-Produkt zu einem Anteil von bis 50% aufweisen, insbesondere von 0,5% bis 35% und besonders bevorzugt von 0,5% bis 25%.The smoking article comprises a shredded, shredded tobacco material product made by any of the foregoing methods or apparatuses. It may have the tobacco material product in a proportion of up to 50%, in particular from 0.5% to 35% and particularly preferably from 0.5% to 25%.
Die Erfindung umfasst ferner die Verwendung eines Ein- oder Zwei-Schneckenförderers mit Scherspaltauslass zum Zerfasern von Tabakmaterial. Als Scherspalt soll im Sinne dieser Erfindung eine Öffnung bezeichnet werden, bei der Material während des Hindurchtretens geschert wird. Bisher sind Extruder - wie eingangs beschrieben - immer lediglich zur Herstellung von Tabakfolie bzw. zum Herstellen von Agglomeraten aus feinsten Tabakpartikeln verwendet worden. Die vorliegende Erfindung beschreibt erstmals eine Verwendung eines Extruders mit Scherspalt zur Zerkleinerung und Zerfaserung von Tabakmaterialien.The invention further includes the use of a one or two worm conveyor with a shear gap outlet for defibering tobacco material. For the purposes of this invention, a shearing gap is an opening in which material is sheared during passage. So far, extruders - as described above - have always been used only for the production of tobacco foil or for producing agglomerates of the finest tobacco particles. The present invention describes for the first time a use of an extruder with a shear gap for the comminution and defibration of tobacco materials.
Im Rahmen der erfindungsgemäßen Verwendung kann das erfindungsgemäße Verfahren in allen Verfahrensvarianten durchgeführt und die erfindungsgemäße Vorrichtung in allen Ausführungsformen verwendet werden.Within the scope of the use according to the invention, the process according to the invention can be carried out in all process variants and the device according to the invention can be used in all embodiments.
Die Erfindung wird im Weiteren anhand von Ausführungsformen näher erläutert. Sie kann alle hierin aufgeführten Merkmale einzeln sowie in jedweder Kombination umfassen. Es wird auf die beiliegenden Zeichnungen Bezug genommen. Es zeigen:
Figur 1- ein Ablaufdiagramm, das schematisch den Ablauf der Tabakvorbe- reitung unter Verwendung der erfindungsgemäßen Druckzerfaserung zeigt;
Figur 2- ein weiteres Ablaufdiagramm mit etwas detaillierterem Schema;
Figur 3- eine Ausführungsform einer erfindungsgemäßen Druckzerfaserungs- vorrichtung;
Figur 4- eine Ausführungsform einer erfindungsgemäßen Druckzerfaserungs- vorrichtung mit vorgeschalteter Druckkonditionierung in einer ersten Ausführungsform; und
Figur 5- ein Druckkonditiönierungs-Druckzerfaserungs-Kombinationsvorrichtung in einer zweiten Ausführungsform.
- FIG. 1
- a flow chart showing schematically the procedure of the tobacco preparation using the pressure pulp according to the invention;
- FIG. 2
- another flowchart with a more detailed schema;
- FIG. 3
- an embodiment of a Druckzerfaserungs- device according to the invention;
- FIG. 4
- an embodiment of a Druckzerfaserungs- device according to the invention with upstream pressure conditioning in a first embodiment; and
- FIG. 5
- a pressure-conferring-pressure-fusing combination device in a second embodiment.
Zunächst soll im Weiteren die Einordnung der erfindungsgemäßen Druckzerfaserung in den Tabakvorbereitungsprozess unter Bezugnahme auf die
In allgemeiner Weise ist der schematische Ablauf der Tabakvorbereitung in
Die Feuchtewerte sind auf Feuchtbasis angegeben und stellen empfohlene und bevorzugte Werte dar. Fachleute können optimale Bedingungen einstellen, wenn sie dem Grundgedanken der Erfindung folgen, und so eine Anpassung an optimale Bedingungen einer bestimmten erfindungsgemäßen Vorrichtung (Expansionsanlage) vornehmen.Moisture values are given in terms of wetness and represent recommended and preferred values. Those skilled in the art can set optimum conditions if they follow the principles of the invention and thus adapt to optimal conditions of a particular device according to the invention (expansion plant).
Die Rohrippen treten typischerweise mit einer Feuchte von etwa 10% in die Konditionierung ein. Die Konditionierung kann unter atmosphärischen Bedingungen erfolgen, vorteilhaft ist eine Konditionierung bei überatmosphärischem Druck, wie beispielsweise in der vorher schon angesprochenen
Beim Zerfasern verlieren die Rippen in der Regel etwas Feuchtigkeit, so dass nun die zerkleinerten Rippen mit 16% bis 42% Feuchte klassifiziert werden. Dort werden zu große Rippenteile wieder zurückgefördert und durchlaufen den bisher beschriebenen Ablauf nochmals. Typischerweise ist dieser Anteil gering und liegt unter 10% der Gesamtmasse. Der andere Anteil der zerkleinerten Rippen kann nun abhängig von den gewünschten Prozessparametern unterschiedlich behandelt werden. Bei Feuchtigkeiten von z.B. 14% bis 15% gehen die Rippen direkt in die Tabakmischung für das Endprodukt Rauchartikel. Bei höheren Feuchten, z.B. 15% bis 40%, durchlaufen die Rippen noch eine Expansion und Trocknung und können danach bei ebenfalls 14% bis 15% Feuchte in die Mischung für das Endprodukt gegeben werden. Dem ist eventuell nochmals eine Klassifizierung vorgeschaltet, damit etwa noch verbleibende größere Teile abgetrennt und zurück zu den Rohrippen gegeben werden, die dann den bisher beschriebenen Prozess erneut durchlaufen. Werden in diesem Prozess statt Rohrippen ZHV- oder TV-Winnowings als Eingangsmaterial verwendet, so endet der Prozess in der Regel vor der ersten Klassifizierung, und die zerfaserten Winnowings gehen direkt ins Endprodukt.When shredded, the ribs usually lose some moisture, so that now the shredded ribs with 16% to 42% moisture are classified. There too large rib parts are conveyed back again and go through the previously described sequence again. Typically, this proportion is low and is less than 10% of the total mass. The other portion of the shredded ribs can now be treated differently depending on the desired process parameters. At humidities of, for example, 14% to 15%, the ribs go directly into the tobacco mixture for the end product smoking article. At higher humidities, eg 15% Up to 40%, the ribs still undergo expansion and drying and can then be added at the same 14% to 15% moisture in the mixture for the final product. This is possibly preceded by a classification, so that about remaining larger parts are separated and added back to the pipe sections, which then go through the process previously described again. If ZHV or TV winnowings are used as input material in this process instead of pipe butt, the process usually ends before the first classification, and the shredded winnowings go directly into the final product.
Die
Die
Anschließend wird das Material erhitzt (ca. 60° bis 180°C) und unter Druck gesetzt (ca. 10 bis 200 bar), um einerseits die gewünschte Geschmacksverbesserung durch chemisch ablaufende Prozesse (z.B. Maillard-Reaktion bzw. Karamellisierung) zu erreichen und andererseits genügend Energie zu speichern, um die Zerfaserung durch Scherung und Entspannung über einen Scherspalt ablaufen zu lassen. Die Druckerzeugung und Erhitzung kann mit handelsüblichen Stopfschnecken durchgeführt werden, deren Gehäuse insbesondere auch beheizt werden können. Solche Anlagen werden im Weiteren noch detaillierter beschrieben.Subsequently, the material is heated (about 60 ° to 180 ° C) and pressurized (about 10 to 200 bar), on the one hand to achieve the desired taste improvement by chemically running processes (eg Maillard reaction or caramelization) and on the other hand Sufficient energy to store the defibration by shearing and relaxing over a shear gap. The pressure generation and heating can be carried out with commercially available stuffing screws whose housing can also be heated in particular. Such systems will be described in more detail below.
Beim Austritt aus dem Scherspalt in die Atmosphäre tritt eine schlagartige Verdampfung des eingelagerten Wassers und gegebenenfalls auch anderer Inhaltsstoffe auf, was dazu führt, dass das Material zusätzlich zur Scherung im Spalt zerfasert und expandiert wird. Die Feuchte des Materials verringert sich durch die Flashverdampfung je nach Prozessdruck und Temperatur um bis zu ca. 10% und des weiteren werden Tabakinhaltsstoffe zum Teil reduziert. Dabei hat es sich als vorteilhaft erwiesen, wenn sich die Scherspaltflächen relativ zueinander in einem gewissen Takt bewegen, um Verstopfungen vorzubeugen und zu beseitigen. Dadurch wird sichergestellt, dass die volle Querschnittsfläche des Spaltes genutzt wird und konstante physikalische Bedingungen am Spalt herrschen, was letztlich zu einem einheitlichen Produkt führt. Hierzu hat es sich weiterhin als vorteilhaft erwiesen, die Spaltflächen zu strukturieren bzw. zu profilieren.Upon exiting the shear gap into the atmosphere, a sudden evaporation of the stored water and optionally also of other ingredients occurs, which leads to the material being defibrated and expanded in addition to the shear in the gap. Depending on the process pressure and temperature, the moisture content of the material is reduced by up to approx. 10% due to the flash evaporation and, in addition, tobacco ingredients are partially reduced. It has proved to be advantageous if the shear gap surfaces move relative to each other in a certain time to prevent clogging and eliminate. This ensures that the full cross-sectional area of the gap is utilized and there are constant physical conditions at the gap, ultimately resulting in a unitary product. For this purpose, it has also proven to be advantageous to structure the gap surfaces or to profile.
Bei der folgenden Abkühlung des Materials von ca. 100°C auf Raumtemperatur, die auf einem Transportband mit Luftabsaugung insbesondere von unten stattfinden kann, verliert das Tabakmaterial durch Verdunstungskühlung weitere Feuchte, so dass es möglich ist, ohne einen Trockner auf eine Endproduktfeuchte zu kommen, die eine direkte Zumischung in die Blatttabakmischung erlaubt.In the subsequent cooling of the material from about 100 ° C to room temperature, which may take place on a conveyor belt with air extraction, in particular from below, the tobacco material loses further moisture by evaporative cooling, so that it is possible to come without a dryer to a final product moisture, which allows a direct blending into the leaf tobacco mixture.
Ob eine Klassifizierung des zerkleinerten Tabakmaterials und die damit verbundene Rückführung der zu großen Teilchen in den Prozess notwendig ist, hängt von dem zu zerkleinernden Material und von der Art der Vorzerkleinerung ab. Bei ZHV-Winnowings oder in der Größe ähnlichem Material ist eine Klassifizierung in der Regel nicht notwendig.Whether a classification of the shredded tobacco material and the associated return of too large particles in the process is necessary depends on the material to be crushed and the type of pre-crushing. For ZHV winnowings or similar sized material, classification is usually not necessary.
Anstatt z.B. mit einer Mühle oder einem Brecher vorzuzerkleinern und mit einer beheizten Stopfschnecke Druck und Temperatur zu erzeugen, bietet es sich vorzugsweise auch an, einen Ein- oder Zweischnecken-Extruder zu benutzen, weil hier das Material durch Scherung vorzerkleinert, durch die Reibung beim Zerkleinern gleichzeitig erwärmt und durch die Kompression der Schnecke ein entsprechender Druck aufgebaut wird. Man kann also mit einem Gerät gleich drei notwendige Prozessschritte zusammenfassen. Dabei muss der Extruder so ausgelegt sein, dass das Material nicht wie bei Extrusionsprozessen sonst üblich und erwünscht vollständig zerkleinert und plastifiziert wird (hohe Dichte), sondern die Faserstruktur des Tabakmaterials erhalten bleibt. Es soll also keine Extrusion im klassischen Sinne ablaufen.Instead of e.g. preferably pre-shredded with a mill or crusher and with a heated plug screw to produce pressure and temperature, it is also preferable to use a single- or twin-screw extruder, because here the material pre-shredded by shearing, heated by the friction during crushing simultaneously and by the compression of the screw, a corresponding pressure is built up. So you can summarize with a device equal to three necessary process steps. In this case, the extruder must be designed so that the material is not otherwise comminuted and plasticized as usual in extrusion processes and desired (high density), but the fiber structure of the tobacco material is maintained. So there should be no extrusion in the classical sense.
Mit dem erfindungsgemäßen Prozess werden alle gesteckten Ziele erreicht:
- geschmackliche Aufwertung bzw. sensorische Verbesserung;
- Absenkung des Verhältnis CO/Kondensat im Rauch (gegenüber anderen Rippenprodukten, z.B. geschnittenen Rippenprodukten);
- Füllfähigkeit je nach Eingangsmaterial ähnlich bei geschnittenem Blatttabak;
- optisch unauffällige Faser ähnlich Blattschnitt;
- drastische Verkürzung von Lagerzeiten beim Feuchten bzw. keine Lagerzeiten bei Druckkonditionierung;
- kein Trockner;
- hohe Materialausbeute (
Kleinteile kleiner als 1 mm wenigerals 10%); und - kompakter Gesamtprozess mit entsprechend niedrigem Platzbedarf und niedrigen Investitions- und Betriebskosten.
- flavor enhancement or sensory enhancement;
- Lowering the CO / condensate ratio in the smoke (compared to other rib products, eg cut rib products);
- Fillability similar to input material, similar to cut leaf tobacco;
- optically inconspicuous fiber similar to leaf cut;
- drastic shortening of storage times during dampening or no storage times during pressure conditioning;
- no dryer;
- high material yield (small parts smaller than 1 mm less than 10%); and
- compact overall process with correspondingly low space requirements and low investment and operating costs.
Eine Ausführungsform der erfindungsgemäßen Vorrichtung wird nunmehr anhand der
Der Außenkegel 10 wird durch eine Gegenhalterung 11 positioniert, die gleichzeitig einen Drehantrieb für den Kegelkörper 10 bereitstellen kann. Mittels dieses Drehantriebs kann der Kegel 10, wie durch den geschwungenen Pfeil dargestellt, um die Mittelachse gedreht werden. Die Verbindung zwischen der Gegenhalterung 11 und dem Kegel 10 ist durch einen Doppelpfeil dargestellt, was bedeutet, dass der Kegel 10 auf der Achse an den Innenkegel 8 herangefahren werden kann. Dort kann er fest in seiner axialen Position gehalten, aber auch axial beweglich angeordnet werden. Mittels dieser Konstruktion lässt sich die Breite des Spaltes einstellen oder anpassen, außerdem wird ein Gegendruck nach links, also in Richtung der Schließung des Spaltes 9 hin erzeugt, vorzugsweise durch hydraulische Mittel.The
Der erste Teil der Zerfaserung der Tabakrippen erfolgt erfindungsgemäß unter überatmosphärischem Druck. Dieser Überdruck wird erzeugt, indem das Tabakmaterial, im speziellen Fall konditionierte Tabakrippen in der Kammer 2 durch die Schnecke 3 gefördert werden, nachdem sie über den Einlass 5 eingetragen wurden. Am Ende der Förderschnecke befindet sich ein Scherspalt-Auslass, der ähnlich wie bei einem Extruder den Förderraum nahezu verschließt. Bevorzugt ist dieser Matritzen-Auslass, wie in
Die Verbindung von Konditionierung und Druckzerfaserung ist abhängig von den Druckverhältnissen, bei denen konditioniert wird. Im einfachsten Fall wird bei atmosphärischer Konditionierung das Tabakmaterial einfach über Förderinnen oder ein Förderband in den Einlass 5, z.B. einen Einlasstrichter, zugeführt. Die Konditionierung kann dann beispielsweise an einer Zwischenstelle des Gehäuses 2 durch Einbringung von Wasser und Casing stattfinden, wie dies mit dem Bezugszeichen 6 aufgezeigt ist.The combination of conditioning and pressure fraying depends on the pressure conditions at which conditioning is performed. In the simplest case, with atmospheric conditioning, the tobacco material is simply conveyed via conveyors or a conveyor belt into the
Der entscheidende Schritt der Zerfaserung erfolgt beim Durchgang sowie beim Austritt aus dem Spalt 9. Beim Durchgang durch den Spalt 9 werden die Tabakrippen einer Scherung zwischen den Spaltwänden ausgesetzt und beim Austritt aus dem Spalt erfolgt die schon vorher angesprochene Flash-Verdampfung. Durch das Zusammenwirken dieser Effekte entsteht das sehr gut zerfaserte Verfahrensprodukt, das mindestens zu einem großen Anteil schon bei der Rauchartikelherstellung verwendet werden kann.The crucial step of the defibration takes place during the passage and the exit from the
Um zu verhindern, dass an dem engen Scherspalt 9 Verstopfungen über einen großen Bereich der Ringfläche bzw. Kegelfläche auftreten, die sich dann schlagartig wieder lösen, hat es sich als hilfreich erwiesen, den Kegel 10 in Drehung um seine Rotationsachse zu halten. Diese Drehung kann kontinuierlich oder unterbrochen in eine Richtung erfolgen oder die Drehrichtung wechseln. Die Drehung kann dabei vollständig sein oder nur Viertel-/ oder Dritteldrehungen oder kleinere/größere Einheiten umfassen.In order to prevent blockages from occurring at the
Zusätzlich hat es sich als vorteilhaft erwiesen, wenn die Oberfläche mindestens eines der Kegel, des Innenkegels am Kopf 8 oder des Außenkegels am Stempel 10 aufgeraut oder profiliert wird, z.B. durch die Einbringung von Rillen oder Kreuzrillen bis zu 2 oder 3 mm Tiefe. Wichtig ist hierbei lediglich eine Aufrauung/Profilierung, die Tiefe und der Verlauf (Richtung) der Rillen können in jeder Weise eingestellt werden. Speziell in Verbindung mit den Drehungen des Kegels 10 lassen sich so Verstopfungen stark reduzieren. Man erhält dadurch homogenere Druckverhältnisse, die auch zu einem homogeneren Endprodukt führen.In addition, it has proven to be advantageous if the surface of at least one of the cones, the inner cone on the
Das erhaltene, zerfaserte Verfahrensprodukt zeigt im Aussehen und in der Verwendung ähnliche Eigenschaften wie sie von geschredderten Rippen bekannt sind. Die erfindungsgemäße Druckzerfaserung hat aber nicht den Nachteil eines hohen Staubanfalls, wie er bei Schreddern von Rippen bekannt ist, außerdem muss nicht so stark vorgefeuchtet werden wie beim Schreddern, so dass spätere Trocknungen stark verringert bzw. eliminiert werden können.The resulting defibrated process product exhibits similar appearance and usage characteristics as are known from shredded ribs. However, the pressure defibration according to the invention does not have the disadvantage of a high dust accumulation, as it is known in shredding ribs, also does not need to be pre-moistened as much as shredding, so that subsequent drying can be greatly reduced or eliminated.
Was die Verbindung bzw. Kombination von Konditionierung und Druckzerfaserung angeht, bieten sich auf der Basis der vorliegenden Erfindung noch zusätzliche Möglichkeiten, die nunmehr anhand der
Es ist im Rahmen der vorliegenden Erfindung natürlich auch möglich, den Austritt aus der Druckkonditionierungskammer 21 mittels einer Zellradschleuse und einem Druckabbau zu betreiben. Dann würde, wie in
Bevorzugt ist aber ein Druckabfall beim Übertritt aus der Druckkonditionierung in die Druckzerfaserung zu vermeiden, um über den gesamten Prozessbereich vom Beginn der Konditionierung bis zur Zerfaserung einen überatmosphärischen Druck bereitstellen zu können, wie in
Nach dem Einbringen der Tabakrippen in die Kammer 21 stehen die Rippen unter überatmosphärischem Druck, der durch Dampfzuführungen gegen die natürlich Leckraten der Zellradschleuse 26 (Spalte und Schöpfvolumen) aufrechterhalten wird. Durch den Dampf werden die Rippen erhitzt und die Feuchtigkeit erhöht. Prinzipiell ist in einer solchen Kammer auch eine Abtrocknung mit übersättigtem Dampf möglich, jedoch ist es für die Anwendung zur Zerfaserung meist schon von Vorteil, wenn die eingetragenen Rippen deutlich höhere Feuchten aufweisen. Mittels der Förderschnecke 22 werden die Tabakrippen durch die Konditionierungskammer 21 gefördert. Dabei können verschiedene Einstellungen getroffen werden (Steigung der Schnecke, Drehzahl und Neigung der Kammer), mit denen die Verweilzeit der Tabakrippen eingestellt werden kann. Sie liegt in der Regel zwischen 2 und 10 Minuten. Nach der Druckkonditionierung, bei der auch die Zugabe von Wasser, Casing- und/oder Flavourmaterial erfolgen kann, werden die Rippen dann über den Auslass 27 in die Druckzerfaserungsvorrichtung 1 übergeben, und dieser Eintrag kann auf einfache Weise erreicht werden, wenn das Gehäuse ebenfalls trichterförmig ausgebildet ist. Die typische Verweilzeit der Rippen im Bereich der Zerfaserung liegt unter 2 Minuten, insbesondere unter 1 Minute. Die Rippen verlassen die Druckzerfaserung dann in dem gewünschten, vorher beschriebenen Zustand.After the introduction of the tobacco ribs in the
Statt der Druckkonditionierungsschnecke kann auch eine Konditionierungsschnecke unter atmosphärischen Drücken Verwendung finden.Instead of the pressure conditioning screw, a conditioning screw under atmospheric pressures can also be used.
Die
In den Fällen der
Claims (34)
- A method for producing cut tobacco material, wherein:- an initial tobacco material is heated and pressurised; and- the heated and pressurised material is fed through a shearing gap (9) and cut, in particular defibrated, by expansion.
- The method according to claim 1, wherein the initial tobacco material is largely a coarse tobacco material, in particular with a particle size of more than 2 mm.
- The method according to claim 1 or 2, wherein the initial tobacco material is a tobacco stem material, in particular with a stem size of more than 2 mm.
- The method according to any one of claims 1 to 3, wherein the initial tobacco material is a winnowing material.
- The method according to any one of claims 1 to 4, which is performed using an initial tobacco material without adding structuring materials.
- The method according to any one of claims 1 to 5, wherein the initial tobacco material is heated to a temperature of 60 to 180°C, in particular 100 to 140°C, preferably 110 to 130°C, and pressurised to 10 to 200 bars, in particular 40 to 150 bars, preferably 60 to 120 bars, wherein the dwell time of the tobacco material in continuous circulation is less than 3 minutes, in particular less than 2 minutes, preferably less than 1 minute.
- The method according to any one of claims 1 to 6, wherein the initial tobacco material is mechanically pressurised, in particular mechanically pressed towards the shearing gap (9) in a chamber (2).
- The method according to claim 7, wherein the initial tobacco material is pressurised by means of a conveyor screw (3) which presses the material towards the outlet end of the chamber (2) of a heatable screw conveyor, at which the shearing gap (9) is disposed.
- The method according to claim 7 or 8, wherein the material is coarsely pre-cut and/or coarsely defibrated in the chamber (2) and/or in the screw conveyor as it is transported to the shearing gap (9).
- The method according to any one of claims 1 to 9, wherein the shearing gap (9) is closed with a bias and is intermittently opened by the pressure of the tobacco material, wherein the material passes through the gap (9).
- The method according to any one of claims 1 to 9, wherein the material is fed through a continuously open shearing gap (9).
- The method according to any one of claims 1 to 11, wherein the shearing gap walls perform a relative movement as the tobacco material is fed through.
- The method according to any one of claims 1 to 12, wherein the tobacco material is expanded to atmospheric pressure as it passes through the shearing gap (9).
- The method according to any one of claims 1 to 13, wherein the tobacco material is conditioned, and/or casing and/or flavouring is added, before or during heating and generating the pressure, wherein the moisture content of the material is increased from about 9 to 12% to about 18 to 45%, in particular 20 to 30%.
- The method according to any one of claims 1 to 14, wherein the tobacco material exhibits a moisture content of about 14 to 42%, preferably 16 to 18%, once it has been expanded and fed through the shearing gap (9).
- The method according to any one of claims 1 to 15, wherein the tobacco material is cooled at room temperature and atmospheric pressure after the shearing gap (9) until it exhibits a moisture content of about 12 to 16%.
- The method according to any one of claims 1 to 16, wherein the cut and pressure-defibrated tobacco material is:- directly provided for further processing as smoking article material if the initial tobacco material is a winnowing material;- subjected to a classification if the initial material is a coarse stem material, wherein the materials which are separated out during classification are subjected to the method again, and the remainder which is not separated out is directly provided for further processing as smoking article material.
- A device for producing cut tobacco material, comprising a heatable pressure chamber (2) which comprises a tobacco material inlet (5) at the low-pressure end and a tobacco material outlet at the pressurised end and a conveyor device (3) for conveying the tobacco material from the inlet (5) to the outlet, wherein the tobacco material outlet has a shearing gap (9) through which the tobacco material passes and is expanded, and the shearing gap (9) comprises gap walls which can be moved relative to each other and perform a relative movement even when the gap distance remains constant.
- The device according to claim 18, characterised in that the gap walls can be moved apart from each other and towards each other.
- The device according to claim 18 or 19, characterised in that the gap walls are biased towards the state in which the gap (9) is closed.
- The device according to claim 18, characterised in that the gap walls can be moved relative to each other at a fixed or fixedly adjustable distance.
- The device according to claim 21, characterised in that the gap walls have a fixed distance of 0.01 mm to 2 mm, in particular 0.1 mm to 0.5 mm.
- The device according to any one of claims 18 to 22, characterised in that the gap walls exhibit roughened or profiled features, in particular grooved or intersecting grooved profiling which is preferably disposed longitudinally or transversely with respect to the direction in which the gap wall moves and in particular exhibits a depth of up to 2 to 3 mm.
- The device according to any one of claims 18 to 23, characterised in that the gap wall disposed on the pressure chamber (2) is stationary, while the co-operating wall is movably disposed on a co-operating holder (11) provided with a movement drive.
- The device according to any one of claims 18 to 24, characterised in that the gap walls can be moved relative to each other continuously or intermittently and in one or two directions or back and forth.
- The device according to any one of claims 18 to 25, characterised in that the gap is an annular gap, in particular a conical gap.
- The device according to any one of claims 24 to 26, characterised in that the pressure chamber (2) comprises a plug screw feeder (3) as a conveyor device for conveying the tobacco material from the inlet to the outlet.
- The device according to claim 27, characterised in that the plug screw feeder (3) exhibits features which reduce the chamber volume towards the region of the outlet, in particular smaller screw pitches.
- The device according to any one of claims 18 to 28, characterised in that mechanical pre-cutting means and/or pre-defibrating means are disposed in the pressure chamber (2).
- The device according to any one of claims 18 to 29, characterised in that a screw chamber pressure-conditioning system (20) is disposed upstream of it in the same pressure chamber housing or an upstream pressure chamber housing.
- The device according to any one of claims 18 to 30, characterised in that the pressure chamber comprises inlets (6, 7) for conditioning agents or casing agents and/or flavourings or steam.
- The use of a plug screw feeder extruder comprising a shearing gap outlet for defibrating tobacco material.
- The use according to claim 32, wherein one or more of the methods according to claims 1 to 17 is/are performed.
- The use according to claim 32 or 33, wherein a device comprising features in accordance with any one of claims 18 to 31 is used to defibrate the tobacco material.
Priority Applications (1)
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PL05811333T PL1827142T3 (en) | 2004-12-09 | 2005-11-28 | Defibration of tobacco material |
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DE102004059388A DE102004059388B4 (en) | 2004-12-09 | 2004-12-09 | Defibration of tobacco material |
DE202004019711U DE202004019711U1 (en) | 2004-12-09 | 2004-12-21 | Apparatus for the production of shredded tobacco material |
PCT/EP2005/012687 WO2006061117A1 (en) | 2004-12-09 | 2005-11-28 | Defibration of tobacco material |
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EP1827142A1 EP1827142A1 (en) | 2007-09-05 |
EP1827142B1 true EP1827142B1 (en) | 2011-06-22 |
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EP (1) | EP1827142B1 (en) |
KR (1) | KR100967767B1 (en) |
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AU (1) | AU2005313656B2 (en) |
CA (1) | CA2584344C (en) |
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US7934509B2 (en) | 2004-12-09 | 2011-05-03 | British American Tobacco (Germany) Gmbh | Defibration of tobacco material |
DE102004059388B4 (en) | 2004-12-09 | 2006-11-30 | British American Tobacco (Germany) Gmbh | Defibration of tobacco material |
DE102006057290B4 (en) * | 2006-12-05 | 2008-10-30 | British American Tobacco (Germany) Gmbh | Tobacco pulp with double-sided auger shaft |
DE102008052209B4 (en) | 2008-10-17 | 2016-05-12 | British American Tobacco (Germany) Gmbh | Modular tobacco preparation with extrusion |
DE102008052720B4 (en) | 2008-10-22 | 2014-01-02 | British American Tobacco (Germany) Gmbh | Extractive tobacco material extrusion |
DE102008059031A1 (en) | 2008-11-26 | 2010-05-27 | British American Tobacco (Germany) Gmbh | Smoke product production by thermal extrusion |
DE102008063613A1 (en) * | 2008-12-18 | 2010-07-01 | British American Tobacco (Germany) Gmbh | Shape and size of cellulosic plant materials |
EP2822407B1 (en) | 2012-03-06 | 2016-05-18 | HT Nutri Sàrl | A method of processing tobacco and its by-products |
GB201312501D0 (en) | 2013-07-12 | 2013-08-28 | British American Tobacco Co | Material for inclusion in a smoking article |
MX2016016524A (en) * | 2014-06-24 | 2017-05-01 | Philip Morris Products Sa | Reconstituted tobacco sheets and related methods. |
SG11201610680QA (en) * | 2014-06-24 | 2017-01-27 | Philip Morris Products Sa | Reconstituted tobacco sheets and related methods |
IT202000004129A1 (en) * | 2020-02-27 | 2021-08-27 | Magg Consulting S R L | Improved Method for Treating Tobacco. |
GB202101101D0 (en) | 2021-01-27 | 2021-03-10 | British American Tobacco Investments Ltd | Non-combustible active substance delivery article design system and method |
CN114403489B (en) * | 2021-12-14 | 2022-12-02 | 上海烟草集团有限责任公司 | Tobacco sheet and preparation method thereof |
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US3098492A (en) * | 1960-11-25 | 1963-07-23 | Nat Starch Chem Corp | Method of making tobacco product |
US3612066A (en) * | 1970-02-05 | 1971-10-12 | Reynolds Tobacco Co R | Denicotinizing process |
LU73096A1 (en) * | 1975-07-29 | 1977-03-24 | ||
JPS6255038A (en) * | 1985-09-03 | 1987-03-10 | 日本たばこ産業株式会社 | Extrusion screw apparatus |
US5076293A (en) * | 1989-06-19 | 1991-12-31 | R. J. Reynolds Tobacco Company | Process and apparatus for the treatment of tobacco material |
US5279312A (en) * | 1991-09-18 | 1994-01-18 | P.T.H.M. Sampoerna | Method for processing dried whole cloves |
DE9208904U1 (en) | 1992-07-03 | 1993-11-04 | Amandus Kahl GmbH & Co., 21465 Reinbek | Device for processing beet pulp |
US5478511A (en) * | 1993-05-07 | 1995-12-26 | Andritz Sprout-Bauer, Inc. | Annular gap expander |
NZ299771A (en) | 1995-11-20 | 1997-11-24 | Bat Cigarettenfab Gmbh | Tobacco preparation with separate treatment of stems and lamina and subsequent blending |
DE10304629B4 (en) * | 2003-02-05 | 2008-10-30 | British American Tobacco (Germany) Gmbh | Pressure conditioning process |
US7934509B2 (en) | 2004-12-09 | 2011-05-03 | British American Tobacco (Germany) Gmbh | Defibration of tobacco material |
DE102004059388B4 (en) * | 2004-12-09 | 2006-11-30 | British American Tobacco (Germany) Gmbh | Defibration of tobacco material |
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- 2005-11-28 WO PCT/EP2005/012687 patent/WO2006061117A1/en active Application Filing
- 2005-11-28 EP EP05811333A patent/EP1827142B1/en active Active
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AR053420A1 (en) | 2007-05-09 |
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EP1827142A1 (en) | 2007-09-05 |
CA2584344C (en) | 2012-01-17 |
AU2005313656B2 (en) | 2009-12-17 |
KR100967767B1 (en) | 2010-07-05 |
US20080142027A1 (en) | 2008-06-19 |
KR20070087000A (en) | 2007-08-27 |
CA2584344A1 (en) | 2006-06-15 |
US7934509B2 (en) | 2011-05-03 |
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