CN85104229B - Colouring-fluorescent dual-purpose flaw detection penetrating fluid - Google Patents
Colouring-fluorescent dual-purpose flaw detection penetrating fluid Download PDFInfo
- Publication number
- CN85104229B CN85104229B CN85104229A CN85104229A CN85104229B CN 85104229 B CN85104229 B CN 85104229B CN 85104229 A CN85104229 A CN 85104229A CN 85104229 A CN85104229 A CN 85104229A CN 85104229 B CN85104229 B CN 85104229B
- Authority
- CN
- China
- Prior art keywords
- flaw detection
- penetrating fluid
- cleaning
- fluorescent
- penetrating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000001514 detection method Methods 0.000 title claims abstract description 22
- 230000000149 penetrating effect Effects 0.000 title claims abstract description 20
- 239000012530 fluid Substances 0.000 title claims abstract description 16
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000007850 fluorescent dye Substances 0.000 claims abstract description 6
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 4
- 239000003350 kerosene Substances 0.000 claims abstract description 4
- 229920000191 poly(N-vinyl pyrrolidone) Polymers 0.000 claims description 3
- LIIDWKDFORMMDQ-UHFFFAOYSA-N 2-[[4-(dipropylamino)phenyl]diazenyl]benzoic acid Chemical compound C1=CC(N(CCC)CCC)=CC=C1N=NC1=CC=CC=C1C(O)=O LIIDWKDFORMMDQ-UHFFFAOYSA-N 0.000 claims description 2
- IQFVPQOLBLOTPF-HKXUKFGYSA-L congo red Chemical compound [Na+].[Na+].C1=CC=CC2=C(N)C(/N=N/C3=CC=C(C=C3)C3=CC=C(C=C3)/N=N/C3=C(C4=CC=CC=C4C(=C3)S([O-])(=O)=O)N)=CC(S([O-])(=O)=O)=C21 IQFVPQOLBLOTPF-HKXUKFGYSA-L 0.000 claims description 2
- ZXJXZNDDNMQXFV-UHFFFAOYSA-M crystal violet Chemical compound [Cl-].C1=CC(N(C)C)=CC=C1[C+](C=1C=CC(=CC=1)N(C)C)C1=CC=C(N(C)C)C=C1 ZXJXZNDDNMQXFV-UHFFFAOYSA-M 0.000 claims description 2
- GNBHRKFJIUUOQI-UHFFFAOYSA-N fluorescein Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC=C(O)C=C1OC1=CC(O)=CC=C21 GNBHRKFJIUUOQI-UHFFFAOYSA-N 0.000 claims description 2
- 238000009659 non-destructive testing Methods 0.000 claims description 2
- GVKCHTBDSMQENH-UHFFFAOYSA-L phloxine B Chemical compound [Na+].[Na+].[O-]C(=O)C1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1C1=C2C=C(Br)C(=O)C(Br)=C2OC2=C(Br)C([O-])=C(Br)C=C21 GVKCHTBDSMQENH-UHFFFAOYSA-L 0.000 claims description 2
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 claims description 2
- 239000007788 liquid Substances 0.000 abstract description 10
- 230000007547 defect Effects 0.000 abstract description 8
- 238000004140 cleaning Methods 0.000 abstract description 6
- 239000000975 dye Substances 0.000 abstract description 4
- 239000002904 solvent Substances 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 4
- 230000035945 sensitivity Effects 0.000 abstract description 3
- 239000012459 cleaning agent Substances 0.000 abstract 2
- 238000004040 coloring Methods 0.000 abstract 1
- 238000007689 inspection Methods 0.000 description 5
- 230000008595 infiltration Effects 0.000 description 4
- 238000001764 infiltration Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 230000035515 penetration Effects 0.000 description 2
- OALHHIHQOFIMEF-UHFFFAOYSA-N 3',6'-dihydroxy-2',4',5',7'-tetraiodo-3h-spiro[2-benzofuran-1,9'-xanthene]-3-one Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC(I)=C(O)C(I)=C1OC1=C(I)C(O)=C(I)C=C21 OALHHIHQOFIMEF-UHFFFAOYSA-N 0.000 description 1
- 208000037656 Respiratory Sounds Diseases 0.000 description 1
- PZTQVMXMKVTIRC-UHFFFAOYSA-L chembl2028348 Chemical compound [Ca+2].[O-]S(=O)(=O)C1=CC(C)=CC=C1N=NC1=C(O)C(C([O-])=O)=CC2=CC=CC=C12 PZTQVMXMKVTIRC-UHFFFAOYSA-L 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 150000002460 imidazoles Chemical class 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- -1 naphthoyl amine Chemical class 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Investigating Materials By The Use Of Optical Means Adapted For Particular Applications (AREA)
Abstract
A coloring-fluorescent dual-purpose flaw detection penetrating fluid for nondestructive detection. It is prepared by adding coloring dye and fluorescent dye simultaneously, and mixing with kerosene, dibutyl phthalate and emulsifier in a certain proportion. The flaw detection liquid can be used in sunlight (or white light) and can also be applied under the irradiation of an ultraviolet lamp in a dark room; the cleaning agent can be used for cleaning, and the cleaning agent can also be used for cleaning. The flaw detection penetrating fluid has multiple performances of dye-penetrant flaw detection, fluorescent flaw detection, solvent removal, water cleaning and the like. The flaw detection liquid has the characteristics of high flaw detection sensitivity; the width of the opening defect is 0.5 mu; and redundant flaw detection liquid can be easily cleaned. In addition, the penetrating fluid has strong penetrating power, short penetrating time, good repeatability, safety to operators and no pollution.
Description
The invention belongs to the penetrating inspection material that is used in the Non-Destructive Testing.
Richard in 1973, L.P. once commented the effect and the principle of penetration flaw detection liquid in the 119th to 140 page of National Aeronautics and Space Administration Special Publication No5113.And US4, patents such as 186,304 and US3,912,653 have been reported the prescription and the performance of fluorescence flaw detection infiltration solution and dye check penetrating fluid.Two class defect detecting liquids respectively have its relative merits:
Excellent, the shortcoming of removal of solvents type dye check penetrating fluid
| Advantage | Shortcoming |
| 1. need not electrical equipment | 1. incendivity is strong |
| 2. be applicable to large-scale workpiece partial check | 2. the remolding sensitivity fluorescence flaw detection infiltration solution is low |
| 3. can be used for not allowing the Workpiece inspection washed | |
| 4. can under available light or white light, directly detect |
Excellent, the shortcoming of water-washing type fluorescence flaw detection infiltration solution
| Advantage | Shortcoming |
| 1. bright fluorescence is arranged | Need be in the check under the uviol lamp of darkroom |
| 2. be easy to washing | |
| 3. be suitable for the check of small workpiece |
In experiment detects, need above-mentioned two kinds of penetrating fluid of flaw detection to be used in combination sometimes, could finally judge alligatoring, avoid omission.Therefore, the objective of the invention is to formulate out a kind of painted-the dual-purpose penetrating fluid of flaw detection of fluorescence, it can be used down at daylight (or white light), also can under the medium ultraviolet light irradiation of darkroom, use; Simultaneously, can either use, also can use as water-washing type as the removal of solvents type.
Key of the present invention is to select for use the special ratios of illuminating colour, fluorescent dye, hydrocarbons, ester class, emulsifying agent.Make it, both had both two kinds of functions of dye penetrant inspection and fluorescent penetrating inspection, also have both solvent cleaning and two kinds of functions of washing simultaneously.According to various material ratios of the present invention, can reach this purpose.
Illuminating colour, fluorescent dye, hydrocarbons (as kerosene), ester class (as dibutyl phthalate), emulsifying agent (as peregal A20) ratio that this penetrating fluid uses are respectively 7%, 6%, 7%, 65%, 15%.Its flaw detection operating procedure comprises and workpiece is given steps such as cleaning, infiltration, cleaning, developing and inspection.
The illuminating colour that this penetrating fluid uses is red for lighting up, phloxine, propyl red, Congo red, methyl violet, oil blue, Oil Yellow, rhodamine etc.The fluorescent dye that this penetrating fluid uses is (as fluoresceins) such as zero class, naphthoyl amine, imidazoles.
Use this penetrating fluid can be at the following developing of daylight (or white light), also can be under uviol lamp (darkroom) developing, can clean by enough clean-out systems, also can wash by water.In addition, can also receive following technique effect:
1. flaw detection sensitivity height.It is qualified that standard flaw detection test specimen is detected.Crackle is high-visible.Can show 0.5 μ flaws.
2. seepage force is strong.Enter in the Surface Flaw easily.
3. bright in colour.
4. required time of penetration is short, generally in 10 minutes.
5. favorable reproducibility.
6. to the workpiece non-corrosiveness.
7. clean easily, water or clean-out system clean all can.
8. environment is not polluted, non-stimulated to skin, wash from skin easily.
Embodiment:
Earlier workpiece is cleaned up with clean-out system and abundant drying, then defect detecting liquid is coated on surface of the work, or workpiece immersed in the defect detecting liquid, or defect detecting liquid injected in the sprayer spray, make defect detecting liquid infiltrate workpiece, defect, water is removed unnecessary penetrating fluid again, after to be dried, apply photographic developer (as magnesia powder), so that the penetrating fluid in the defective is adsorbed to surface of the work, then the flaw detection usefulness uviol lamp under or under daylight, observe, then can see the image of defective.The prescription of used defect detecting liquid is as follows:
Material weight percentage
Illuminating colour lights up red 7%
Fluorescent dye fluorescein 6%
Kerosene 7%
Dibutyl phthalate 65%
Peregal A20 15%
Claims (1)
1, a kind of dual-purpose penetrating fluid of flaw detection of painted-fluorescence that is used for Non-Destructive Testing, it is characterized in that it is with illuminating colour (, phloxine red as lighting up, propyl red, Congo red, methyl violet, oil blue, Oil Yellow, rhodamine), fluorescent dye (as fluorescein), and kerosene, dibutyl phthalate and emulsifying agent (peregal A-20) to be respectively 7%, 6%, 7%, 65%, 15% ratio in this percent by weight respectively formulated.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN85104229A CN85104229B (en) | 1985-05-31 | 1985-05-31 | Colouring-fluorescent dual-purpose flaw detection penetrating fluid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN85104229A CN85104229B (en) | 1985-05-31 | 1985-05-31 | Colouring-fluorescent dual-purpose flaw detection penetrating fluid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN85104229A CN85104229A (en) | 1986-07-09 |
| CN85104229B true CN85104229B (en) | 1988-05-25 |
Family
ID=4793712
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN85104229A Expired CN85104229B (en) | 1985-05-31 | 1985-05-31 | Colouring-fluorescent dual-purpose flaw detection penetrating fluid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN85104229B (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101196477B (en) * | 2007-12-29 | 2010-06-02 | 李建明 | Anti-rust defect detecting liquid and its preparing technique |
| CN108444958B (en) * | 2018-02-08 | 2020-10-23 | 浙江绿岛科技有限公司 | Nondestructive flaw detection aerosol |
| CN108760709A (en) * | 2018-07-05 | 2018-11-06 | 江苏德意高航空智能装备股份有限公司 | Coloring and the dual-purpose flaw detection cleaning paper handkerchief of fluorescence and paper handkerchief Cleaning application |
| CN108864745A (en) * | 2018-07-05 | 2018-11-23 | 江苏德意高航空智能装备股份有限公司 | Safety and environmental protection colorant |
| CN108827924A (en) * | 2018-07-05 | 2018-11-16 | 江苏德意高航空智能装备股份有限公司 | Coloring and the dual-purpose flaw detection paper handkerchief of fluorescence and paper handkerchief infiltration applications |
| CN110157218B (en) * | 2019-06-11 | 2021-08-31 | 沈阳中科腐蚀控制工程技术中心 | Coloring agent and production method thereof |
| CN111766252B (en) * | 2020-06-08 | 2023-04-14 | 广东三和化工科技有限公司 | Aerosol paint and preparation method thereof |
| JP7367173B1 (en) * | 2022-12-20 | 2023-10-23 | マークテック株式会社 | Reused penetrant test liquid and penetrant test method using the penetrant test method |
| CN116410742B (en) * | 2023-02-03 | 2024-10-01 | 江苏普洋新材料科技有限公司 | Biodegradable water-based fluorescent penetrating fluid |
-
1985
- 1985-05-31 CN CN85104229A patent/CN85104229B/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CN85104229A (en) | 1986-07-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US2920203A (en) | Fluorescent penetrant inspection materials and methods | |
| CN85104229B (en) | Colouring-fluorescent dual-purpose flaw detection penetrating fluid | |
| JPS6471122A (en) | Method of inspecting quality of reticle mask pattern and the like, its object for monitor and method of inspecting object | |
| CN102539435A (en) | High-sensitivity coloring-fluorescence dual-purpose flaw detection permeation liquid | |
| US3856465A (en) | Leak detection coating for aircraft flexible fuel cells | |
| US3915885A (en) | Water washable dye penetrant composition and method utilizing same | |
| US3311479A (en) | Penetrant inspection process and compositions | |
| US3777157A (en) | Water washable dye penetrant composition and method of application | |
| US3929664A (en) | Water-washable inspection penetrant employing triglycerides and polyglycerides of fatty acids | |
| US3108187A (en) | Flaw detection method using fluorescent penetrant and a fluorescent developer | |
| CN113684103A (en) | Fluorescent cleaning agent | |
| US4186304A (en) | Extender for dye penetrant composition | |
| CN109187571A (en) | A kind of water-washing type dye check agent and preparation method thereof | |
| US2461494A (en) | Method and composition for flaw detection | |
| GB819925A (en) | Improvements in or relating to methods of detecting surface discontinuities in articles | |
| Issaq et al. | Isolation of stable mutagenic photodecomposition products of benzo (a) pyrene by thin-layer chromatography | |
| EP0831321A3 (en) | Self-checking crack detection apparatus | |
| US3930407A (en) | Water-washable inspection penetrant employing mineral solvent and a fatty acid solubility promoter | |
| Sawicki et al. | The various quenching effects in thin-layer chromatography: Application to air pollution | |
| US3931733A (en) | Method and means of accelerating removal of background entrapments in the inspection penetrant process | |
| DE58909481D1 (en) | Method for the detection of substances with hydrolase activity. | |
| JPS60171438A (en) | Surface flaw inspection | |
| GB2222879A (en) | Crack detecting apparatus | |
| US3671183A (en) | Manufacturing a sensitive non-flammable dye penetrant | |
| CA2120948A1 (en) | An inspection device for detecting surface faults, and an instrument incorporating such a device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| C10 | Entry into substantive examination | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| C13 | Decision | ||
| GR02 | Examined patent application | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |