CN203291551U - Multifunctional dynamic extraction unit used for extracting ecdysone - Google Patents
Multifunctional dynamic extraction unit used for extracting ecdysone Download PDFInfo
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- CN203291551U CN203291551U CN2013203088814U CN201320308881U CN203291551U CN 203291551 U CN203291551 U CN 203291551U CN 2013203088814 U CN2013203088814 U CN 2013203088814U CN 201320308881 U CN201320308881 U CN 201320308881U CN 203291551 U CN203291551 U CN 203291551U
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Abstract
The utility model discloses a multifunctional dynamic extraction unit used for extracting ecdysone, which comprises an extraction pot, a first condenser and a concentrator, wherein a solvent vapor outlet of the extraction pot is connected with a solvent inlet of the first condenser by a pipeline; a solvent outlet of the first condenser is connected with a reflux port of the extraction pot by a pipeline; a secondary vapor outlet of the concentrator is connected with a secondary vapor inlet of the extraction pot by a pipeline; a discharge port of the extraction pot is connected with a feed port of the concentrator; an upright second condenser is arranged at the upper part of the extraction pot; the lower end of the upright second condenser is communicated with the extraction pot; the upper end of the upright second condenser is connected with the solvent inlet of the first condenser by a pipeline; the solvent outlet of the first condenser is connected with a first cooler; and the secondary vapor outlet of the concentrator is connected with a second solvent recovery device by a pipeline. The multifunctional dynamic extraction unit is high in production efficiency, low in energy consumption, simple to operate and high in automation degree, can achieve dynamic extraction, and can recover solvents with different concentrations.
Description
Technical field
The utility model relates to a kind of extraction equipment, is specifically related to a kind of multi-functional Dynamic Extraction unit for extracting moulting hormone.
Background technology
Plant extracts need adopt extraction, concentration technology to extract active ingredient usually from plant, is used for pharmacy, and the characteristics such as the content of the active ingredient of extraction and change of properties depend on this link to a great extent.Existing extraction, concentrator on the market at present, complex structure mostly, and can only carry out static extraction and concentration, and extraction and concentration efficiency is not high, consumes energy larger, and solvent load is large, and complex operation can not be realized automation.
Summary of the invention
The purpose of this utility model is for the deficiencies in the prior art, a kind of multi-functional Dynamic Extraction unit for extracting moulting hormone is provided, the multi-functional Dynamic Extraction unit production efficiency that should be used for the extraction moulting hormone is high, can realize Dynamic Extraction, and it is low to consume energy, simple to operate, automaticity is high, can reclaim the solvent of variable concentrations.
the purpose of this utility model is achieved in that a kind of multi-functional Dynamic Extraction unit for extracting moulting hormone, comprise extractor, the first condenser and inspissator, described extractor is provided with heating jacket, the bottom of described extractor is provided with slag unloading device, the top of described extractor is provided with charging aperture, refluxing opening, indirect steam import and solvent vapo(u)r outlet, the bottom of described extractor is provided with discharging opening, the solvent vapo(u)r outlet of described extractor is connected by pipeline with the solvent inlet of the first condenser, the solvent outlet of described the first condenser is connected by pipeline with the refluxing opening of extractor, the indirect steam outlet of described inspissator is connected by pipeline with the indirect steam import of extractor, the discharging opening of described extractor is connected with the charging aperture of inspissator, the top of described extractor is provided with the second upright condenser, the lower end of described the second condenser uprightly communicates with the extractor of extractor, the upper end of described the second condenser uprightly is connected by pipeline with the solvent inlet of the first condenser, the solvent outlet of described the first condenser is connected with the first cooler by pipeline, form the first solvent recovery unit, the indirect steam outlet of described inspissator is connected with the second solvent recovery unit by pipeline, described the second solvent recovery unit is by the 3rd condenser, the second cooler, formed by flow container, the solvent inlet of described the 3rd condenser is connected by pipeline with the outlet of the indirect steam of inspissator, the solvent outlet of described the 3rd condenser is connected with the solvent inlet of the second cooler, the solvent outlet of described the second cooler is connected with being subjected to flow container, be provided with filter between the discharging opening of described extractor and the charging aperture of inspissator.
The cylindrical shell of described extractor is up big and down small, and the diameter of bottom cylindrical shell is less than the diameter of top cylindrical shell, and the bottom barrel wall is established heating jacket, and the top barrel wall is provided with heat-insulation layer.
Described slag unloading device comprises air pump, connecting rod and pneumatic discharge cover, and described air pump is connected with pneumatic discharge cover by connecting rod.
Described filter is duplex strainer.
The beneficial effects of the utility model are: because the outlet of the indirect steam of inspissator of the present utility model is connected by pipeline with the indirect steam import of extractor.The concentrated indirect steam that produces, as the thermal source of medicinal material extract, can be saved the heating energy consumption more than 50%.Extract, concentrated can carrying out simultaneously, and the reflux condensation mode liquid temp is again near boiling temperature in extractor, makes the utility model extraction time short, extract quality obviously improves, extract medicinal component quality improves, and has improved the purity of liquid.
The top of described extractor is provided with the second upright condenser, and the lower end of described the second condenser uprightly communicates with the extractor of extractor.Extractor lower pipeline and inspissator communicate in leaching process, can realize malleation and negative pressure in extractor by the heat exchange of turning and tune up the second condenser down in leaching process.By turning the heat exchange of the second condenser down, make in extractor and produce malleation, when liquid flows to inspissator in a large number, produce negative pressure in extractor.A large amount of hydrothermal solutions that flow into inspissator make the withdrawal liquid in inspissator pass back in a large number in extractor, fill up negative pressure in extractor, after mixing up positive/negative-pressure, when malleation is excessive or negative pressure when excessive, equipment does not need external force, can self control at random by the flow rate of liquid own, formed hot reflux Dynamic Extraction unit, automaticity is high, and has saved manpower, and is simple to operate.Therefore, the utility model can adopt normal pressure, negative pressure, malleation technological operation water extraction and alcohol extracting, and particularly the low temperature for blackspiked lovegrass herb with root (carrying the plant of moulting hormone) extracts, concentrates, and receives the cream rate high.Because taking Dynamic Extraction, blackspiked lovegrass herb with root and the moulting hormone high gradient that is dissolved in water, increased the motive force that moulting hormone leaches, and increased the rate of extract.More than before comparable, conventional equipment is carried 5-20% more.Contrast traditional lixiviate, the effective ingredient yield improves 20%～40%.
The solvent outlet of described the first condenser is connected with the first cooler by pipeline, forms the first solvent recovery unit, and the indirect steam outlet of described inspissator is connected with the second solvent recovery unit by pipeline.When material did not need to extract again, extractor and inspissator can pass through respectively the solvent of the first solvent recovery unit, the second solvent recovery unit recovery variable concentrations.The utility model not only can separately use but also can supportingly use together.The second solvent recovery unit recovered solvent can remove the alcohol basin, also can be back in extractor as novel solvent.While extracting medicinal material, only add solvent one time, recycle in a cover water-tight equipment; Solvent in the dregs of a decoction can reclaim substantially fully, and the solvent of recyclable variable concentrations also, and solvent load is few, and consumption rate reduces.
The utility model equipment is simple, and utilization rate of equipment and installations is high.
Description of drawings
Fig. 1 is structural representation of the present utility model.
In accompanying drawing, 1 is extractor, and 2 is the first condenser, and 3 is inspissator, and 4 is heating jacket, 5 is slag unloading device, and 6 is the second condenser, and 7 is the first cooler, and 8 is the 3rd condenser, and 9 is the second cooler, 10 for being subjected to flow container, and 11 is filter, and 12 is heat-insulation layer, and 13 is charging aperture.
The specific embodiment
Referring to Fig. 1, a kind of multi-functional Dynamic Extraction unit for extracting moulting hormone, comprise extractor 1, the first condenser 2 and inspissator 3.Described inspissator 3 is comprised of heater and evaporimeter.Described extractor 1 is provided with heating jacket 4.Described heating jacket 4 is provided with steam inlet and steam (vapor) outlet.The bottom of described extractor 1 is provided with slag unloading device 5.Described slag unloading device 5 comprises air pump, connecting rod and pneumatic discharge cover, and described air pump is connected with pneumatic discharge cover by connecting rod.The top of described extractor 1 is provided with charging aperture 13, refluxing opening, indirect steam import and solvent vapo(u)r outlet, the bottom of described extractor 1 is provided with discharging opening, the solvent vapo(u)r outlet of described extractor 1 is connected by pipeline with the solvent inlet of the first condenser 2, and the solvent outlet of described the first condenser 2 is connected by pipeline with the refluxing opening of extractor.The pipeline that connects the refluxing opening of the outlet of the first condenser 2 and extractor is provided with sample tap and the first visor.The indirect steam outlet of described inspissator 3 is connected by pipeline with the indirect steam import of extractor 1.The concentrated indirect steam that produces, as the thermal source of medicinal material extract, can be saved the heating energy consumption more than 50%.Extract, concentrated can carrying out simultaneously, and the reflux condensation mode liquid temp is again near boiling temperature in extractor, makes the utility model extraction time short, extract quality obviously improves, extract medicinal component quality improves, and has improved the purity of liquid.The discharging opening of described extractor is connected with the charging aperture of inspissator.The top of described extractor is provided with the second upright condenser 6, and the lower end of described the second condenser 6 uprightly communicates with the extractor of extractor.Can realize malleation and negative pressure in extractor by the heat exchange of turning and tune up the second condenser down in leaching process.Extractor lower pipeline and inspissator communicate in leaching process,, by turning the heat exchange of the second condenser down, make in extractor and produce malleation, when liquid flows to inspissator in a large number, produce negative pressure in extractor.A large amount of hydrothermal solutions that flow into inspissator make the withdrawal liquid in inspissator pass back in a large number in extractor, fill up negative pressure in extractor, after mixing up positive/negative-pressure, when malleation is excessive or negative pressure when excessive, equipment does not need external force, can self control at random by the flow rate of liquid own, has formed hot reflux Dynamic Extraction unit, and saved manpower, simple to operate.Therefore, the utility model can adopt normal pressure, negative pressure, malleation technological operation water extraction and alcohol extracting, and particularly the low temperature for blackspiked lovegrass herb with root (carrying the plant of moulting hormone) extracts, concentrates, and receives the cream rate high.Because taking Dynamic Extraction, blackspiked lovegrass herb with root and the moulting hormone high gradient that is dissolved in water, increased the motive force that moulting hormone leaches, and increased the rate of extract.More than before comparable, conventional equipment is carried 5-20% more.Contrast traditional lixiviate, the effective ingredient yield improves 20%～40%.The upper end of described the second condenser 6 uprightly is connected by pipeline with the solvent inlet of the first condenser 2, the solvent outlet of described the first condenser 2 is connected with the first cooler 7 by pipeline, form the first solvent recovery unit, the indirect steam outlet of described inspissator 3 is connected with the second solvent recovery unit by pipeline.When material did not need to extract again, extractor and inspissator can pass through respectively the solvent of the first solvent recovery unit, the second solvent recovery unit recovery variable concentrations.The utility model not only can separately use but also can supportingly use together.The second solvent recovery unit recovered solvent can remove the alcohol basin, also can be back in extractor as novel solvent.Described the second solvent recovery unit by the 3rd condenser 8, the second cooler 9, formed by flow container 10, the solvent inlet of described the 3rd condenser 8 is connected by pipeline with the indirect steam outlet of inspissator 3, the solvent outlet of described the 3rd condenser 8 is connected with the solvent inlet of the second cooler 9, and the solvent outlet of described the second cooler 9 is connected with being subjected to flow container 10.Be provided with filter 11 between the charging aperture of the discharging opening of described extractor 1 and inspissator 3.The inlet of described filter 11 is connected with the discharging opening of extractor 1, and the liquid outlet of filter 11 is connected with the charging aperture of inspissator 3.Described filter 11 is duplex strainer.Connect the inlet of duplex strainer and the pipeline of the discharging opening bottom extractor and be provided with the second visor.Each pipeline is provided with valve.The cylindrical shell of described extractor is up big and down small, and the diameter of the bottom cylindrical shell of extractor is less than the diameter of top cylindrical shell, and the bottom barrel wall of extractor is established heating jacket.The bottom barrel diameter that is provided with heating jacket of described extractor is little, when extractor extracts, material is in bottom, because of the bottom barrel diameter of extractor little, thermal source easily penetrates, compared to existing technology in up and down equally large extractor compare, the utility model is short heat time heating time, power consumption is few, and yield is high.The top barrel wall of extractor 1 is provided with heat-insulation layer 12, more is conducive to energy-saving consumption-reducing.Described heat-insulation layer 12 is heat preservation sandwich layer.In described heat preservation sandwich layer, insulation material is set.
Claims (4)
1. multi-functional Dynamic Extraction unit that be used for to extract moulting hormone, comprise extractor, the first condenser and inspissator, described extractor is provided with heating jacket, the bottom of described extractor is provided with slag unloading device, the top of described extractor is provided with charging aperture, refluxing opening, indirect steam import and solvent vapo(u)r outlet, the bottom of described extractor is provided with discharging opening, the solvent vapo(u)r outlet of described extractor is connected by pipeline with the solvent inlet of the first condenser, the solvent outlet of described the first condenser is connected by pipeline with the refluxing opening of extractor, the indirect steam outlet of described inspissator is connected by pipeline with the indirect steam import of extractor, the discharging opening of described extractor is connected with the charging aperture of inspissator, it is characterized in that: the top of described extractor is provided with the second upright condenser, the lower end of described the second condenser uprightly communicates with the extractor of extractor, the upper end of described the second condenser uprightly is connected by pipeline with the solvent inlet of the first condenser, the solvent outlet of described the first condenser is connected with the first cooler by pipeline, form the first solvent recovery unit, the indirect steam outlet of described inspissator is connected with the second solvent recovery unit by pipeline, described the second solvent recovery unit is by the 3rd condenser, the second cooler, formed by flow container, the solvent inlet of described the 3rd condenser is connected by pipeline with the outlet of the indirect steam of inspissator, the solvent outlet of described the 3rd condenser is connected with the solvent inlet of the second cooler, the solvent outlet of described the second cooler is connected with being subjected to flow container, be provided with filter between the discharging opening of described extractor and the charging aperture of inspissator.
2. the multi-functional Dynamic Extraction unit for extracting moulting hormone according to claim 1, it is characterized in that: the cylindrical shell of described extractor is up big and down small, the diameter of bottom cylindrical shell is less than the diameter of top cylindrical shell, and the bottom barrel wall is established heating jacket, and the top barrel wall is provided with heat-insulation layer.
3. the multi-functional Dynamic Extraction unit for extracting moulting hormone according to claim 1, it is characterized in that: described slag unloading device comprises air pump, connecting rod and pneumatic discharge cover, described air pump is connected with pneumatic discharge cover by connecting rod.
4. the multi-functional Dynamic Extraction unit for extracting moulting hormone according to claim 1, it is characterized in that: described filter is duplex strainer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013203088814U CN203291551U (en) | 2013-05-31 | 2013-05-31 | Multifunctional dynamic extraction unit used for extracting ecdysone |
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| CN2013203088814U CN203291551U (en) | 2013-05-31 | 2013-05-31 | Multifunctional dynamic extraction unit used for extracting ecdysone |
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| CN203291551U true CN203291551U (en) | 2013-11-20 |
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| CN2013203088814U Withdrawn - After Issue CN203291551U (en) | 2013-05-31 | 2013-05-31 | Multifunctional dynamic extraction unit used for extracting ecdysone |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103252109A (en) * | 2013-05-31 | 2013-08-21 | 四川杰象药材原料有限公司 | Multifunctional dynamic extracting unit for extracting molting hormone |
-
2013
- 2013-05-31 CN CN2013203088814U patent/CN203291551U/en not_active Withdrawn - After Issue
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103252109A (en) * | 2013-05-31 | 2013-08-21 | 四川杰象药材原料有限公司 | Multifunctional dynamic extracting unit for extracting molting hormone |
| CN103252109B (en) * | 2013-05-31 | 2015-05-27 | 四川杰象药材原料有限公司 | Multifunctional dynamic extracting unit for extracting molting hormone |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20131120 Effective date of abandoning: 20150527 |
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| RGAV | Abandon patent right to avoid regrant |