CN206492228U - A kind of gas-liquid separation device and the single-action concentrator with the device - Google Patents
A kind of gas-liquid separation device and the single-action concentrator with the device Download PDFInfo
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- CN206492228U CN206492228U CN201621468148.9U CN201621468148U CN206492228U CN 206492228 U CN206492228 U CN 206492228U CN 201621468148 U CN201621468148 U CN 201621468148U CN 206492228 U CN206492228 U CN 206492228U
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- liquid separation
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- separation device
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- 239000007788 liquid Substances 0.000 title claims abstract description 116
- 238000000926 separation method Methods 0.000 title claims abstract description 64
- 239000000463 material Substances 0.000 claims abstract description 50
- 238000010438 heat treatment Methods 0.000 claims abstract description 39
- 238000009834 vaporization Methods 0.000 claims abstract description 35
- 230000008016 vaporization Effects 0.000 claims abstract description 35
- 238000011084 recovery Methods 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 230000008676 import Effects 0.000 claims description 5
- 239000003814 drug Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 5
- 238000009833 condensation Methods 0.000 description 11
- 230000005494 condensation Effects 0.000 description 11
- 238000005265 energy consumption Methods 0.000 description 4
- 230000003139 buffering effect Effects 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229960000074 biopharmaceutical Drugs 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of gas-liquid separation device and the single-action concentrator with the device, including the heating chamber being sequentially connected, vaporization chamber, gas-liquid separation device and condenser, wherein, charging aperture and final material outlet are respectively arranged with heating chamber, vaporization chamber bottom is provided with material recycle outlet and connected with heating chamber bottom, and vaporization chamber top is connected with gas-liquid separation device bottom by recovery channel.In medicine enriching stage, in gas-liquid separation device, play cushioning effect, it is to avoid the escape of material, can further recovered material, improve gas-liquid separation efficiency, reduce material loss, improve yield.
Description
Technical field
The utility model belongs to medicine concentration technique field, specially a kind of gas-liquid separation device and the list with the device
Imitate concentrator.
Background technology
After the completion of biopharmaceutical technology, medicine preparation, it usually needs finished product can just be obtained by being concentrated, existing skill
In art, it is evaporated, is directly condensed after evaporation into vaporization chamber after generally the aqueous solution containing medicine is heated, causes to steam
Hair efficiency is bad, high energy consumption, concentrate and vapor low separation efficiency, easily escapes liquid, and material loss is big, and yield is not high.
The content of the invention
The utility model provides a kind of gas-liquid separation device and with the device aiming at above-mentioned defect
Single-action concentrator.The technical problems to be solved in the utility model is, in medicine enriching stage, in gas-liquid separation device, to play
Cushioning effect, it is to avoid the escape of material, can further recovered material, improve gas-liquid separation efficiency, reduce material loss, carry
High yield.
The technical solution of the utility model is,
A kind of gas-liquid separation device, including cushion chamber and the liquid storage cylinder of the inverted pyramidal structures below cushion chamber, delay
Rush chamber to connect with the cavity of liquid storage cylinder, opposite sides is respectively arranged with air inlet and gas outlet, liquid storage cylinder lower end in the middle part of cushion chamber
Liquid outlet is provided with, liquid outlet is connected with U type pipes.
One end of U-tube is import, and the other end is outlet, and liquid outlet is connected with the import of U-tube one end, and U-tube is another
The outlet height at end is less than liquid outlet.Gas with vapor, in the cushion chamber of gas-liquid separation device water vapor condensation into
Liquid is fallen into liquid storage cylinder, then enters U-tube by liquid outlet.
A kind of single-action concentrator with described gas-liquid separation device, including be sequentially connected heating chamber, vaporization chamber,
Gas-liquid separation device and condenser, wherein, charging aperture and final material outlet are respectively arranged with heating chamber, vaporization chamber bottom is set
It is equipped with material recycle outlet to connect with heating chamber bottom, is connected at the top of vaporization chamber with the air inlet of gas-liquid separation device, vaporization chamber
The recovery channel on top is connected with the liquid outlet of gas-liquid separation device bottom by U-tube, and the liquid in U-tube can form water
Envelope, prevents that gas is returned in vaporization chamber by recovery channel in gas-liquid separation device, the gas outlet of gas-liquid separation device and condensation
Device top is connected.
Heating chamber is shell and tube or dividing wall type structure.
Charging aperture is located at heating chamber bottom.
Final material outlet is located at heating chamber bottom.
Described condenser is connected with vacuum extractor by vacuum pipe.
Described condenser is connected with condensation water storage tank.
The beneficial effects of the utility model are：The utility model includes the heating chamber being sequentially connected, vaporization chamber, gas-liquid separation
Device and condenser, material are preheated after entering heating chamber, are concentrated subsequently into vaporization chamber, steam enters gas-liquid separation
Device carries out gas-liquid separation；Steam in gas-liquid separation device passes through natural cooling, and a part is condensed into liquid and returns to vaporization chamber,
Remaining steam is condensed into condenser, and condensed water enters condensation water storage tank, facilitates the recycling of condensed water.
Zymotic fluid continuously enters heating chamber under vacuum drive by charging aperture, and vaporization chamber, the material of atomization are entered after heating
Because vapour, liquid separation are realized in the effect such as gravity, liquid falls into vaporization chamber bottom as heavy phase, then returned to by Matter Transfer mouth plus
Hot cell.Water vapour is introduced into gas-liquid separation device and enters row buffering, air-flow enters in gas-liquid separation device before condenser is entered,
Stream pressure diminishes, it is ensured that when slug, foam, play cushioning effect, it is to avoid the escape of material, same in surge chamber
Realize that the vapour in water vapour, liquid are separated due to the effect of gravity, liquid is back to vaporization chamber as heavy phase by refluxing opening, due to
The presence of pressure differential, vapor enters condenser.
The material returned to by the material recycle outlet below vaporization chamber after the concentration of heating chamber is to having just enter into heating chamber
Initial material is preheated, it is ensured that temperature when entering evaporator is lifted as early as possible, takes full advantage of the heat of the material after concentration
Amount, reduces energy consumption.
The apparatus structure of the present invention is compact, and without unnecessary device, equipment loss is small, and in gas-liquid separation device, can
Further recovered material, improves gas-liquid separation efficiency, reduces material loss, improve yield.
Brief description of the drawings：
Fig. 1 show basic structure schematic diagram of the present utility model.
In figure, 1. heating chambers, 2. vaporization chambers, 3. gas-liquid separation devices, 4. condensers, 5. condensation water storage tanks, 6. charging apertures,
7. final material is exported, the outlet of 8. material recycles, 9. recovery channels, 10. vacuum pipes, 11. cushion chambers, 12. liquid storage cylinders,
13.U type pipes, 14. air inlets, 15. gas outlets, 16. liquid outlets.
Embodiment：
In order to more fully understand the utility model, technical side of the present utility model is described in detail with instantiation below
Case, but the utility model is not limited thereto.
Embodiment 1
A kind of gas-liquid separation device 3, including interconnected cushion chamber 11 and the reverse taper positioned at the lower section of cushion chamber 11
The liquid storage cylinder 12 of structure, the middle part of cushion chamber 11 is respectively arranged with air inlet 14 and gas outlet 15, and the lower end of liquid storage cylinder 12 is provided with out
Liquid mouthful 16, liquid outlet 16 is connected with U types pipe 13.
Liquid outlet 16 is connected with the import of the one end of U-tube 13, and the outlet height of the other end of U-tube 13 is less than liquid outlet 16.
Gas with vapor, water vapor condensation is fallen into liquid storage cylinder 12 into liquid in gas-liquid separation device 3, then by going out liquid
Mouth 16 enters U-tube 13.
A kind of single-action concentrator with described gas-liquid separation device, including be sequentially connected heating chamber 1, vaporization chamber
2nd, gas-liquid separation device 3 and condenser 4, wherein, charging aperture 6 and final material outlet 7, evaporation are respectively arranged with heating chamber 1
The bottom of room 2 is provided with material recycle outlet 8 and connected with the bottom of heating chamber 1, the top of vaporization chamber 2 and the air inlet of gas-liquid separation device 3
Mouth 14 is connected, and the recovery channel on the top of vaporization chamber 2 is connected with the liquid outlet 16 of the bottom of gas-liquid separation device 3 by U-tube 13, U
Liquid in type pipe 13 can form water seal, prevent that gas is returned in vaporization chamber 2 by recovery channel in gas-liquid separation device 3, gas
The gas outlet 15 of liquid separating apparatus 3 and the connection of the top of condenser 4.
Heating chamber 1 is tubular structure.Initial material is outside tubulation, and final material is internally formed convection current in tubulation.
Charging aperture 6 is located at the bottom of heating chamber 1.
Final material outlet 7 is located at the bottom of heating chamber 1.
Described condenser 4 is connected with vacuum extractor by vacuum pipe 10.
Described condenser 4 is connected with condensation water storage tank 5.
Material is preheated after entering heating chamber 1, is concentrated subsequently into vaporization chamber 2, and steam is filled into gas-liquid separation
Put 3 carry out gas-liquid separations；Steam in gas-liquid separation device 3 passes through natural cooling, and a part is condensed into liquid and returns to vaporization chamber
2, remaining steam is condensed into condenser 4, and condensed water enters condensation water storage tank 5, facilitates the recycling of condensed water.
The material returned to by the material recycle outlet 8 of the lower section of vaporization chamber 2 after the concentration of heating chamber 1 is to having just enter into heating chamber
1 initial material is preheated, it is ensured that temperature when entering evaporator 2 is lifted as early as possible, takes full advantage of the material after concentration
Heat, reduce energy consumption.
The present invention apparatus structure it is compact, without unnecessary device, equipment loss is small, gas-liquid separation device 3 use so that
Steam has the temperature-fall period of a buffering after being come out from evaporator 2, slow down temperature reducing rate, the huge temperature difference is not had to cold
Condenser 4 causes damage；And in gas-liquid separation device 3, can further recovered material, improve gas-liquid separation efficiency, reduce
Material loss, improves yield.
Embodiment 2
A kind of gas-liquid separation device 3, including interconnected cushion chamber 11 and the reverse taper positioned at the lower section of cushion chamber 11
The liquid storage cylinder 12 of structure, the middle part of cushion chamber 11 is respectively arranged with air inlet 14 and gas outlet 15, and the lower end of liquid storage cylinder 12 is provided with out
Liquid mouthful 16, liquid outlet 16 is connected with U types pipe 13.
Liquid outlet 16 is connected with the import of the one end of U-tube 13, and the outlet height of the other end of U-tube 13 is less than liquid outlet 16.
Gas with vapor, water vapor condensation is fallen into liquid storage cylinder 12 into liquid in gas-liquid separation device 3, then by going out liquid
Mouth 16 enters U-tube 13.
A kind of single-action concentrator with described gas-liquid separation device, including be sequentially connected heating chamber 1, vaporization chamber
2nd, gas-liquid separation device 3 and condenser 4, wherein, charging aperture 6 and final material outlet 7, evaporation are respectively arranged with heating chamber 1
The bottom of room 2 is provided with material recycle outlet 8 and connected with the bottom of heating chamber 1, the top of vaporization chamber 2 and the air inlet of gas-liquid separation device 3
Mouth 14 is connected, and the recovery channel on the top of vaporization chamber 2 is connected with the liquid outlet 16 of the bottom of gas-liquid separation device 3 by U-tube 13, U
Liquid in type pipe 13 can form water seal, prevent that gas is returned in vaporization chamber 2 by recovery channel in gas-liquid separation device 3, gas
The gas outlet 15 of liquid separating apparatus 3 and the connection of the top of condenser 4.
Heating chamber 1 is dividing wall type structure.Initial material and final material carry out heat exchange.
Charging aperture 6 is located at the bottom of heating chamber 1.
Final material outlet 7 is located at the bottom of heating chamber 1.
Described gas-liquid separation device 3 is gas-liquid separation device.
Described condenser 4 is connected with vacuum extractor by vacuum pipe 10.
Described condenser 4 is connected with condensation water storage tank 5.
Material is preheated after entering heating chamber 1, is concentrated subsequently into vaporization chamber 2, and steam is filled into gas-liquid separation
Put 3 carry out gas-liquid separations；Steam in gas-liquid separation device 3 passes through natural cooling, and a part is condensed into liquid and returns to vaporization chamber
2, remaining steam is condensed into condenser 4, and condensed water enters condensation water storage tank 5, facilitates the recycling of condensed water.
The material returned to by the material recycle outlet 8 of the lower section of vaporization chamber 2 after the concentration of heating chamber 1 is to having just enter into heating chamber
1 initial material is preheated, it is ensured that temperature when entering evaporator 2 is lifted as early as possible, takes full advantage of the material after concentration
Heat, reduce energy consumption.
The present invention apparatus structure it is compact, without unnecessary device, equipment loss is small, gas-liquid separation device 3 use so that
Steam has the temperature-fall period of a buffering after being come out from evaporator 2, slow down temperature reducing rate, the huge temperature difference is not had to cold
Condenser 4 causes damage；And in gas-liquid separation device 3, can further recovered material, improve gas-liquid separation efficiency, reduce
Material loss, improves yield.
Claims (7)
1. a kind of gas-liquid separation device, it is characterised in that falling including interconnected cushion chamber and below cushion chamber
Air inlet and gas outlet are respectively arranged with the middle part of the liquid storage cylinder of cone structure, cushion chamber, liquid storage cylinder lower end is provided with liquid outlet, gone out
Liquid mouthful is connected with U type pipes.
2. a kind of gas-liquid separation device according to claim 1, it is characterised in that liquid outlet and the import of U-tube one end
Connection, the outlet height of the U-tube other end is less than liquid outlet.
3. a kind of single-action concentrator with gas-liquid separation device as claimed in claim 1, it is characterised in that including successively
Heating chamber, vaporization chamber, gas-liquid separation device and the condenser of connection, wherein, charging aperture is respectively arranged with heating chamber and final
Material outlet, vaporization chamber bottom is provided with material recycle outlet and connected with heating chamber bottom, is filled at the top of vaporization chamber with gas-liquid separation
The air inlet connection put, the recovery channel on vaporization chamber top is connected with the liquid outlet of gas-liquid separation device bottom by U-tube, gas
The gas outlet of liquid separating apparatus and the connection of condenser top.
4. a kind of single-action concentrator according to claim 3, it is characterised in that charging aperture is located at heating chamber bottom.
5. a kind of single-action concentrator according to claim 3, it is characterised in that final material outlet is located at heating chamber bottom
End.
6. a kind of single-action concentrator according to claim 3, it is characterised in that described condenser passes through vacuum pipe
It is connected with vacuum extractor.
7. a kind of single-action concentrator according to claim 3, it is characterised in that described condenser is connected with condensed water
Storage tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621468148.9U CN206492228U (en) | 2016-12-29 | 2016-12-29 | A kind of gas-liquid separation device and the single-action concentrator with the device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621468148.9U CN206492228U (en) | 2016-12-29 | 2016-12-29 | A kind of gas-liquid separation device and the single-action concentrator with the device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206492228U true CN206492228U (en) | 2017-09-15 |
Family
ID=59801796
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621468148.9U Expired - Fee Related CN206492228U (en) | 2016-12-29 | 2016-12-29 | A kind of gas-liquid separation device and the single-action concentrator with the device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206492228U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107398088A (en) * | 2017-09-18 | 2017-11-28 | 盐城方正医药科技有限公司 | A kind of Simvastatin production enrichment facility |
| CN107537168A (en) * | 2017-10-19 | 2018-01-05 | 榆林学院 | A kind of regulation and control fixed gas scapus dynamic characteristic promotes the device of steam condensation |
| CN107551590A (en) * | 2017-10-30 | 2018-01-09 | 新中天环保股份有限公司 | Solvent slop EGR |
| CN114455552A (en) * | 2022-03-07 | 2022-05-10 | 盛隆资源再生（无锡）有限公司 | Treatment device and treatment method for high-COD waste acid |
-
2016
- 2016-12-29 CN CN201621468148.9U patent/CN206492228U/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107398088A (en) * | 2017-09-18 | 2017-11-28 | 盐城方正医药科技有限公司 | A kind of Simvastatin production enrichment facility |
| CN107537168A (en) * | 2017-10-19 | 2018-01-05 | 榆林学院 | A kind of regulation and control fixed gas scapus dynamic characteristic promotes the device of steam condensation |
| CN107551590A (en) * | 2017-10-30 | 2018-01-09 | 新中天环保股份有限公司 | Solvent slop EGR |
| CN107551590B (en) * | 2017-10-30 | 2020-05-26 | 新中天环保股份有限公司 | Waste solvent recycling device |
| CN114455552A (en) * | 2022-03-07 | 2022-05-10 | 盛隆资源再生（无锡）有限公司 | Treatment device and treatment method for high-COD waste acid |
| CN114455552B (en) * | 2022-03-07 | 2023-03-31 | 盛隆资源再生（无锡）有限公司 | Treatment device and treatment method for high-COD waste acid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Gas -liquid separation and have device's single -action concentrator Effective date of registration: 20190402 Granted publication date: 20170915 Pledgee: Qilu bank Limited by Share Ltd. Binzhou branch Pledgor: SHANDONG BAOLI ZAITI BIOTECHNOLOGY CO.,LTD. Registration number: 2019370000063 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20200514 Granted publication date: 20170915 Pledgee: Qilu bank Limited by Share Ltd. Binzhou branch Pledgor: SHANDONG BAOLI ZAITI BIOTECHNOLOGY Co.,Ltd. Registration number: 2019370000063 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170915 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |