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CN1931710B - Bleaching powder concentrate producing process - Google Patents

Bleaching powder concentrate producing process Download PDF

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Publication number
CN1931710B
CN1931710B CN2006101160094A CN200610116009A CN1931710B CN 1931710 B CN1931710 B CN 1931710B CN 2006101160094 A CN2006101160094 A CN 2006101160094A CN 200610116009 A CN200610116009 A CN 200610116009A CN 1931710 B CN1931710 B CN 1931710B
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China
Prior art keywords
blade
drying oven
bleaching powder
lower coating
high test
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CN2006101160094A
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CN1931710A (en
Inventor
岳群
王建勋
吴志敏
金卫东
杨丽君
孙建平
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Shanghai Chlor Alkali Chemical Co Ltd
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Shanghai Chlor Alkali Chemical Co Ltd
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Abstract

The present invention discloses one kind of bleaching powder concentrate producing process, which includes drying crude bleaching powder concentrate product containing water in a drying furnace with rotary scraper. The drying furnace includes furnace body, crude bleaching powder concentrate product inlet, hot blast inlet, product outlet, motor set below the furnace body, stirring shaft and strip scraper. The process of the present invention is simple, has high drying efficiency, low power consumption and low environmental pollution, and is suitable for industrial production.

Description

The production method of high test bleaching powder
Technical field
The present invention relates to a kind of production method of high test bleaching powder, relate in particular to the drying means in the high test bleaching powder production process.
Background technology
High test bleaching powder, its chemical name is a Losantin, is a kind of important chemical feedstocks, has in fields such as food, hospital, swimming pool, public place, Industrial Wastewater Treatment and military projects very to use widely.
The production of high test bleaching powder generally includes following steps: slaked lime, caustic soda and chlorine reaction generated the chlorination slurry, after separating, obtains to contain the high test bleaching powder crude product of moisture, and dry then, remove moisture, refining back obtains finished product.
In the production method originally, drying is carried out in pan dryer, and the existing remarkable defective of this method is that material decomposes easily, fault handling time is long, and material loss is big, and drying efficiency is affected, simultaneously, energy consumption is higher, easy contaminate environment, and labour intensity is big.
Summary of the invention
The technical issues that need to address of the present invention are the drying production methods that disclose a kind of high test bleaching powder, to overcome the above-mentioned defective that original technology exists.
Method of the present invention comprises the steps:
Slaked lime, caustic soda and chlorine reaction are generated the chlorination slurry, after separating, obtain to contain the high test bleaching powder crude product of moisture, send in the drying oven that is provided with revolving scraper, adopt warm air drying, collect the product at drying oven top then, it is characterized in that, said drying oven comprises:
The drying oven body of heater;
Be arranged on the high test bleaching powder crude product inlet at drying oven body of heater middle part;
Be arranged on the hot-wind inlet on the drying oven body of heater of high test bleaching powder crude product inlet below;
Be arranged on the products export at drying oven body of heater top;
Setting is the motor of dry stove below;
One end is connected with the output shaft of motor, the other end is arranged on the stir shaft in the drying oven;
One end is fixed on the stir shaft, the internal protecting wall of the other end and said drying oven leaves the strip scraper in gap, the position that said scraper is provided with below the high test bleaching powder crude product inlet, hot-wind inlet above;
Said scraper comprises upper blade and lower coating blade, and upper blade is arranged on the top of lower coating blade;
The hot blast temperature of sending into drying oven from hot-wind inlet is 130~170 ℃, and the weight water content of sending into the high test bleaching powder crude product of drying oven from high test bleaching powder crude product inlet is 40~50%, and based on the weight of said bleaching powder crude product, hot blast rate is 20000~30000 meters 3/ hour, the linear velocity of hot blast in drying oven is≤25 meter per seconds, stirring velocity is≤130 rev/mins; Bleaching the residence time of smart crude product in drying oven is≤5 seconds.
The product that is obtained, weight water content are 4~10%, can satisfy the needs that use in relevant field fully.
By above-mentioned disclosed technical scheme as seen, method of the present invention, equipment is simple, and processing ease, material can not glue wall in drying oven, the drying efficiency height, thus reduced energy consumption and environmental pollution, be convenient to industrializing implementation.
Description of drawings
Fig. 1 is the drying oven structural representation.
Fig. 2 is the scraper synoptic diagram.
Fig. 3 is that A-A among Fig. 1 is to synoptic diagram.
Embodiment
Referring to Fig. 1 and Fig. 3, said drying oven comprises:
Drying oven body of heater 1;
Be arranged on the high test bleaching powder crude product inlet 2 at drying oven body of heater 1 middle part;
Be arranged on enter the mouth hot-wind inlet 3 on the drying oven body of heater of 2 belows of high test bleaching powder crude product;
Be arranged on the products export 4 at drying oven body of heater 1 top;
Be arranged on the motor 5 of drying oven below;
One end is connected with the output shaft of motor 5, the other end is arranged on the stir shaft 6 in the drying oven;
One end is fixed on the stir shaft 6, the internal protecting wall of the other end and said drying oven leaves the strip scraper in gap 7, the position that said scraper is provided with below the high test bleaching powder crude product inlet 2, hot-wind inlet 3 above;
According to preferable methods of the present invention, the width in gap 7 is 10~30mm;
Said scraper comprises upper blade 8 and lower coating blade 9, and upper blade 8 is arranged on the top of lower coating blade 9;
Said upper blade 8 comprises upper blade bar 10 and blade 11, scraping knife bar 10 1 ends is fixed on the stir shaft 6, blade 11 is fixed on the other end of scraping knife bar 10, the number of plies of upper blade 8 is 2~4 layers, every layer is provided with 2 and scrapes knife bar 10 and blade 11, from top to down, scrape the length of knife bar (10) and successively decrease successively, as shown in Figure 2;
Said lower coating blade 9 comprises lower coating blade bar 12, blade 11 and lower coating blade frame 13, lower coating blade frame 13 is triangular in shape, be fixed on the stir shaft 6, scraping knife bar 12 1 ends is fixed on the lower coating blade frame 13, blade 11 is fixed on the lower coating blade frame 13, the number of plies of lower coating blade bar 12 is 2~4, and every layer is provided with 2 lower coating blade bars 12, blade 11, as shown in Figure 2.
Embodiment 1
Adopt Fig. 1, Fig. 2 and drying oven shown in Figure 3, highly be 5.5 meters, diameter is 1.6 meters, the width in gap 7 is 10~30mm, and the number of plies of upper blade 8 is 3, scrapes knife bar 10 and blade 11 for 2 every layer, the number of plies of lower coating blade bar 12 is 3, every layer of 2 lower coating blade bar 12 and blade 11.
Being that 40~50% high test bleaching powder crude product is sent into drying oven with 1600 kilograms/hour flow from high test bleaching powder crude product inlet with the weight water content, is 130~170 ℃ hot blast with temperature, with 20000~30000 meters 3/ hour flow send into drying oven from hot-wind inlet, stirring velocity is≤130 rev/mins, the weight water content of the high test bleaching powder of the product of discharging from the products export 4 at drying oven body of heater 1 top is 4~10%.

Claims (6)

1. the production method of a high test bleaching powder comprises the steps: to contain the high test bleaching powder crude product of moisture, sends in the drying oven that is provided with revolving scraper, adopts warm air drying, collects the product at drying oven top then, it is characterized in that said drying oven comprises:
Drying oven body of heater (1);
Be arranged on the high test bleaching powder crude product inlet (2) at drying oven body of heater (1) middle part;
Be arranged on the hot-wind inlet (3) on the drying oven body of heater of high test bleaching powder crude product inlet (2) below;
Be arranged on the products export (4) at drying oven body of heater (1) top;
Be arranged on the motor (5) of drying oven below;
One end is connected with the output shaft of motor (5), the other end is arranged on the stir shaft (6) in the drying oven;
The strip scraper that one end is fixed on that stir shaft (6) is gone up, the other end and the internal protecting wall of said drying oven leave gap (7), the position that said scraper is provided with below high test bleaching powder crude product inlet (2), the top of hot-wind inlet (3);
Said scraper comprises upper blade (8) and lower coating blade (9), and upper blade (8) is arranged on the top of lower coating blade (9);
The hot blast temperature of sending into drying oven from hot-wind inlet is 130~170 ℃, and the weight water content of sending into the high test bleaching powder crude product of drying oven from high test bleaching powder crude product inlet is 40~50%, and based on the weight of said high test bleaching powder crude product, hot blast rate is 20000~30000 meters 3/ hour, the linear velocity of hot blast in drying oven is≤25 meter per seconds, stirring velocity is≤130 rev/mins; The residence time of high test bleaching powder crude product in drying oven is≤5 seconds.
2. method according to claim 1 is characterized in that, the width of gap (7) is 10~30mm.
3. method according to claim 1 is characterized in that, said upper blade (8) comprises upper blade bar (10) and blade (11), and upper blade bar (10) one ends are fixed on the stir shaft (6), and blade (11) is fixed on the other end of upper blade bar (10).
4. method according to claim 3 is characterized in that, the number of plies of upper blade (8) is 2~4, and every layer is provided with 2 upper blade bars (10) and blade (11), and from top to down, the length of upper blade bar (10) is successively decreased successively.
5. method according to claim 1, it is characterized in that, said lower coating blade (9) comprises lower coating blade bar (12), blade (11) and lower coating blade frame (13), lower coating blade frame (13) is triangular in shape, be fixed on the stir shaft (6), lower coating blade bar (12) one ends are fixed on the lower coating blade frame (13), and blade (11) is fixed on the lower coating blade frame (13).
6. method according to claim 5 is characterized in that, the number of plies of lower coating blade (9) is 2~4, and every layer is provided with 2 lower coating blade bars (12) and blade (11).
CN2006101160094A 2006-09-13 2006-09-13 Bleaching powder concentrate producing process Active CN1931710B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2006101160094A CN1931710B (en) 2006-09-13 2006-09-13 Bleaching powder concentrate producing process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2006101160094A CN1931710B (en) 2006-09-13 2006-09-13 Bleaching powder concentrate producing process

Publications (2)

Publication Number Publication Date
CN1931710A CN1931710A (en) 2007-03-21
CN1931710B true CN1931710B (en) 2010-08-25

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101602487B (en) * 2009-03-03 2012-04-25 王嘉兴 Preparation method of calcium hypochlorite, sodium chloride and sulfuric acid employing limestone
CN104743516A (en) * 2015-03-31 2015-07-01 陈益铭 Rotary kiln production method and equipment for bleaching powder product

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87100005A (en) * 1987-01-03 1988-07-20 C-I-L公司 The production method of Losantin
CN1047265A (en) * 1989-05-18 1990-11-28 奥林公司 Produce the modifying device of instant granulated product

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87100005A (en) * 1987-01-03 1988-07-20 C-I-L公司 The production method of Losantin
CN1047265A (en) * 1989-05-18 1990-11-28 奥林公司 Produce the modifying device of instant granulated product

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
JP特开平9-86903A 1997.03.31

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