CN1985969A - Jinqing detoxicating preparation and new preparing process - Google Patents
Jinqing detoxicating preparation and new preparing process Download PDFInfo
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- CN1985969A CN1985969A CN 200610165475 CN200610165475A CN1985969A CN 1985969 A CN1985969 A CN 1985969A CN 200610165475 CN200610165475 CN 200610165475 CN 200610165475 A CN200610165475 A CN 200610165475A CN 1985969 A CN1985969 A CN 1985969A
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Abstract
The present invention relates to Chinese medicine composition and its preparation, and is especially one kind of Chinese medicine composition for treating cold, fever, headache, cough, pain throat and other diseases and its preparation process. The Chinese medicine composition is preferably prepared into dripping pill and soft capsule.
Description
Technical field:
The present invention relates to a kind of Chinese medicine composition and preparation technology thereof, particularly a kind of cold, fever that is used for, headache, the prescription and the preparation technology thereof of disease such as cough, have sore throat.
Background technology:
Cold, fever, headache, disease such as cough, have sore throat is clinically to see that symptom, the traditional Chinese medical science often take relieving the exterior syndrome with drugs of pungent in flavor and cool in nature more, the means of heat-clearing and toxic substances removing are treated it, and evident in efficacy.The Jinqing detoxicating ball is that it represents medicine.But in the practice, because this medicine is medical material to be beaten powder be used as medicine in preparation, cause impurity many, shortcoming such as dosage is big has a strong impact on its clinical practice.
The preparation of process extraction process preparation of the present invention is easy to dissolving and absorption than elite and thick putting that ordinary pill more can collect medicine, and curative effect is fast, and administration time is short, and therefore, curative effect is better.
The purpose of this invention is to provide a kind of therapeutic domain wide, easily accept, easily absorb, the preparation technology of efficient, low dosage, the Chinese medicine dripping pills that has no side effect, soft capsule, granule, chewable tablet, its pill that makes can be used for curing mainly cold, fever, headache, disease such as cough, have sore throat.
Summary of the invention:
The present invention relates to a kind of prescription and preparation technology thereof of Chinese medicine preparation, it is characterized in that, the preparation of per 1000 dosage units is prepared from by following proportion raw material:
62.5～250 parts of 31.5～126 parts of wooden Folium Isatidiss of 62.5～250 parts of Pericarpium Citri Reticulataes of Flos Lonicerae
31.5～126 parts of 62.5～250 portions of Herba Schizonepetae of 31.5～126 portions of Herba Menthaes of Herba Lophatheri
50～200 parts of 31.5～126 parts of Herba Houttuyniae of wood 50～200 portions of Radix Glycyrrhizaes of Radix Isatidis
Preferably:
125 parts of 63 parts of wooden Folium Isatidiss of 125 parts of Pericarpium Citri Reticulataes of Flos Lonicerae
63 parts of 125 portions of Herba Schizonepetae of 63 portions of Herba Menthaes of Herba Lophatheri
100 parts of 63 parts of Herba Houttuyniae of wood 100 portions of Radix Glycyrrhizaes of Radix Isatidis
In more than forming, the weight of medicine is calculated with crude drug, and per 1 part can be 1 gram, also can be kilogram or ton, if be unit with gram, this prescription composition can be made into 1000 doses of pharmaceutical preparatioies.Described 1000 doses of fingers, the final drug preparation of making, as make 1000 of soft capsule preparations, drop pill 1000 balls, granule 1000g etc., also can make big packing as granule, as 100～500 bags, specifically can be 100 bags, 125 bags, 200 bags, 250 bags, 500 bags etc., every bag can be used as taking dose 1 time.
More than form, can be made into the preparation of 50～1000 taking doses,, make 125 bags, take 1～2 bag at every turn, can take altogether 62.5～125 times as granule.
More than form to be by weight as proportioning, when producing, can increase or reduce according to corresponding proportion, as large-scale production can be unit with the kilogram, or be unit with the ton, small-scale production can be unit with the milligram also, weight can increase or reduce, but the constant rate of the raw medicinal herbs weight proportion between each composition.
The raw material of Chinese medicine of said ratio extracts processing through new technology of the present invention, obtain the active constituents of medicine of preparation of the present invention, add suitable excipient as required and make suitable medicinal any dosage form, said preparation can be drop pill, capsule, granule, tablet, mixture, soft extract, fluid extract and extractum.
The above new technology of the present invention may further comprise the steps:
Method a:(technology 1.)
(1) gets four Chinese medicine materials such as Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae, adopt steam distillation (or supercritical extraction):, extract according to an appendix XD of pharmacopeia in 2005 essential oil extraction method, till no longer increasing to the volatile oil height the medical material chopping; The volatile oil β-CDBao He, optimised process is: β-CD is 1: 6～12 with the water ratio, and oil is 1: 4～12 with β-CD ratio, and ultrasonic 30～70min gets clathrate;
(2) get the residue medical material, with decocting with water 2～5 times, each 0.5～3.5 hour, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 6～15 times of amount 60～95% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby.
Above active component is the active constituents of medicine of preparation of the present invention, and this active component is suitable for preparing various preparations such as drop pill of the present invention and soft capsule.
Method b:(technology 2.)
(1) getting Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae medical material beats powder and is used as medicine;
(2) prescription residue medical material is handled the same;
(3) above active component lumps together the active constituents of medicine into preparation of the present invention, and this active component is suitable for preparing various preparations such as tablet of the present invention and capsule.
The active constituents of medicine of the preparation of the present invention that above method obtains can be prepared into preparation of the present invention through further processing.
Preparation of the present invention, different dosage form method difference below is the preparation method of several preferred dosage form.
(1) preparation of drop pill
Drop pill of the present invention, wherein the ratio of active component and adjuvant is 1: 0.5～10, and preferred ratio is 1: 2～4, and most preferred ratio is 1: 3.The above adjuvant be specially molecular weight polyethylene glycol between 400 to 10000 Polyethylene Glycol and their mixture, as PEG400 (PEG400), Macrogol 2000, Macrogol 4000, polyethylene glycol 6000 or their mixture or other suitable other auxiliary elements of making drop pill, as glycerol, gelatin or stearic acid sodium etc.
Following steps are taked in the preparation of drop pill of the present invention:
1. be ready to following raw material: active component, adjuvant and/or other inactive ingredients;
2. with the above-mentioned raw materials mix homogeneously;
3. add the transconversion into heat material, move into the drip irrigation of drop pill machine, medicinal liquid splashes in the liquid sub liquid paraffin by water dropper, removes liquid paraffin, selects ball, promptly.
(2) preparation of soft capsule
Soft capsule preparation of the present invention is that active component and pharmaceutically useful organic solvent and the material of making soft capsule shell are formed.Organic solvent wherein is selected from PEG400, Tween 80, glycerol, propylene glycol, isopropyl alcohol, dehydrogenation soybean oil, vegetable oil, aromatic oil, the material of wherein making soft capsule shell is gelatin or arabic gum, water, plasticizer and antiseptic, the weight ratio of gelatin or arabic gum and plasticizer is 1.0: 0.4～1.0 in the soft capsule shell, and the weight ratio of gelatin and water is 1.0: 0.8～1.2; The content of active component is 50mg～500mg in every soft capsule.
The preparation method of preparation of the present invention, the process following steps:
A. get gelatin, glycerol, pure water adds thermosol, adds an amount of antiseptic, preparation rubber;
B. get active component and be dissolved in organic solvent, add suitable quantity of water, be prepared into soft capsule through encapsulating machine.
(3) preparation process of granule is as follows: with the gained active component, add a certain amount of correctives, filler, lubricant, granulate, promptly get granule.
(4) preparation method of chewable tablet is as follows: with the gained active component, add a certain amount of correctives, filler, lubricant, granulate, and drying, tabletting promptly gets chewable tablet.
Filler described in the preparation of granule, chewable tablet is selected from one or more the mixture in lactose, sucrose, dextrin, starch, microcrystalline Cellulose, mannitol, pregelatinized Starch, sorbitol, the xylitol etc.;
Described correctives one of is selected from Rhizoma et radix valerianae, Fructus Pruni pseudocerasi, Fructus Vitis viniferae, Fructus Citri tangerinae, Fructus Citri Limoniae, Herba Menthae, Fructus Fragariae Ananssae, Fructus Musae, Fructus Ananadis comosi, honey peach essence, maltose alcohol, saccharin sodium, protein sugar, sucrose, aspartame, the stevioside or wherein several mixture;
Suitable lubricant comprises wherein one or more such as magnesium stearate, Pulvis Talci, micropowder silica gel.
The specific embodiment:
Further specify the present invention by the following examples, include but not limited to the following example.
Embodiment 1:
The preparation method of drop pill of the present invention:
Prescription:
Flos Lonicerae 187.5g Pericarpium Citri Reticulatae 94.5g wood Folium Isatidis 187.5g
Herba Lophatheri 94.5g Herba Menthae 187.5g Herba Schizonepetae 94.5g
Wood Radix Isatidis 150g Radix Glycyrrhizae 94.5g Herba Houttuyniae 150g
PEG4000 100g
Make 1000 balls
Preparation method:
(1) gets four Chinese medicine materials such as Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae, adopt steam distillation (or supercritical extraction):, extract according to an appendix XD of pharmacopeia in 2005 essential oil extraction method, till no longer increasing to the volatile oil height the medical material chopping; The volatile oil β-CDBao He, optimised process is: β-CD is 1: 8 with the water ratio, and oil is 1: 6 with β-CD, and ultrasonic 30min gets clathrate;
(2) get the residue medical material, with decocting with water 3 times, each 1.5 hours, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 10 times of amount 80% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby;
(3) with above-mentioned extract obtained mixing, the PEG4000 that adds recipe quantity puts into the vessel in heating dissolving, and jolting makes and dissolves into uniform solution, inserts in the fluid reservoir.Keep 80 ℃ the system of dripping temperature, and a control speed, condensed fluid is a liquid paraffin, drips system promptly.
Embodiment 2:
Preparation of soft capsule method of the present invention:
Prescription:
Flos Lonicerae 562.5g Pericarpium Citri Reticulatae 283.5g wood Folium Isatidis 562.5g
Herba Lophatheri 283.5g Herba Menthae 562.5g Herba Schizonepetae 283.5g
Wood Radix Isatidis 450g Radix Glycyrrhizae 283.5g Herba Houttuyniae 450g
PEG400 300g
Make 1000
Preparation method:
(1) gets four Chinese medicine materials such as Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae, adopt steam distillation (or supercritical extraction):, extract according to an appendix XD of pharmacopeia in 2005 essential oil extraction method, till no longer increasing to the volatile oil height the medical material chopping; The volatile oil β-CDBao He, optimised process is: β-CD is 1: 8 with the water ratio, and oil is 1: 6 with β-CD ratio, and ultrasonic 30min gets clathrate;
(2) get the residue medical material, with decocting with water 3 times, each 1.5 hours, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 10 times of amount 80% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby;
(3) with above-mentioned extract obtained mixing, add an amount of PEG400 and mix and mixing, add the PEG400 of surplus then, promptly get medicinal liquid.It is standby in addition to join gelatin solution by certain prescription.The condition that control is suitable is regulated content weight, obtains soft capsule in the soft capsule machine.
Embodiment 3:
The preparation method of granule of the present invention:
Prescription:
Flos Lonicerae 250g Pericarpium Citri Reticulatae 126g wood Folium Isatidis 250g
Herba Lophatheri 126g Herba Menthae 250g Herba Schizonepetae 126g
Wood Radix Isatidis 200g Radix Glycyrrhizae 126g Herba Houttuyniae 200g
Make 1000g
Preparation method:
(1) getting Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae medical material beats powder and is used as medicine;
(2) get the residue medical material, with decocting with water 3 times, each 1.5 hours, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 10 times of amount 80% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby;
(3) with above-mentioned extract obtained mixing, add aspartame 5.0g, dextrin 220.0g, to granulate, drying sprays into essence 5.0g, promptly gets granule 1000g.
Embodiment 4:
The preparation method of chewable tablet of the present invention:
Prescription:
Flos Lonicerae 125g Pericarpium Citri Reticulatae 63g wood Folium Isatidis 125g
Herba Lophatheri 63g Herba Menthae 125g Herba Schizonepetae 63g
Wood Radix Isatidis 100g Radix Glycyrrhizae 63g Herba Houttuyniae 100g
Make 1000
Preparation method:
(1) getting Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae medical material beats powder and is used as medicine;
(2) get the residue medical material, with decocting with water 3 times, each 1.5 hours, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 10 times of amount 80% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby;
(3) with above-mentioned extract obtained mixing, add aspartame 3.0g, mannitol 200.0g, granulation, drying adds magnesium stearate 3.0g, mixing, tabletting promptly gets 1000 of chewable tablet.
Claims (10)
1, a kind of Chinese medicine preparation is characterized in that per 1000 dosage units are made by the following weight proportion raw material:
62.5～250 parts of 31.5～126 parts of wooden Folium Isatidiss of 62.5～250 parts of Pericarpium Citri Reticulataes of Flos Lonicerae
31.5～126 parts of 62.5～250 portions of Herba Schizonepetae of 31.5～126 portions of Herba Menthaes of Herba Lophatheri
50～200 parts of 31.5～126 parts of Herba Houttuyniae of wood 50～200 portions of Radix Glycyrrhizaes of Radix Isatidis.
2, the compound preparation of claim 1 is characterized in that, per 1000 dosage units are made by the following weight proportion raw material:
125 parts of 63 parts of wooden Folium Isatidiss of 125 parts of Pericarpium Citri Reticulataes of Flos Lonicerae
63 parts of 125 portions of Herba Schizonepetae of 63 portions of Herba Menthaes of Herba Lophatheri
100 parts of 63 parts of Herba Houttuyniae of wood 100 portions of Radix Glycyrrhizaes of Radix Isatidis.
3, claim 1 or any one Chinese medicine preparation of 2 are drop pill, capsule, granule, tablet, mixture, soft extract, fluid extract and extractum.
4, the Chinese medicine preparation of claim 3 through described raw material is extracted processing, obtains active component, adds suitable adjuvant as required and makes.
5, the Chinese medicine preparation of claim 4 is characterized in that, described active component prepares through following steps:
Method a:(technology 1.)
(1) gets four Chinese medicine materials such as Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae, adopt steam distillation (or supercritical extraction):, extract according to an appendix XD of pharmacopeia in 2005 essential oil extraction method, till no longer increasing to the volatile oil height the medical material chopping; The volatile oil β-CDBao He, optimised process is: β-CD is 1: 6～12 with the water ratio, and oil is 1: 4～12 with β-CD ratio, and ultrasonic 30～70min gets clathrate;
(2) get the residue medical material, with decocting with water 2～5 times, each 0.5～3.5 hour, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 6～15 times of amount 60～95% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby.
Above active component is the active constituents of medicine of preparation of the present invention, and this active component is suitable for preparing various preparations such as drop pill of the present invention and soft capsule.
Method b:(technology 2.)
(1) getting Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae medical material beats powder and is used as medicine;
(2) prescription residue medical material is handled the same;
(3) above active component lumps together the active constituents of medicine into preparation of the present invention, and this active component is suitable for preparing various preparations such as tablet of the present invention and capsule.
6, the Chinese medicine preparation of claim 5 is characterized in that:
Described drop pill, wherein the ratio of active component and adjuvant is 1: 0.5～10, described adjuvant be molecular weight between 400 to 10000 Polyethylene Glycol and their mixture, be selected from PEG400 (or 600), Macrogol 2000, Macrogol 4000, polyethylene glycol 6000 or their mixture.
Its preparation method is: active constituents of medicine and proper auxiliary materials behind 60～115 ℃ of mix homogeneously, are regulated the water dropper size with control drop pill weight, are that the coolant system of dripping forms with dimethicone or liquid paraffin, and coolant temperature is-10～5 ℃.
7, the Chinese medicine preparation of claim 5 is characterized in that:
Described soft capsule, its content is made up of active component and suitable substrate, and wherein the content of active component is 50mg～500mg in every soft capsule; Substrate wherein is selected from wherein one or more of PEG400, Tween 80, glycerol, propylene glycol, isopropyl alcohol, dehydrogenation soybean oil, vegetable oil, aromatic oil, animal wet goods.
Its preparation method is: with active constituents of medicine and proper auxiliary materials mix homogeneously, obtain uniform suspension and/or solution, regulate content weight, compacting, dry getting final product.
8, the Chinese medicine preparation of claim 5 is characterized in that:
The preparation process of described granule is as follows: with above-mentioned extract obtained, add a certain amount of filler, correctives, lubricant, granulate, promptly get granule;
The preparation method of chewable tablet is as follows: with above-mentioned extract obtained, adds a certain amount of filler, correctives, lubricant, granulates, and drying, tabletting promptly gets chewable tablet.
9, the Chinese medicine preparation of claim 8 is characterized in that:
Described filler is selected from one or more the mixture in lactose, sucrose, dextrin, starch, microcrystalline Cellulose, mannitol, pregelatinized Starch, sorbitol, the xylitol etc.;
Described correctives one of is selected from Rhizoma et radix valerianae, Fructus Pruni pseudocerasi, Fructus Vitis viniferae, Fructus Citri tangerinae, Fructus Citri Limoniae, Herba Menthae, Fructus Fragariae Ananssae, Fructus Musae, Fructus Ananadis comosi, honey peach essence, maltose alcohol, saccharin sodium, protein sugar, sucrose, aspartame, the stevioside or wherein several mixture;
Suitable lubricant comprises wherein one or more such as magnesium stearate, Pulvis Talci, micropowder silica gel.
10, the preparation method of any one Chinese medicine preparation of claim 1～9 is characterized in that, the process following steps:
Described raw material of Chinese medicine is extracted processing, obtain active component, add suitable adjuvant and make; Wherein said active component prepares through following steps:
Method a:(technology 1.)
(1) gets four Chinese medicine materials such as Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae, adopt steam distillation (or supercritical extraction):, extract according to an appendix XD of pharmacopeia in 2005 essential oil extraction method, till no longer increasing to the volatile oil height the medical material chopping; The volatile oil β-CDBao He, optimised process is: β-CD is 1: 6～12 with the water ratio, and oil is 1: 4～12 with β-CD ratio, and ultrasonic 30～70min gets clathrate;
(2) get the residue medical material, with decocting with water 2～5 times, each 0.5～3.5 hour, collecting decoction filtered, and filtrate is condensed into certain volume, stirs evenly with 6～15 times of amount 60～95% ethanol, leaves standstill, and filters, and filtrate decompression is condensed into thick extractum, and is standby.
Above active component is the active constituents of medicine of preparation of the present invention, and this active component is suitable for preparing various preparations such as drop pill of the present invention and soft capsule.
Method b:(technology 2.)
(1) getting Pericarpium Citri Reticulatae, Herba Menthae, Herba Schizonepetae, Herba Houttuyniae medical material beats powder and is used as medicine;
(2) prescription residue medical material is handled the same;
(3) above active component lumps together the active constituents of medicine into preparation of the present invention, and this active component is suitable for preparing various preparations such as tablet of the present invention and capsule.
Described drop pill, wherein the ratio of active component and adjuvant is 1: 0.5～10, described adjuvant be molecular weight between 400 to 10000 Polyethylene Glycol and their mixture, be selected from PEG400 (or 600), Macrogol 2000, Macrogol 4000, polyethylene glycol 6000 or their mixture.
Its preparation method is: active constituents of medicine and proper auxiliary materials behind 60～115 ℃ of mix homogeneously, are regulated the water dropper size with control drop pill weight, are that the coolant system of dripping forms with dimethicone or liquid paraffin, and coolant temperature is-10～5 ℃.
Described soft capsule, its content is made up of active component and suitable substrate, and wherein the content of active component is 50mg～500mg in every soft capsule; Substrate wherein is selected from wherein one or more of PEG400, Tween 80, glycerol, propylene glycol, isopropyl alcohol, dehydrogenation soybean oil, vegetable oil, aromatic oil, animal wet goods.
Its preparation method is: active constituents of medicine is mixed with proper auxiliary materials, obtain uniform suspension and/or solution, regulate content weight, compacting, dry getting final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610165475 CN1985969A (en) | 2006-12-20 | 2006-12-20 | Jinqing detoxicating preparation and new preparing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610165475 CN1985969A (en) | 2006-12-20 | 2006-12-20 | Jinqing detoxicating preparation and new preparing process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1985969A true CN1985969A (en) | 2007-06-27 |
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ID=38182998
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200610165475 Pending CN1985969A (en) | 2006-12-20 | 2006-12-20 | Jinqing detoxicating preparation and new preparing process |
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| Country | Link |
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| CN (1) | CN1985969A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114917301A (en) * | 2022-04-28 | 2022-08-19 | 黄守坤 | Treatment medicament for daily cold |
-
2006
- 2006-12-20 CN CN 200610165475 patent/CN1985969A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114917301A (en) * | 2022-04-28 | 2022-08-19 | 黄守坤 | Treatment medicament for daily cold |
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Open date: 20070627 |